CN106929714B - A kind of preparation method of high intensity tableware aluminium foil - Google Patents

A kind of preparation method of high intensity tableware aluminium foil Download PDF

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Publication number
CN106929714B
CN106929714B CN201710283142.7A CN201710283142A CN106929714B CN 106929714 B CN106929714 B CN 106929714B CN 201710283142 A CN201710283142 A CN 201710283142A CN 106929714 B CN106929714 B CN 106929714B
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aluminium
rolling
cold rolling
temperature
tableware
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CN106929714A (en
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张安乐
韩成艺
刘雪梅
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LUOYANG LONGDING ALUMINUM CO Ltd
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LUOYANG LONGDING ALUMINUM CO Ltd
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    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C21/00Alloys based on aluminium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B1/00Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations
    • B21B1/40Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling foils which present special problems, e.g. because of thinness
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C21/00Alloys based on aluminium
    • C22C21/06Alloys based on aluminium with magnesium as the next major constituent
    • C22C21/08Alloys based on aluminium with magnesium as the next major constituent with silicon
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/04Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/04Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon
    • C22F1/047Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon of alloys with magnesium as the next major constituent

Abstract

A kind of preparation method of high intensity tableware aluminium foil, electrolytic aluminium liquid and aluminium ingot are first smelted into aluminum melt, 3~5mm thickness aluminium is prepared by casting and rolling process again to roll up, then roll by cold rolling → slitting trimming → paper tinsel → finished product cutting → finished products → inspection packaging prepares high intensity tableware aluminium foil, wherein slitting trimming, finished product cuts and checks that routinely technique carries out packaging, 0.05 ~ 0.095mm thick aluminum foils volume after finished products just becomes tableware aluminium foil, tensile strength >=220Mpa of the tableware aluminium foil after testing, elongation percentage >=6%, cupping >=4mm, casting and secondary remelting process present invention eliminates aluminium ingot, through measuring and calculating:Aluminium damage and the scaling loss of 2~4% aluminium during aluminium ingot secondary remelting that molten aluminum casts during aluminium ingot 0.4~0.5% can be reduced, the energy has been saved, has improved production efficiency and yield rate.

Description

A kind of preparation method of high intensity tableware aluminium foil
Technical field
The invention belongs to aluminium foil processing technique field, especially a kind of preparation method of high intensity tableware aluminium foil.
Background technology
Tableware aluminium foil is also commonly called as container foil, is a kind of aluminium foil for being widely used in the fields such as inflight meal, fast food packaging, tool There is the features such as beautiful, generous, clean, hygienic.Being commonly used for the alloy of production containers paper tinsel currently on the market has 8011,3003 etc.. But although such alloy has preferable plastic deformation ability, intensity is generally between 120~150Mpa, relatively low intensity Aluminium foil is caused after cutlery box is struck out, there is the defects of being easily deformed, damaging.And if to keep the good resistance to deformation of cutlery box Ability, then be necessarily required to increase aluminum foil thickness, cause waste of material.
3004 alloys become the first choice of production tableware aluminium foil with its excellent performance, and 3004 alloys prepare the normal of tableware Lv Be Advising technological process is:Melting and casting → hot rolling → cold rolling → intermediate annealing → slitting trimming → paper tinsel rolls → and finished product cutting → finished product moves back Fire → inspection packaging, 3004 alloys prepare each operation in the common process of tableware Lv Be and are summarized as follows:
First, melting and casting:
Conventional 3004 alloy castings use direct-cooled casting ingot process, aluminium ingot, solid during melting using content more than 99.7% Waste material, which is put into smelting furnace, carries out melting, is configured by alloying component, the process such as aluminum melt processing to be to ensure melt quality, melt Chemical composition should meet requirement in national standard GB/T3190-2012 to 3004 alloy compositions and referring to following table.Smelting furnace Temperature control system in the range of 750 ± 5 DEG C, hydrogen content control in below 0.14ml/100gAl, casting using rotation air blast into The online degasification of row, filtering use 30PPi+50PPi double-stage filterings, and alterant uses Al-5Ti-B, and aluminum melt is formed by mold The ingot casting of 400~600mm thickness.
2nd, hot rolling:
First the ingot casting saw head milling face that above-mentioned founding is processed is reheated again, 20~25 are kept the temperature under the conditions of 480~520 DEG C Hour, then the ingot casting after heating is thick to 6~8mm by the roughing mill cogging multi- pass rolling of big processing capacity and as coils It is transferred to cold rolling process.
3rd, cold rolling:
Between 6~8mm thickness hot rolled coils are cold rolled to 1.0~2.0mm thickness through multi-pass cold rolling, then moved back among high temperature Fire, continues to be cold rolled to trimming thickness being transferred to slitting trimming process again after cooling.
4th, high temperature intermediate annealing:
High temperature intermediate annealing process is:When insulation 20~25 is small under the conditions of 530~560 DEG C.
5th, slitting trimming:
Each deflector roll in guide passage must be wiped during slitting trimming clearly, each deflector roll is wiped clearly with alcohol or acetone, it is ensured that aluminium is rolled up Surface cannot have mark, viscous aluminium, scratch, scuffing, and end face is not allow for small broken sea of burr, turriform, scollop, scallop, edge etc., middle Trimming staggered floor is necessarily less than 2mm, and turriform is less than 5mm.
6th, paper tinsel rolls:
By several passes to finishing pass, aluminium foil surface is not allow for residual greasy dirt;Surface is not allow for elongated Or any surface defect for influencing to use such as discontinuity scratch, scuffing, Periodic Traveling mark, bright wisp and bright band, hidden bar, informal voucher.
7th, finished product is cut:
Each deflector roll in guide passage must be wiped during cutting clearly, each deflector roll is wiped clearly with alcohol or acetone;Ensure that aluminium rolls up surface Cannot there are mark, viscous aluminium, scratch, scuffing.The aluminium volume of cutting, which is placed on floor, must pad the big cardboard of lastblock, not allow directly to fall Ground.Small broken sea of burr, turriform, scollop, scallop, edge etc. is not allow for during cutting, cutting staggered floor is necessarily less than 0.5mm.After cutting Rouleau end face must totally, neatly;The rouleau lot number and specification cut must write on the surface of aluminium volume with marking pen.
8th, finished products;
During finished products with the sealing of high temperature resistant aluminum foil and adhesive tape ensure cannot after loose layer can stock shelf shove charge anneal.0.05~ 0.095mm thickness, when insulation 20~30 is small under the conditions of 220~260 DEG C.Material is unable to blanking rack after annealing is come out of the stove.After annealing Material completely cold must turn lower process.
9th, check and pack;
Mainly check that aluminum foil thickness, width must not exceed the margin of tolerance during finished product inspection, end face must not jagged, flange, Wound, staggered floor must not exceed 0.5mm.Compliant sleeve, material have to comply with customer requirement, and sleeve both sides stretch out aluminium foil end face and are respectively 5mm.It is required that accomplishing that tensile strength reaches 220Mpa or so, packed after qualified according to the packing instructions of tableware aluminium foil.
Its tensile strength of the aluminium foil of technique preparation can reach 220Mpa, but since production process is more, production cycle length, The factors such as cost height, at present to being rarely reported using 3004 alloy production tablewares with aluminium foil.Therefore using short route process, reduction Production cost becomes the important subject of 3004 alloy tableware aluminium foils of production at present.
The content of the invention
To solve the above problems, the present invention provides a kind of preparation method of high intensity tableware aluminium foil, first by electrolytic aluminium liquid Be smelted into aluminum melt with aluminium ingot and 3~5mm thickness aluminium volume produced using casting and rolling process, then by cold rolling and intermediate annealing, Paper tinsel rolls and the reasonable setting of the procedure parameter such as finished products, substantially reduces technological process, reduces production cost, prepares Go out its tensile strength >=220Mpa of high intensity tableware aluminium foil, elongation percentage >=6%, cupping >=4mm.
In order to realize foregoing invention purpose, the present invention adopts the following technical scheme that:
Electrolytic aluminium liquid and aluminium ingot are first smelted into aluminium and melted by a kind of preparation method of high intensity tableware aluminium foil, the preparation method Body, then 3~5mm thickness aluminium is prepared by casting and rolling process and is rolled up, then → finished product point is rolled by cold rolling → slitting trimming → paper tinsel Cut → finished products → inspection packaging prepares high intensity tableware aluminium foil, wherein slitting trimming, finished product cutting and check that packaging is pressed Common process carries out, it is characterized in that:
1) electrolytic aluminium liquid and aluminium ingot are smelted into aluminum melt:
By the electrolytic aluminium liquid of 80~90% parts by weight and the aluminium ingot of 10~20% parts by weight and aluminium content >=99.7% together It is put into smelting furnace and carries out melting and prepare aluminum melt, melting Control for Kiln Temperature is in the range of 750 ± 5 DEG C, aluminum melt during melting Chemical composition should meet following table requirement after testing, and require degasification, slagging-off totally and stir to ensure aluminum melt Quality.
2) 3~5mm thickness aluminium is prepared by casting and rolling process to roll up:
During continuous casting by by the bast mouth that heat safe inorganic non-metallic material is process by aluminum melt equivalent, note at the uniform velocity In the steel band for entering two opposite direction rotatings, and it is connected on the outside of two steel bands with recirculated cooling water, the heat in aluminum melt passes through steel Band and cooling water are pulled away, and the temperature of aluminum melt is maintained at 685 ± 10 DEG C of scopes during continuous casting, and casting speed is controlled in 8~11m/ Min, the slab thickness of casting are controlled in 19 ± 1mm, it is desirable to by adjusting cooling water pressure and flow to ensure strand temperature Control is in 520~580 DEG C of scopes;
The slab of continuous casting is directly entered three tandem mills and is lubricated and is cooled down using emulsion, the processing of the first passes Rate control 50~60% and rolling inlet temperature control at 420~500 DEG C and outlet temperature control at 360~420 DEG C, second Passes working modulus control 25~35% and rolling inlet temperature control at 330~390 DEG C and outlet temperature control 290 ~360 DEG C, the control of the 3rd pass reduction is controlled at 250~320 DEG C and outlet temperature control in 20~33% and inlet temperature At 220~250 DEG C, 3~5mm thickness aluminium volume is prepared through the processing of the 3rd passage;
3) cold rolling:
Continuous casting and rolling prepares directly upper cold mill complex after 3~5mm thickness aluminium volume and carries out each passage cold rolling and roll out 0.16 ~0.28mm cold rolling coils, the allocative decision of each passage cold rolling are:3.0~5.0mm → 2.0~3.5mm → intermediate annealing → 1.3~ 2.3mm → 0.9~1.6mm → 0.64~1.15mm → 0.45~0.81mm → 0.32~0.57mm → 0.23~0.40mm → 0.16~0.28mm → trimming, wherein 3.0~5.0mm → 2.0~3.5mm cold rolling pass working modulus control 25~35% it Between, remaining each cold rolling pass working modulus control is first by the cold rolling coil of 2.0~3.5mm thickness at 22.5~35.5%, intermediate annealing It is put into annealing furnace, 4h is kept the temperature when furnace temperature being raised to 220 DEG C with 2h afterwards, 10 is kept the temperature when furnace temperature then being raised to 530 DEG C with 3h ~20h, then when furnace temperature is dropped to 460 DEG C with 2h, keep the temperature 4h, come out of the stove when furnace temperature finally being dropped to 170 DEG C, cold after intermediate annealing 2.0~3.5mm thickness cold rolling coils should be checked by rolling volume and needing air-cooled to less than 60 DEG C to be transferred to subsequently each passes, when intermediate annealing again End face situation, checks that end socket whether using volume phenomenon whether is touched between high temperature gummed tape, whether firm, each cold rolling coil, checks stove Whether be stained with the circulated air hood of son aluminium end and whether remove it is clean just can be into furnace annealing;
Each cold rolling pass process is required to be lubricated and cooled down using ROLLING OIL, and pay attention to wiping clearly in guide passage each leads Roller, prevents surface of aluminum plate from having mark, viscous the defects of hindering;
4) paper tinsel rolls:
The cold rolling coil progress paper tinsel of 0.16~0.28mm thickness is rolled and prepares 0.05~0.095mm aluminium foils, each passage paper tinsel rolls Allocative decision be:0.16~0.28mm → 0.12~0.20mm → 0.09~0.15mm → 0.05~0.095mm, each passage paper tinsel Working roll must be replaced when rolling, clear each roller wiped in guide passage, supporting stick surface is not all right must to replace support roller;Rolling by Must be clean, its surface must purge clean and be not allow for residual greasy dirt when being rolled up to 0.05~0.095 thick aluminum foil, and surface does not permit Permitted to have any surfaces for influencing to use such as the scratch of elongated or discontinuity, scuffing, Periodic Traveling mark, bright wisp and bright band, hidden bar, informal voucher Defect;
5) finished products:
0.05~0.095mm thick aluminum foils are rolled into finished products are carried out in annealing furnace, furnace temperature is first raised to 210 DEG C with 4h Shi Baowen 20h, simultaneously cooled to room temperature of coming out of the stove when furnace temperature then being dropped to 170 DEG C;
The end face situation of 0.05~0.095mm thick aluminum foils volume should be checked during finished products, checks whether end socket uses high temperature Volume phenomenon whether is touched between adhesive tape, whether firm, each aluminum foil coil, checks whether be stained with aluminium foil simultaneously on the circulated air hood of stove Whether remove totally just can be into furnace annealing;
0.05~0.095mm thick aluminum foils volume after finished products just becomes tableware aluminium foil, after testing the tableware aluminium foil Tensile strength >=220Mpa, elongation percentage >=6%, cupping >=4mm.
Due to using technical solution as described above, the present invention produces following good effect:
1st, during melting of the present invention using the electrolytic aluminium liquid of 80~90% parts by weight and 10~20% parts by weight and aluminium content >= 99.7% aluminium ingot, which is together put into smelting furnace, carries out melting, while by the tire bag refining techniques of high-temperature electrolysis molten aluminum and changes Into the refinery practice in smelting furnace, such as increase time of repose, short time multiple refining technique, ensure that aluminum melt quality, from And realize and continuous casting and rolling volume abbreviated system is directly produced using electrolytic aluminium liquid.Compared with common process, the casting of aluminium ingot is eliminated Make with secondary remelting process, through measuring and calculating:Can reduce molten aluminum cast during aluminium ingot 0.4~0.5% aluminium damage and aluminium ingot it is secondary The scaling loss of 2~4% aluminium, has saved the energy in reflow process, improves production efficiency and yield rate.
2nd, directly rolled up using continuous casting and rolling process for production with aluminum melt production 3~5mm thickness aluminium, with traditional direct-cooled ingot casting heat Roll process is compared, and Ha Ziliete continuous casting and rolling Aluminum sheets production technologies eliminate the big plate ingot casting of traditional hot rolled alloy, ingot blank saw The multiple tracks links such as head milling face reheats again, the roughing mill split rolling method of big processing capacity, it is energy-saving, reduce carbon dioxide row Put, it is cost-effective, there is obvious economic benefit and social benefit.
3rd, conventional tableware is between the hot rolling material of 6~8mm thickness is rolled down to 1.0~2.0mm thickness, so with 3004 alloy aluminium foils Intermediate annealing afterwards, when being then rolled down to base material thickness trimming turn paper tinsel rolling.And the present invention is by continuous casting and rolling 3~5mm thickness aluminium Intermediate annealing is carried out when rolling up cold rolling a time to 2~3.5mm thickness cold rolling coils, the cold rolling coil after intermediate annealing carries out remaining each road again Secondary rolling, this method are saved 1~2 passage than traditional processing technology and are processed, and reduce production cost.
Embodiment
The present invention is a kind of preparation method of high intensity tableware aluminium foil, and electrolytic aluminium liquid and aluminium ingot are first smelted into aluminium by the present invention Melt simultaneously prepares 3-5mm thickness aluminium volume using casting and rolling process, then is rolled by cold rolling, paper tinsel and the procedure such as finished products The reasonable setting of parameter, high intensity tableware aluminium foil is directly prepared so as to fulfill aluminum melt, substantially reduces technological process, is reduced Production cost.
The total preparation method of the present invention is:Electrolytic aluminium liquid and aluminium ingot are smelted into aluminum melt → by casting and rolling process system → finished product cutting → finished products → inspection technology of the package preparation is rolled for 3~5mm thickness aluminium volume → cold rolling → slitting trimming → paper tinsel is gone out Go out high intensity tableware aluminium foil, wherein routinely technique carries out for slitting trimming, finished product cutting and inspection packaging, and not described part is with reference to the back of the body Scape technology related content.
The present invention can be explained in more detail by the following examples, the invention is not limited in the following examples, The open purpose of the present invention is intended to all changes and improvements in the protection scope of the invention.
First, electrolytic aluminium liquid and aluminium ingot are smelted into aluminum melt:
By the electrolytic aluminium liquid of 80~90% parts by weight and the aluminium ingot of 10~20% parts by weight and aluminium content >=99.7% together It is put into smelting furnace and carries out melting and prepare aluminum melt, melting Control for Kiln Temperature is in the range of 750 ± 5 DEG C, aluminum melt during melting Chemical composition should meet following table requirement after testing, and require to carry out degasification, slagging-off totally and stir to ensure that aluminium melts The quality of body;
The present invention is that a kind of improve on the basis of 3004 alloys is formulated, by upper table this it appears that aluminium of the present invention melts The chemical composition of body is formed in place of the micro change with 3004 alloy compositions.
2nd, 4.5mm thickness aluminium is prepared by casting and rolling process to roll up:
During continuous casting by by the bast mouth that heat safe inorganic non-metallic material is process by aluminum melt equivalent, note at the uniform velocity In the steel band for entering two opposite direction rotatings, and it is connected on the outside of two steel bands with recirculated cooling water, the heat in aluminum melt passes through steel Band and cooling water are pulled away, and the temperature of aluminum melt is maintained at 685 DEG C during continuous casting, casting speed control in 8.5m/min, casting Slab thickness is controlled in 19mm, it is desirable to by adjusting cooling water pressure and flow to ensure strand temperature control 520~580 DEG C scope.
The slab of continuous casting is directly entered three tandem mills and is lubricated and is cooled down using emulsion, the processing of the first passes Rate control 50% and rolling inlet temperature control at 490 DEG C and outlet temperature control at 420 DEG C, the second passage Reduction by rolling Control 32% and rolling inlet temperature control at 390 DEG C and outlet temperature control at 330 DEG C, the 3rd pass reduction control exists 33% and inlet temperature control at 300 DEG C and outlet temperature control at 225 DEG C, through the 3rd passage processing prepare 4.5mm thickness aluminium Volume.
3rd, cold rolling:
Directly upper cold mill complex carries out each passage cold rolling and rolls out 0.25mm after 4.5mm thickness aluminium volume is prepared in continuous casting and rolling Thick cold rolling coil, the allocative decision of each passage cold rolling are:Each cold rolling pass operation of rolling of 0.25mm thickness cold rolling coils is:4.5mm→ 3.0mm → intermediate annealing → 2.0mm → 1.55mm → 1.15mm → 0.86mm → 0.63mm → 0.45mm → 0.33mm → 0.25mm → trimming.
The cold rolling coil of 3.0mm thickness is first put into annealing furnace during intermediate annealing, is protected when furnace temperature being raised to 220 DEG C with 2h afterwards Warm 4h, keeps the temperature 10~20h when furnace temperature then being raised to 530 DEG C with 3h, then when furnace temperature is dropped to 460 DEG C with 2h keeps the temperature 4h, finally To come out of the stove when furnace temperature is dropped to 170 DEG C, the cold rolling coil after intermediate annealing needs air-cooled to less than 60 DEG C to be transferred to follow-up each passes again, Should check the end face situation of 3.0mm thickness cold rolling coils during intermediate annealing, check end socket whether using high temperature gummed tape, whether firmly, it is each Volume phenomenon whether is touched between cold rolling coil, checks whether to be stained with aluminium end on the circulated air hood of stove and whether remove and totally just may be used Into furnace annealing.
Each cold rolling pass process is required to be lubricated and cooled down using ROLLING OIL, and pay attention to wiping clearly in guide passage each leads Roller, prevents surface of aluminum plate from having mark, viscous the defects of hindering, and aluminium volume surface is not allow for bright wisp, bright band and aberration during each passage cold rolling, Surface purging has to totally, be not allow for residual greasy dirt, routinely technical requirements perform cold rolling speed.
4th, the reference common process process of slitting trimming:
Each deflector roll in guide passage must be wiped during slitting trimming clearly, each deflector roll is wiped clearly with alcohol or acetone, it is ensured that aluminium is rolled up Surface cannot have mark, viscous aluminium, scratch, scuffing, and end face is not allow for small broken sea of burr, turriform, scollop, scallop, edge etc., middle Trimming staggered floor is necessarily less than 2mm, and turriform is less than 5mm.
5th, paper tinsel rolls:
The cold rolling coil progress paper tinsel of 0.25mm thickness is rolled and prepares 0.073mm thickness aluminium aluminium foils, the distribution side that each passage paper tinsel rolls Case is:0.25mm → 0.17mm → 0.125mm → 0.073mm, each passage paper tinsel must replace working roll when rolling, clear to wipe in guide passage Each roller, supporting stick surface is not all right must to replace support roller.ROLLING OIL must be clean, when being rolled up to 0.073mm thick aluminum foils its Surface must purge clean and be not allow for remaining greasy dirt.Surface is not allow for the scratch of elongated or discontinuity, scratches, Periodic Traveling print Any surface defect for influencing to use such as trace, bright wisp and bright band, hidden bar, informal voucher.Paper tinsel rolls speed, and routinely technical requirements perform.
6th, the reference common process process of finished product cutting:
Thick paper tinsel must wipe each deflector roll in guide passage clearly when cutting cutting, each deflector roll is wiped clearly with alcohol or acetone;Ensure aluminium Volume surface cannot have mark, viscous aluminium, scratch, scuffing, and end face is not allow for small broken sea of burr, turriform, scollop, scallop, edge etc., in Between trimming staggered floor be necessarily less than 2mm.The aluminium volume of cutting, which is placed on floor, must pad the big cardboard of lastblock, not allow directly to land.Point Pay attention to checking aluminium foil surface whether there is greasy dirt when cutting, surface must not be sent to annealing operation with greasy dirt.
Small broken sea of burr, turriform, scollop, scallop, edge etc. is not allow for during cutting, cutting staggered floor is necessarily less than 0.5mm.Point Rouleau end face after cutting must totally, neatly;The rouleau lot number and specification cut must write with chalk on the surface of aluminium volume;Point The examination paper cut must be firm with three high temperature foil tape seals, prevents that annealing is loose.
7th, finished products:
0.073mm thick aluminum foils are rolled into finished products are carried out in annealing furnace, kept the temperature when furnace temperature first being raised to 210 DEG C with 4h 20h, simultaneously cooled to room temperature of coming out of the stove when furnace temperature then being dropped to 170 DEG C.It should check that 0.073mm thick aluminum foils are rolled up during finished products End face situation, check whether end socket using between high temperature gummed tape, whether firm, each aluminum foil coil touch volume phenomenon, check Whether be stained with the circulated air hood of stove aluminium foil and whether remove it is clean just can be into furnace annealing.
0.073mm thick aluminum foils volume after finished products just becomes tableware aluminium foil, and the tableware aluminium foil is after testing after testing Its tensile strength >=220Mpa, optimum tensile strength can even reach 250Mpa, elongation percentage >=6%, cupping >=4mm.Detection Reference method is as follows:According to standard GB/T/T228.1-2010《Metal material stretching test》It is processed into 5 times of standard tensile examinations Sample, electronics are stretching on Japanese Shimadzu AGS-X 1KN precision tension testers and carry out, and draw speed reference value is 1mm/min.Press According to national standard GB/T 4156-2007《Metal sheet and strip Erichsen test》, cupping test is micro- in GBW-60B Carried out on the automatic cupping testing machine of machine screen display, punching speed reference is 0.1mm/min.
8th, the reference common process process of packaging is checked:
Mainly check that aluminum foil thickness, width must not exceed the margin of tolerance during finished product inspection, end face must not jagged, flange, Wound, staggered floor must not exceed 0.5mm.Compliant sleeve, material have to comply with customer requirement, and sleeve both sides stretch out aluminium foil end face and are respectively 5mm.Packed after passed examination according to the packing instructions of tableware aluminium foil.
The technical solution or embodiment selected herein for the open purpose of the present invention, are presently considered to be suitable , it should be appreciated that:It is contemplated that belong to all changes of the embodiment in this design and the scope of the invention including all Change and improve.

Claims (1)

1. electrolytic aluminium liquid and aluminium ingot are first smelted into aluminum melt by a kind of preparation method of high intensity tableware aluminium foil, the preparation method, 3~5mm thickness aluminium is prepared by casting and rolling process again to roll up, then roll by cold rolling → slitting trimming → paper tinsel → finished product cutting → Finished products → inspection packaging prepares high intensity tableware aluminium foil, wherein slitting trimming, finished product cutting and inspection packaging routinely Technique carries out, it is characterized in that:
1) electrolytic aluminium liquid and aluminium ingot are smelted into aluminum melt:
The electrolytic aluminium liquid of 80~90% parts by weight and the aluminium ingot of 10~20% parts by weight and aluminium content >=99.7% are together put into Melting is carried out in smelting furnace and prepares aluminum melt, melting Control for Kiln Temperature is in the range of 750 ± 5 DEG C, the chemistry of aluminum melt during melting Component should meet following table requirement after testing, and require degasification, slagging-off totally and stir to ensure the quality of aluminum melt;
2) 3~5mm thickness aluminium is prepared by casting and rolling process to roll up:
During continuous casting by by the bast mouth that heat safe inorganic non-metallic material is process by aluminum melt equivalent, injection two at the uniform velocity In the steel band of root opposite direction rotating, and be connected on the outside of two steel bands with recirculated cooling water, the heat in aluminum melt by steel band and Cooling water is pulled away, and the temperature of aluminum melt is maintained at 685 ± 10 DEG C of scopes during continuous casting, casting speed control in 8~11m/min, The slab thickness of casting is controlled in 19 ± 1mm, it is desirable to by adjusting cooling water pressure and flow to ensure strand temperature control In 520~580 DEG C of scopes;
The slab of continuous casting is directly entered three tandem mills and is lubricated and is cooled down using emulsion, the first passage Reduction by rolling control System 50~60% and rolling inlet temperature control at 420~500 DEG C and outlet temperature control at 360~420 DEG C, the second passage Reduction by rolling control 25~35% and rolling inlet temperature control at 330~390 DEG C and outlet temperature control 290~ 360 DEG C, the 3rd pass reduction control 20~33% and inlet temperature control at 250~320 DEG C and outlet temperature control exist 220~250 DEG C, 3~5mm thickness aluminium volume is prepared through the processing of the 3rd passage;
3) cold rolling:
Continuous casting and rolling prepare directly upper cold mill complex after 3~5mm thickness aluminium volume carry out each passage cold rolling and roll out 0.16~ 0.28mm cold rolling coils, the allocative decision of each passage cold rolling are:3.0~5.0mm → 2.0~3.5mm → intermediate annealing → 1.3~ 2.3mm → 0.9~1.6mm → 0.64~1.15mm → 0.45~0.81mm → 0.32~0.57mm → 0.23~0.40mm → 0.16~0.28mm → trimming, wherein 3.0~5.0mm → 2.0~3.5mm cold rolling pass working modulus control 25~35% it Between, remaining each cold rolling pass working modulus control is first by the cold rolling coil of 2.0~3.5mm thickness at 22.5~35.5%, intermediate annealing It is put into annealing furnace, 4h is kept the temperature when furnace temperature being raised to 220 DEG C with 2h afterwards, 10 is kept the temperature when furnace temperature then being raised to 530 DEG C with 3h ~20h, then when furnace temperature is dropped to 460 DEG C with 2h, keep the temperature 4h, come out of the stove when furnace temperature finally being dropped to 170 DEG C, cold after intermediate annealing 2.0~3.5mm thickness cold rolling coils should be checked by rolling volume and needing air-cooled to less than 60 DEG C to be transferred to subsequently each passes, when intermediate annealing again End face situation, checks that end socket whether using volume phenomenon whether is touched between high temperature gummed tape, whether firm, each cold rolling coil, checks stove Whether be stained with the circulated air hood of son aluminium end and whether remove it is clean just can be into furnace annealing;
Each cold rolling pass process is required to be lubricated and cooled down using ROLLING OIL, pays attention to wiping each deflector roll in guide passage clearly, prevents Only surface of aluminum plate has mark, glues and hinder defect;
4) paper tinsel rolls:
The cold rolling coil progress paper tinsel of 0.16~0.28mm thickness is rolled and prepares 0.05~0.095mm aluminium foils, point that each passage paper tinsel rolls It is with scheme:0.16~0.28mm → 0.12~0.20mm → 0.09~0.15mm → 0.05~0.095mm, when each passage paper tinsel rolls Working roll must be replaced, clear each roller wiped in guide passage, roll surface is not all right must to replace support roller;ROLLING OIL must Must be clean, its surface must purge clean and be not allow for residual greasy dirt when being rolled up to 0.05~0.095mm thick aluminum foils, and surface is not Allow have the scratch of elongated or discontinuity, scuffing, periodicity mark, bright wisp and any table for influencing to use of bright band, hidden bar, informal voucher Planar defect;
5) finished products:
0.05~0.095mm thick aluminum foils are rolled into finished products are carried out in annealing furnace, protected when furnace temperature first being raised to 210 DEG C with 4h Warm 20h, simultaneously cooled to room temperature of coming out of the stove when furnace temperature then being dropped to 170 DEG C;
Should be checked during finished products 0.05~0.095mm thick aluminum foils volume end face situation, check end socket whether using high temperature gummed tape, Whether touch volume phenomenon between whether firm, each aluminum foil coil, check whether be stained with the circulated air hood of stove aluminium foil and whether Removing totally just can be into furnace annealing;
0.05~0.095mm thick aluminum foils volume after finished products just becomes the tension of tableware aluminium foil, after testing the tableware aluminium foil Intensity >=220MPa, elongation percentage >=6%, cupping >=4mm.
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CN110484755A (en) * 2019-08-30 2019-11-22 洛阳龙鼎铝业有限公司 A kind of preparation method of high intensity aluminum foil for household use
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