CN106830949A - A kind of ceramic sintering method - Google Patents

A kind of ceramic sintering method Download PDF

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Publication number
CN106830949A
CN106830949A CN201710086661.4A CN201710086661A CN106830949A CN 106830949 A CN106830949 A CN 106830949A CN 201710086661 A CN201710086661 A CN 201710086661A CN 106830949 A CN106830949 A CN 106830949A
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China
Prior art keywords
kiln
plate
high temperature
kiln plate
temperature resistant
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CN201710086661.4A
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CN106830949B (en
Inventor
谢生林
倪永林
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Lixil American Standard Sanitary Ware Manufacturing Shanghai Co Ltd
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Lixil American Standard Sanitary Ware Manufacturing Shanghai Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/64Burning or sintering processes
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D5/00Supports, screens, or the like for the charge within the furnace

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Ceramic Engineering (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Furnace Charging Or Discharging (AREA)
  • Compositions Of Oxide Ceramics (AREA)

Abstract

A kind of ceramic sintering method, including:The first kiln plate is horizontally disposed with kiln;Multiple high temperature resistant balls are laid in first kiln plate;At least two piece second kiln plate for carrying out even support in the bottom of ceramic body is laid on the multiple high temperature resistant ball, gap is respectively provided between adjacent second kiln plate;Ceramic body is placed in second kiln plate, makes its bottom by least two piece second kiln plate even support;Start kiln and fire the ceramic body, 1,100 1300 DEG C of firing temperature, 68 hours time.The inventive method is during firing ceramics base substrate, second kiln plate can be relatively moved as base substrate shrinkage stress draws, the shrinkage stress of product is discharged with this, thoroughly solve the problem on deformation of high-end straight flange product, improve the sintering qualified rate of product, also the quality of such product is improved, cost is reduced.

Description

A kind of ceramic sintering method
Technical field
The present invention relates to ceramic fabrication technique, more particularly to a kind of ceramic sintering method.
Background technology
Existing ceramic body product need to be formed because of the particularity of firing process, final products by high-temperature firing, burnt till During base substrate product 3 have 10% or so contraction, and the kiln furnitures for being used for support product are non-shrinking, therefore base substrate product 3 faces contacted with kiln furnitures 4 just generate shrinks poor, produces shrinkage stress to cause product to burn till the deformation of contact surface (referring to Fig. 5 (a) and Fig. 5 (b)), become to burn till waste product.
Existing factory is the such contraction distortion of solution, by the way of being burnt in the pad of 4 upper berth mud plate of kiln furnitures 5.But because of mud plate Low intensity, weight capacity is poor, is easily broken in sintering process.Mud plate 5 causes base substrate product 3 from the breaking part A of mud plate 5 after being broken Deformed (referring to Fig. 6 (a) and Fig. 6 (b)), and the mud plate burnt can not be recycled.
The content of the invention
Based on this, for above-mentioned technical problem, there is provided a kind of ceramic body support kiln furnitures.
In order to solve the above technical problems, the present invention is adopted the following technical scheme that:
A kind of ceramic sintering method, including:
The first kiln plate is horizontally disposed with kiln;
Multiple high temperature resistant balls are laid in first kiln plate;
Laid on the multiple high temperature resistant ball for carrying out at least two piece of even support in the bottom of ceramic body Two kiln plates, gap is respectively provided between adjacent second kiln plate;
Ceramic body is placed in second kiln plate, makes its bottom by least two piece second kiln plate even support;
Start kiln and fire the ceramic body, 1100-1300 DEG C of firing temperature, time 6-8 hours.
This programme also includes:It is provided for carrying out spacing gear on the outside of the high temperature resistant ball in first kiln plate Frame, its thickness is slightly below the diameter of the high temperature resistant ball.
The gap is 30mm-40mm.
Second kiln plate is four pieces, and four piece of second kiln plate is layed on the multiple high temperature resistant ball in 2 × 2 matrixes, and Even support is in the bottom of ceramic body.
The high temperature resistant ball uses high temperature oxidation resisting aluminium ball, high-temperature resistant silicon carbide ball or the refractory ceramics of diameter 20mm Ball.
The thickness of the gear frame is 15-18mm.
Second kiln plate is rectangle.
The gap is 30mm.
1200 DEG C of the firing temperature, 7 hours time.
During firing ceramics base substrate, the second kiln plate can make phase to the inventive method as base substrate shrinkage stress draws To movement, the shrinkage stress of product is discharged with this, thoroughly solve the problem on deformation of high-end straight flange product, improve burning till for product Qualification rate, also improves the quality of such product, reduces cost.
Brief description of the drawings
The present invention is described in detail with reference to the accompanying drawings and detailed description:
Fig. 1 is the schematic diagram of the inventive method;
Fig. 2 is the top view of Fig. 1;
Fig. 3 is schematic diagram of the inventive method after burning till;
Fig. 4 is the top view of Fig. 3;
Fig. 5 (a) is the schematic diagram after base substrate product is burnt till by conventional method;
Fig. 5 (b) is the top view of Fig. 5 (a);
Fig. 6 (a) is that base substrate product overlays the schematic diagram after mud plate pad burns by tradition;
Fig. 6 (b) is the top view of Fig. 6 (a).
Specific embodiment
As Figure 1-4, a kind of ceramic sintering method, including:
First, the first kiln plate 110 is horizontally disposed with kiln.
2nd, multiple high temperature resistant balls 130 are laid in the first kiln plate 110.
3rd, laid on multiple high temperature resistant balls 130 for carrying out at least two pieces of even support in the bottom of ceramic body 2 Second kiln plate 120, gap is respectively provided between adjacent second kiln plate, it is ensured that the second kiln plate 120 will not be interfered when mobile and touched Hit.
Specifically, the second kiln plate 120 is rectangle, and above-mentioned gap is 30mm-40mm.
When the shape matching of ceramic body product is special, such as strip, the contraction of its narrower side can be ignored, this When, the second kiln plate 120 selects two pieces or three pieces.
3rd, ceramic body 2 is placed in the second kiln plate 120, its bottom is uniformly propped up by least two piece second kiln plate 120 Support.
Preferably, the second kiln plate 120 is four pieces, four piece of second kiln plate 120 is layed in multiple high temperature resistant balls in 2 × 2 matrixes On 130, and even support is in the bottom corner of ceramic body 2.
By measuring the contraction data of the four direction of ceramic body product and kiln plate contact surface, it is determined that at high temperature its Relative displacement can occur apart from 30mm under theory state, therefore above-mentioned gap is 30mm.
4th, kiln firing ceramics base substrate 2,1300-1400 DEG C of firing temperature, time 6-8 hours are started.
Preferably, 1200 DEG C of firing temperature, 7 hours time, efficiency high, to burn till quality good.
Spacing in order to be carried out to high temperature resistant ball 130, the inventive method is also provided in high temperature resistant in the first kiln plate 110 Ball outside carries out spacing gear frame 140, and the diameter that its thickness is slightly below high temperature resistant ball 130 (can not be less than the height of high temperature resistant ball 130 The half of degree).
Wherein, high temperature resistant ball uses high temperature oxidation resisting aluminium ball, high-temperature resistant silicon carbide ball or the refractory ceramics of diameter 20mm Ball, the thickness for keeping off frame 140 is 15-18mm.
During firing ceramics base substrate, the second kiln plate 120 can be with the traction of base substrate shrinkage stress for the inventive method Relatively move, the shrinkage stress of product is discharged with this, thoroughly solve the problem on deformation of high-end straight flange product, improve product Sintering qualified rate, also improves the quality of such product, reduces cost.
Embodiment 1
A kind of ceramic sintering method, including:
First, the first kiln plate 110 is horizontally disposed with kiln.
2nd, multiple refractory ceramics balls 130 are laid in the first kiln plate 110.
3rd, two piece of second kiln plate 120, the gap between adjacent second kiln plate are laid on multiple refractory ceramics balls 130 It is 35mm.
3rd, ceramic body 2 is placed in the second kiln plate 120, makes its bottom by two piece of second even support of kiln plate 120.
4th, it is provided for carrying out spacing gear frame 140 in the outside of refractory ceramics ball 130 in the first kiln plate 110, it is thick It is 15mm to spend.
5th, kiln firing ceramics base substrate 2,1300 DEG C of firing temperature, 8 hours time are started.
The ceramic body that the present embodiment is fired is that, to strip, the contraction of its narrower side can be ignored, therefore the second kiln Plate 120 selects two pieces.
Embodiment 2
A kind of ceramic sintering method, including:
First, the first kiln plate 110 is horizontally disposed with kiln.
2nd, multiple high temperature oxidation resisting aluminium balls 130 are laid in the first kiln plate 110.
3rd, four pieces of second kiln plates 120 in 2 × 2 matrixes, adjacent second are laid in multiple high temperature oxidation resisting aluminium balls 130 Gap between kiln plate is 30mm.
3rd, ceramic body 2 is placed in the second kiln plate 120, makes its bottom by four piece of second even support of kiln plate 120.
4th, it is provided for carrying out spacing gear frame 140 in the outside of high temperature oxidation resisting aluminium ball 130 in the first kiln plate 110, its Thickness is 16mm.
5th, kiln firing ceramics base substrate 2,1200 DEG C of firing temperature, 7 hours time are started.
The ceramic body that the present embodiment is fired is the much the same regular shape of length and width, therefore the second kiln plate 120 selects four pieces.
But, those of ordinary skill in the art is it should be appreciated that the embodiment of the above is intended merely to explanation originally Invention, and be not used as being limitation of the invention, as long as in spirit of the invention, to embodiment described above Change, modification will all fall in the range of claims of the present invention.

Claims (9)

1. a kind of ceramic sintering method, it is characterised in that including:
The first kiln plate is horizontally disposed with kiln;
Multiple high temperature resistant balls are laid in first kiln plate;
At least two piece second kiln for carrying out even support in the bottom of ceramic body is laid on the multiple high temperature resistant ball Plate, gap is respectively provided between adjacent second kiln plate;
Ceramic body is placed in second kiln plate, makes its bottom by least two piece second kiln plate even support;
Start kiln and fire the ceramic body, 1100-1300 DEG C of firing temperature, time 6-8 hours.
2. a kind of ceramic sintering method according to claim 1, it is characterised in that also include:In first kiln plate It is provided for carrying out spacing gear frame on the outside of the high temperature resistant ball, its thickness is slightly below the diameter of the high temperature resistant ball.
3. a kind of ceramic sintering method according to claim 2, it is characterised in that the gap is 30mm-40mm.
4. a kind of ceramic sintering method according to Claims 2 or 3, it is characterised in that second kiln plate is four pieces, four The kiln plate of block second is layed on the multiple high temperature resistant ball in 2 × 2 matrixes, and even support is in the bottom of ceramic body.
5. a kind of ceramic sintering method according to claim 4, it is characterised in that the high temperature resistant ball uses diameter 20mm High temperature oxidation resisting aluminium ball, high-temperature resistant silicon carbide ball or refractory ceramics ball.
6. a kind of ceramic sintering method according to claim 5, it is characterised in that the thickness of the gear frame is 15-18mm.
7. a kind of ceramic sintering method according to claim 6, it is characterised in that second kiln plate is rectangle.
8. a kind of ceramic sintering method according to claim 7, it is characterised in that the gap is 30mm.
9. a kind of ceramic sintering method according to claim 8, it is characterised in that 1200 DEG C of the firing temperature, time 7 Hour.
CN201710086661.4A 2017-02-17 2017-02-17 A kind of ceramic sintering method Active CN106830949B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110108130A (en) * 2019-04-30 2019-08-09 惠达卫浴股份有限公司 A kind of kiln-loading method of sanitary ceramics
CN112503948A (en) * 2020-10-28 2021-03-16 横店集团东磁股份有限公司 Bearing device and method for improving size precision of sintered ferrite product
CN113277835A (en) * 2020-02-20 2021-08-20 广州市尤特新材料有限公司 Positioning tool and sintering method of planar target

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3904352A (en) * 1974-01-17 1975-09-09 Coors Porcelain Co Assembly and method for supporting ceramics and the like during firing
CN101219898A (en) * 2007-12-22 2008-07-16 淄博华创精细陶瓷有限公司 Ceramic product baking and kiln-loading method
CN103438712A (en) * 2013-08-13 2013-12-11 上海高诚艺术包装有限公司 Firing method of large-scale flat-plate ceramics
CN203489672U (en) * 2013-08-13 2014-03-19 上海高诚艺术包装有限公司 Sintering device for large flat plate ceramic

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3904352A (en) * 1974-01-17 1975-09-09 Coors Porcelain Co Assembly and method for supporting ceramics and the like during firing
CN101219898A (en) * 2007-12-22 2008-07-16 淄博华创精细陶瓷有限公司 Ceramic product baking and kiln-loading method
CN103438712A (en) * 2013-08-13 2013-12-11 上海高诚艺术包装有限公司 Firing method of large-scale flat-plate ceramics
CN203489672U (en) * 2013-08-13 2014-03-19 上海高诚艺术包装有限公司 Sintering device for large flat plate ceramic

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110108130A (en) * 2019-04-30 2019-08-09 惠达卫浴股份有限公司 A kind of kiln-loading method of sanitary ceramics
CN113277835A (en) * 2020-02-20 2021-08-20 广州市尤特新材料有限公司 Positioning tool and sintering method of planar target
CN113277835B (en) * 2020-02-20 2022-10-11 广州市尤特新材料有限公司 Positioning tool and sintering method of planar target
CN112503948A (en) * 2020-10-28 2021-03-16 横店集团东磁股份有限公司 Bearing device and method for improving size precision of sintered ferrite product
CN112503948B (en) * 2020-10-28 2021-10-22 横店集团东磁股份有限公司 Bearing device and method for improving size precision of sintered ferrite product

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