CN107022204A - A kind of dye formulation of paper support product and preparation method thereof - Google Patents
A kind of dye formulation of paper support product and preparation method thereof Download PDFInfo
- Publication number
- CN107022204A CN107022204A CN201710348664.0A CN201710348664A CN107022204A CN 107022204 A CN107022204 A CN 107022204A CN 201710348664 A CN201710348664 A CN 201710348664A CN 107022204 A CN107022204 A CN 107022204A
- Authority
- CN
- China
- Prior art keywords
- blending
- mass fraction
- dyestuff
- paper support
- dye formulation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0033—Blends of pigments; Mixtured crystals; Solid solutions
- C09B67/0041—Blends of pigments; Mixtured crystals; Solid solutions mixtures containing one azo dye
Abstract
The present invention relates to a kind of dye formulation of paper support product, it is made up of the component blending of following mass fraction：Direct fast light black G, mass fraction is 80 90；Directly yellow 4, mass fraction is 10 12；Direct green 6, mass fraction is 0.5 1.5.The invention further relates to a kind of preparation method of the dye formulation of paper support product, comprise the following steps：Step 1: accurately weighing each component, install respectively；Step 2: screening out slag by shaking, and the quality of loss is accurately refilled after sieve by amount of slag；Step 3: each component is all added blending in blending tank roller；Step 4: sampling Detection is chemically examined after blending；Step 5: chemical examination warehousing after passing packaging.The color of dye formulation of the present invention is unique, it is difficult to imitates, will not fade.Its preparation method mixes each component dyestuff according in formulary, first passes through to shake before mixing and screens out slag, dyestuff is easier mixing, and color is more stable, reduces dyestuff and is detained, and saves loss and percent defective, and production configuration equipment is few, particularly opens toner equipment and reduces 60%.
Description
Technical field
The present invention relates to a kind of paper support arts, specifically a kind of dye formulation of paper support product and preparation method thereof.
Background technology
Paper support product usually requires to be dyed, and conventional dye formulation and the defect of preparation method are：
1. dyestuff delivers step more and needs successively order, cause easily error and each color has relatively large deviation；
2. due to not focusing on, dyestuff by mixing sieving processing, does not occur slag charge easily；
3. the existing mode fed intake, can cause the zwitterion in dyestuff slurry chaotic；
4. Conventional dye formula easily fades, product surface is rough.
Accordingly, it would be desirable to further improve.
The content of the invention
It is an object of the invention to overcome the shortcomings of that above-mentioned prior art is present, and a kind of dyestuff of paper support product is provided and matched somebody with somebody
Side, its formulation stable, color are unique, be difficult to imitate.
The object of the present invention is achieved like this：
A kind of dye formulation of paper support product, is made up of the component blending of following mass fraction：
Direct fast light black G, mass fraction is 80-90；
Directly yellow 4, mass fraction is 10-12；
Direct green 6, mass fraction is 0.5-1.5.
Further, the dye formulation of paper support product of the present invention, is made up of the component blending of following mass fraction：
Direct fast light black G, mass fraction is 87.2；
Directly yellow 4, mass fraction is 11.8；
Direct green 6, mass fraction is 1.
Dye formulation of the present invention has the beneficial effect that：
Dyestuff matches colour mixture using said components, and color is unique, it is difficult to imitates, will not fade, dyestuff is formed by blending, without
Dyestuff is separately delivered, formulation stable reduces dyestuff trapping phenomena, loss 1.2% or so can be saved, it is annual to save a large amount of productions
Cost.
The preparation method of the dye formulation of foregoing invention paper support product, it is produced by focusing on mode, production configuration
Equipment is few, and the preparation method comprises the following steps：
Step 1: accurately weighing each component, install respectively；
Step 2: screening out slag by shaking, and the quality of loss is accurately refilled after sieve by amount of slag；
Step 3: each component is all added blending in blending tank roller；
Step 4: sampling Detection is chemically examined after blending；
Step 5: chemical examination warehousing after passing packaging.
The duration of runs of the blending tank roller is 3-5 hours.
More than 6 tons of the blending amount of the dyestuff, takes 3 points of front and back position in blending tank roller as sample survey, centre
Randomly select at 2 points as sample survey in position；4-6 tons of the blending amount of dyestuff, takes the point conduct of front and back position 2 in blending tank roller
Sample survey, centre position randomly select at 2 points as sample survey；1-3 tons of the blending amount of dyestuff, before taking in blending tank roller
2 points of position randomly selects at 1 point as sample survey as sample survey, centre position afterwards；Below 1 ton of the blending amount of dyestuff, take
Random site in blending tank roller extracts at 3 points and is used as sample survey.
The preparation method of dye formulation of the present invention has the beneficial effect that：
Each component dyestuff is mixed according in formulary, is first passed through to shake before mixing and is screened out slag, dyestuff is easier mixing, and color is more steady
It is fixed, reduce dyestuff and be detained, save loss and percent defective, production configuration equipment is few, particularly opens toner equipment and reduces by 60%, materials
Accurately, convenient production.
Embodiment
With reference to embodiment, the invention will be further described.
The dye formulation of this paper support product, is made up of the component blending of following mass fraction：
Direct fast light black G, mass fraction is 80-90；
Directly yellow 4, mass fraction is 10-12；
Direct green 6, mass fraction is 0.5-1.5.
As preferred embodiment, the dye formulation of paper support product of the present invention can be further by following mass fraction
Component blending is constituted：
Direct fast light black G, mass fraction is 87.2；
Directly yellow 4, mass fraction is 11.8；
Direct green 6, mass fraction is 1.
Direct fast light black G（CAS：6428-31-5）, alias direct fast black；Direct fast black L-3BG；Direct black L-
3BQ。
Directly yellow 4（CAS：3051-11-4）Alias:Benthiocarb；Ethiofencarb；Ethiofencarb granule；Except aphid prestige；Vegetable aphid
Prestige；2- [(ethylmercapto group) methyl] phenol methylcarbamate；2- (second sulfidomethyl) phenyl N- methyl carbamates；Go out and flutter
Dissipate.
Direct green 6（CAS：4335-09-5）Alias:Hydroxyl-the 6- of 4- amino -5 [[4 '-[(4- hydroxy phenyls) azo] [1,
1 '-diphenyl] -4- bases] azo] -3- [(4- nitrobenzophenones) azo] -2,7- naphthalene disulfonic acid disodium salts；Direct black green B；Directly
Black green NB；Direct dark green B；Directly boil green；Diamine green B.
The dye formulation of the present invention, with unique color, it is difficult to imitate, will not fade, dyestuff is formed by blending, nothing
It need to separate and deliver dyestuff, formulation stable reduces dyestuff trapping phenomena, loss 1.2% or so can be saved, it is annual to save a large amount of raw
Cost is produced, dyestuff surface is smooth.
Because dye colour uniqueness is stable, enterprise can reduce the percent defective produced by color problem, reach that 15% is left
The right side, is that enterprise creates bigger profit.
The difference of paper support product is required for reply different clients, can also further research and develop and be helped using various specialties
Agent, using the principle that counteracts each other, is successively gradually added various auxiliary agents, so that product is better than like product of the same trade, makes visitor
Family is preferentially purchased.
The preparation method of the dye formulation of paper support product of the present invention, comprises the following steps：
Step 1: accurately weighing each component, install respectively；
Step 2: screening out slag by shaking, and the quality of loss is accurately refilled after sieve by amount of slag；
Step 3: each component is all added blending in blending tank roller, the duration of runs of the blending tank roller is small for 3-5
When；
Step 4: sampling Detection is chemically examined after blending；
Step 5: chemical examination warehousing after passing packaging.
More specifically, the preparation method of the dye formulation of paper support product of the present invention is：Respectively by the component percentage in formula
It is general by 1 ton of production calculation every time than correct amount, that is, take " Direct fast light black G " 872kg, " 4 " 118kg of direct Huang, " direct
Green 6 " 10kg, install respectively.Then removed slag, installed respectively with the screening of 20 eye mesh screens respectively at normal temperatures, slag weight is then claimed respectively,
Respectively weight is refilled with sieved kind toner（The quantity of slag）.Whole dye materials are added in blending tank roller again, blending is started
Tank rollers running is shut down after 4 hours.It is last respectively taken in the position of the left, center, right of blending tank roller three 10g test power point and
Coloured light, the bid of three models consistent, it is possible to which discharge packs standby, otherwise needs to continue to start the rolling of blending tank
Cylinder operation half an hour, then detect, untill chemical examination detection is qualified.
The requirement of sampling Detection chemical examination is as follows：
First, sampling is required
More than 6 tons of the blending amount of dyestuff, takes 3 points of front and back position in blending tank roller random as sample survey, centre position
Extract at 2 points as sample survey.
4-6 tons of the blending amount of dyestuff, take 2 points of front and back position in blending tank roller as sample survey, centre position with
Machine extracts at 2 points and is used as sample survey.
1-3 tons of the blending amount of dyestuff, take 2 points of front and back position in blending tank roller as sample survey, centre position with
Machine extracts at 1 point and is used as sample survey.
Below 1 ton of the blending amount of dyestuff, the random site in blending tank roller is taken to extract as sample survey at 3 points.
Wherein, it is desirable to which single dyestuff is weighed in 10g, it is necessary to carry out weighing sample with the scale being accurate to gram.
2nd, examination requirements
The detection for carrying out each index with standard sample is contrasted, and dye sample is analyzed comprehensively, including UV, dye line or dye paper
Deng drawing the power point and coloured light of dyestuff, then carry out lab scale compounding according to result, if the dyestuff of colorant match, from suitable
Dyestuff carries out colorant match and drawn a design, until coloured light is consistent with power point
If sample has irregular phenomenon, proper extension compounding time is needed, then repeated sampling carries out detection until uniformity.
If a little position testing result it is consistent, but coloured light has deviation, by technical staff calculate needed for component increment,
Add and continue blending appropriate time after roller, then repeated sampling is detected, until qualified.
If a little position testing result it is consistent, and conform to quality requirements, then sample is as qualified, laboratory notify into
Row packaging.
Claims (5)
1. a kind of dye formulation of paper support product, it is characterised in that be made up of the component blending of following mass fraction：
Direct fast light black G, mass fraction is 80-90；
Directly yellow 4, mass fraction is 10-12；
Direct green 6, mass fraction is 0.5-1.5.
2. the dye formulation of paper support product according to claim 1, it is characterised in that the component by following mass fraction
Blending is constituted：
Direct fast light black G, mass fraction is 87.2；
Directly yellow 4, mass fraction is 11.8；
Direct green 6, mass fraction is 1.
3. the preparation method of the dye formulation of paper support product according to claim 1, it is characterised in that comprise the following steps：
Step 1: accurately weighing each component, install respectively；
Step 2: screening out slag by shaking, and the quality of loss is accurately refilled after sieve by amount of slag；
Step 3: each component is all added blending in blending tank roller；
Step 4: sampling Detection is chemically examined after blending；
Step 5: chemical examination warehousing after passing packaging.
4. the preparation method of the dye formulation of paper support product according to claim 1, it is characterised in that the blending tank roller
The duration of runs be 3-5 hours.
5. the preparation method of the dye formulation of paper support product according to claim 1, it is characterised in that the blending of the dyestuff
More than 6 tons of amount, takes 3 points of front and back position in blending tank roller as sample survey, centre position and randomly selects at 2 points as inspection
Sample；4-6 tons of the blending amount of dyestuff, takes 2 points of front and back position in blending tank roller to be taken out at random as sample survey, centre position
Take at 2 points as sample survey；1-3 tons of the blending amount of dyestuff, take 2 points of front and back position in blending tank roller as sample survey,
Randomly select at 1 point as sample survey in centre position；Below 1 ton of the blending amount of dyestuff, the random site in blending tank roller is taken
Extract at 3 points as sample survey.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710348664.0A CN107022204A (en) | 2017-05-17 | 2017-05-17 | A kind of dye formulation of paper support product and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710348664.0A CN107022204A (en) | 2017-05-17 | 2017-05-17 | A kind of dye formulation of paper support product and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107022204A true CN107022204A (en) | 2017-08-08 |
Family
ID=59529356
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710348664.0A Pending CN107022204A (en) | 2017-05-17 | 2017-05-17 | A kind of dye formulation of paper support product and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107022204A (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4699628A (en) * | 1985-08-16 | 1987-10-13 | The Atul Products Limited | Process for the preparation of a water soluble direct green polyazo dyestuffs mixture in situ and water soluble direct green polyazo dyestuffs mixture obtained thereby |
| CN1774541A (en) * | 2003-04-14 | 2006-05-17 | 西巴特殊化学品控股有限公司 | Paper coating compositions. |
| CN101580643A (en) * | 2009-03-31 | 2009-11-18 | 天津市亚东化工染料厂 | Pollution-free production technology of direct fast black G |
| CN102348768A (en) * | 2009-03-13 | 2012-02-08 | 巴斯夫欧洲公司 | Aqueous direct dye formulations |
| CN104250454A (en) * | 2013-06-25 | 2014-12-31 | 天津市大港染化厂 | Preparation method of Direct Black 19 |
| CN106283883A (en) * | 2016-08-12 | 2017-01-04 | 上海洗霸科技股份有限公司 | A kind of hybrid solid dyestuff and application thereof |
-
2017
- 2017-05-17 CN CN201710348664.0A patent/CN107022204A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4699628A (en) * | 1985-08-16 | 1987-10-13 | The Atul Products Limited | Process for the preparation of a water soluble direct green polyazo dyestuffs mixture in situ and water soluble direct green polyazo dyestuffs mixture obtained thereby |
| CN1774541A (en) * | 2003-04-14 | 2006-05-17 | 西巴特殊化学品控股有限公司 | Paper coating compositions. |
| CN102348768A (en) * | 2009-03-13 | 2012-02-08 | 巴斯夫欧洲公司 | Aqueous direct dye formulations |
| CN101580643A (en) * | 2009-03-31 | 2009-11-18 | 天津市亚东化工染料厂 | Pollution-free production technology of direct fast black G |
| CN104250454A (en) * | 2013-06-25 | 2014-12-31 | 天津市大港染化厂 | Preparation method of Direct Black 19 |
| CN106283883A (en) * | 2016-08-12 | 2017-01-04 | 上海洗霸科技股份有限公司 | A kind of hybrid solid dyestuff and application thereof |
Non-Patent Citations (2)
| Title |
|---|
| 张红鸣: "《工业产品着色与配色技术》", 30 September 1999, 中国轻工业出版社 * |
| 高树珍: "《染料化学》", 30 September 2009, 哈尔滨工程大学出版社 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Otsuka | Comparative particle size determination of phenacetin bulk powder by using Kubelka–Munk theory and principal component regression analysis based on near-infrared spectroscopy | |
| Lei et al. | Neurochemical profile of the mouse hypothalamus using in vivo 1H MRS at 14.1 T | |
| Li et al. | Identification of gap junction blockers using automated fluorescence microscopy imaging | |
| Sui et al. | Optimization of a Yellow fluorescent protein-based iodide influx high-throughput screening assay for cystic fibrosis transmembrane conductance regulator (CFTR) modulators | |
| CN108407191A (en) | A kind of plastics color blending technique | |
| CN109187381A (en) | A kind of method of quick measurement Machine-made Sand MB value | |
| CN107022204A (en) | A kind of dye formulation of paper support product and preparation method thereof | |
| CN103444940A (en) | Method of correcting product colors | |
| AU2009221475A1 (en) | Method for monitoring a mixture of at least two components | |
| Koch et al. | Certification of reference materials for ochratoxin A analysis in coffee and wine | |
| So et al. | Exchange protein directly activated by cAMP (Epac) 1 plays an essential role in stress-induced exercise capacity by regulating PGC-1α and fatty acid metabolism in skeletal muscle | |
| CN113092604B (en) | Rapid detection method for three common anesthetics in aquatic product | |
| CN108663246B (en) | Benzophenone purity standard substance and preparation method thereof | |
| CN110018036A (en) | A kind of method for quickly detecting of solid powder material color difference | |
| CN106454325A (en) | Mobile phone camera module distortion test method | |
| CN208427407U (en) | A kind of rolling clamp for piano plate | |
| JP3444818B2 (en) | Inspection method and management method of coating liquid for electrophotographic photoreceptor | |
| CN108508053A (en) | A kind of detection method of the atomic physical imperfection of systematicness | |
| CN104893396B (en) | The shading process of golden thin film | |
| Boehm et al. | Sixth workshop on software quality | |
| CN104991032B (en) | Differentiate to adulterate in Fructus Schisandrae Chinensis the thin layer chromatography of Fructus Schisandrae Sphenantherae | |
| CN107727543B (en) | Coal water slurry slurrying test method | |
| Zhang et al. | Determination of domperidone in human plasma using liquid chromatography coupled to tandem mass spectrometry and its pharmacokinetic study | |
| Jiang et al. | Noncontact and rapid analysis of the quality of the recording coating on ink jet printing by near-infrared spectroscopy | |
| CN103267575B (en) | Quick determination method for chromatic aberration of basic dyestuff |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170808 |
|
| RJ01 | Rejection of invention patent application after publication |