CN106753622A - A kind of sludge petroleum charred slurry and preparation method thereof - Google Patents

A kind of sludge petroleum charred slurry and preparation method thereof Download PDF

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Publication number
CN106753622A
CN106753622A CN201611150359.2A CN201611150359A CN106753622A CN 106753622 A CN106753622 A CN 106753622A CN 201611150359 A CN201611150359 A CN 201611150359A CN 106753622 A CN106753622 A CN 106753622A
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parts
sludge
petroleum coke
petroleum
water
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刘子杰
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Qinzhou University
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Qinzhou University
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/32—Liquid carbonaceous fuels consisting of coal-oil suspensions or aqueous emulsions or oil emulsions
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L10/00—Use of additives to fuels or fires for particular purposes
    • C10L10/18—Use of additives to fuels or fires for particular purposes use of detergents or dispersants for purposes not provided for in groups C10L10/02 - C10L10/16
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/24—Organic compounds containing sulfur, selenium and/or tellurium
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/24—Organic compounds containing sulfur, selenium and/or tellurium
    • C10L1/2406—Organic compounds containing sulfur, selenium and/or tellurium mercaptans; hydrocarbon sulfides
    • C10L1/2412—Organic compounds containing sulfur, selenium and/or tellurium mercaptans; hydrocarbon sulfides sulfur bond to an aromatic radical
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/24—Organic compounds containing sulfur, selenium and/or tellurium
    • C10L1/2431—Organic compounds containing sulfur, selenium and/or tellurium sulfur bond to oxygen, e.g. sulfones, sulfoxides
    • C10L1/2437—Sulfonic acids; Derivatives thereof, e.g. sulfonamides, sulfosuccinic acid esters
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/24—Organic compounds containing sulfur, selenium and/or tellurium
    • C10L1/2462—Organic compounds containing sulfur, selenium and/or tellurium macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/24—Organic compounds containing sulfur, selenium and/or tellurium
    • C10L1/2462—Organic compounds containing sulfur, selenium and/or tellurium macromolecular compounds
    • C10L1/2475—Organic compounds containing sulfur, selenium and/or tellurium macromolecular compounds obtained otherwise than by reactions only involving unsaturated carbon to carbon bonds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L2200/00—Components of fuel compositions
    • C10L2200/04—Organic compounds
    • C10L2200/0461—Fractions defined by their origin
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L2300/00—Mixture of two or more additives covered by the same group of C10L1/00 - C10L1/308
    • C10L2300/20—Mixture of two components
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L2300/00—Mixture of two or more additives covered by the same group of C10L1/00 - C10L1/308
    • C10L2300/30—Mixture of three components

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Combustion & Propulsion (AREA)
  • Liquid Carbonaceous Fuels (AREA)
  • Solid Fuels And Fuel-Associated Substances (AREA)

Abstract

The invention discloses a kind of sludge petroleum charred slurry and preparation method thereof, it is made up of following mass fraction formula components：16 18 parts of petroleum coke, 68 parts of lignosulfonates, 35 parts of surfactant, 12 parts of stabilizer, 16 18 parts of sludge, 5 15 parts of naphthalene sulfonate, 46 parts of polycarboxylic acid salt, 46 parts of humic-acid kind, 13 parts of dispersant, 6 10 parts of high sulfur petroleum coke, 16 18 parts of black liquid, 13 parts of improved chemical, 100 200 parts of water, the present invention can be as fuel combustion, or gasification production synthesis gas and hydrogen.The calorific value in sludge can not only be made to be fully used, and it is high to also overcome the heat treatment power consumption of existing water-containing sludge, the problems such as tail gas and residue poisonous and harmful refractory reason, with larger industrial applications prospect.

Description

A kind of sludge petroleum charred slurry and preparation method thereof
Technical field
The present invention relates to sludge petroleum charred slurry field, in particular to a kind of sludge petroleum charred slurry and preparation method thereof.
Background technology
Oil refining industry will produce bulk petroleum burnt every year.The key component of petroleum coke is hydrocarbon, the heating of its low level Amount is about 1.5~2 times of coal.With the increase of crude oil sulfur content, the quantity of high sulfur petroleum coke of the sulfur content more than 3% significantly increases Plus.High sulfur petroleum coke directly is used, a large amount of SO2 can be produced；And gasification is directly used in, though generation SO2 can be avoided (to generate H2S, easily It is recovered as sulphur), but because petroleum coke activity is poor, fuel utilization efficiency is not high.Petroleum coke slurrying existence and stability is poor simultaneously The shortcomings of.
The reasonable treatment of water-containing sludge and recycling are the key subjects of sewage disposal and environmental protection.It is each at present Plant in water-containing sludge processing method, heat treatment method most has prospect.Sludge heat treatment can not only rapidly and largely make dirt Mud reaches minimizing, and the calorific value in sludge can also be made to obtain certain utilization.But, large quantity of moisture, one are contained in sludge As up to 80% or so, existing heat treatment method generally requires and sludge is pre-dried, and removes large quantity of moisture therein.Sludge Being pre-dried need to consume amount of heat, and can produce the poisonous and hazardous stench tail gas of a large amount of refractory reasons, cause existing sludge Heat treatment technics high cost, power consumption is high, the problems such as tail gas refractory reason.
The content of the invention
The invention provides a kind of sludge petroleum charred slurry and preparation method thereof, the present invention can be as fuel combustion, or gas Metaplasia production of synthetic gas and hydrogen.The calorific value in sludge can not only be made to be fully used, and also overcome existing water-containing sludge Heat treatment power consumption is high, the problems such as tail gas and residue poisonous and harmful refractory reason, with larger industrial applications prospect.
To achieve the above object, the present invention provides following technical scheme：
A kind of sludge petroleum charred slurry and preparation method thereof, is made up of following mass fraction formula components：Petroleum coke 16-18 Part, lignosulfonates 6-8 parts, surfactant 3-5 parts, stabilizer 1-2 parts, sludge 16-18 parts, naphthalene sulfonate 5-15 parts, Polycarboxylic acid salt 4-6 parts, humic-acid kind 4-6 parts, dispersant 1-3 parts, high sulfur petroleum coke 6-10 parts, black liquid 16-18 parts, change 1-3 parts, water 100-200 parts of medicament of property.
Further：It is made up of following mass fraction formula components：16 parts of petroleum coke, 6 parts of lignosulfonates, surface-active 3 parts of agent, 1 part of stabilizer, 16 parts of sludge, 5 parts of naphthalene sulfonate, 4 parts of polycarboxylic acid salt, 4 parts of humic-acid kind, 1 part of dispersant, high-sulfur 6 parts of petroleum coke, 16 parts of black liquid, 1 part of improved chemical, 100 parts of water.
Further：It is made up of following mass fraction formula components：17 parts of petroleum coke, 7 parts of lignosulfonates, surface-active 4 parts of agent, 1.5 parts of stabilizer, 17 parts of sludge, 10 parts of naphthalene sulfonate, 5 parts of polycarboxylic acid salt, 5 parts of humic-acid kind, 2 parts of dispersant, 8 parts of high sulfur petroleum coke, 17 parts of black liquid, 2 parts of improved chemical, 150 parts of water.
Further：It is made up of following mass fraction formula components：18 parts of petroleum coke, 8 parts of lignosulfonates, surface-active 5 parts of agent, 2 parts of stabilizer, 18 parts of sludge, 15 parts of naphthalene sulfonate, 6 parts of polycarboxylic acid salt, 6 parts of humic-acid kind, 3 parts of dispersant, height 10 parts of sulphur petroleum coke, 18 parts of black liquid, 3 parts of improved chemical, 200 parts of water.
Further：Preparation method of the present invention has following steps：
Step one, oily sludge and oily sludge improved chemical are mixed and are diluted with water, and prepare modified oily sludge Mixed liquor；
Step 2, will petroleum coke, dispersant and modified oily sludge mixed liquor add grinding machine in grind, make solid particle grain Footpath
≤0.5mm；
Step 3, will step 2 gained add surplus stock mix after be made pulpous state, both finished product.
The beneficial effects of the invention are as follows：
1st, the present invention can be as fuel combustion, or gasification production synthesis gas and hydrogen；
2nd, the calorific value in sludge can not only be made to be fully used, and also overcomes existing water-containing sludge heat treatment power consumption The problems such as height, tail gas and residue poisonous and harmful refractory reason, with larger industrial applications prospect.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, Obviously, described embodiment is only a part of embodiment of the invention, rather than whole embodiments.Based in the present invention Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, all Belong to the scope of protection of the invention.
Embodiment one：
A kind of sludge petroleum charred slurry is made up of following mass fraction formula components：Petroleum coke 16-18 parts, lignosulfonates 6-8 parts, surfactant 3-5 parts, stabilizer 1-2 parts, sludge 16-18 parts, naphthalene sulfonate 5-15 parts, polycarboxylic acid salt 4-6 parts, Humic-acid kind 4-6 parts, dispersant 1-3 parts, high sulfur petroleum coke 6-10 parts, black liquid 16-18 parts, improved chemical 1-3 parts, water 100-200 parts.
Embodiment two：
A kind of sludge petroleum charred slurry is made up of following mass fraction formula components：16 parts of petroleum coke, lignosulfonates 6 Part, 3 parts of surfactant, 1 part of stabilizer, 16 parts of sludge, 5 parts of naphthalene sulfonate, 4 parts of polycarboxylic acid salt, humic-acid kind 4 part, point 1 part of powder, 6 parts of high sulfur petroleum coke, 16 parts of black liquid, 1 part of improved chemical, 100 parts of water.
Embodiment three：
A kind of sludge petroleum charred slurry is made up of following mass fraction formula components：17 parts of petroleum coke, lignosulfonates 7 Part, 4 parts of surfactant, 1.5 parts of stabilizer, 17 parts of sludge, 10 parts of naphthalene sulfonate, 5 parts of polycarboxylic acid salt, 5 parts of humic-acid kind, 2 parts of dispersant, 8 parts of high sulfur petroleum coke, 17 parts of black liquid, 2 parts of improved chemical, 150 parts of water.
Example IV：
A kind of sludge petroleum charred slurry is made up of following mass fraction formula components：18 parts of petroleum coke, lignosulfonates 8 Part, 5 parts of surfactant, 2 parts of stabilizer, 18 parts of sludge, 15 parts of naphthalene sulfonate, 6 parts of polycarboxylic acid salt, humic-acid kind 6 part, point 3 parts of powder, 10 parts of high sulfur petroleum coke, 18 parts of black liquid, 3 parts of improved chemical, 200 parts of water.
Embodiment five：
A kind of preparation method preparation method of sludge petroleum charred slurry comprises the following steps：
Step one, oily sludge and oily sludge improved chemical are mixed and are diluted with water, and prepare modified oily sludge Mixed liquor；
Step 2, will petroleum coke, dispersant and modified oily sludge mixed liquor add grinding machine in grind, make solid particle grain Footpath
≤0.5mm；
Step 3, will step 2 gained add surplus stock mix after be made pulpous state, both finished product.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each implementation method is only wrapped Containing an independent technical scheme, this narrating mode of specification is only that for clarity, those skilled in the art should Specification an as entirety, the technical scheme in each embodiment can also be formed into those skilled in the art through appropriately combined May be appreciated other embodiment.

Claims (5)

1. a kind of sludge petroleum charred slurry, it is characterised in that：It is made up of following mass fraction formula components：
Petroleum coke 16-18 parts, lignosulfonates 6-8 parts, surfactant 3-5 parts, stabilizer 1-2 parts, sludge 16-18 parts, Naphthalene sulfonate 5-15 parts, polycarboxylic acid salt 4-6 parts, humic-acid kind 4-6 parts, dispersant 1-3 parts, high sulfur petroleum coke 6-10 parts, make 16-18 parts, improved chemical 1-3 parts, water 100-200 parts of paper black liquor.
2. a kind of sludge petroleum charred slurry according to claim 1, it is characterised in that：By following mass fraction formula components group Into：
16 parts of petroleum coke, 6 parts of lignosulfonates, 3 parts of surfactant, 1 part of stabilizer, 16 parts of sludge, 5 parts of naphthalene sulfonate, 4 parts of polycarboxylic acid salt, 4 parts of humic-acid kind, 1 part of dispersant, 6 parts of high sulfur petroleum coke, 16 parts of black liquid, 1 part of improved chemical, water 100 parts.
3. a kind of sludge petroleum charred slurry according to claim 1, it is characterised in that：By following mass fraction formula components group Into：
17 parts of petroleum coke, 7 parts of lignosulfonates, 4 parts of surfactant, 1.5 parts of stabilizer, 17 parts of sludge, naphthalene sulfonate 10 Part, 5 parts of polycarboxylic acid salt, 5 parts of humic-acid kind, 2 parts of dispersant, 8 parts of high sulfur petroleum coke, 17 parts of black liquid, improved chemical 2 Part, 150 parts of water.
4. a kind of sludge petroleum charred slurry according to claim 1, it is characterised in that：By following mass fraction formula components group Into：
18 parts of petroleum coke, 8 parts of lignosulfonates, 5 parts of surfactant, 2 parts of stabilizer, 18 parts of sludge, 15 parts of naphthalene sulfonate, 6 parts of polycarboxylic acid salt, 6 parts of humic-acid kind, 3 parts of dispersant, 10 parts of high sulfur petroleum coke, 18 parts of black liquid, 3 parts of improved chemical, 200 parts of water.
5. a kind of a kind of preparation method of sludge petroleum charred slurry according to claim 1, it is characterised in that：Including following step Suddenly：
Step one, oily sludge and oily sludge improved chemical are mixed and are diluted with water, and prepare modified oily sludge mixing Liquid；
Step 2, will petroleum coke, dispersant and modified oily sludge mixed liquor add grinding machine in grind, make solid grain size≤ 0.5mm；
Step 3, will step 2 gained add surplus stock mix after be made pulpous state, both finished product.
CN201611150359.2A 2016-12-14 2016-12-14 A kind of sludge petroleum charred slurry and preparation method thereof Pending CN106753622A (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103060031A (en) * 2012-12-26 2013-04-24 东南大学 Papermaking black liquor modified sludge-petroleum coke slurry and preparation method thereof
CN103468333A (en) * 2012-06-06 2013-12-25 中国石油天然气股份有限公司 Oily sludge coke water slurry and preparation method thereof
CN104651003A (en) * 2013-11-22 2015-05-27 中国石油天然气股份有限公司 Sludge coke slurry and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103468333A (en) * 2012-06-06 2013-12-25 中国石油天然气股份有限公司 Oily sludge coke water slurry and preparation method thereof
CN103060031A (en) * 2012-12-26 2013-04-24 东南大学 Papermaking black liquor modified sludge-petroleum coke slurry and preparation method thereof
CN104651003A (en) * 2013-11-22 2015-05-27 中国石油天然气股份有限公司 Sludge coke slurry and preparation method thereof

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