CN106963888A - A kind of rhizoma Gastrodiae processing method for improving gastrodin content - Google Patents
A kind of rhizoma Gastrodiae processing method for improving gastrodin content Download PDFInfo
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- CN106963888A CN106963888A CN201710370335.6A CN201710370335A CN106963888A CN 106963888 A CN106963888 A CN 106963888A CN 201710370335 A CN201710370335 A CN 201710370335A CN 106963888 A CN106963888 A CN 106963888A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/898—Orchidaceae (Orchid family)
- A61K36/8988—Gastrodia
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/13—Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/19—Preparation or pretreatment of starting material involving fermentation using yeast, bacteria or both; enzymatic treatment
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Abstract
The invention provides a kind of rhizoma Gastrodiae processing method for improving gastrodin content, belong to the processing method technical field of Chinese medicine.This method step：1) to clean；2) finish；3) medium well softens；4) cut into slices；5) dry；6) pack.The present invention adds salt solution cleaning thorough using ultrasonic wave, and inhibit scattering and disappearing for effective component, the loss of Gastrodin is reduced using microwave de-enzyming, medium well softening is cooked using boiling water plus disodium hydrogen phosphate, it has been maximally maintained the nutritional ingredient of rhizoma Gastrodiae, using vacuum refrigeration+infrared hot-air combination, not only drying efficiency is high, and remains each nutritional ingredient and product color of rhizoma Gastrodiae, the content of Gastrodin is improved 36.2%.
Description
Technical field
The invention belongs to the processing method technical field of Chinese medicine, specifically a kind of rhizoma Gastrodiae processing side for improving gastrodin content
Method.
Background technology
Rhizoma Gastrodiae, also known as rhizoma gastrodiae, solely shake sesame, from it is female, close from grass, refreshing grass, yellow moccasin flower, Mokpo, RHIZONA GASTRODIAE, DINGFENGCAO, Bai Long
Skin etc., belongs to orchid family Gastrodia herbaceos perennial, and its stem tuber is medicinal part.Modern pharmacology research shows that rhizoma Gastrodiae has
There are enhancing immunity of organisms, wind resistance diseases caused by dampness, antithrombotic, hypoglycemic, sterilization, brain tonic removing free radical and anti-aging.
The active component of rhizoma Gastrodiae is Gastrodin, and the height of gastrodin content in gastrodia elata blume is to weigh the good and bad important indicator of Rhizoma Gastrodiae, because
This Chinese Pharmacopoeia using Gastrodin as Rhizoma Gastrodiae quality evaluation index.
Preparation process method is to influence the key factor of gastrodin content in gastrodia elata blume, because Gastrodin is not only with free state
It is present in rhizoma Gastrodiae, but also to be combined in the form of ester in the acidic materials of rhizoma Gastrodiae cell, the day under appropriate heating condition
Numb element can be discharged, so as to improve the content of Gastrodin in Gastrodia eleta Bl., boiling is one of conventional rhizoma Gastrodiae processing method, research
Show that, because fresh rhizoma Gastrodiae water content is high, directly heating boiling can cause Gastrodin to hydrolyze directly through water boiling after rhizoma Gastrodiae harvesting, from
And cause the reduction of its content, but if softened using other method, it is more that the content of Gastrodin then declines, and China is special
Sharp file CN102894241 discloses a kind of efficient processing technology for improving gastrodin content in gastrodia elata blume, and the invention is by fresh rhizoma Gastrodiae
After harvest, high intensity and low intensive microwave segmental machining are directly used, although can increase containing for Gastrodin to a certain extent
Amount, but be due to no medium well softening, this Drying rate of the rhizoma Gastrodiae processed is low, and fiber crops see shrivelled, influence yield and quality in vitro,
Reduce the commodity of Rhizoma Gastrodiae.If the rhizoma Gastrodiae of fresh harvest first finished in microwave, reduce entering after its water content
Row cooks medium well softening, so not only increases the content of Gastrodin, and increase its yield and marketing quality simultaneously.Meanwhile,
It is long using the time needed for traditional smoke-dried beancurd drying mode because the water content of fresh rhizoma Gastrodiae is high, easily occur to rot and after smoke-dried beancurd
The content of active ingredient especially Gastrodin of rhizoma Gastrodiae drastically decline, cause the economic benefit of medicinal herb grower's planting rhizoma gastrodiae low.In order to
The content of Gastrodin is improved, is badly in need of proposing a kind of effective rhizoma Gastrodiae processing method.
The content of the invention
The invention aims to solve rhizoma Gastrodiae process time long and process in destructible gastrodin content the problem of,
There is provided a kind of processing method for improving gastrodin content.
In order to achieve the above object, the present invention uses following technical scheme.
1) clean：Fresh block rhizoma Gastrodiae rhizome is used into the NaCl aqueous solution that ultrasonic wave adds mass concentration for 3%-5%
Cleaning, cleaning frequency is 15-20kHz, and cleaning power is 50-80W, and the water temperature of cleaning is 25-30 DEG C, scavenging period 3-
4min, is then rinsed one time, is classified again with clear water, and one, two, three, four grades are divided into by size；
2) finish：The rhizoma Gastrodiae being classified is finished with microwave, fixing power is 700-800W, and frequency is 890-
940mHz, one-level fixing 8-10min, two grades of fixing 6-8min, three-level fixing 4-6min, level Four fixing 2-4min；
3) medium well softens：Disodium hydrogen phosphate is added to be cooked with boiling water in the rhizoma Gastrodiae after fixing, i.e., by the day of same levels
Fiber crops are put into a collection of progress boiling water cooking, until the saturating heart takes out, one-level brew time 9-12min, two grades of brew time 7-
10min, three-level brew time 5-8min, level Four brew time 4-6min, 1kg rhizoma Gastrodiae add 2-2.2g disodium hydrogen phosphates；
4) cut into slices：The rhizoma Gastrodiae rhizome cooked is dried in the air cool, artificial slices across is carried out, slice thickness is 3-6mm；
5) dry：Rhizoma Gastrodiae section is placed in after -20 DEG C of refrigerator freezing processing 2-3h, is transferred in vacuum freeze drier, very
Reciprocal of duty cycle 0.05-0.08KPa, -60 DEG C of dry 5-7h, then medicinal material is inserted in 55-60 DEG C of electric heating constant-temperature blowing drying box dry,
After drying time 4-6h, sweating is taken out, urgent need is put into infrared drying oven, is dried 20-40min with 800-1000W power, is made medicine
Material water tariff collection is below 12%；
6) pack：The dry Processed Product of Rhizoma Gastrodiae of vacuum packaging is carried out using food product packaging machines PVC/PE materials, will be packaged
Processed Product of Rhizoma Gastrodiae be placed at 2-5 DEG C preserve.
Above-mentioned steps 1) described in grade scale be：The fresh rhizoma Gastrodiae weight of one-level is more than 250g, and two grades of fresh rhizoma Gastrodiae weight are
125-250g, the fresh rhizoma Gastrodiae weight of three-level is 83-125g, and level Four is fresh below rhizoma Gastrodiae weight 83g.
The advantageous effects of the present invention：It is thorough using ultrasonic wave plus salt solution cleaning, and inhibit scattering and disappearing for effective component,
The loss of Gastrodin is reduced using microwave de-enzyming, medium well softening is cooked using boiling water plus disodium hydrogen phosphate, farthest protected
The nutritional ingredient of rhizoma Gastrodiae is held, not only drying efficiency is high using vacuum refrigeration+infrared hot-air combination, and remains each of rhizoma Gastrodiae
Nutritional ingredient and product color, especially make the content of Gastrodin improve 36.2%.
Embodiment
With reference to embodiment further make detailed elaboration to technical scheme, but the not all present invention in pairs
Scope is limited.
Embodiment 1
1) clean：By fresh block rhizoma Gastrodiae rhizome use ultrasonic wave add mass concentration for 3% NaCl aqueous cleanings,
Cleaning frequency is 15kHz, and cleaning power is 50W, and the water temperature of cleaning is 25 DEG C, and then scavenging period 3min is rushed again with clear water
Wash one time, be classified, one, two, three, four grades are divided into by size；
2) finish：The rhizoma Gastrodiae being classified is finished with microwave, fixing power is 700W, and frequency is 890mHz, one-level
Finish 8min, two grades of fixing 6min, three-level fixing 4min, level Four fixing 2min；
3) medium well softens：Disodium hydrogen phosphate is added to be cooked with boiling water in the rhizoma Gastrodiae after fixing, i.e., by the day of same levels
Fiber crops are put into a collection of progress boiling water cooking, until the saturating heart takes out, one-level brew time 9min, two grades of brew time 7min, three-level
Brew time 5min, level Four brew time 4min, 1kg rhizoma Gastrodiae add 2g disodium hydrogen phosphates；
4) cut into slices：The rhizoma Gastrodiae rhizome cooked is dried in the air cool, artificial slices across is carried out, slice thickness is 5mm；
5) dry：Rhizoma Gastrodiae section is placed in after -20 DEG C of refrigerator freezing processing 2h, is transferred in vacuum freeze drier, vacuum
0.05KPa, -60 DEG C of dry 5h are spent, then medicinal material is inserted in 55 DEG C of electric heating constant-temperature blowing drying boxes and dried, drying time 6h
Afterwards, take out sweating, urgent need be put into infrared drying oven, with 800W power dry 40min, make medicinal material water tariff collection 12% with
Under；
6) pack：The dry Processed Product of Rhizoma Gastrodiae of vacuum packaging is carried out using food product packaging machines PVC/PE materials, will be packaged
Processed Product of Rhizoma Gastrodiae be placed at 2 DEG C preserve.
Embodiment 2
1) clean：By fresh block rhizoma Gastrodiae rhizome use ultrasonic wave add mass concentration for 5% NaCl aqueous cleanings,
Cleaning frequency is 20kHz, and cleaning power is 80W, and the water temperature of cleaning is 30 DEG C, and then scavenging period 4min is rushed again with clear water
Wash one time, be classified, one, two, three, four grades are divided into by size；
2) finish：The rhizoma Gastrodiae being classified is finished with microwave, fixing power is 800W, and frequency is 940mHz, one-level
Finish 10min, two grades of fixing 8min, three-level fixing 6min, level Four fixing 4min；
3) medium well softens：Disodium hydrogen phosphate is added to be cooked with boiling water in the rhizoma Gastrodiae after fixing, i.e., by the day of same levels
Fiber crops are put into a collection of progress boiling water cooking, until the saturating heart takes out, one-level brew time 12min, two grades of brew time 10min, three
Level brew time 8min, level Four brew time 6min, 1kg rhizoma Gastrodiae adds 2.2g disodium hydrogen phosphates；
4) cut into slices：The rhizoma Gastrodiae rhizome cooked is dried in the air cool, artificial slices across is carried out, slice thickness is 6mm；
5) dry：Rhizoma Gastrodiae section is placed in after -20 DEG C of refrigerator freezing processing 3h, is transferred in vacuum freeze drier, vacuum
0.08KPa, -60 DEG C of dry 7h are spent, then medicinal material is inserted in 60 DEG C of electric heating constant-temperature blowing drying boxes and dried, drying time 6h
Afterwards, take out sweating, urgent need be put into infrared drying oven, with 1000W power dry 40min, make medicinal material water tariff collection 12% with
Under；
6) pack：The dry Processed Product of Rhizoma Gastrodiae of vacuum packaging is carried out using food product packaging machines PVC/PE materials, will be packaged
Processed Product of Rhizoma Gastrodiae be placed at 5 DEG C preserve.
Embodiment 3
1) clean：By fresh block rhizoma Gastrodiae rhizome use ultrasonic wave add mass concentration for 4% NaCl aqueous cleanings,
Cleaning frequency is 18kHz, and cleaning power is 65W, and the water temperature of cleaning is 28 DEG C, and then scavenging period 4min is rushed again with clear water
Wash one time, be classified, one, two, three, four grades are divided into by size；
2) finish：The rhizoma Gastrodiae being classified is finished with microwave, fixing power is 800W, and frequency is 920mHz, one-level
Finish 9min, two grades of fixing 7min, three-level fixing 5min, level Four fixing 3min；
3) medium well softens：Disodium hydrogen phosphate is added to be cooked with boiling water in the rhizoma Gastrodiae after fixing, i.e., by the day of same levels
Fiber crops are put into a collection of progress boiling water cooking, until the saturating heart takes out, one-level brew time 10min, two grades of brew time 8min, three-level
Brew time 6min, level Four brew time 4min, 1kg rhizoma Gastrodiae add 2.1g disodium hydrogen phosphates；
4) cut into slices：The rhizoma Gastrodiae rhizome cooked is dried in the air cool, artificial slices across is carried out, slice thickness is 5mm；
5) dry：Rhizoma Gastrodiae section is placed in after -20 DEG C of refrigerator freezing processing 2.5h, is transferred in vacuum freeze drier, very
Reciprocal of duty cycle 0.06KPa, -60 DEG C of dry 6h, then medicinal material is inserted in 58 DEG C of electric heating constant-temperature blowing drying boxes dry, drying time 5h
Afterwards, take out sweating, urgent need be put into infrared drying oven, with 900W power dry 30min, make medicinal material water tariff collection 12% with
Under；
6) pack：The dry Processed Product of Rhizoma Gastrodiae of vacuum packaging is carried out using food product packaging machines PVC/PE materials, will be packaged
Processed Product of Rhizoma Gastrodiae be placed at 4 DEG C preserve.
The fresh deep red rhizoma Gastrodiae harvested using Longnan of Gansu Province as material, using the local traditional smoke-dried beancurd processing mode of south of Gansu Province as pair
According to, difference of the different processing methods to rhizoma Gastrodiae character is analyzed, and the gastrodin content of rhizoma Gastrodiae after processing is determined using HPLC, by table
1 as can be seen that the rhizoma Gastrodiae color and luster processed using processing method of the present invention is bright in vain, and gastrodin content is improved than traditional smoke-dried beancurd method
36.2%.
The difference of the different processing methods rhizoma Gastrodiae sample property of table 1
| Character | Local tradition smoke-dried beancurd mode | The embodiment of the present invention 3 |
| The time required to drying | 5-8d | 10-13h |
| Surface color | Yellowish-brown | Milky |
| Smell | Bitter is pungent, with smoke | Bitter |
| Saponin content | 0.58% | 0.79% |
Claims (2)
1. a kind of rhizoma Gastrodiae processing method for improving gastrodin content, it is characterised in that use following steps：
1) clean：Fresh block rhizoma Gastrodiae rhizome is used into the NaCl aqueous cleanings that ultrasonic wave adds mass concentration for 3%-5%,
Cleaning frequency is 15-20kHz, and cleaning power is 50-80W, and the water temperature of cleaning is 25-30 DEG C, scavenging period 3-4min, then
Rinsed one time, be classified again with clear water, one, two, three, four grades are divided into by size；
2) finish：The rhizoma Gastrodiae being classified is finished with microwave, fixing power is 700-800W, and frequency is 890-940mHz,
One-level fixing 8-10min, two grades of fixing 6-8min, three-level fixing 4-6min, level Four fixing 2-4min；
3) medium well softens：Add disodium hydrogen phosphate to be cooked with boiling water in the rhizoma Gastrodiae after fixing, i.e., put the rhizoma Gastrodiae of same levels
To with a collection of progress boiling water cooking, until the saturating heart takes out, one-level brew time 9-12min, two grades of brew time 7-10min, three
Level brew time 5-8min, level Four brew time 4-6min, 1kg rhizoma Gastrodiae adds 2-2.2g disodium hydrogen phosphates；
4) cut into slices：The rhizoma Gastrodiae rhizome cooked is dried in the air cool, artificial slices across is carried out, slice thickness is 3-6mm；
5) dry：Rhizoma Gastrodiae section is placed in after -20 DEG C of refrigerator freezing processing 2-3h, is transferred in vacuum freeze drier, vacuum
0.05-0.08KPa, -60 DEG C of dry 5-7h, then medicinal material is inserted in 55-60 DEG C of electric heating constant-temperature blowing drying box and dried, dry
After time 4-6h, sweating is taken out, urgent need is put into infrared drying oven, is dried 20-40min with 800-1000W power, is made medicinal material water
Divide and be maintained at less than 12%；
6) pack：The dry Processed Product of Rhizoma Gastrodiae of vacuum packaging is carried out using food product packaging machines PVC/PE materials, by packaged day
Numb medicine materical crude slice is placed at 2-5 DEG C and preserved.
2. a kind of rhizoma Gastrodiae processing method for improving gastrodin content as claimed in claim 1, it is characterised in that the fresh rhizoma Gastrodiae of one-level
Weight is more than 250g, and two grades of fresh rhizoma Gastrodiae weight are 125-250g, and the fresh rhizoma Gastrodiae weight of three-level is 83-125g, and level Four is fresh rhizoma Gastrodiae
Below weight 83g.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110140961A (en) * | 2019-06-06 | 2019-08-20 | 宁强县林业经济发展研究中心 | A kind of Rhizoma Gastrodiae oil tea production method |
| CN111513161A (en) * | 2020-05-11 | 2020-08-11 | 白山靖珍天麻开发有限公司 | Preparation method of Changbai mountain wuzhu gastrodia tuber block tea |
| CN113267005A (en) * | 2021-05-14 | 2021-08-17 | 云南优源农业科技开发有限公司 | High-efficiency drying method for gastrodia elata |
| CN116735514A (en) * | 2023-08-11 | 2023-09-12 | 昆明理工大学 | Method for rapidly detecting gastrodia elata sulfuration markers by nano-enzyme combined liquid-liquid microextraction |
-
2017
- 2017-05-23 CN CN201710370335.6A patent/CN106963888A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110140961A (en) * | 2019-06-06 | 2019-08-20 | 宁强县林业经济发展研究中心 | A kind of Rhizoma Gastrodiae oil tea production method |
| CN111513161A (en) * | 2020-05-11 | 2020-08-11 | 白山靖珍天麻开发有限公司 | Preparation method of Changbai mountain wuzhu gastrodia tuber block tea |
| CN113267005A (en) * | 2021-05-14 | 2021-08-17 | 云南优源农业科技开发有限公司 | High-efficiency drying method for gastrodia elata |
| CN116735514A (en) * | 2023-08-11 | 2023-09-12 | 昆明理工大学 | Method for rapidly detecting gastrodia elata sulfuration markers by nano-enzyme combined liquid-liquid microextraction |
| CN116735514B (en) * | 2023-08-11 | 2023-11-03 | 昆明理工大学 | Method for rapidly detecting gastrodia elata sulfuration markers by nano-enzyme combined liquid-liquid microextraction |
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