CN106957606A - It is a kind of can selfreparing high molecular nanometer tyre cement and preparation method thereof - Google Patents
It is a kind of can selfreparing high molecular nanometer tyre cement and preparation method thereof Download PDFInfo
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- CN106957606A CN106957606A CN201710229504.4A CN201710229504A CN106957606A CN 106957606 A CN106957606 A CN 106957606A CN 201710229504 A CN201710229504 A CN 201710229504A CN 106957606 A CN106957606 A CN 106957606A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J4/00—Adhesives based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; adhesives, based on monomers of macromolecular compounds of groups C09J183/00 - C09J183/16
- C09J4/06—Organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond in combination with a macromolecular compound other than an unsaturated polymer of groups C09J159/00 - C09J187/00
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/74—Mixing; Kneading using other mixers or combinations of mixers, e.g. of dissimilar mixers ; Plant
- B29B7/7476—Systems, i.e. flow charts or diagrams; Plants
- B29B7/7495—Systems, i.e. flow charts or diagrams; Plants for mixing rubber
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
Abstract
The present invention disclose it is a kind of can selfreparing high molecular nanometer tyre cement, it is prepared from the following raw materials in parts by weight, including 15 22 parts of acrylic acid, 8 10 parts of silica flour, 13 18 parts of nonyl phenol, 9 15 parts of ammonium hydroxide, 48 parts of nano zine oxide, 13 16 parts of Nano silica sol, 20 24 parts of isocyanates, 37 parts of Arcton 11, 5 15 parts of waterglass, 22 24 parts of amino resins, 6 10 parts of sorbitan monooleate, 12 15 parts of ammonium polyphosphate, 58 parts of Firebrake ZB, 7 11 parts of methyl anyl alcohol, 13 18 parts of active carbon nanoparticles, 16 20 parts of vinyl acetate, 22 24 parts of cobalt soap, different 12 16 parts of n-nonanoic acid, 18 22 parts of polyurethane, 6 10 parts of titanium dioxide, 24 28 parts of 13 18 parts of trichloro ethylene and dibasic ester.The high molecular nanometer tyre cement adhesion strength is high, and antiageing effect is good, and washing shrinkage is small, can reach the effect repaired automatically with molding bonded under normal temperature.
Description
Technical field
The present invention relates to it is a kind of can selfreparing high molecular nanometer tyre cement and preparation method thereof.
Background technology
Existing mending agent is a kind of nonpoisonous and tasteless nonflammable liquid for not gluing tire, can tire patching, and can inflate.Mending agent
Main component be usually rubber and aerating agent, ph values are neutral.After tire is punctured gas leakage, as long as mending agent is connected into wheel
Above tire, the valve of mending agent is pressed, can be automatic toward wheel tyre cavity pressurization contracting air, while the white that can also inject as hair jelly
Tyre cement.After tire positive pressure is normal, start automobile just can on the way travel again.In general, mending agent is added toward tire
After once, the leakage as long as liquid of wheel tyre cavity does not volatilize, even if being punctured again with rear tyre, without tire patching.Tire
Interior tyre cement can voluntarily mend the leak on tire under pressure.Although the practicality of mending agent is stronger, work as
When the leak of tire is with diameter greater than more than 6mm, this small tool just seems unable to do what one wishes.So, within 6 millimeters of diameter
Tire acanthopore, 100% simple and fast full capping of this practical mending agent energy, without jack, tire is taken off without unloading tire, at once complete
Into automatic inflating, tire patching.Also there are some car owners to worry the quality and effect of this kind of product, but matter as a fire singeing one's eyebrows can be solved as one
Urgency small tool, still highly use.
Emergency：Shoot benefit, most common tire patching mode is to fill in special adhesive tape, tire patching shop at the Zha Dong positions of tire
Master worker it is generally referred to as formula tire patching of shooting.The largest benefit of this method is efficient and convenient, it is only necessary to a few minutes, and
Tire need not be prized from steel ring, and the defect for formula tire patching of shooting is not durable enough, is also difficult to deal with larger in addition
Wound, therefore be typically only capable to as a kind of provisional remedial measure.
Stifled scarce formula：Paste and mend, also a kind of tire patching mode is viscous benefit.So-called viscous mend is to unload injured tire from steel ring
Under, find after wound, special tire patching rubber is sticked from inner layer of tire, so as to complete mending-leakage.The advantage of this method is can
To be repaired to larger wound, shortcoming is still not durable enough, after water logging after a while and running at high speed, is repaiied
It can be leaked air again at benefit.
Resultant：Fire is mended, and most thoroughly tire patching measure is the fire benefit often said.Fire, which is mended, will equally prize lower tire, then will be special
Raw stock is attached at wound, and then wound is toasted with baking machine, until raw stock is fitted completely with tire.Fire is mended
Benefit be it is extremely durable, substantially without worry can repeat gas leakage.But it also has shortcoming, that is, technical requirements during construction
Higher, because duration and degree of heating control when baking is bad, it is likely that can be burned by tire, serious can also be deformed, like that
One, the damage to tire can be just big.
DIY formulas：Mending agent is mended, and numerous automatic tyre mending agents has certain effect on the market, but also has simultaneously very strong
Limitation.Such as the tire of mending-leakage is just difficult to work if gas light leak.The maximum defect of this mending agent
It is to have very big corrosivity, either steel ring or alloy wheel rim, larger damage can all be had for a long time by getting off, and this damage
The result directly resulted in is that steel ring does not cause gas leakage sternly with tire seal.
Existing tyre cement adhesion strength is not high, and antiageing effect is bad, and washing shrinkage is larger, it is not possible to be bonded under normal temperature
Type, does not reach the effect repaired automatically.
The content of the invention
In consideration of it, high it is an object of the present invention to provide a kind of adhesion strength, antiageing effect is good, and washing shrinkage is small, can be with normal temperature
Lower molding bonded, reach the effect repaired automatically can selfreparing high molecular nanometer tyre cement.
In order to solve the above-mentioned technical problem, the technical scheme is that：
It is a kind of can selfreparing high molecular nanometer tyre cement, be prepared from the following raw materials in parts by weight, including acrylic acid 15-22
Part, 8-10 parts of silica flour, 13-18 parts of nonyl phenol, 9-15 parts of ammonium hydroxide, 4-8 parts of nano zine oxide, Nano silica sol 13-16
Part, 20-24 parts of isocyanates, 3-7 parts of Arcton 11,5-15 parts of waterglass, 22-24 parts of amino resins, anhydrous sorbitol list
6-10 parts of oleate, 12-15 parts of ammonium polyphosphate, 5-8 parts of Firebrake ZB, 7-11 parts of methyl anyl alcohol, 13-18 parts of active carbon nanoparticles,
16-20 parts of vinyl acetate, 22-24 parts of cobalt soap, different n-nonanoic acid 12-16 parts, 18-22 parts of polyurethane, 6-10 parts of titanium dioxide, trichloro ethylene
13-18 parts and 24-28 parts of dibasic ester.
Preferably, be prepared from the following raw materials in parts by weight, including 15 parts of acrylic acid, 8 parts of silica flour, nonyl phenol 13
Part, 9 parts of ammonium hydroxide, 4 parts of nano zine oxide, 13 parts of Nano silica sol, 20 parts of isocyanates, 3 parts of Arcton 11, waterglass
5 parts, 22 parts of amino resins, 6 parts of sorbitan monooleate, 12 parts of ammonium polyphosphate, 5 parts of Firebrake ZB, 7 parts of methyl anyl alcohol,
13 parts of active carbon nanoparticles, 16 parts of vinyl acetate, 22 parts of cobalt soap, 12 parts of different n-nonanoic acid, 18 parts of polyurethane, 6 parts of titanium dioxide, trichloro ethylene
13 parts and 24 parts of dibasic ester.
Preferably, be prepared from the following raw materials in parts by weight, including 18.5 parts of acrylic acid, 9 parts of silica flour, nonyl phenol
15.5 parts, 12 parts of ammonium hydroxide, 6 parts of nano zine oxide, 14.5 parts of Nano silica sol, 22 parts of isocyanates, Arcton 11 5
Part, 10 parts of waterglass, 23 parts of amino resins, 8 parts of sorbitan monooleate, 13.5 parts of ammonium polyphosphate, Firebrake ZB 6.5
Part, 9 parts of methyl anyl alcohol, 15.5 parts of active carbon nanoparticles, 18 parts of vinyl acetate, 23 parts of cobalt soap, 14 parts of different n-nonanoic acid, 19 parts of polyurethane,
26 parts of 8 parts of titanium dioxide, 15.5 parts of trichloro ethylene and dibasic ester.
Preferably, be prepared from the following raw materials in parts by weight, including 22 parts of acrylic acid, 10 parts of silica flour, nonyl phenol 18
Part, 15 parts of ammonium hydroxide, 8 parts of nano zine oxide, 16 parts of Nano silica sol, 24 parts of isocyanates, 7 parts of Arcton 11, water glass
15 parts of glass, 24 parts of amino resins, 10 parts of sorbitan monooleate, 15 parts of ammonium polyphosphate, 8 parts of Firebrake ZB, methyl anyl alcohol
11 parts, 18 parts of active carbon nanoparticles, 20 parts of vinyl acetate, 24 parts of cobalt soap, 16 parts of different n-nonanoic acid, 22 parts of polyurethane, 10 parts of titanium dioxide, three
28 parts of 18 parts of vinyl chloride and dibasic ester.
The invention solves the problems that another technical problem for provide it is a kind of can selfreparing high molecular nanometer tyre cement preparation
Method, comprises the following steps：
1）By 15-22 parts of acrylic acid, 8-10 parts of silica flour, 13-18 parts of nonyl phenol, 9-15 parts of ammonium hydroxide, nano zine oxide 4-8
Part, 13-16 parts of Nano silica sol, 20-24 parts of isocyanates, 3-7 parts of Arcton 11,5-15 parts of waterglass, amino resins 22-
24 parts, 6-10 parts of sorbitan monooleate put into oil bath pan, regulation preheating temperature is 65-70 DEG C, heating 5-7 point
Clock, it is standby；
2）By step 1）Gained raw material is put into colloid mill, and regulation rotating speed is 5500-6800r/min, is ground 12-15 minutes,
It is standby；
3）By 12-15 parts of ammonium polyphosphate, 5-8 parts of Firebrake ZB, 7-11 parts of methyl anyl alcohol, 13-18 parts of active carbon nanoparticles, acetic acid second
16-20 parts of alkene, 22-24 parts of cobalt soap, different n-nonanoic acid 12-16 parts, 18-22 parts of polyurethane, 6-10 parts of titanium dioxide, trichloro ethylene 13-18
24-28 parts of part and dibasic ester are put into reactor, and regulation speed of agitator is 2200-2400r/min, and heating-up temperature is 45-
55 DEG C, react 6-10 minutes, it is standby；
4）By step 2) gained raw material and step 3）Gained raw material is put into banbury, and regulation heating-up temperature is 95-120 DEG C,
Mixing 25-35 minutes, it is standby；
5）By step 4）Gained raw material is put into vacuum kettle, and it is 220-240r/min, reaction that mixing speed is adjusted at normal temperatures
Time is 8-12 minutes, standby；
6）By step 5）Gained raw material puts into tank body interior sealing, and storage is preserved in the cool, you can.
The technology of the present invention effect major embodiment is in the following areas：The active carbon nanoparticles of addition, nano zine oxide, nano silicasol
Glue make it that tyre cement granularity is small, and adhesion strength is high；The vinyl acetate of addition, cobalt soap, different n-nonanoic acid, polyurethane, titanium dioxide, trichlorine
Ethene and dibasic ester have anti-aging function, non-aging using tyre cement long service life；The acrylic acid of addition, quartz
Powder, nonyl phenol, ammonium hydroxide, n-nonanoic acid, polyurethane, Arcton 11 and dibasic ester make it that tyre cement washing shrinkage is small so that mend
Tire glue laminating is unlikely to deform on tire, can reach the effect repaired automatically with molding bonded under normal temperature.
Embodiment
Embodiment 1
It is a kind of can selfreparing high molecular nanometer tyre cement, be prepared from the following raw materials in parts by weight, including 15 parts of acrylic acid, stone
8 parts of English powder, 13 parts of nonyl phenol, 9 parts of ammonium hydroxide, 4 parts of nano zine oxide, 13 parts of Nano silica sol, 20 parts of isocyanates, trichlorine
3 parts of fluoromethane, 5 parts of waterglass, 22 parts of amino resins, 6 parts of sorbitan monooleate, 12 parts of ammonium polyphosphate, Firebrake ZB 5
Part, 7 parts of methyl anyl alcohol, 13 parts of active carbon nanoparticles, 16 parts of vinyl acetate, 22 parts of cobalt soap, 12 parts of different n-nonanoic acid, 18 parts of polyurethane, titanium
24 parts of 6 parts of white powder, 13 parts of trichloro ethylene and dibasic ester.
It is a kind of can selfreparing high molecular nanometer tyre cement preparation method, comprise the following steps：
1）By 15 parts of acrylic acid, 8 parts of silica flour, 13 parts of nonyl phenol, 9 parts of ammonium hydroxide, 4 parts of nano zine oxide, Nano silica sol
13 parts, 20 parts of isocyanates, 3 parts of Arcton 11,5 parts of waterglass, 22 parts of amino resins, 6 parts of sorbitan monooleate
Put into oil bath pan, regulation preheating temperature is 65-70 DEG C, is heated 5-7 minutes, standby；
2）By step 1）Gained raw material is put into colloid mill, and regulation rotating speed is 5500-6800r/min, is ground 12-15 minutes,
It is standby；
3）By 12 parts of ammonium polyphosphate, 5 parts of Firebrake ZB, 7 parts of methyl anyl alcohol, 13 parts of active carbon nanoparticles, 16 parts of vinyl acetate, cobalt soap
24 parts of 22 parts, 12 parts of different n-nonanoic acid, 18 parts of polyurethane, 6 parts of titanium dioxide, 13 parts of trichloro ethylene and dibasic ester put into reactor
In, regulation speed of agitator is 2200-2400r/min, and heating-up temperature is 45-55 DEG C, is reacted 6-10 minutes, standby；
4）By step 2) gained raw material and step 3）Gained raw material is put into banbury, and regulation heating-up temperature is 95-120 DEG C,
Mixing 25-35 minutes, it is standby；
5）By step 4）Gained raw material is put into vacuum kettle, and it is 220-240r/min, reaction that mixing speed is adjusted at normal temperatures
Time is 8-12 minutes, standby；
6）By step 5）Gained raw material puts into tank body interior sealing, and storage is preserved in the cool, you can.
Embodiment 2
It is a kind of can selfreparing high molecular nanometer tyre cement, be prepared from the following raw materials in parts by weight, including 18.5 parts of acrylic acid,
9 parts of silica flour, 15.5 parts of nonyl phenol, 12 parts of ammonium hydroxide, 6 parts of nano zine oxide, 14.5 parts of Nano silica sol, isocyanates 22
Part, 5 parts of Arcton 11,10 parts of waterglass, 23 parts of amino resins, 8 parts of sorbitan monooleate, ammonium polyphosphate 13.5
Part, 6.5 parts of Firebrake ZB, 9 parts of methyl anyl alcohol, 15.5 parts of active carbon nanoparticles, 18 parts of vinyl acetate, 23 parts of cobalt soap, 14 parts of different n-nonanoic acid,
26 parts of 19 parts of polyurethane, 8 parts of titanium dioxide, 15.5 parts of trichloro ethylene and dibasic ester.
It is a kind of can selfreparing high molecular nanometer tyre cement preparation method, comprise the following steps：
1）By 18.5 parts of acrylic acid, 9 parts of silica flour, 15.5 parts of nonyl phenol, 12 parts of ammonium hydroxide, 6 parts of nano zine oxide, nano-silicon
14.5 parts of colloidal sol, 22 parts of isocyanates, 5 parts of Arcton 11,10 parts of waterglass, 23 parts of amino resins, anhydrous sorbitol list oil
8 parts of acid esters is put into oil bath pan, and regulation preheating temperature is 65-70 DEG C, is heated 5-7 minutes, standby；
2）By step 1）Gained raw material is put into colloid mill, and regulation rotating speed is 5500-6800r/min, is ground 12-15 minutes,
It is standby；
3）By 13.5 parts of ammonium polyphosphate, 6.5 parts of Firebrake ZB, 9 parts of methyl anyl alcohol, 15.5 parts of active carbon nanoparticles, vinyl acetate 18
Part, 23 parts of cobalt soap, 14 parts of different n-nonanoic acid, 19 parts of polyurethane, 8 parts of titanium dioxide, 15.5 parts of trichloro ethylene and 26 parts of inputs of dibasic ester
Into reactor, regulation speed of agitator is 2200-2400r/min, and heating-up temperature is 45-55 DEG C, is reacted 6-10 minutes, standby；
4）By step 2) gained raw material and step 3）Gained raw material is put into banbury, and regulation heating-up temperature is 95-120 DEG C,
Mixing 25-35 minutes, it is standby；
5）By step 4）Gained raw material is put into vacuum kettle, and it is 220-240r/min, reaction that mixing speed is adjusted at normal temperatures
Time is 8-12 minutes, standby；
6）By step 5）Gained raw material puts into tank body interior sealing, and storage is preserved in the cool, you can.
Embodiment 3
It is a kind of can selfreparing high molecular nanometer tyre cement, be prepared from the following raw materials in parts by weight, including 22 parts of acrylic acid, stone
10 parts of English powder, 18 parts of nonyl phenol, 15 parts of ammonium hydroxide, 8 parts of nano zine oxide, 16 parts of Nano silica sol, 24 parts of isocyanates, three
7 parts of chlorofluoromethane, 15 parts of waterglass, 24 parts of amino resins, 10 parts of sorbitan monooleate, 15 parts of ammonium polyphosphate, boron
Sour 8 parts of zinc, 11 parts of methyl anyl alcohol, 18 parts of active carbon nanoparticles, 20 parts of vinyl acetate, 24 parts of cobalt soap, 16 parts of different n-nonanoic acid, polyurethane 22
Part, 10 parts of titanium dioxide, 18 parts of trichloro ethylene and 28 parts of dibasic ester.
It is a kind of can selfreparing high molecular nanometer tyre cement preparation method, comprise the following steps：
1）By 22 parts of acrylic acid, 10 parts of silica flour, 18 parts of nonyl phenol, 15 parts of ammonium hydroxide, 8 parts of nano zine oxide, nano silicasol
16 parts of glue, 24 parts of isocyanates, 7 parts of Arcton 11,15 parts of waterglass, 24 parts of amino resins, sorbitan monooleate
10 parts are put into oil bath pan, and regulation preheating temperature is 65-70 DEG C, is heated 5-7 minutes, standby；
2）By step 1）Gained raw material is put into colloid mill, and regulation rotating speed is 5500-6800r/min, is ground 12-15 minutes,
It is standby；
3）By 15 parts of ammonium polyphosphate, 8 parts of Firebrake ZB, 11 parts of methyl anyl alcohol, 18 parts of active carbon nanoparticles, 20 parts of vinyl acetate, cobalt
28 parts of 24 parts of soap, 16 parts of different n-nonanoic acid, 22 parts of polyurethane, 10 parts of titanium dioxide, 18 parts of trichloro ethylene and dibasic ester put into reaction
In kettle, regulation speed of agitator is 2200-2400r/min, and heating-up temperature is 45-55 DEG C, is reacted 6-10 minutes, standby；
4）By step 2) gained raw material and step 3）Gained raw material is put into banbury, and regulation heating-up temperature is 95-120 DEG C,
Mixing 25-35 minutes, it is standby；
5）By step 4）Gained raw material is put into vacuum kettle, and it is 220-240r/min, reaction that mixing speed is adjusted at normal temperatures
Time is 8-12 minutes, standby；
6）By step 5）Gained raw material puts into tank body interior sealing, and storage is preserved in the cool, you can.
Experimental example
Experimental subjects：The tyre cement for choosing common tyre cement, special tyre cement and the present invention carries out test comparison.
Requirement of experiment：The tyre cement of common tyre cement, special tyre cement and the present invention is respectively coated on three tires
Broken hole position, and the holes of three tires is in the same size, the consistency of thickness of coating.
Experimental method：The glue of coating is detected：It is anti-aging to be detected by ageing oven, and adjust survey
It is 120 DEG C to try temperature, and relative humidity is 85%, and air pressure is 106kPa, and ozone concentration is 45%, and ultraviolet illumination intensity is
25uw/cm2, obtain ageing time；Adhesion strength detection is measured using GB 1720-1979 glued membranes attachment amylograph；
Washing shrinkage is detected using GB/T 426-1978 standards by shrinkage tester device.
The growth conditions of three plants of ancient trees, such as following table are recorded after 3 months：
With reference to upper table, the different experimental subjects of three groups of contrast is by the data obtained by experiment, the anti-aging effect of tyre cement of the invention
More preferably, adhesion strength is higher, and washing shrinkage is smaller for fruit.
The technology of the present invention effect major embodiment is in the following areas：The active carbon nanoparticles of addition, nano zine oxide, nano silicasol
Glue make it that tyre cement granularity is small, and adhesion strength is high；The vinyl acetate of addition, cobalt soap, different n-nonanoic acid, polyurethane, titanium dioxide, trichlorine
Ethene and dibasic ester have anti-aging function, non-aging using tyre cement long service life；The acrylic acid of addition, quartz
Powder, nonyl phenol, ammonium hydroxide, n-nonanoic acid, polyurethane, Arcton 11 and dibasic ester make it that tyre cement washing shrinkage is small so that mend
Tire glue laminating is unlikely to deform on tire, can reach the effect repaired automatically with molding bonded under normal temperature.
Certainly, it is the representative instance of the present invention above, in addition, the present invention can also have other a variety of specific implementations
The technical scheme of mode, all use equivalents or equivalent transformation formation, all falls within the scope of protection of present invention.
Claims (5)
1. it is a kind of can selfreparing high molecular nanometer tyre cement, it is characterised in that：It is prepared from the following raw materials in parts by weight, including
15-22 parts of acrylic acid, 8-10 parts of silica flour, 13-18 parts of nonyl phenol, 9-15 parts of ammonium hydroxide, 4-8 parts of nano zine oxide, nanometer
13-16 parts of Ludox, 20-24 parts of isocyanates, 3-7 parts of Arcton 11,5-15 parts of waterglass, 22-24 parts of amino resins, mistake
6-10 parts of water sorbitol monooleate, 12-15 parts of ammonium polyphosphate, 5-8 parts of Firebrake ZB, 7-11 parts of methyl anyl alcohol, nano active
13-18 parts of charcoal, 16-20 parts of vinyl acetate, 22-24 parts of cobalt soap, different n-nonanoic acid 12-16 parts, 18-22 parts of polyurethane, titanium dioxide 6-10
24-28 parts of part, 13-18 parts of trichloro ethylene and dibasic ester.
2. it is as claimed in claim 1 it is a kind of can selfreparing high molecular nanometer tyre cement, it is characterised in that：By following parts by weight
Several raw materials are made, including 15 parts of acrylic acid, 8 parts of silica flour, 13 parts of nonyl phenol, 9 parts of ammonium hydroxide, 4 parts of nano zine oxide, receive
13 parts of Ludox of rice, 20 parts of isocyanates, 3 parts of Arcton 11,5 parts of waterglass, 22 parts of amino resins, anhydrous sorbitol list oil
6 parts of acid esters, 12 parts of ammonium polyphosphate, 5 parts of Firebrake ZB, 7 parts of methyl anyl alcohol, 13 parts of active carbon nanoparticles, 16 parts of vinyl acetate, cobalt soap
24 parts of 22 parts, 12 parts of different n-nonanoic acid, 18 parts of polyurethane, 6 parts of titanium dioxide, 13 parts of trichloro ethylene and dibasic ester.
3. it is as claimed in claim 1 it is a kind of can selfreparing high molecular nanometer tyre cement, it is characterised in that：By following parts by weight
Several raw materials are made, including 18.5 parts of acrylic acid, 9 parts of silica flour, 15.5 parts of nonyl phenol, 12 parts of ammonium hydroxide, nano zine oxide 6
Part, 14.5 parts of Nano silica sol, 22 parts of isocyanates, 5 parts of Arcton 11,10 parts of waterglass, 23 parts of amino resins, dehydration mountain
8 parts of pears alcohol monoleate, 13.5 parts of ammonium polyphosphate, 6.5 parts of Firebrake ZB, 9 parts of methyl anyl alcohol, 15.5 parts of active carbon nanoparticles, vinegar
Sour 18 parts of ethene, 23 parts of cobalt soap, 14 parts of different n-nonanoic acid, 19 parts of polyurethane, 8 parts of titanium dioxide, 15.5 parts of trichloro ethylene and dibasic ester
26 parts.
4. it is as claimed in claim 1 it is a kind of can selfreparing high molecular nanometer tyre cement, it is characterised in that：By following parts by weight
Several raw materials are made, including 22 parts of acrylic acid, 10 parts of silica flour, 18 parts of nonyl phenol, 15 parts of ammonium hydroxide, 8 parts of nano zine oxide,
16 parts of Nano silica sol, 24 parts of isocyanates, 7 parts of Arcton 11,15 parts of waterglass, 24 parts of amino resins, anhydrous sorbitol
10 parts of monoleate, 15 parts of ammonium polyphosphate, 8 parts of Firebrake ZB, 11 parts of methyl anyl alcohol, 18 parts of active carbon nanoparticles, vinyl acetate 20
Part, 24 parts of cobalt soap, 16 parts of different n-nonanoic acid, 22 parts of polyurethane, 10 parts of titanium dioxide, 18 parts of trichloro ethylene and 28 parts of dibasic ester.
5. it is a kind of can selfreparing high molecular nanometer tyre cement preparation method, it is characterised in that：Comprise the following steps：
1）By 15-22 parts of acrylic acid, 8-10 parts of silica flour, 13-18 parts of nonyl phenol, 9-15 parts of ammonium hydroxide, nano zine oxide 4-8
Part, 13-16 parts of Nano silica sol, 20-24 parts of isocyanates, 3-7 parts of Arcton 11,5-15 parts of waterglass, amino resins 22-
24 parts, 6-10 parts of sorbitan monooleate put into oil bath pan, regulation preheating temperature is 65-70 DEG C, heating 5-7 point
Clock, it is standby；
2）By step 1）Gained raw material is put into colloid mill, and regulation rotating speed is 5500-6800r/min, is ground 12-15 minutes,
It is standby；
3）By 12-15 parts of ammonium polyphosphate, 5-8 parts of Firebrake ZB, 7-11 parts of methyl anyl alcohol, 13-18 parts of active carbon nanoparticles, acetic acid second
16-20 parts of alkene, 22-24 parts of cobalt soap, different n-nonanoic acid 12-16 parts, 18-22 parts of polyurethane, 6-10 parts of titanium dioxide, trichloro ethylene 13-18
24-28 parts of part and dibasic ester are put into reactor, and regulation speed of agitator is 2200-2400r/min, and heating-up temperature is 45-
55 DEG C, react 6-10 minutes, it is standby；
4）By step 2) gained raw material and step 3）Gained raw material is put into banbury, and regulation heating-up temperature is 95-120 DEG C,
Mixing 25-35 minutes, it is standby；
5）By step 4）Gained raw material is put into vacuum kettle, and it is 220-240r/min, reaction that mixing speed is adjusted at normal temperatures
Time is 8-12 minutes, standby；
6）By step 5）Gained raw material puts into tank body interior sealing, and storage is preserved in the cool, you can.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201710229504.4A CN106957606A (en) | 2017-04-10 | 2017-04-10 | It is a kind of can selfreparing high molecular nanometer tyre cement and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710229504.4A CN106957606A (en) | 2017-04-10 | 2017-04-10 | It is a kind of can selfreparing high molecular nanometer tyre cement and preparation method thereof |
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| CN106957606A true CN106957606A (en) | 2017-07-18 |
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| CN201710229504.4A Pending CN106957606A (en) | 2017-04-10 | 2017-04-10 | It is a kind of can selfreparing high molecular nanometer tyre cement and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108192555A (en) * | 2018-02-12 | 2018-06-22 | 中山爵邦时装科技有限公司 | A kind of adhesive composition and its application in clothing |
| CN108308774A (en) * | 2018-04-23 | 2018-07-24 | 中山爵邦时装科技有限公司 | A kind of production method of seamless jeans |
| CN108378447A (en) * | 2018-02-12 | 2018-08-10 | 中山爵邦时装科技有限公司 | A kind of production method of seamless split clothes |
| CN108576998A (en) * | 2018-04-23 | 2018-09-28 | 中山爵邦时装科技有限公司 | A kind of production method of seamless knitting shirt |
| CN108948666A (en) * | 2018-07-06 | 2018-12-07 | 佛山市高明区爪和新材料科技有限公司 | A kind of preparation method of Automatic-inflating tyre repair liquid |
| CN113416513A (en) * | 2021-06-22 | 2021-09-21 | 东莞市宝临塑胶有限公司 | Macromolecular automatic inflation tire repair liquid and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104804681A (en) * | 2015-04-20 | 2015-07-29 | 东莞平障王汽车配件有限公司 | Material with automatic memory recovery function, and leak-proof anti-puncturing tire containing material |
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- 2017-04-10 CN CN201710229504.4A patent/CN106957606A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104804681A (en) * | 2015-04-20 | 2015-07-29 | 东莞平障王汽车配件有限公司 | Material with automatic memory recovery function, and leak-proof anti-puncturing tire containing material |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108192555A (en) * | 2018-02-12 | 2018-06-22 | 中山爵邦时装科技有限公司 | A kind of adhesive composition and its application in clothing |
| CN108378447A (en) * | 2018-02-12 | 2018-08-10 | 中山爵邦时装科技有限公司 | A kind of production method of seamless split clothes |
| CN108308774A (en) * | 2018-04-23 | 2018-07-24 | 中山爵邦时装科技有限公司 | A kind of production method of seamless jeans |
| CN108576998A (en) * | 2018-04-23 | 2018-09-28 | 中山爵邦时装科技有限公司 | A kind of production method of seamless knitting shirt |
| CN108948666A (en) * | 2018-07-06 | 2018-12-07 | 佛山市高明区爪和新材料科技有限公司 | A kind of preparation method of Automatic-inflating tyre repair liquid |
| CN113416513A (en) * | 2021-06-22 | 2021-09-21 | 东莞市宝临塑胶有限公司 | Macromolecular automatic inflation tire repair liquid and preparation method thereof |
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