CN106834068A - The separation method of white wine and white wine harmful substance - Google Patents
The separation method of white wine and white wine harmful substance Download PDFInfo
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- CN106834068A CN106834068A CN201710250795.5A CN201710250795A CN106834068A CN 106834068 A CN106834068 A CN 106834068A CN 201710250795 A CN201710250795 A CN 201710250795A CN 106834068 A CN106834068 A CN 106834068A
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H6/00—Methods for increasing the alcohol content of fermented solutions or alcoholic beverages
- C12H6/02—Methods for increasing the alcohol content of fermented solutions or alcoholic beverages by distillation
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- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
Abstract
The invention provides a kind of white wine and the separation method of white wine harmful substance, it is related to the technical field of food.The separation method of the white wine harmful substance that the present invention is provided, by steps such as first time separated, gaseous state separation, Liquid segregation, second separateds, the content of the harmful substance such as formaldehyde, methyl alcohol, lead, sulphur, plasticiser, free radical in white wine is effectively reduced.According to white wine obtained in the separation method that the present invention is provided, its harmful substance contents is extremely low, and the content of wherein lead ion and methyl alcohol is below 0.005mg/mL, is significantly less than the requirement standard of country, is a kind of white wine of ecological safety health.
Description
Technical field
The present invention relates to food technology field, more particularly, to a kind of white wine and the separation method of white wine harmful substance.
Background technology
White wine is a kind of distinctive Spirit of China, through distillation after being made fermented grain or fermentation by starch or saccharine material
.White wine as a kind of special drink, in the historical progress of China, always along with literature, art continuing to develop and
Change, along with the happiness, anger, grief and joy of the men of literature and writing, deduces into one bright jewel of oriental cultural.Even to this day, liquor culture
Still the various aspects in life are full of, the small poly-, relatives of friend meet, holidays etc. occasion, all unavoidably drink one, two glasss
White wine is showing celebration.
Wine is the mixture of various chemical compositions, and water and ethanol are its topmost compositions.But, in addition, white
In the preparation process of wine, some harmful trace elements are also created, although these micro- contents are low, such as
Fruit is drunk excessive, it will greatly harm is produced to health.Such as formaldehyde, methyl alcohol, sulphur, plasticiser, lead, free radical etc.,
All it is that common are harmful material in white wine, in the production process of white wine, the control to harmful substance contents in white wine should be increased.
Although but still be there are problems that in the presence of the method for harmful substance in some removal white wine now, for example removal effect is not
The problems such as good, high cost.It is therefore needed to provide a kind of method for isolating and purifying, harmful in white wine effectively to remove
Material, improves the security of white wine, make people enjoy white wine it is delicious while, it is not necessary to the danger that excessive worry white wine brings
Evil.
In view of this, it is special to propose the present invention.
The content of the invention
Of the invention that the first purpose is to provide a kind of separation method of white wine harmful substance, the second object of the present invention exists
In providing a kind of white wine, to alleviate present in prior art harmful substance contents problem higher in white wine.
The invention provides a kind of separation method of white wine harmful substance, the separation method includes：
First time separated：It is the first control temperature to control temperature in distiller, to separate boiling point less than the first control
The harmful substance of temperature；Then, it is the second control temperature to control temperature in distiller, to separate boiling point higher than the second control temperature
Harmful substance, and make white wine as a vapor enter gaseous state separation process；
Gaseous state is separated：White wine steam is by nuisances such as filtering material removal methyl alcohol, lead, plasticiser, sulphur, zinc, free radicals
Matter, and it is condensed into liquid into Liquid segregation process；
Liquid segregation：White wine liquid is by nuisances such as filtering material removal methyl alcohol, lead, plasticiser, sulphur, zinc, free radicals
Matter, and enter second separated process；
Second separated：It is the first control temperature to control temperature in distiller, to separate boiling point less than the first control
The harmful substance of temperature；Then, it is the second control temperature to control temperature in distiller, to separate boiling point higher than the second control temperature
Harmful substance, and white wine is entered condensing unit as a vapor, obtain harmful substance and divided after the condensation of white wine steam
From white wine；
Described first controls temperature for less than 75 DEG C, and described second controls temperature for more than 80 DEG C.
Further, described first temperature is controlled for 70~75 DEG C.
Further, described second temperature is controlled for 80~95 DEG C.
Further, the filtering material includes mineral matter.
Further, the filtering material includes activated carbon.
Further, the filtering material also includes energy of a quantum h substance, and the energy of a quantum h substance can
Ionize inert substance.
Further, the filtering material also includes energy of a quantum h substance, and the energy of a quantum h substance can
Ionize inert substance.
In addition, present invention also offers a kind of white wine, the separation method described in the white wine eliminates harmful substance.
Further, the content of lead ion is less than 0.005mg/mL in the white wine.
Further, the content of the methanol in wine is less than 0.005mg/mL.
The separation method of the white wine harmful substance that the present invention is provided, by first time separated, gaseous state separation, liquid point
From steps such as, second separateds, the content of harmful substance in white wine is effectively reduced, it is treated according to the separation method
White wine, its harmful substance contents is extremely low, and the content of wherein lead ion and methyl alcohol is below 0.005mg/mL, is significantly less than country
Requirement standard.
Brief description of the drawings
In order to illustrate more clearly of the specific embodiment of the invention or technical scheme of the prior art, below will be to specific
The accompanying drawing to be used needed for implementation method or description of the prior art is briefly described, it should be apparent that, in describing below
Accompanying drawing is some embodiments of the present invention, for those of ordinary skill in the art, before creative work is not paid
Put, other accompanying drawings can also be obtained according to these accompanying drawings.
Fig. 1 is the process chart of the separation method that the embodiment of the present invention 1 is provided；
Fig. 2 is that the white wine composition of the separation method that the embodiment of the present invention 1 is provided moves towards figure.
Specific embodiment
Technical scheme is clearly and completely described below in conjunction with embodiment, it is clear that described reality
It is a part of embodiment of the invention to apply example, rather than whole embodiments.Based on the embodiment in the present invention, the common skill in this area
The every other embodiment that art personnel are obtained under the premise of creative work is not made, belongs to the model of present invention protection
Enclose.
The invention provides a kind of separation method of white wine harmful substance, including：
First time separated：It is the first control temperature to control temperature in distiller, to separate boiling point less than the first control
The harmful substance of temperature；Then, it is the second control temperature to control temperature in distiller, to separate boiling point higher than the second control temperature
Harmful substance, and make white wine as a vapor enter gaseous state separation process；
Gaseous state is separated：White wine steam is by nuisances such as filtering material removal methyl alcohol, lead, plasticiser, sulphur, zinc, free radicals
Matter, and it is condensed into liquid into Liquid segregation process；
Liquid segregation：White wine liquid is by nuisances such as filtering material removal methyl alcohol, lead, plasticiser, sulphur, zinc, free radicals
Matter, and enter second separated process；
Second separated：It is the first control temperature to control temperature in distiller, to separate boiling point less than the first control
The harmful substance of temperature；Then, it is the second control temperature to control temperature in distiller, to separate boiling point higher than the second control temperature
Harmful substance, and white wine is entered condensing unit as a vapor, obtain harmful substance and divided after the condensation of white wine steam
From white wine；
Wherein, first temperature is controlled for less than 75 DEG C, described second controls temperature for more than 80 DEG C.
Wherein, in first time separated, it is the first control temperature (70~75 DEG C) that temperature in distiller is controlled first,
To separate harmful substance of the boiling point less than the first control temperature.Because the boiling point of white wine active ingredient ethanol is 77 DEG C, therefore,
When the temperature of distiller is less than the first control temperature, boiling point can be in gaseous form less than the harmful substance of the first control temperature
It is separated, and white wine active ingredient ethanol then may proceed to be retained in distiller.Then, it is the to control in distiller temperature
Two controls temperature (80~95 DEG C), to separate harmful substance of the boiling point higher than the second control temperature.Due to white wine active ingredient second
The boiling point of alcohol is 77 DEG C, therefore, when the temperature in distiller is higher than the second control temperature, ethanol evaporation is gaseous state, and with white
The form of wine steam enters into gaseous state separation process, and white wine mid-boiling point can be protected still higher than the harmful substance of the second control temperature
Stay in distiller, realize that the first time of white wine separates.
After white wine steam enters gaseous state separation process, white wine steam by filtering material, filtering material can remove methyl alcohol,
The harmful substances such as lead, plasticiser, sulphur, zinc, free radical, realize second separation of white wine；Meanwhile, white wine steam divides into gaseous state
After process, temperature reduction, white wine can be condensed into liquid, Liquid segregation process is entered into the form of white wine liquid.
After white wine liquid enters Liquid segregation process, white wine liquid by filtering material, filtering material can remove methyl alcohol,
The harmful substances such as lead, plasticiser, sulphur, zinc, free radical, realize that the third time of white wine is separated.
It is similar to first time separated process into second separated process by the white wine of Liquid segregation, it is first
It is the first control temperature (70~75 DEG C) first to control temperature in distiller, harmful less than the first control temperature to separate boiling point
Material.Because the boiling point of white wine active ingredient ethanol is 77 DEG C, therefore, when the temperature of distiller is less than the first control temperature,
Boiling point can be separated in gaseous form less than the harmful substance of the first control temperature, and white wine active ingredient ethanol then can
In remaining in distiller.Then, it is the second control temperature (80~95 DEG C) to control temperature in distiller, high to separate boiling point
In the harmful substance of the second control temperature.Because the boiling point of white wine active ingredient ethanol is 77 DEG C, therefore, when the temperature in distiller
When degree is higher than the second control temperature, ethanol evaporation is gaseous state, and enters condensing unit in the form of white wine steam, and is boiled in white wine
Point can be remained in distiller higher than the harmful substance of the second control temperature, and the white wine steam into condensing unit is condensed into
After liquid, that is, the white wine finished product of the harmful substance that is effectively removed.
Second separated is combined with first time separated, can reach the effect that more effective harmful substance is separate
Really.
By after the separation method treatment that the present invention is provided, can substantially reduce formaldehyde in white wine, methyl alcohol, sulphur, plasticiser,
The content of the harmful substances such as lead, free radical.
In one preferred embodiment, first control temperature for 70 DEG C~75 DEG C, for example, can be, but be not limited to 70
DEG C, 71 DEG C, 72 DEG C, 73 DEG C, 74 DEG C or 75 DEG C.
Another preferred embodiment in, second controls temperature for 80 DEG C~95 DEG C, for example, can be, but be not limited to
81 DEG C, 82 DEG C, 83 DEG C, 84 DEG C, 85 DEG C, 86 DEG C, 87 DEG C, 88 DEG C, 90 DEG C, 91 DEG C, 92 DEG C, 93 DEG C, 94 DEG C or 95 DEG C.
Another preferred embodiment in, filtering material includes mineral matter, and mineral matter can adsorb methyl alcohol, lead, modeling
The harmful substances such as agent, sulphur, zinc, free radical.
Another preferred embodiment in, filtering material includes activated carbon, and activated carbon can adsorb methyl alcohol, lead, modeling
The harmful substances such as agent, sulphur, zinc, free radical.
Another preferred embodiment in, filtering material also include energy of a quantum h substance, energy of a quantum release
Material can ionize inert substance, in order to removed by mineral matter or charcoal absorption.
In addition, present invention also offers a kind of white wine, the white wine that the present invention is provided is to be eliminated according to above-mentioned separation method
The ecological safety health care wine of harmful substance, the content of wherein harmful substance is low, for example, the content of lead ion and methyl alcohol is below
0.005mg/mL。
In order to contribute to it is clearer understand present disclosure, in conjunction with specific embodiment, to of the invention interior
Appearance is described in detail.
Embodiment 1
A kind of separation method of white wine harmful substance is present embodiments provided, Fig. 1 is the process chart of separation method, figure
2 move towards figure for composition, as follows with reference to Fig. 1 and Fig. 2 specific explanations：
The white wine of harmful substance to be removed is placed in the first distiller, control first the temperature of the first distiller for 70~
75 DEG C, due to white wine active ingredient ethanol boiling point be 77 DEG C, therefore, the lower harmful substance of boiling point can in gaseous form by
Separate, and enter harmful substance collector, and white wine active ingredient ethanol then may proceed to be retained in the first distiller.Then,
It is 80~95 DEG C to control temperature in the first distiller, because the boiling point of white wine active ingredient ethanol is 77 DEG C, therefore, ethanol can steam
It is gaseous state to send out, and gaseous state separation process is entered into the form of white wine steam, and white wine mid-boiling point harmful substance higher can be still
So it is retained in distiller, realizes that the first time of white wine separates.
White wine steam enters into and gaseous state separation process is carried out in gaseous state filter, there is filtering material in gaseous state filter,
When white wine steam passes through filtering material, filtering material can remove the nuisances such as formaldehyde, methyl alcohol, lead, sulphur, plasticiser, free radical
The content of matter, realizes second separation of white wine；Meanwhile, after white wine steam enters gaseous state filter, temperature reduction, white wine can be cold
Congeal into liquid, entered into liquid-state filter device in the form of white wine liquid.
White wine liquid enters into and Liquid segregation process is carried out in liquid-state filter device, there is filtering material in liquid-state filter device,
When white wine liquid passes through filtering material, filtering material can remove the nuisances such as formaldehyde, methyl alcohol, lead, sulphur, plasticiser, free radical
The content of matter, realizes that the third time of white wine is separated.
In the present embodiment, the filtering material in gaseous state filter and liquid-state filter device is activated carbon.
By the white wine of Liquid segregation, into after-fractionating device, the temperature that after-fractionating device is controlled first is 70~75
DEG C, because the boiling point of white wine active ingredient ethanol is 77 DEG C, therefore, the lower harmful substance of boiling point can be divided in gaseous form
From, and enter harmful substance collector, and white wine active ingredient ethanol then may proceed to be retained in after-fractionating device.Then, control
Temperature is 80~95 DEG C in after-fractionating device processed, because the boiling point of white wine active ingredient ethanol is 77 DEG C, therefore, ethanol can evaporate
It is gaseous state, and is entered into entrance condensing unit in the form of white wine steam, and white wine mid-boiling point harmful substance higher can be still
So be retained in distiller, into condensing unit white wine steam be condensed into liquid after, that is, be effectively removed harmful substance
White wine finished product.
Embodiment 2
The present embodiment is the change on the basis of embodiment 1, in the present embodiment, in gaseous state filter and liquid-state filter device
Filtering material be mineral matter, it is in addition, identical with the content of embodiment 1.
Embodiment 3
The present embodiment is the change on the basis of embodiment 1, in the present embodiment, in gaseous state filter and liquid-state filter device
Filtering material be activated carbon and mineral matter, it is in addition, identical with the content of embodiment 1.
After white wine first passes through activated carbon filtering, then filtered by mineral matter, can more effectively removed harmful in white wine
Material.
Embodiment 4
The present embodiment is the change on the basis of embodiment 1, in the present embodiment, in gaseous state filter and liquid-state filter device
Filtering material be energy of a quantum release pearl, activated carbon and mineral matter, it is in addition, identical with the content of embodiment 1.
After white wine first passes through energy of a quantum release pearl, energy of a quantum release pearl can promote inert substance to ionize, then pass through
The filtering of activated carbon and mineral matter is crossed, the harmful substance in white wine can be more effectively removed.
Additionally, inventor has also carried out the detection of harmful substance to the white wine after being processed according to the method for embodiment 1 to 4, have
Hold in vivo as follows.
The measure of methanol in wine content
Using gas chromatography, the content of methanol in wine is determined.
(1) reagent：Methyl alcohol standard items, absolute ethyl alcohol
(2) chromatographic condition：
Chromatographic column：Capillary chromatographic column AC20
Carrier gas：Nitrogen, flow velocity 8mL/min
220 DEG C of injector temperature, shunt ratio 5:1
Temperature programming：35 DEG C of holding 4min, 200 DEG C are risen to 4 DEG C/min, keep 10min
Detector temperature：220 DEG C, tail blows 30mL/min, and hydrogen flow rate is 40mL/min, and air velocity is 400mL/min
Sample size：0.4μL
(3) Specification Curve of Increasing
Methyl alcohol standard items are configured to 0.2,0.5,1,2,4 μ g/mL concentration, 0.4 μ L are taken successively and is injected in gas chromatograph
It is measured, with concentration as abscissa, peak area is that ordinate draws standard curve.
(4) sample analysis
0.4 μ L Wine Samples to be measured are taken, is measured in injection gas chromatograph, record peak area, and it is bent according to standard
The content of methyl alcohol in line computation Wine Sample to be measured.
The measure of lead content in white wine
Using atomic absorption spectrophotometer method, the content of lead in white wine is determined.
(1) reagent
Dithizone
(2) testing conditions
Atomic absorption spectrophotometer, Detection wavelength 283.3nm, lamp current 2.0mA, oil-free air compressor pressure
0.3Mpa, gas flow 1600mL/min, combustion gas height 5mm.
(3) Specification Curve of Increasing
Plumbi nitras standard items are configured to 0.5,1,1.5,2,2.5,3mg/L concentration, entered with atomic absorption spectrophotometer
Row is determined, and with concentration as abscissa, absorbance is that ordinate draws standard curve.
(4) sample analysis
10mL Wine Samples are drawn in sample dissolving cup, are placed on 105 DEG C of electric hot plates and are concentrated by evaporation to nearly dry (1mL~2mL),
Cooling is removed, is transferred in 10mL volumetric flasks with 0.5mol/L nitric acid and constant volume is shaken up, carried out with atomic absorption spectrophotometer
Determine, record peak area, and the content of lead in Wine Sample to be measured is calculated according to standard curve.
With reference to above-mentioned content assaying method, the inspection to carrying out harmful substance according to the white wine after the treatment of embodiment 1-4 methods
Survey, concrete outcome is as shown in table 1.
The content of methyl alcohol and lead in the different Wine Samples of table 1
| Group | Methyl alcohol (mg/mL) | Lead (mg/mL) |
| It is untreated | 3.8 | 1.4 |
| Embodiment 1 | Must not detect (<0.005) | |
| Embodiment 2 | Must not detect (<0.005) | |
| Embodiment 3 | Must not detect (<0.005) | Must not detect (<0.005) |
| Embodiment 4 | Must not detect (<0.005) | Must not detect (<0.005) |
Note：* represent compared with untreated fish group, there is significant difference (P<0.05)
Wherein, untreated samples refer to without the original Wine Sample of harmful substance separating treatment.Can be sent out by the data of table 1
It is existing, by after the separation method treatment that the present invention is provided, the harmful substance contents such as methyl alcohol and lead in white wine have significantly
Decline, meet nation's security standard, be a kind of white wine of ecological safety health.
Additionally, be can be seen that when while using activated carbon and mineral matter as filtering material by the data of table 1, have more preferably
Separating effect, and when energy of a quantum release pearl and activated carbon and mineral matter are shared, separating effect achieves significant progress.
Finally it should be noted that：Various embodiments above is merely illustrative of the technical solution of the present invention, rather than its limitations；To the greatest extent
Pipe has been described in detail with reference to foregoing embodiments to the present invention, it will be understood by those within the art that：Its according to
The technical scheme described in foregoing embodiments can so be modified, or which part or all technical characteristic are entered
Row equivalent；And these modifications or replacement, the essence of appropriate technical solution is departed from various embodiments of the present invention technology
The scope of scheme.
Claims (10)
1. a kind of separation method of white wine harmful substance, it is characterised in that the separation method includes：
First time separated：It is the first control temperature to control temperature in distiller, to separate boiling point less than the first control temperature
Harmful substance；Then, it is the second control temperature to control temperature in distiller, to separate boiling point having higher than the second control temperature
Evil material, and white wine is entered gaseous state separation process as a vapor；
Gaseous state is separated：White wine steam removes the harmful substances such as methyl alcohol, lead, plasticiser, sulphur, zinc, free radical by filtering material, and
It is condensed into liquid into Liquid segregation process；
Liquid segregation：White wine liquid removes the harmful substances such as methyl alcohol, lead, plasticiser, sulphur, zinc, free radical by filtering material, and
Into second separated process；
Second separated：It is the first control temperature to control temperature in distiller, to separate boiling point less than the first control temperature
Harmful substance；Then, it is the second control temperature to control temperature in distiller, to separate boiling point having higher than the second control temperature
Evil material, and white wine is entered condensing unit as a vapor, obtain what harmful substance was separate after the condensation of white wine steam
White wine；
Described first controls temperature for less than 75 DEG C, and described second controls temperature for more than 80 DEG C.
2. separation method according to claim 1, it is characterised in that described first to control temperature be 70~75 DEG C.
3. separation method according to claim 1, it is characterised in that described second to control temperature be 80~95 DEG C.
4. separation method according to claim 1, it is characterised in that the filtering material includes mineral matter.
5. separation method according to claim 1, it is characterised in that the filtering material includes activated carbon.
6. separation method according to claim 4, it is characterised in that the filtering material also includes energy of a quantum releaser
Matter, the energy of a quantum h substance can ionize inert substance.
7. separation method according to claim 5, it is characterised in that the filtering material also includes energy of a quantum releaser
Matter, the energy of a quantum h substance can ionize inert substance.
8. a kind of white wine, it is characterised in that the white wine has been eliminated according to the separation method described in claim any one of 1-7
Evil material.
9. white wine according to claim 8, it is characterised in that the content of lead ion is less than 0.005mg/ in the white wine
mL。
10. white wine according to claim 8, it is characterised in that the content of the methanol in wine is less than 0.005mg/mL.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710250795.5A CN106834068B (en) | 2017-04-17 | 2017-04-17 | Method for separating white spirit and harmful substances in white spirit |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710250795.5A CN106834068B (en) | 2017-04-17 | 2017-04-17 | Method for separating white spirit and harmful substances in white spirit |
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| CN106834068B CN106834068B (en) | 2020-09-04 |
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ID=59148002
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| CN108614061A (en) * | 2018-07-02 | 2018-10-02 | 山东师范大学 | A method of plasticiser in removal absolute ethyl alcohol and hexamethylene |
| CN115261179A (en) * | 2022-08-23 | 2022-11-01 | 劲牌有限公司 | Method for reducing content of formaldehyde in white spirit |
| CN116218626A (en) * | 2023-03-09 | 2023-06-06 | 上海信悉智能技术有限公司 | Small-molecular low-deuterium white spirit and preparation process thereof |
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| CN116218626A (en) * | 2023-03-09 | 2023-06-06 | 上海信悉智能技术有限公司 | Small-molecular low-deuterium white spirit and preparation process thereof |
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| Publication number | Publication date |
|---|---|
| CN106834068B (en) | 2020-09-04 |
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