CN106957153A - A kind of method of vehicle glass plated film - Google Patents

A kind of method of vehicle glass plated film Download PDF

Info

Publication number
CN106957153A
CN106957153A CN201710178508.4A CN201710178508A CN106957153A CN 106957153 A CN106957153 A CN 106957153A CN 201710178508 A CN201710178508 A CN 201710178508A CN 106957153 A CN106957153 A CN 106957153A
Authority
CN
China
Prior art keywords
cleaning
plated film
vacuum
vehicle glass
substrate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201710178508.4A
Other languages
Chinese (zh)
Inventor
魏芳芳
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hefei Xieyao Glassware Co Ltd
Original Assignee
Hefei Xieyao Glassware Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hefei Xieyao Glassware Co Ltd filed Critical Hefei Xieyao Glassware Co Ltd
Priority to CN201710178508.4A priority Critical patent/CN106957153A/en
Publication of CN106957153A publication Critical patent/CN106957153A/en
Withdrawn legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/34Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
    • C03C17/3411Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions with at least two coatings of inorganic materials
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/34Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
    • C03C17/36Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
    • C03C17/40Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal all coatings being metal coatings
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2217/00Coatings on glass
    • C03C2217/20Materials for coating a single layer on glass
    • C03C2217/25Metals
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2217/00Coatings on glass
    • C03C2217/20Materials for coating a single layer on glass
    • C03C2217/25Metals
    • C03C2217/251Al, Cu, Mg or noble metals
    • C03C2217/253Cu
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2217/00Coatings on glass
    • C03C2217/20Materials for coating a single layer on glass
    • C03C2217/25Metals
    • C03C2217/251Al, Cu, Mg or noble metals
    • C03C2217/254Noble metals
    • C03C2217/256Ag
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2218/00Methods for coating glass
    • C03C2218/10Deposition methods
    • C03C2218/15Deposition methods from the vapour phase
    • C03C2218/151Deposition methods from the vapour phase by vacuum evaporation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Surface Treatment Of Glass (AREA)

Abstract

The invention discloses a kind of method of vehicle glass plated film, comprise the following steps:(1)The preparation of substrate;(2)Vacuum coating, the preparation of substrate includes placing the substrate on support and then carries out cleaning, drying for surface;Wherein the cleaning of substrate surface is cleaned including organic cleaning solvent, aqueous cleaning agent cleaning, pure water rinsing, isopropanol dehydration, and then isopropanol draws drying slowly;Organic cleaning solvent cleaning, aqueous cleaning agent cleaning are ultrasonic wave cleaning;Using technical scheme, institute's plated film has higher transmissivity to visible ray, there is very high reflectivity to infrared ray, with good heat-proof quality, makes the light of in-car soft, mitigates driver and crew because the sense of fatigue that the irradiation of high light is produced;Ensure the thickness of film layer and the uniformity of coating.

Description

A kind of method of vehicle glass plated film
Technical field
The invention belongs to automobile manufacturing field, it is more particularly related to a kind of method of vehicle glass plated film.
Background technology
Coating film on glass, using reflectance coating technique or the composition of improvement glass, changes glass optics properties, makes the sun visible Light enters in compartment, stops the ultraviolet and infrared ray of sunshine, not only alleviates the hardship for the sweltering heat that occupant is subject to, while allowing car Interior light is soft, mitigates driver and crew because the sense of fatigue that the irradiation of high light is produced, the thickness of film layer and the uniformity of coating, Quality influence on coated glass is very big.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of automobile of the uniformity of thickness for ensureing film layer and coating The method of coating film on glass.
To achieve these goals, the technical scheme taken of the present invention is:A kind of side of the vehicle glass plated film provided Method, comprises the following steps:
(1) preparation of substrate;(2) vacuum coating.
A kind of method of vehicle glass plated film disclosed by the invention, the preparation of substrate includes placing the substrate on support then Carry out cleaning, drying for surface;Wherein the cleaning of substrate surface is cleaned including organic cleaning solvent, aqueous cleaning agent cleaning, Pure water is rinsed, isopropanol dehydration, and then isopropanol draws drying slowly.
A kind of method of vehicle glass plated film disclosed by the invention, organic cleaning solvent cleaning, aqueous cleaning agent cleaning Cleaned for ultrasonic wave.
A kind of method of vehicle glass plated film disclosed by the invention, vacuum coating is vacuum vapor plating, and vacuum state is adopted The surface of glass is attached to the compound of silver, copper, tin metal or its silver, copper, tin of more than two layers of electron gun evaporation.
A kind of method of vehicle glass plated film disclosed by the invention, film thickness is 140nm~180nm.
A kind of method of vehicle glass plated film disclosed by the invention, vacuum vapor plating is completed in vacuum storehouse, very The vacuum of hole capital after selling all securities is 4 × 10-3It is more than handkerchief.
A kind of method of vehicle glass plated film disclosed by the invention, comprises the following steps:(1) preparation of substrate;(2) vacuum Plated film, the preparation of substrate includes placing the substrate on support and then carries out cleaning, drying for surface;The wherein cleaning of substrate surface Including organic cleaning solvent cleaning, aqueous cleaning agent cleaning, pure water are rinsed, isopropanol dehydration, and then isopropanol draws drying slowly; Organic cleaning solvent cleaning, aqueous cleaning agent cleaning are ultrasonic wave cleaning;Using technical scheme, cleaned before plated film The major pollutants cleaned before plated film are greasy dirt, impression of the hand, dust etc., and coating quality depends on the cleanliness factor of substrate, therefore, this hair Bright use ultrasonic wave organic cleaning solvent cleaning, then using the cleaning of ultrasonic wave aqueous cleaning agent, then further using pure Water is rinsed, and then isopropanol draws drying slowly, it is to avoid dry the quality that washmarking reduction plated film is left on meron surface;Vacuum coating is Vacuum vapor plating, vacuum state is using the silver of more than two layers of electron gun evaporation, copper, tin metal or its silver, copper, the compound of tin It is attached to the surface of glass;This film has higher transmissivity to visible ray, has very high reflectivity to infrared ray, with good Heat-proof quality, allow in-car light it is soft, mitigate driver and crew because high light irradiation produce sense of fatigue;Ensure film layer Thickness and the uniformity of coating;Film thickness is 140nm~180nm;The thickness of film layer, not only influences the quality of vehicle glass, shadow The sight for mitigating driver and crew is rung, the safe driving to automobile plays a decisive role, and vacuum vapor plating is complete in vacuum storehouse Into, the vacuum in vacuum storehouse is 4 × 10-3It is more than handkerchief;The thinner thickness of vacuum vapor plating film layer, can not only ensure plated film Quality, while saving coating material, vacuum has direct influence, the higher film layer of vacuum on the thickness and the uniformity of film layer Quality it is better, still, the requirement of too high vacuum to equipment is higher, increases the cost of equipment, and rational vacuum is protected While demonstrate,proving film quality, production cost is reduced.
Below with reference to embodiment, the present invention is described in detail.
Embodiment
Below by the description to embodiment, shape to the embodiment of the present invention such as involved each component, Construction, the mutual alignment between each several part and annexation, the effect of each several part and operation principle, manufacturing process and operate with Method etc., is described in further detail, to help those skilled in the art to have inventive concept of the invention, technical scheme More complete, accurate and deep understanding.
A kind of method for vehicle glass plated film that the present embodiment is related to, comprises the following steps:(1) preparation of substrate;(2) it is true Empty plated film, the preparation of substrate includes placing the substrate on support and then carries out cleaning, drying for surface;Wherein substrate surface is clear Clean including organic cleaning solvent cleaning, aqueous cleaning agent cleaning, pure water are rinsed, isopropanol dehydration, and then isopropanol draws dry slowly It is dry;Organic cleaning solvent cleaning, aqueous cleaning agent cleaning are ultrasonic wave cleaning;Using technical scheme, before plated film The major pollutants cleaned before cleaning plated film are greasy dirt, impression of the hand, dust etc., and coating quality depends on the cleanliness factor of substrate, therefore, Then the present invention is further adopted using the cleaning of ultrasonic wave organic cleaning solvent, then using the cleaning of ultrasonic wave aqueous cleaning agent Rinsed with pure water, then isopropanol draws drying slowly, it is to avoid dry the quality that washmarking reduction plated film is left on meron surface;Vacuum Deposition Film is vacuum vapor plating, and vacuum state is using the silver of more than two layers of electron gun evaporation, copper, tin metal or its silver, copper, the change of tin Compound is attached to the surface of glass;This film has higher transmissivity to visible ray, has very high reflectivity to infrared ray, has Good heat-proof quality, makes the light of in-car soft, mitigates driver and crew because the sense of fatigue that the irradiation of high light is produced;Ensure film The thickness of layer and the uniformity of coating;Film thickness is 140nm~180nm;The thickness of film layer, not only influences the matter of vehicle glass Amount, influence mitigates the sight of driver and crew, and the safe driving to automobile plays a decisive role, and vacuum vapor plating is in vacuum storehouse Interior completion, the vacuum in vacuum storehouse is 4 × 10-3It is more than handkerchief;The thinner thickness of vacuum vapor plating film layer, can not only ensure The quality of plated film, while saving coating material, vacuum has direct influence to the thickness and the uniformity of film layer, and vacuum is higher The quality of film layer is better, still, and the requirement of too high vacuum to equipment is higher, increases the cost of equipment, rational vacuum While degree ensures film quality, production cost is reduced.
Using technical scheme, the consistency of vehicle glass plated film is high, intensity and good endurance, adhesive strength Height, by test, coating film on glass hardness:4300HV;Coefficient of friction:0.21VSNi;Oxidation resistance temperature:1200 DEG C, the sun is visible Light transmission rate>90%, ultraviolet and infrared ray<5%.
The present invention is exemplarily described above in association with embodiment, it is clear that the present invention is implemented not by above-mentioned side The limitation of formula, if the improvement for the various unsubstantialities that method of the present invention design and technical scheme are carried out is employed, or without Improve and the design of the present invention and technical scheme are directly applied into other occasions, within protection scope of the present invention.

Claims (6)

1. a kind of method of vehicle glass plated film, it is characterised in that:Comprise the following steps:
(1)The preparation of substrate;
(2)Vacuum coating.
2. according to a kind of method of vehicle glass plated film described in claim 1, it is characterised in that:The preparation bag of described substrate Include and place the substrate on support and then carry out cleaning, drying for surface;Wherein the cleaning of substrate surface is cleaned including organic solvent Agent is cleaned, aqueous cleaning agent cleaning, pure water rinsing, isopropanol dehydration, and then isopropanol draws drying slowly.
3. according to a kind of method of vehicle glass plated film described in claim 2, it is characterised in that:Described organic solvent cleaning Agent cleaning, aqueous cleaning agent cleaning are ultrasonic wave cleaning.
4. according to a kind of method of vehicle glass plated film described in claim 1, it is characterised in that:Described vacuum coating is true Empty evaporation coating, vacuum state is attached using the compound of silver, copper, tin metal or its silver, copper, tin of more than two layers of electron gun evaporation On the surface of glass.
5. according to a kind of method of vehicle glass plated film described in claim 1 or 4, it is characterised in that:Described film thickness is 140nm~180nm。
6. according to a kind of method of vehicle glass plated film described in claim 1, it is characterised in that:Described vacuum vapor plating Completed in vacuum storehouse, the vacuum in vacuum storehouse is 4 × 10-3It is more than handkerchief.
CN201710178508.4A 2017-03-23 2017-03-23 A kind of method of vehicle glass plated film Withdrawn CN106957153A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710178508.4A CN106957153A (en) 2017-03-23 2017-03-23 A kind of method of vehicle glass plated film

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710178508.4A CN106957153A (en) 2017-03-23 2017-03-23 A kind of method of vehicle glass plated film

Publications (1)

Publication Number Publication Date
CN106957153A true CN106957153A (en) 2017-07-18

Family

ID=59471158

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710178508.4A Withdrawn CN106957153A (en) 2017-03-23 2017-03-23 A kind of method of vehicle glass plated film

Country Status (1)

Country Link
CN (1) CN106957153A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108311463A (en) * 2017-12-19 2018-07-24 湖南中锂新材料有限公司 Film cleaning method and device
CN109553308A (en) * 2018-12-29 2019-04-02 河南中汇新材科技有限公司 Self-cleaning glass and its manufacturing method
CN117995953A (en) * 2024-04-02 2024-05-07 深圳市华皓伟业光电有限公司 Device with high-light-transmittance fluorescent film and preparation method thereof

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101186449A (en) * 2007-12-07 2008-05-28 宋秀宁 Multiple film series film coated glass and preparing method thereof

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101186449A (en) * 2007-12-07 2008-05-28 宋秀宁 Multiple film series film coated glass and preparing method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
赵金柱等: "《玻璃深加工技术与设备》", 31 March 2012, 化学工业出版社 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108311463A (en) * 2017-12-19 2018-07-24 湖南中锂新材料有限公司 Film cleaning method and device
CN109553308A (en) * 2018-12-29 2019-04-02 河南中汇新材科技有限公司 Self-cleaning glass and its manufacturing method
CN117995953A (en) * 2024-04-02 2024-05-07 深圳市华皓伟业光电有限公司 Device with high-light-transmittance fluorescent film and preparation method thereof

Similar Documents

Publication Publication Date Title
TWI441944B (en) A light reflecting plate, a manufacturing method thereof, and a light reflecting device
EP2646382B1 (en) Anti-glare surface treatment method and articles thereof
US9085484B2 (en) Anti-glare surface treatment method and articles thereof
CN106957153A (en) A kind of method of vehicle glass plated film
CN107924002A (en) Translucency structure, its manufacture method and article
JP2021504282A (en) Glass sheet coated with thin stack and enamel layer
US20140370303A1 (en) Antimicrobial glass articles and methods of making and using same
TW201539050A (en) Infrared reflecting substrate and method for producing same
EP2952939A1 (en) Method for producing infrared radiation reflecting film
TW201337316A (en) Coated articles including anti-fingerprint and/or smudge-reducing coatings, and/or methods of making the same
CN108623179A (en) Glare proof glass substrate
CN106575005A (en) Infrared-reflecting film
SE503967C2 (en) Methods for making a reflective article
CN105859153A (en) Antifogging antireflection visible-light double-function coated glass and preparation method thereof
EP2029497B1 (en) Coated glass sheet
JP2014170171A (en) Transparent heat shield film with anti-reflection properties
US20090220685A1 (en) Mirror with epoxy paint layer having good resistance to handling
CN107619197A (en) A kind of compound caesium tungsten nanometer thermal insulation coating glass and its manufacture method
JP2017506731A (en) Coating that selectively absorbs radiation and method for obtaining the coating at ambient temperature
WO2017094736A1 (en) Glass manufacturing method
CN109957758B (en) Colorful aluminum product and preparation method thereof, mobile phone middle frame and mobile phone shell
JP2015030874A (en) Antifouling processing method of antibacterial product
RU2017127198A (en) Architectural glass with a low emission coating, having a multilayer structure having high strength, and / or a method for its manufacture
WO2018181444A1 (en) Heat-shielding heat insulating substrate
CN109082639A (en) A kind of uvioresistant plating ZnO/SiO2The superlattices automobile PET pad pasting of nanometer multilayer material

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WW01 Invention patent application withdrawn after publication

Application publication date: 20170718

WW01 Invention patent application withdrawn after publication