CN106987273A - Catalysis pressurization Light chlorimation directly agitates method to produce Modified Chlorinated Paraffin method - Google Patents

Catalysis pressurization Light chlorimation directly agitates method to produce Modified Chlorinated Paraffin method Download PDF

Info

Publication number
CN106987273A
CN106987273A CN201710242255.2A CN201710242255A CN106987273A CN 106987273 A CN106987273 A CN 106987273A CN 201710242255 A CN201710242255 A CN 201710242255A CN 106987273 A CN106987273 A CN 106987273A
Authority
CN
China
Prior art keywords
kettle
paraffin
chlorine
chlorinated paraffin
produce modified
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201710242255.2A
Other languages
Chinese (zh)
Inventor
林群祥
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201710242255.2A priority Critical patent/CN106987273A/en
Publication of CN106987273A publication Critical patent/CN106987273A/en
Withdrawn legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G73/00—Recovery or refining of mineral waxes, e.g. montan wax
    • C10G73/38—Chemical modification of petroleum

Landscapes

  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Title of the present invention is that catalysis pressurization Light chlorimation directly agitates method to produce Modified Chlorinated Paraffin method, belong to chlorinated paraffin technical field, in order to improve chlorinated paraffin speed of production, based on it is improved former 87106851.6 patent adopt the technical scheme that increase catalyst ketone peroxide in paraffin, pressure increases to 1 kg/cm in kettle, install light source in kettle additional, the chlorine that 87106851.6 devices are changed to the supply of chlorine source is directly placed into agitation device, starting paraffin is heated to certain temperature (110 DEG C or so), then (5% or so) adds polyethylene and carries out heating fusing by a certain percentage, then chlorination in input kettle, and ensure polyethylene as fusing shape using heat, a kind of faster production method is provided.

Description

Catalysis pressurization Light chlorimation directly agitates method to produce Modified Chlorinated Paraffin method
(1) technical field：The present invention relates to a kind of method for producing Modified Chlorinated Paraffin.
(2) background technology：" equipment for preparation of paraffin chloride by forced circulating blast method " (former patent No.：87106851.6) its Technical scheme is：By chlorine feeding reactor space, the hydrogen chloride gas of chlorine and reaction generation is extracted out, through jet pump and reservoir Groove, is only absorbed by the water, and remaining chlorine drum is pressed into agitation device, so continuous fast reaction.But for producing chlorinated paraffin speed also not Enough ideals, especially produce high chlorinated paraffin product, and to the reaction later stage, speed eases up.
(3) content of the invention：The task of the present invention be based on to former 87106851.6 patent of invention it is a kind of improve there is provided A kind of method of faster production Modified Chlorinated Paraffin, is adopted the technical scheme that plus catalyst, device, which is improved in pressure, kettle, to be added Light source is loaded onto, the chlorine supplied by chlorine source is passed directly into agitation device, and material in reactor is agitated.Starting paraffin is heated To certain temperature (110 DEG C or so), then (5% or so) adds polyethylene and carries out heating fusing by a certain percentage, then puts into Chlorination in kettle, and ensure that polyethylene, as fusing shape, so agitates lower add to agitate raising reaction speed in forced circulation using heat.
(4) embodiment：A set of " equipment for preparation of paraffin chloride by forced circulating blast method ", uses 500 liters of reactions Kettle, adds ketone peroxide in paraffin in advance, and concentration is 0.01~6.00%, make in device pressure bring up to 1 kilogram/it is flat Square centimetre, 1000 watts of mercury lamps are installed additional in its reactor, and the reaction chlorine of its chlorine source supply is passed directly into agitation device in kettle, raw material Heating paraffin is to certain temperature (110 DEG C or so), and then (5% or so) adds polyethylene and carries out heating fusing by a certain percentage, Then chlorination in input kettle, and ensure polyethylene as fusing shape using heat.
Present invention operation and " equipment for preparation of paraffin chloride by forced circulating blast method " are same.

Claims (1)

1. one kind catalysis pressurization Light chlorimation directly agitates method to produce Modified Chlorinated Paraffin method, including chlorine and hydrogen chloride gas Extract out, hydrogen chloride gas is only absorbed by the water in jet pump and hopper, remaining chlorine drum is pressed into agitation device, so continuous, its feature It is：It is 0.01~6.00% ketone peroxide catalyzed that concentration is added in paraffin, increases reaction pressure, kettle is built with light source chlorination Chlorine source chlorine is directly placed into agitation device in kettle.Starting paraffin is heated to certain temperature (110 DEG C or so), then by a certain percentage (5% or so) add polyethylene and carry out heating fusing, then put into chlorination in kettle, and ensure polyethylene as fusing shape using heat.
CN201710242255.2A 2017-04-04 2017-04-04 Catalysis pressurization Light chlorimation directly agitates method to produce Modified Chlorinated Paraffin method Withdrawn CN106987273A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710242255.2A CN106987273A (en) 2017-04-04 2017-04-04 Catalysis pressurization Light chlorimation directly agitates method to produce Modified Chlorinated Paraffin method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710242255.2A CN106987273A (en) 2017-04-04 2017-04-04 Catalysis pressurization Light chlorimation directly agitates method to produce Modified Chlorinated Paraffin method

Publications (1)

Publication Number Publication Date
CN106987273A true CN106987273A (en) 2017-07-28

Family

ID=59415149

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710242255.2A Withdrawn CN106987273A (en) 2017-04-04 2017-04-04 Catalysis pressurization Light chlorimation directly agitates method to produce Modified Chlorinated Paraffin method

Country Status (1)

Country Link
CN (1) CN106987273A (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4101397A (en) * 1976-04-02 1978-07-18 Dynamit Nobel Aktiengesellschaft Process for the preparation of alpha-chloromethylsilanes
CN1105372A (en) * 1994-01-12 1995-07-19 林群祥 Chlorinated polyvinyl paraffin wax
CN105838440A (en) * 2016-05-06 2016-08-10 林群祥 Method for producing chlorinated paraffin-70 through catalytic pressurizing photo-chlorination direct agitating gas heating and cooling method

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4101397A (en) * 1976-04-02 1978-07-18 Dynamit Nobel Aktiengesellschaft Process for the preparation of alpha-chloromethylsilanes
CN1105372A (en) * 1994-01-12 1995-07-19 林群祥 Chlorinated polyvinyl paraffin wax
CN105838440A (en) * 2016-05-06 2016-08-10 林群祥 Method for producing chlorinated paraffin-70 through catalytic pressurizing photo-chlorination direct agitating gas heating and cooling method

Similar Documents

Publication Publication Date Title
CN105838440A (en) Method for producing chlorinated paraffin-70 through catalytic pressurizing photo-chlorination direct agitating gas heating and cooling method
CN105838434A (en) Method for producing chlorinated paraffin-70 through catalytic pressurizing photo-chlorination bubbling agitating gas heating and cooling method
CN105925311A (en) Method for producing chlorinated paraffin-70 through catalyzing, pressurizing and direct gas agitating cold-hot method
CN105838430A (en) Method for producing chlorinated paraffin by catalytic pressurization photo-chlorination direct agitation process
CN106987273A (en) Catalysis pressurization Light chlorimation directly agitates method to produce Modified Chlorinated Paraffin method
CN105838439A (en) Method for producing chlorinated paraffin-70 through catalytic pressurizing photo-chlorination agitating gas heating and cooling method
CN106929103A (en) Catalysis pressurization Light chlorimation bubbling agitates method to produce Modified Chlorinated Paraffin method
CN106995722A (en) Catalysis pressurization Light chlorimation agitates method to produce Modified Chlorinated Paraffin method
CN105838432A (en) Method for producing chlorcosane through catalytic light chlorination direct propelling method
CN107057762A (en) Catalytic light chlorination directly agitates method to produce Modified Chlorinated Paraffin method
CN106995721A (en) The hot method production method of Modified Chlorinated Paraffin 70 of air cooling is directly agitated in catalysis pressurization
CN107057761A (en) Catalysis pressurization directly agitates method to produce Modified Chlorinated Paraffin method
CN106947534A (en) Pressurization Light chlorimation directly agitates method to produce Modified Chlorinated Paraffin method
CN106929102A (en) Method is directly agitated to produce Modified Chlorinated Paraffin method
CN106957683A (en) Pressurization Light chlorimation agitates method to produce Modified Chlorinated Paraffin method
CN107057760A (en) Catalytic light chlorination agitates method to produce Modified Chlorinated Paraffin method
CN106987270A (en) Catalysis directly agitates method to produce Modified Chlorinated Paraffin method
CN106957684A (en) Catalysis pressurization agitates method to produce Modified Chlorinated Paraffin method
CN106957690A (en) Pressurization Light chlorimation bubbling agitates method to produce Modified Chlorinated Paraffin method
CN106957688A (en) Catalytic light chlorination bubbling agitates method to produce Modified Chlorinated Paraffin method
CN106957682A (en) Light chlorimation directly agitates method to produce Modified Chlorinated Paraffin method
CN106987272A (en) Pressurization Light chlorimation bubbling agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling
CN106947535A (en) Light chlorimation agitates method to produce Modified Chlorinated Paraffin method
CN106957689A (en) Pressurization bubbling agitates method to produce Modified Chlorinated Paraffin method
CN106929104A (en) Catalysis pressurization Light chlorimation directly agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WW01 Invention patent application withdrawn after publication

Application publication date: 20170728

WW01 Invention patent application withdrawn after publication