CN106884347A - A kind of dyeing liquor for print and dye micro fiber leather and wool and its preparation method and application - Google Patents
A kind of dyeing liquor for print and dye micro fiber leather and wool and its preparation method and application Download PDFInfo
- Publication number
- CN106884347A CN106884347A CN201710262626.3A CN201710262626A CN106884347A CN 106884347 A CN106884347 A CN 106884347A CN 201710262626 A CN201710262626 A CN 201710262626A CN 106884347 A CN106884347 A CN 106884347A
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- Prior art keywords
- parts
- acetic acid
- wool
- dyeing liquor
- micro fiber
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/52—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
- D06P1/5207—Macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- D06P1/5214—Polymers of unsaturated compounds containing no COOH groups or functional derivatives thereof
- D06P1/5221—Polymers of unsaturated hydrocarbons, e.g. polystyrene polyalkylene
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65118—Compounds containing hydroxyl groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/653—Nitrogen-free carboxylic acids or their salts
- D06P1/6533—Aliphatic, araliphatic or cycloaliphatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/14—Wool
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/24—Polyamides; Polyurethanes
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Coloring (AREA)
Abstract
The invention discloses a kind of dyeing liquor for print and dye micro fiber leather and wool and its preparation method and application, the dyeing liquor is made up of the following raw material according to weight portion:39 parts of terpene resin, 11 19 parts of resveratrol, 23 31 parts of acetic acid, 15 25 parts of dyestuff, 7 15 parts of acetic acid chlorhexidine.Take resveratrol and dyestuff is inserted in 75% ethanol and stirred, add acetic acid, the stirring of acetic acid chlorhexidine, ultrasound, be subsequently adding terpene resin intensification, ultrasonic, cooling and obtain final product.The present invention can significantly improve dyestuff to micro fiber leather, the color firmness of wool, water resistance and resistant of high or low temperature, to wool not damaged, it is ensured that the quality after woolen dyed.The present invention also to being made dyeing liquor using the sensitive color dyestuff such as emerald green blue, gorgeous orchid or fluorescent dye, after carrying out dyeing treatment to micro fiber leather and wool, does not produce form and aspect to change substantially, it is applied widely, low production cost, dyeing is relatively low compared with simple, cost, is suitable to large-scale production.
Description
Technical field
The present invention relates to printing technology field, specifically a kind of dyeing liquor and its preparation for print and dye micro fiber leather and wool
Methods and applications.
Background technology
Micro fiber leather full name is " superfine fibre enhancing leather ".It has extremely excellent anti-wear performance, and excellent is ventilative, resistance to
Ageing properties, soft comfortable has very strong pliability and the environment protecting advocated now.Micro fiber leather is best regenerated bark,
Feel is more soft than as corium, and micro fiber leather belongs to the high-grade leather of a kind of new development in synthetic leather, belongs to new skin
Material species.Because it has the advantages that wear-resisting, cold-resistant, ventilative, ageing-resistant, soft texture, environmental protection and outward appearance are beautiful, it has also become generation
For the most ideal chose of natural leather.Superfine fiber chemical leather is made up of nylon superfine fiber and polyurethane two parts, but a lot
Dyestuff has colouring effect well in addition to having preferable coloring to polyurethane, also to polyamide fibre, and both coloured light difference can make most
Whole Color deviates to be envisioned.And wool causes existing coloring material to cause to damage to it due to its unique quality, quality
Decline.Coloring material of the prior art is all specific to obtained in certain fabric, certain dyestuff, small using scope, unfavorable
In popularization.
The content of the invention
It is an object of the invention to provide a kind of dyeing liquor for print and dye micro fiber leather and wool and preparation method thereof and should
With to solve the problems, such as to be proposed in above-mentioned background technology.
To achieve the above object, the present invention provides following technical scheme:
A kind of dyeing liquor for print and dye micro fiber leather and wool, is made up of the following raw material according to weight portion:Terpene resin
3-9 parts, resveratrol 11-19 parts, acetic acid 23-31 parts, dyestuff 15-25 parts, 7-15 parts of acetic acid chlorhexidine.
As further scheme of the invention:The dyeing liquor for print and dye micro fiber leather and wool, by following according to weight
Measure the raw material composition of part:Terpene resin 5-7 parts, resveratrol 13-17 parts, acetic acid 25-29 parts, dyestuff 18-22 parts, acetic acid chlorine
Determine 9-13 parts.
As further scheme of the invention:The dyeing liquor for print and dye micro fiber leather and wool, by following according to weight
Measure the raw material composition of part:6 parts of terpene resin, 15 parts of resveratrol, 27 parts of acetic acid, 20 parts of dyestuff, 11 parts of acetic acid chlorhexidine.
A kind of preparation method of dyeing liquor for print and dye micro fiber leather and wool, comprises the following steps:
(1) take resveratrol to be inserted in 75% ethanol of 8-10 times of the two weight with dyestuff, stirring 25-30min is obtained mixed
Close liquid A;
(2) take acetic acid to insert in mixed liquor A, stir 45-50min, add acetic acid chlorhexidine, be obtained after stirring 22-30min
Mixed liquid B;
(3) mixture B is carried out into ultrasonically treated 30-35min, is subsequently adding terpene resin, be warming up to 65-68 DEG C and ultrasound
Treatment 55-60min, cooling obtains final product dyeing liquor.
As further scheme of the invention:In step (1), mixing speed is 400-600r/min.
As further scheme of the invention:In step (2), mixing speed is 600-800r/min.
As further scheme of the invention:In step (3), ultrasonic power is 800-1000W.
Application of the dyeing liquor in micro fiber leather printing and dyeing.
Application of the dyeing liquor in wool printing and dyeing.
Compared with prior art, the beneficial effects of the invention are as follows:
The present invention by dyestuff and terpene resin, resveratrol, acetic acid, dyeing liquor obtained in acetic acid chlorhexidine, not only with dye
Material compatibility is good, effectively improves the dyestuff uniformity, and can significantly improve dyestuff to micro fiber leather, the color firmness of wool, resistance to
Aqueous and resistant of high or low temperature, can there is preferable coloring to polyurethane, also there is colouring effect, Color well to polyamide fibre
Expected imagination can be reached, the present invention is widely used in superfine fibre micro fiber leather field.Additionally, the present invention is to wool
Not damaged, it is ensured that the quality after woolen dyed.The present invention of the sensitive color dyestuff such as emerald green blue, gorgeous orchid or fluorescent dye also to being made
Dyeing liquor, after carrying out dyeing treatment to micro fiber leather and wool, does not produce form and aspect to change substantially, applied widely.Present invention system
Standby process is simple, easy to operate, easy to control, low production cost, dyeing are relatively low compared with simple, cost, are suitable to large-scale production.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described,
Obviously, described embodiment is only a part of embodiment of the invention, rather than whole embodiments.Based in the present invention
Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, all
Belong to the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, a kind of dyeing liquor for print and dye micro fiber leather and wool is made up of following raw material:Terpenes tree
Fat 3kg, resveratrol 11kg, acetic acid 23kg, dyestuff 15kg, acetic acid chlorhexidine 7kg.
Take resveratrol to be inserted in the ethanol of volumetric concentration 75% of 8 times of the two weight with dyestuff, stir 25min, stirring speed
It is 400r/min to spend, and mixed liquor A is obtained.Take acetic acid to insert in mixed liquor A, stir 45min, add acetic acid chlorhexidine, stirring
22min, mixing speed is 600r/min, and mixed liquid B is obtained.Mixture B is carried out into ultrasonically treated 30min, terpenes is subsequently adding
Resin, is warming up to 65 DEG C and ultrasonically treated 55min, and ultrasonic power is 800W, and cooling obtains final product dyeing liquor.
Embodiment 2
In the embodiment of the present invention, a kind of dyeing liquor for print and dye micro fiber leather and wool is made up of following raw material:Terpenes tree
Fat 9kg, resveratrol 19kg, acetic acid 31kg, dyestuff 25kg, acetic acid chlorhexidine 15kg.
Take resveratrol to be inserted in 75% ethanol of 10 times of the two weight with dyestuff, stir 30min, mixing speed is
600r/min, is obtained mixed liquor A.Take acetic acid to insert in mixed liquor A, stir 50min, add acetic acid chlorhexidine, stir 30min,
Mixing speed is 800r/min, and mixed liquid B is obtained.Mixture B is carried out into ultrasonically treated 35min, terpene resin is subsequently adding, risen
To 68 DEG C and ultrasonically treated 60min, ultrasonic power is 1000W to temperature, and cooling obtains final product dyeing liquor.
Embodiment 3
In the embodiment of the present invention, a kind of dyeing liquor for print and dye micro fiber leather and wool is made up of following raw material:Terpenes tree
Fat 5kg, resveratrol 13kg, acetic acid 25kg, dyestuff 18kg, acetic acid chlorhexidine 9kg.
Take resveratrol to be inserted in 75% ethanol of 9 times of the two weight with dyestuff, stir 28min, mixing speed is 500r/
Min, is obtained mixed liquor A.Take acetic acid to insert in mixed liquor A, stir 48min, add acetic acid chlorhexidine, stir 26min, stirring speed
It is 700r/min to spend, and mixed liquid B is obtained.Mixture B is carried out into ultrasonically treated 32min, terpene resin is subsequently adding, 66 are warming up to
DEG C and ultrasonically treated 58min, ultrasonic power is 900W, cooling obtain final product dyeing liquor.
Embodiment 4
In the embodiment of the present invention, a kind of dyeing liquor for print and dye micro fiber leather and wool is made up of following raw material:Terpenes tree
Fat 7kg, resveratrol 17kg, acetic acid 29kg, dyestuff 22kg, acetic acid chlorhexidine 13kg.
Take resveratrol to be inserted in 75% ethanol of 9 times of the two weight with dyestuff, stir 28min, mixing speed is 500r/
Min, is obtained mixed liquor A.Take acetic acid to insert in mixed liquor A, stir 48min, add acetic acid chlorhexidine, stir 26min, stirring speed
It is 700r/min to spend, and mixed liquid B is obtained.Mixture B is carried out into ultrasonically treated 32min, terpene resin is subsequently adding, 66 are warming up to
DEG C and ultrasonically treated 58min, ultrasonic power is 900W, cooling obtain final product dyeing liquor.
Embodiment 5
In the embodiment of the present invention, a kind of dyeing liquor for print and dye micro fiber leather and wool is made up of following raw material:Terpenes tree
Fat 6kg, resveratrol 15kg, acetic acid 27kg, dyestuff 20kg, acetic acid chlorhexidine 11kg.
Take resveratrol to be inserted in 75% ethanol of 9 times of the two weight with dyestuff, stir 28min, mixing speed is 500r/
Min, is obtained mixed liquor A.Take acetic acid to insert in mixed liquor A, stir 48min, add acetic acid chlorhexidine, stir 26min, stirring speed
It is 700r/min to spend, and mixed liquid B is obtained.Mixture B is carried out into ultrasonically treated 32min, terpene resin is subsequently adding, 66 are warming up to
DEG C and ultrasonically treated 58min, ultrasonic power is 900W, cooling obtain final product dyeing liquor.
Obtained dyeing liquor in embodiment 1-5 is processed into fabric and the measure of dyefastness is carried out:Colour fasteness to sunlight is adopted
Determined with GB/T 8427-2008, colour fastness to rubbing is determined using GB/T 3920-2008, washing color fastness uses GB/T
3921-2008 is determined.Determined according to above-mentioned dyeing condition and fastness, the dyeing data and color fastness of above-mentioned 5 dyeing liquors are shown in Table
1。
Table 1
Additionally, the present invention is made dyeing liquor using the sensitive color dyestuff such as emerald green blue, gorgeous orchid and fluorescent dye, to micro fiber leather and
After wool carries out dyeing treatment, every fastness test is no less than 4, the particularly dyeing liquor of embodiment 5, and each fastness test is 5,
Substantially form and aspect are not produced to change.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be in other specific forms realized.Therefore, no matter
From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit requires to be limited rather than described above, it is intended that all in the implication and scope of the equivalency of claim by falling
Change is included in the present invention.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each implementation method is only wrapped
Containing an independent technical scheme, this narrating mode of specification is only that for clarity, those skilled in the art should
Specification an as entirety, the technical scheme in each embodiment can also be formed into those skilled in the art through appropriately combined
May be appreciated other embodiment.
Claims (9)
1. a kind of dyeing liquor for print and dye micro fiber leather and wool, it is characterised in that be made up of the following raw material according to weight portion:
Terpene resin 3-9 parts, resveratrol 11-19 parts, acetic acid 23-31 parts, dyestuff 15-25 parts, 7-15 parts of acetic acid chlorhexidine.
2. the dyeing liquor for print and dye micro fiber leather and wool according to claim 1, it is characterised in that by following according to weight
Measure the raw material composition of part:Terpene resin 5-7 parts, resveratrol 13-17 parts, acetic acid 25-29 parts, dyestuff 18-22 parts, acetic acid chlorine
Determine 9-13 parts.
3. the dyeing liquor for print and dye micro fiber leather and wool according to claim 1, it is characterised in that by following according to weight
Measure the raw material composition of part:6 parts of terpene resin, 15 parts of resveratrol, 27 parts of acetic acid, 20 parts of dyestuff, 11 parts of acetic acid chlorhexidine.
4. the preparation method of a kind of dyeing liquor for print and dye micro fiber leather and wool, it is characterised in that comprise the following steps:
(1) take resveratrol to be inserted in 75% ethanol of 8-10 times of the two weight with dyestuff, stirring 25-30min is obtained mixed liquor
A;
(2) take acetic acid to insert in mixed liquor A, stir 45-50min, add acetic acid chlorhexidine, mixing is obtained after stirring 22-30min
Liquid B;
(3) mixture B is carried out into ultrasonically treated 30-35min, is subsequently adding terpene resin, be warming up to 65-68 DEG C and ultrasonically treated
55-60min, cooling obtains final product dyeing liquor.
5. the preparation method of the dyeing liquor for print and dye micro fiber leather and wool according to claim 4, it is characterised in that step
Suddenly in (1), mixing speed is 400-600r/min.
6. the preparation method of the dyeing liquor for print and dye micro fiber leather and wool according to claim 4, it is characterised in that step
Suddenly in (2), mixing speed is 600-800r/min.
7. the preparation method of the dyeing liquor for print and dye micro fiber leather and wool according to claim 4, it is characterised in that step
Suddenly in (3), ultrasonic power is 800-1000W.
8. application of the dyeing liquor as described in claim 1-3 is any in micro fiber leather printing and dyeing.
9. application of the dyeing liquor as described in claim 1-3 is any in wool printing and dyeing.
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CN201710262626.3A CN106884347A (en) | 2017-04-20 | 2017-04-20 | A kind of dyeing liquor for print and dye micro fiber leather and wool and its preparation method and application |
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CN201710262626.3A CN106884347A (en) | 2017-04-20 | 2017-04-20 | A kind of dyeing liquor for print and dye micro fiber leather and wool and its preparation method and application |
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Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1043957A (en) * | 1989-01-04 | 1990-07-18 | 袁守熙 | Non-pollution dual tanning technology for glutaric aldehyde pigskin leather |
CN102747600A (en) * | 2012-05-24 | 2012-10-24 | 太仓市名流制衣有限公司 | Dyeing process of wool-rabbit hair blended yarns |
CN104389203A (en) * | 2014-12-17 | 2015-03-04 | 无锡瑞贝纺织品实业有限公司 | Wool levelling agent and preparation method thereof |
CN104988633A (en) * | 2015-06-15 | 2015-10-21 | 福建凤竹纺织科技股份有限公司 | High-elastic and high-fluffy ultra-cotton-imitated fabric and production technology of same |
CN105220535A (en) * | 2015-10-20 | 2016-01-06 | 湖州申祥丝织有限责任公司 | A kind of Novel wool levelling agent and preparation method thereof |
-
2017
- 2017-04-20 CN CN201710262626.3A patent/CN106884347A/en active Pending
Patent Citations (5)
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---|---|---|---|---|
CN1043957A (en) * | 1989-01-04 | 1990-07-18 | 袁守熙 | Non-pollution dual tanning technology for glutaric aldehyde pigskin leather |
CN102747600A (en) * | 2012-05-24 | 2012-10-24 | 太仓市名流制衣有限公司 | Dyeing process of wool-rabbit hair blended yarns |
CN104389203A (en) * | 2014-12-17 | 2015-03-04 | 无锡瑞贝纺织品实业有限公司 | Wool levelling agent and preparation method thereof |
CN104988633A (en) * | 2015-06-15 | 2015-10-21 | 福建凤竹纺织科技股份有限公司 | High-elastic and high-fluffy ultra-cotton-imitated fabric and production technology of same |
CN105220535A (en) * | 2015-10-20 | 2016-01-06 | 湖州申祥丝织有限责任公司 | A kind of Novel wool levelling agent and preparation method thereof |
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Application publication date: 20170623 |