CN106758147A - 基于纳米镁铁氧体的磁性涤纶织物制备方法 - Google Patents
基于纳米镁铁氧体的磁性涤纶织物制备方法 Download PDFInfo
- Publication number
- CN106758147A CN106758147A CN201611089373.6A CN201611089373A CN106758147A CN 106758147 A CN106758147 A CN 106758147A CN 201611089373 A CN201611089373 A CN 201611089373A CN 106758147 A CN106758147 A CN 106758147A
- Authority
- CN
- China
- Prior art keywords
- nanometer
- dacron
- ethanol
- phenol
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229920004934 Dacron® Polymers 0.000 title claims abstract description 29
- 239000005020 polyethylene terephthalate Substances 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 54
- 239000011777 magnesium Substances 0.000 claims abstract description 38
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims abstract description 20
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229910052749 magnesium Inorganic materials 0.000 claims abstract description 16
- 229910000859 α-Fe Inorganic materials 0.000 claims abstract description 16
- 239000011259 mixed solution Substances 0.000 claims abstract description 11
- 230000005308 ferrimagnetism Effects 0.000 claims abstract description 9
- 239000006185 dispersion Substances 0.000 claims abstract description 7
- 238000009413 insulation Methods 0.000 claims abstract description 7
- 238000002604 ultrasonography Methods 0.000 claims abstract description 7
- 239000000243 solution Substances 0.000 claims description 7
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims 2
- 229910052742 iron Inorganic materials 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 4
- 238000009988 textile finishing Methods 0.000 abstract description 2
- 239000004744 fabric Substances 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 229920004933 Terylene® Polymers 0.000 description 2
- 238000001467 acupuncture Methods 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 206010001497 Agitation Diseases 0.000 description 1
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000003562 lightweight material Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000000554 physical therapy Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/49—Oxides or hydroxides of elements of Groups 8, 9,10 or 18 of the Periodic Table; Ferrates; Cobaltates; Nickelates; Ruthenates; Osmates; Rhodates; Iridates; Palladates; Platinates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Paints Or Removers (AREA)
Abstract
本发明提供了一种基于纳米镁铁氧体的磁性涤纶织物制备方法,涉及纺织品整理技术领域,该方法包括如下步骤:(1)将苯酚溶于乙醇中;(2)将纳米镁铁氧体MgFe2O4分散到乙醇/苯酚混合溶液中,超声下得到纳米镁铁氧体分散溶液;(3)将涤纶织物投入到上述染液中,振荡加热至40~60ºC,保温持续5~30min;(4)最后分别用乙醇洗涤数次,取出后80ºC下烘干,即可获得纳米镁铁氧体磁性涤纶织物。本制备技术过程简单,不需要高温条件和复杂的反应设备;制备的纳米镁铁氧体磁性涤纶织物的耐久性好。
Description
技术领域
本发明涉及纺织品整理技术领域,具体涉及一种基于纳米镁铁氧体的磁性涤纶织物制备方法。
背景技术
现代医学表明,弱磁场可以使人的兴奋性增高,呈现活跃反应。在人体穴位处的磁力线可以穿透这些穴位,起到如中医针灸一样的作用。因此穿着这样的织物随时进行人体全方位理疗。基于这种原理,采用磁性纤维生产出的纺织品能调整人体机能、提高人体抗病能力,起到医疗保健作用。以涤纶为基底的复合磁性织物由于质量轻,原料易得,价格便宜,稳定性好等特点,是最有前途的磁性织物之一。目前,基于纳米镁铁氧体MgFe2O4的磁性涤纶织物制备方法主要有共混法和涂层法。
发明内容
本发明所要解决的问题是提供一种制备工艺简单,稳定性好的基于纳米镁铁氧体的磁性涤纶织物制备方法,本发明采取如下技术方案。
一种基于纳米镁铁氧体的磁性涤纶织物制备方法,包括如下步骤:(1)将苯酚溶于乙醇中;(2)将纳米镁铁氧体MgFe2O4分散于乙醇/苯酚混合溶液中,超声下得到纳米镁铁氧体分散溶液;(3)将涤纶织物投入到上述溶液中,振荡加热至30~60ºC,保温持续5~30min;(4)分别用乙醇洗涤数次,取出后80ºC下烘干,即可获得纳米镁铁氧体磁性涤纶织物。
进一步的,所述的乙醇/苯酚混合溶液的乙醇与苯酚的质量比为1:0.1~3。
进一步的,所述的纳米镁铁氧体与乙醇/苯酚混合溶液的质量比为1:100~1000。
本发明的有益效果在于,基于纳米镁铁氧体的磁性涤纶织物制备方法简单,不需要高温条件和复杂的反应设备;制备的纳米镁铁氧体磁性涤纶织物的耐久性好。
具体实施方式
下文将结合具体实施例详细描述本发明。应当注意的是,下述实施例中描述的技术特征或者技术特征的组合不应当被认为是孤立的,它们可以被相互组合从而达到更好的技术效果。
实施例1
基于纳米镁铁氧体的磁性涤纶织物制备方法详细步骤如下:
(1)将20g苯酚溶于180g乙醇中;
(2)将0.2g纳米镁铁氧体分散于乙醇/苯酚混合溶液中,超声下得到纳米镁铁氧体分散溶液;
(3)将10g涤纶织物投入到上述溶液中,振荡加热至40ºC,保温持续30min;
(4)分别用乙醇洗涤数次,取出后80ºC下烘干,即可获得纳米镁铁氧体磁性涤纶织物。
实施例2
基于纳米镁铁氧体的磁性涤纶织物制备方法详细步骤如下:
(1)将300g苯酚溶于100g乙醇中;
(2)将4g纳米镁铁氧体分散于乙醇/苯酚混合溶液中,超声下得到纳米镁铁氧体分散溶液;
(3)将10g涤纶织物投入到上述溶液中,振荡加热至60ºC,保温持续5min;
(4)分别用乙醇洗涤数次,取出后80ºC下烘干,即可获得纳米镁铁氧体磁性涤纶织物。
实施例3
基于纳米镁铁氧体的磁性涤纶织物制备方法详细步骤如下:
(1)将50g苯酚溶于250g乙醇中;
(2)将2g纳米镁铁氧体分散于乙醇/苯酚混合溶液中,超声下得到纳米镁铁氧体分散溶液;
(3)将10g涤纶织物投入到上述溶液中,振荡加热至50ºC,保温持续10min;
(4)分别用乙醇洗涤数次,取出后80ºC下烘干,即可获得纳米镁铁氧体磁性涤纶织物。
实施例4
基于纳米镁铁氧体的磁性涤纶织物制备方法详细步骤如下:
(1)将200g苯酚溶于200g乙醇中;
(2)将3g纳米镁铁氧体分散于乙醇/苯酚混合溶液中,超声下得到纳米镁铁氧体分散溶液;
(3)将10g涤纶织物投入到上述溶液中,振荡加热至40ºC,保温持续15min;
(4)分别用乙醇洗涤数次,取出后80ºC下烘干,即可获得纳米镁铁氧体磁性涤纶织物。
本文虽然已经给出了本发明的一些实施例,但是本领域的技术人员应当理解,在不脱离本发明精神的情况下,可以对本文的实施例进行改变。上述实施例只是示例性的,不应以本文的实施例作为本发明权利范围的限定。
Claims (3)
1.一种基于纳米镁铁氧体的磁性涤纶织物制备方法,其特征在于,包括如下步骤:
(1)将苯酚溶于乙醇中;
(2)将纳米镁铁氧体MgFe2O4分散于乙醇/苯酚混合溶液中,超声下得到纳米镁铁氧体分散溶液;
(3)将涤纶织物投入到上述溶液中,振荡加热至40~60ºC,保温持续5~30min;
(4)分别用乙醇洗涤数次,取出后80ºC下烘干,即可获得纳米镁铁氧体磁性涤纶织物。
2.如权利要求1所述的基于纳米镁铁氧体的磁性涤纶织物制备方法,所述的乙醇/苯酚混合溶液的乙醇与苯酚的质量比为1:0.1~3。
3.如权利要求1所述的基于纳米镁铁氧体的磁性涤纶织物制备方法,所述的纳米镁铁氧体与乙醇/苯酚混合溶液的质量比为1:100~1000。
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201611089373.6A CN106758147A (zh) | 2016-12-01 | 2016-12-01 | 基于纳米镁铁氧体的磁性涤纶织物制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201611089373.6A CN106758147A (zh) | 2016-12-01 | 2016-12-01 | 基于纳米镁铁氧体的磁性涤纶织物制备方法 |
Publications (1)
Publication Number | Publication Date |
---|---|
CN106758147A true CN106758147A (zh) | 2017-05-31 |
Family
ID=58915301
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201611089373.6A Pending CN106758147A (zh) | 2016-12-01 | 2016-12-01 | 基于纳米镁铁氧体的磁性涤纶织物制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN106758147A (zh) |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101135071A (zh) * | 2007-06-22 | 2008-03-05 | 上海兰度科技有限公司 | 一种纳米吸波纤维及其制备方法 |
CN104652122A (zh) * | 2013-11-20 | 2015-05-27 | 光州科学技术院 | 电磁波屏蔽材料的制备方法 |
CN105113217A (zh) * | 2015-09-09 | 2015-12-02 | 卜庆革 | 可同时吸收低频和高频电磁波的复合纤维及其制备方法 |
CN105256533A (zh) * | 2015-11-16 | 2016-01-20 | 西安工程大学 | 一种磁性载药织物的制备方法 |
-
2016
- 2016-12-01 CN CN201611089373.6A patent/CN106758147A/zh active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101135071A (zh) * | 2007-06-22 | 2008-03-05 | 上海兰度科技有限公司 | 一种纳米吸波纤维及其制备方法 |
CN104652122A (zh) * | 2013-11-20 | 2015-05-27 | 光州科学技术院 | 电磁波屏蔽材料的制备方法 |
CN105113217A (zh) * | 2015-09-09 | 2015-12-02 | 卜庆革 | 可同时吸收低频和高频电磁波的复合纤维及其制备方法 |
CN105256533A (zh) * | 2015-11-16 | 2016-01-20 | 西安工程大学 | 一种磁性载药织物的制备方法 |
Non-Patent Citations (1)
Title |
---|
董静: "MgFe2O4涤纶复合材料的制备及其处理染料废水的研究", 《中国学位论文全文数据库》 * |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN102389620B (zh) | 多功能纳米能量粒 | |
CN104178834B (zh) | 一种中药粘胶纤维保健面料 | |
CN102733199B (zh) | 含砭石的布料及其生产工艺 | |
CN102268326B (zh) | 缓释可控薰衣草精油微胶囊、整理剂及其制备方法和应用 | |
CN108783617A (zh) | 具有微循环理疗功能的智能男女内裤 | |
CN106555330A (zh) | 在涤纶织物上负载纳米四氧化三铁的方法 | |
CN106758147A (zh) | 基于纳米镁铁氧体的磁性涤纶织物制备方法 | |
KR20120133048A (ko) | 안티셀룰라이트 캡슐이 혼입된 기능성 의류 | |
CN103845479A (zh) | 治疗肠风下血的中药 | |
CN203969242U (zh) | 一种中药敷贴套装 | |
CN104490184A (zh) | 一种保健型舒压被 | |
CN201695175U (zh) | 多功能保健桑蚕丝绒毡 | |
CN101204472B (zh) | 一种治疗软疖红肿的外用药物 | |
CN205814858U (zh) | 一种抗皱提升的医用面罩 | |
CN205272728U (zh) | 一种具有保健功能的家纺面料 | |
CN103655823B (zh) | 一种治疗萎缩性胃炎的中草药组合物及其制备方法 | |
CN108842257A (zh) | 一种保健除菌面料 | |
CN203400294U (zh) | 一种新型足部被动锻炼袜 | |
CN103014972A (zh) | 一种空芯结构的抗皱真丝面料的制备方法 | |
CN101524226A (zh) | 治疗神经衰弱的蚕丝被的生产方法 | |
CN203000450U (zh) | 一种抗菌地毯 | |
CN107898019A (zh) | 一种运动服装 | |
CN101204475B (zh) | 一种治疗手足皮肤瘙痒症的浸泡药物 | |
CN206463417U (zh) | 一种随意调节负重的跑步用绑腿装置 | |
CN101199704B (zh) | 一种治疗暑疖溃烂的外用药物 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
WD01 | Invention patent application deemed withdrawn after publication | ||
WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170531 |