CN106885763A - A kind of online particle image particle size analyzing device - Google Patents

A kind of online particle image particle size analyzing device Download PDF

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Publication number
CN106885763A
CN106885763A CN201710094040.0A CN201710094040A CN106885763A CN 106885763 A CN106885763 A CN 106885763A CN 201710094040 A CN201710094040 A CN 201710094040A CN 106885763 A CN106885763 A CN 106885763A
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CN
China
Prior art keywords
compressed air
speed camera
sampling
dispersed material
sampling container
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710094040.0A
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Chinese (zh)
Inventor
汪敏
徐麒涛
施小烽
江高贤
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Wan Cheng Environmental Protection Technology Co Ltd
Original Assignee
Shanghai Wan Cheng Environmental Protection Technology Co Ltd
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Filing date
Publication date
Application filed by Shanghai Wan Cheng Environmental Protection Technology Co Ltd filed Critical Shanghai Wan Cheng Environmental Protection Technology Co Ltd
Priority to CN201710094040.0A priority Critical patent/CN106885763A/en
Publication of CN106885763A publication Critical patent/CN106885763A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume, or surface-area of porous materials
    • G01N15/02Investigating particle size or size distribution
    • G01N15/0205Investigating particle size or size distribution by optical means, e.g. by light scattering, diffraction, holography or imaging
    • G01N15/0227Investigating particle size or size distribution by optical means, e.g. by light scattering, diffraction, holography or imaging using imaging, e.g. a projected image of suspension; using holography
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N2001/1006Dispersed solids

Abstract

A kind of online particle image particle size analyzing device disclosed by the invention, including sampling container, sampling compressed air hose, probe tube, dispersed material joint, air compressor, high speed video camera, powder retrieving pipe and host computer, granular material is fallen into sampling container, granule materials are inhaled into probe tube, and be delivered in dispersed material joint via probe tube, dispersed material joint is passed through the compressed air of air compressor generation, compressed air dispels the material in dispersed material joint, and the material of even thickness is fallen into high-speed camera region;High-speed camera carries out taking pictures at a high speed to the dispersed material fallen into high-speed camera region, the particle indexing of dispersed material is recorded, host computer is collected the image of high-speed camera shooting and captured image is analyzed by grading analysis software, obtains the distribution situation of sample granularity.The present invention is not influenceed by the concentration of taken material, and measurement data accuracy is high, can obtain the data such as morphological parameters.

Description

A kind of online particle image particle size analyzing device
Technical field
The present invention relates to the technical field of analytical instruments in manufacture of cement quality control, more particularly to one kind is for analyzing dry The online particle image particle size analyzing device of the size distribution of property particle.
Background technology
Size distribution refers to the percentage that is occupied of different-grain diameter particle in all particles for constitute cement.Size distribution Measure is not only a kind of effective ways of control cement granules fineness, what is more important its by the excellent of the links such as grinding, classification The foundation for providing and preparing is provided.The size distribution situation of cement will greatly influence the intensity of concrete, and the measurement of size distribution is right The quality control of the concrete of final molding, and in process of production optimize how production technology, improve the matter of product Amount, reduces energy consumption, reduces the aspects such as production cost and produces greatly effect.
At present in the production process of cement, in order to control the quality of product, online grain size analysis uses laser grain Degree analyzer, its measuring principle is theoretical using laser diffractometry and mie light scattering, sets up and characterizes particle size fraction abundance and each spy Determine the mathematics physics model of the light energy of acquisition at angle, measure luminous energy, the luminous energy measured by special angle is compared with total luminous energy Compared with the abundance proportional quantities for releasing the corresponding grain-size grade of particle swarm, calculate indirectly with particle size distribution data table, distribution curve, compare table The result such as area, D10, D50, D90, its measurement data is influenceed larger by the concentration of taken material, and measurement data accuracy is not good, And cannot obtain including " morphological parameters " including draw ratio, ball-type degree.
Therefore, applicant carried out beneficial exploration and trial, have found result of the above problems, will be detailed below being situated between The technical scheme for continuing is produced under this background.
The content of the invention
The technical problems to be solved by the invention:There is measurement data for existing laser particle size analyzer to receive to take thing The problems such as concentration of material influences that larger, measurement data accuracy is not good, cannot obtain morphological parameters, and provide a kind of for analyzing The online particle image particle size analyzing device of the size distribution of dryness particle.
Technical problem solved by the invention can be realized using following technical scheme:
A kind of online particle image particle size analyzing device, including:
One is arranged on the sampling container in cement tremie pipe, a material collection is offered at the top of the sampling container and is opened Mouthful;
One sampling compressed air hose, the first end of the sampling compressed air hose is penetrated in the cement tremie pipe and passed through The side of the sampling container simultaneously extends into the bottom of the sampling container;
One probe tube, the first end of the probe tube is penetrated in the cement tremie pipe and through the side of the sampling container Face simultaneously extends into the bottom of the sampling container, and its first end is oppositely arranged with the first end of the sampling compressed air hose;
One dispersed material joint, the dispersed material joint has a dispersion compressed air interface, a sample connection and Dispersed material is exported, and the sample connection of the dispersed material joint is connected with the second end of the probe tube;
One air compressor, the compressed air outlet of the air compressor is respectively with the of the sampling compressed air hose The dispersion compressed air interface connection of two ends and the dispersed material joint;
One high speed video camera, the high speed video camera includes that high-speed camera and composition have a high-speed camera area Domain, the camera of the high-speed camera is directed at the high-speed camera region and can carry out high speed bat to the high-speed camera region According to, a material inlet is offered at the top of the high-speed camera region, its bottom offers a material outlet, the material inlet It is connected with the dispersed material outlet of the dispersed material joint;
One powder retrieving pipe, one end of the powder retrieving pipe is connected with the material outlet in the high-speed camera region, its other end with Cement tremie pipe is connected and positioned at the lower section of the sampling container;And
One host computer, the host computer is connected with the high-speed camera and air compressor respectively.
In a preferred embodiment of the invention, compressed air hose, the cleaning compressed air hose also are cleaned including one One end penetrate in the cement tremie pipe and connected with the bottom of the sampling container, its other end and the air compressor Compressed air outlet connection.
In a preferred embodiment of the invention, the first end of the sampling compressed air hose is in coniform, and it first Bore of the bore at end less than the first end of the probe tube.
In a preferred embodiment of the invention, the installed in front in the camera of the high-speed camera has one micro- Mirror.
In a preferred embodiment of the invention, also including one be connected with the host computer for display data result Display.
The operation principle of online particle image particle size analyzing device of the invention is as follows:
Granular material is fallen into sampling container, and the compressed air that air compressor is produced is entered by sampling compressed air hose Enter in sampling container, negative pressure, such particle are formed between the first end and the first end of probe tube that now sample compressed air hose Material is inhaled into probe tube, and is delivered in dispersed material joint via probe tube, and the dispersion compression of dispersed material joint is empty Gas interface is passed through the compressed air of air compressor generation, and compressed air dispels the material in dispersed material joint, and thickness is equal Even material is fallen into high-speed camera region;Now, high-speed camera is carried out to the dispersed material fallen into high-speed camera region Take pictures at a high speed, the indexing of the particle of dispersed material is recorded, host computer is collected the image that high-speed camera shoots and passed through Grain analysis software is analyzed to captured image, obtains the distribution situation of sample granularity.Finally, the material warp of even thickness Powder retrieving pipe is crossed to return in cement tremie pipe.
As a result of technical scheme as above, the beneficial effects of the present invention are:Sampling mode of the invention simply has Effect, can obtain the material of even thickness, then carry out IMAQ using high-speed camera, by grading analysis software to being taken the photograph The image for taking is analyzed, and can not only obtain all kinds of " the monomer attributes " of material and including including draw ratio, ball-type degree " morphological parameters ", " particle diameter distribution " data and chart of sample can also be obtained, and export D10, D50 equal distribution feature ginseng Number, takes the distribution that material really reflects actual particle.The present invention is not influenceed by the concentration of taken material, and measurement data is accurate Degree is high, can obtain the data such as morphological parameters.
Brief description of the drawings
In order to illustrate more clearly about the embodiment of the present invention or technical scheme of the prior art, below will be to embodiment or existing The accompanying drawing to be used needed for having technology description is briefly described, it should be apparent that, drawings in the following description are only this Some embodiments of invention, for those of ordinary skill in the art, on the premise of not paying creative work, can be with Other accompanying drawings are obtained according to these accompanying drawings.
Fig. 1 is structural representation of the invention.
Specific embodiment
In order that technological means, creation characteristic, reached purpose and effect that the present invention is realized are easy to understand, tie below Conjunction is specifically illustrating, and the present invention is expanded on further.
Referring to Fig. 1, what is be given in figure is a kind of online particle image particle size analyzing device, including sampling container 100, sampling Compressed air hose 200, probe tube 300, dispersed material joint 400, air compressor (not shown), high speed video camera 500th, powder retrieving pipe 600, display 700 and host computer 800.
Sampling container 100 is arranged in cement tremie pipe 10, and the top of sampling container 10 offers a material collection opening 110, the material fallen in cement tremie pipe 10 enters in sampling container 100 via material collection opening 110.
The first end 210 for sampling compressed air hose 200 is penetrated in cement tremie pipe 10 and through the side of sampling container 100 And the bottom of sampling container 100 is extended into, its second end 210 is connected with the compressed air outlet of air compressor.Probe tube 300 First end 310 penetrate in cement tremie pipe 10 and through the side of sampling container 100 and extend into the bottom of sampling container 100 Portion, its first end 310 is oppositely arranged with the first end 210 of sampling compressed air hose 200.Taken to preferably be inhaled into material In sample pipe, the first end 210 for sampling compressed air hose 200 is in coniform, and the bore of its first end 210 is less than probe tube 300 The bore of first end 310.
There is dispersed material joint 400 a dispersion compressed air interface 410, a sample connection 420 and a dispersed material to go out Mouth 430, the dispersion compressed air interface 410 of dispersed material joint 400 is connected with the compressed air outlet of air compressor, and it takes Sample interface 420 is connected with the second end 320 of probe tube 300.
High speed video camera 500 includes that high-speed camera 510 and composition have a high-speed camera region 520, high-speed camera The camera alignment high-speed camera region 520 of machine 510 simultaneously can carry out taking pictures at a high speed to high-speed camera region 520, high-speed camera area The top in domain 520 offers a material inlet 521, and its bottom offers a material outlet 522, the thing in high-speed camera region 520 Material import 521 is connected with the dispersed material outlet 430 of dispersed material joint 400.In the front side of the camera of high-speed camera 510 One microscope 530 is installed, so that the image that high-speed camera 510 is absorbed becomes apparent from.
One end 610 of powder retrieving pipe 600 is connected with the material outlet 522 in high-speed camera region 520, its other end 620 and water Mud tremie pipe 10 is connected and positioned at the lower section of sampling container 100.
Host computer 800 is connected with high speed video camera 500, air compressor and display screen 700 respectively, display screen 700 For showing the data result after host computer analysis.
Additionally, cleaning compressed air hose 900 present invention additionally comprises one, the one end 910 for cleaning compressed air hose 900 penetrates water Connect in mud tremie pipe 10 and with the bottom of sampling container 100, its other end 920 connects with the compressed air outlet of air compressor Connect, when cleaning is needed in sampling container 100, clean and compressed air is passed through in compressed air hose 900, compressed air enters sampling In container 100 and the material in sampling container 100 is blown out from material collection opening 110.
General principle of the invention and principal character and advantages of the present invention has been shown and described above.The technology of the industry Personnel it should be appreciated that the present invention is not limited to the above embodiments, simply explanation described in above-described embodiment and specification this The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appending claims and its Equivalent thereof.

Claims (5)

1. a kind of online particle image particle size analyzing device, it is characterised in that including:
One is arranged on the sampling container in cement tremie pipe, and a material collection opening is offered at the top of the sampling container;
One sampling compressed air hose, the first end of the sampling compressed air hose is penetrated in the cement tremie pipe and through described The side of sampling container simultaneously extends into the bottom of the sampling container;
One probe tube, the first end of the probe tube is penetrated in the cement tremie pipe and through the side of the sampling container simultaneously The bottom of the sampling container is extended into, its first end is oppositely arranged with the first end of the sampling compressed air hose;
One dispersed material joint, the dispersed material joint has a dispersion compressed air interface, a sample connection and a dispersion Material outlet, the sample connection of the dispersed material joint is connected with the second end of the probe tube;
One air compressor, the compressed air outlet of the air compressor respectively with the second end of the sampling compressed air hose Dispersion compressed air interface with the dispersed material joint is connected;
One high speed video camera, the high speed video camera includes that high-speed camera and composition have a high-speed camera region, institute The camera for stating high-speed camera is directed at the high-speed camera region and the high-speed camera region can be carried out to take pictures at a high speed, institute State and a material inlet is offered at the top of high-speed camera region, its bottom offers a material outlet, the material inlet and institute State the dispersed material outlet connection of dispersed material joint;
One powder retrieving pipe, one end of the powder retrieving pipe is connected with the material outlet in the high-speed camera region, its other end and cement Tremie pipe is connected and positioned at the lower section of the sampling container;And
One host computer, the host computer is connected with the high-speed camera and air compressor respectively.
2. particle image particle size analyzing device as claimed in claim 1 online, it is characterised in that also clean compression including empty Tracheae, one end of the cleaning compressed air hose penetrates in the cement tremie pipe and is connected with the bottom of the sampling container, Its other end is connected with the compressed air outlet of the air compressor.
3. particle image particle size analyzing device as claimed in claim 1 online, it is characterised in that the sampling compressed air hose First end in coniform, the bore of the bore less than the first end of the probe tube of its first end.
4. particle image particle size analyzing device as claimed in claim 1 online, it is characterised in that in the high-speed camera The installed in front of camera has a microscope.
5. particle image particle size analyzing device as claimed in claim 1 online, it is characterised in that also upper with described including The display for display data result of machine connection.
CN201710094040.0A 2017-02-21 2017-02-21 A kind of online particle image particle size analyzing device Pending CN106885763A (en)

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Application Number Priority Date Filing Date Title
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108776100A (en) * 2018-06-19 2018-11-09 西南科技大学城市学院 A kind of material particles automatic measurement mechanism
CN109557002A (en) * 2019-01-17 2019-04-02 福建南方路面机械有限公司 One kind is gathered materials particle shape granularity on-line measuring device
CN109839336A (en) * 2019-04-24 2019-06-04 江苏一夫科技股份有限公司 Cytochrome P--450 on-line checking analyzer

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CN105699258A (en) * 2016-01-28 2016-06-22 华侨大学 Online detection device and method of fine aggregates
CN205749201U (en) * 2016-06-29 2016-11-30 响水中联水泥有限公司 A kind of cement granularity on-line measuring device improving measurement effect
CN206594017U (en) * 2017-02-21 2017-10-27 上海万澄环保科技有限公司 A kind of online particle image particle size analyzing device

Patent Citations (9)

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Publication number Priority date Publication date Assignee Title
JP2001074641A (en) * 1999-06-30 2001-03-23 Nikkiso Co Ltd Grain size distribution-measuring device
CN2681116Y (en) * 2003-03-25 2005-02-23 新疆电力科学研究院 Solid particle sampler
CN2645076Y (en) * 2003-09-26 2004-09-29 成都精新粉体测试设备有限公司 Laser particles size distribution tester
CN2655219Y (en) * 2003-10-22 2004-11-10 中国石化仪征化纤股份有限公司 Negative pressure sampler for granular material
CN104614293A (en) * 2015-02-02 2015-05-13 响水中联水泥有限公司 On-line cement particle size detection method and one-line cement particle size device
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CN206594017U (en) * 2017-02-21 2017-10-27 上海万澄环保科技有限公司 A kind of online particle image particle size analyzing device

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108776100A (en) * 2018-06-19 2018-11-09 西南科技大学城市学院 A kind of material particles automatic measurement mechanism
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CN109557002A (en) * 2019-01-17 2019-04-02 福建南方路面机械有限公司 One kind is gathered materials particle shape granularity on-line measuring device
CN109557002B (en) * 2019-01-17 2024-03-19 福建南方路面机械股份有限公司 Aggregate particle shape granularity on-line measuring device
CN109839336A (en) * 2019-04-24 2019-06-04 江苏一夫科技股份有限公司 Cytochrome P--450 on-line checking analyzer
CN109839336B (en) * 2019-04-24 2019-07-19 江苏一夫科技股份有限公司 Cytochrome P--450 on-line checking analyzer

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