CN106957153A - A kind of method of vehicle glass plated film - Google Patents
A kind of method of vehicle glass plated film Download PDFInfo
- Publication number
- CN106957153A CN106957153A CN201710178508.4A CN201710178508A CN106957153A CN 106957153 A CN106957153 A CN 106957153A CN 201710178508 A CN201710178508 A CN 201710178508A CN 106957153 A CN106957153 A CN 106957153A
- Authority
- CN
- China
- Prior art keywords
- cleaning
- plated film
- vacuum
- vehicle glass
- substrate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
- C03C17/3411—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions with at least two coatings of inorganic materials
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
- C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
- C03C17/40—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal all coatings being metal coatings
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/20—Materials for coating a single layer on glass
- C03C2217/25—Metals
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/20—Materials for coating a single layer on glass
- C03C2217/25—Metals
- C03C2217/251—Al, Cu, Mg or noble metals
- C03C2217/253—Cu
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/20—Materials for coating a single layer on glass
- C03C2217/25—Metals
- C03C2217/251—Al, Cu, Mg or noble metals
- C03C2217/254—Noble metals
- C03C2217/256—Ag
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
- C03C2218/10—Deposition methods
- C03C2218/15—Deposition methods from the vapour phase
- C03C2218/151—Deposition methods from the vapour phase by vacuum evaporation
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Surface Treatment Of Glass (AREA)
Abstract
The invention discloses a kind of method of vehicle glass plated film, comprise the following steps：（1）The preparation of substrate；（2）Vacuum coating, the preparation of substrate includes placing the substrate on support and then carries out cleaning, drying for surface；Wherein the cleaning of substrate surface is cleaned including organic cleaning solvent, aqueous cleaning agent cleaning, pure water rinsing, isopropanol dehydration, and then isopropanol draws drying slowly；Organic cleaning solvent cleaning, aqueous cleaning agent cleaning are ultrasonic wave cleaning；Using technical scheme, institute's plated film has higher transmissivity to visible ray, there is very high reflectivity to infrared ray, with good heat-proof quality, makes the light of in-car soft, mitigates driver and crew because the sense of fatigue that the irradiation of high light is produced；Ensure the thickness of film layer and the uniformity of coating.
Description
Technical field
The invention belongs to automobile manufacturing field, it is more particularly related to a kind of method of vehicle glass plated film.
Background technology
Coating film on glass, using reflectance coating technique or the composition of improvement glass, changes glass optics properties, makes the sun visible
Light enters in compartment, stops the ultraviolet and infrared ray of sunshine, not only alleviates the hardship for the sweltering heat that occupant is subject to, while allowing car
Interior light is soft, mitigates driver and crew because the sense of fatigue that the irradiation of high light is produced, the thickness of film layer and the uniformity of coating,
Quality influence on coated glass is very big.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of automobile of the uniformity of thickness for ensureing film layer and coating
The method of coating film on glass.
To achieve these goals, the technical scheme taken of the present invention is：A kind of side of the vehicle glass plated film provided
Method, comprises the following steps：
(1) preparation of substrate；(2) vacuum coating.
A kind of method of vehicle glass plated film disclosed by the invention, the preparation of substrate includes placing the substrate on support then
Carry out cleaning, drying for surface；Wherein the cleaning of substrate surface is cleaned including organic cleaning solvent, aqueous cleaning agent cleaning,
Pure water is rinsed, isopropanol dehydration, and then isopropanol draws drying slowly.
A kind of method of vehicle glass plated film disclosed by the invention, organic cleaning solvent cleaning, aqueous cleaning agent cleaning
Cleaned for ultrasonic wave.
A kind of method of vehicle glass plated film disclosed by the invention, vacuum coating is vacuum vapor plating, and vacuum state is adopted
The surface of glass is attached to the compound of silver, copper, tin metal or its silver, copper, tin of more than two layers of electron gun evaporation.
A kind of method of vehicle glass plated film disclosed by the invention, film thickness is 140nm~180nm.
A kind of method of vehicle glass plated film disclosed by the invention, vacuum vapor plating is completed in vacuum storehouse, very
The vacuum of hole capital after selling all securities is 4 × 10-3It is more than handkerchief.
A kind of method of vehicle glass plated film disclosed by the invention, comprises the following steps：(1) preparation of substrate；(2) vacuum
Plated film, the preparation of substrate includes placing the substrate on support and then carries out cleaning, drying for surface；The wherein cleaning of substrate surface
Including organic cleaning solvent cleaning, aqueous cleaning agent cleaning, pure water are rinsed, isopropanol dehydration, and then isopropanol draws drying slowly；
Organic cleaning solvent cleaning, aqueous cleaning agent cleaning are ultrasonic wave cleaning；Using technical scheme, cleaned before plated film
The major pollutants cleaned before plated film are greasy dirt, impression of the hand, dust etc., and coating quality depends on the cleanliness factor of substrate, therefore, this hair
Bright use ultrasonic wave organic cleaning solvent cleaning, then using the cleaning of ultrasonic wave aqueous cleaning agent, then further using pure
Water is rinsed, and then isopropanol draws drying slowly, it is to avoid dry the quality that washmarking reduction plated film is left on meron surface；Vacuum coating is
Vacuum vapor plating, vacuum state is using the silver of more than two layers of electron gun evaporation, copper, tin metal or its silver, copper, the compound of tin
It is attached to the surface of glass；This film has higher transmissivity to visible ray, has very high reflectivity to infrared ray, with good
Heat-proof quality, allow in-car light it is soft, mitigate driver and crew because high light irradiation produce sense of fatigue；Ensure film layer
Thickness and the uniformity of coating；Film thickness is 140nm~180nm；The thickness of film layer, not only influences the quality of vehicle glass, shadow
The sight for mitigating driver and crew is rung, the safe driving to automobile plays a decisive role, and vacuum vapor plating is complete in vacuum storehouse
Into, the vacuum in vacuum storehouse is 4 × 10-3It is more than handkerchief；The thinner thickness of vacuum vapor plating film layer, can not only ensure plated film
Quality, while saving coating material, vacuum has direct influence, the higher film layer of vacuum on the thickness and the uniformity of film layer
Quality it is better, still, the requirement of too high vacuum to equipment is higher, increases the cost of equipment, and rational vacuum is protected
While demonstrate,proving film quality, production cost is reduced.
Below with reference to embodiment, the present invention is described in detail.
Embodiment
Below by the description to embodiment, shape to the embodiment of the present invention such as involved each component,
Construction, the mutual alignment between each several part and annexation, the effect of each several part and operation principle, manufacturing process and operate with
Method etc., is described in further detail, to help those skilled in the art to have inventive concept of the invention, technical scheme
More complete, accurate and deep understanding.
A kind of method for vehicle glass plated film that the present embodiment is related to, comprises the following steps：(1) preparation of substrate；(2) it is true
Empty plated film, the preparation of substrate includes placing the substrate on support and then carries out cleaning, drying for surface；Wherein substrate surface is clear
Clean including organic cleaning solvent cleaning, aqueous cleaning agent cleaning, pure water are rinsed, isopropanol dehydration, and then isopropanol draws dry slowly
It is dry；Organic cleaning solvent cleaning, aqueous cleaning agent cleaning are ultrasonic wave cleaning；Using technical scheme, before plated film
The major pollutants cleaned before cleaning plated film are greasy dirt, impression of the hand, dust etc., and coating quality depends on the cleanliness factor of substrate, therefore,
Then the present invention is further adopted using the cleaning of ultrasonic wave organic cleaning solvent, then using the cleaning of ultrasonic wave aqueous cleaning agent
Rinsed with pure water, then isopropanol draws drying slowly, it is to avoid dry the quality that washmarking reduction plated film is left on meron surface；Vacuum Deposition
Film is vacuum vapor plating, and vacuum state is using the silver of more than two layers of electron gun evaporation, copper, tin metal or its silver, copper, the change of tin
Compound is attached to the surface of glass；This film has higher transmissivity to visible ray, has very high reflectivity to infrared ray, has
Good heat-proof quality, makes the light of in-car soft, mitigates driver and crew because the sense of fatigue that the irradiation of high light is produced；Ensure film
The thickness of layer and the uniformity of coating；Film thickness is 140nm~180nm；The thickness of film layer, not only influences the matter of vehicle glass
Amount, influence mitigates the sight of driver and crew, and the safe driving to automobile plays a decisive role, and vacuum vapor plating is in vacuum storehouse
Interior completion, the vacuum in vacuum storehouse is 4 × 10-3It is more than handkerchief；The thinner thickness of vacuum vapor plating film layer, can not only ensure
The quality of plated film, while saving coating material, vacuum has direct influence to the thickness and the uniformity of film layer, and vacuum is higher
The quality of film layer is better, still, and the requirement of too high vacuum to equipment is higher, increases the cost of equipment, rational vacuum
While degree ensures film quality, production cost is reduced.
Using technical scheme, the consistency of vehicle glass plated film is high, intensity and good endurance, adhesive strength
Height, by test, coating film on glass hardness:4300HV；Coefficient of friction:0.21VSNi；Oxidation resistance temperature:1200 DEG C, the sun is visible
Light transmission rate>90%, ultraviolet and infrared ray<5%.
The present invention is exemplarily described above in association with embodiment, it is clear that the present invention is implemented not by above-mentioned side
The limitation of formula, if the improvement for the various unsubstantialities that method of the present invention design and technical scheme are carried out is employed, or without
Improve and the design of the present invention and technical scheme are directly applied into other occasions, within protection scope of the present invention.
Claims (6)
1. a kind of method of vehicle glass plated film, it is characterised in that：Comprise the following steps：
（1）The preparation of substrate；
（2）Vacuum coating.
2. according to a kind of method of vehicle glass plated film described in claim 1, it is characterised in that：The preparation bag of described substrate
Include and place the substrate on support and then carry out cleaning, drying for surface；Wherein the cleaning of substrate surface is cleaned including organic solvent
Agent is cleaned, aqueous cleaning agent cleaning, pure water rinsing, isopropanol dehydration, and then isopropanol draws drying slowly.
3. according to a kind of method of vehicle glass plated film described in claim 2, it is characterised in that：Described organic solvent cleaning
Agent cleaning, aqueous cleaning agent cleaning are ultrasonic wave cleaning.
4. according to a kind of method of vehicle glass plated film described in claim 1, it is characterised in that：Described vacuum coating is true
Empty evaporation coating, vacuum state is attached using the compound of silver, copper, tin metal or its silver, copper, tin of more than two layers of electron gun evaporation
On the surface of glass.
5. according to a kind of method of vehicle glass plated film described in claim 1 or 4, it is characterised in that：Described film thickness is
140nm~180nm。
6. according to a kind of method of vehicle glass plated film described in claim 1, it is characterised in that：Described vacuum vapor plating
Completed in vacuum storehouse, the vacuum in vacuum storehouse is 4 × 10-3It is more than handkerchief.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710178508.4A CN106957153A (en) | 2017-03-23 | 2017-03-23 | A kind of method of vehicle glass plated film |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710178508.4A CN106957153A (en) | 2017-03-23 | 2017-03-23 | A kind of method of vehicle glass plated film |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106957153A true CN106957153A (en) | 2017-07-18 |
Family
ID=59471158
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710178508.4A Withdrawn CN106957153A (en) | 2017-03-23 | 2017-03-23 | A kind of method of vehicle glass plated film |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106957153A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108311463A (en) * | 2017-12-19 | 2018-07-24 | 湖南中锂新材料有限公司 | Film cleaning method and device |
| CN109553308A (en) * | 2018-12-29 | 2019-04-02 | 河南中汇新材科技有限公司 | Self-cleaning glass and its manufacturing method |
| CN117995953A (en) * | 2024-04-02 | 2024-05-07 | 深圳市华皓伟业光电有限公司 | Device with high-light-transmittance fluorescent film and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101186449A (en) * | 2007-12-07 | 2008-05-28 | 宋秀宁 | Multiple film series film coated glass and preparing method thereof |
-
2017
- 2017-03-23 CN CN201710178508.4A patent/CN106957153A/en not_active Withdrawn
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101186449A (en) * | 2007-12-07 | 2008-05-28 | 宋秀宁 | Multiple film series film coated glass and preparing method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 赵金柱等: "《玻璃深加工技术与设备》", 31 March 2012, 化学工业出版社 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108311463A (en) * | 2017-12-19 | 2018-07-24 | 湖南中锂新材料有限公司 | Film cleaning method and device |
| CN109553308A (en) * | 2018-12-29 | 2019-04-02 | 河南中汇新材科技有限公司 | Self-cleaning glass and its manufacturing method |
| CN117995953A (en) * | 2024-04-02 | 2024-05-07 | 深圳市华皓伟业光电有限公司 | Device with high-light-transmittance fluorescent film and preparation method thereof |
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|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20170718 |
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| WW01 | Invention patent application withdrawn after publication |