CN106751942A - A kind of super abrasive static-free glue band - Google Patents

A kind of super abrasive static-free glue band Download PDF

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Publication number
CN106751942A
CN106751942A CN201611094141.XA CN201611094141A CN106751942A CN 106751942 A CN106751942 A CN 106751942A CN 201611094141 A CN201611094141 A CN 201611094141A CN 106751942 A CN106751942 A CN 106751942A
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CN
China
Prior art keywords
parts
static
microwave treatment
glue band
super abrasive
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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CN201611094141.XA
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Chinese (zh)
Inventor
不公告发明人
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Zhengzhou Yuanran Biology Technology Co Ltd
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Zhengzhou Yuanran Biology Technology Co Ltd
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Priority to CN201611094141.XA priority Critical patent/CN106751942A/en
Publication of CN106751942A publication Critical patent/CN106751942A/en
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L93/00—Compositions of natural resins; Compositions of derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J7/00—Adhesives in the form of films or foils
    • C09J7/20—Adhesives in the form of films or foils characterised by their carriers
    • C09J7/22—Plastics; Metallised plastics
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00—Properties
    • C08L2201/04—Antistatic
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/14—Polymer mixtures characterised by other features containing polymeric additives characterised by shape
    • C08L2205/16—Fibres; Fibrils
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J2301/00—Additional features of adhesives in the form of films or foils
    • C09J2301/40—Additional features of adhesives in the form of films or foils characterized by the presence of essential components
    • C09J2301/41—Additional features of adhesives in the form of films or foils characterized by the presence of essential components additives as essential feature of the carrier layer

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Polishing Bodies And Polishing Tools (AREA)
  • Manufacture Of Macromolecular Shaped Articles (AREA)

Abstract

The invention discloses a kind of super abrasive static-free glue band, the super abrasive static-free glue band is according to the raw material of weight portion：25 37 parts of natural resin, 13 20 parts of phenolic resin, 24 parts of ammonium persulfate, 5 10 parts of Graphene, 8 10 parts of polyester fiber, 48 parts of barium sulfate, 26 parts of 1,3 propane sultone, 27 parts of 2 chlorine, 3 picolinic acid, 24 parts of methyl acrylate, 12 parts of EDTA；Natural resin, phenolic resin, ammonium persulfate, Graphene, polyester fiber, barium sulfate, 1 are weighed in proportion, 3 propane sultones, the picolinic acid of 2 chlorine 3, methyl acrylate, EDTA, stir and evenly mix rear microwave treatment, the power of microwave treatment is 200 300W, microwave treatment time is 10 20min, and microwave treatment is put into reactor after terminating, and pressure is set to 7 10MPa, reacted under the catalysis of platinum filament, reaction terminates rear extrusion molding and obtains final product.Super abrasive static-free glue band prepared by the present invention has wear-resisting and antistatic function concurrently, and antistatic performance persistently, can be used, high financial profit, low cost, long service life under various Different climate damp conditions.

Description

A kind of super abrasive static-free glue band
Technical field
The present invention relates to a kind of field of material technology, specifically a kind of super abrasive static-free glue band.
Background technology
At present, static-free glue band is a kind of general electronic package material, is widely employed for the envelope of electronic product Among dress processing procedure, integrated circuit can not only be closed, to completely cut off external environment condition, and generally there is anti-static function, can be kept away Exempt from electrostatic to damage integrated circuit.Generally, package adhesive tape be a laminate structure, its from lower to upper include a substrate layer, Matrix of the substrate layer as an aluminium plating membrane is attached on one adhesive layer.Reprocessing fits the aluminium plating membrane in this substrate layer Top surface and impedance is provided.Static-free glue band is all single structure in the prior art, without optical characteristics, without water proofing property Can, antistatic performance is undesirable, be difficult to pull apart, not environmentally etc. the shortcomings of.Surface is easy in use for existing adhesive tape simultaneously Scratch, wearability is poor.
The content of the invention
It is an object of the invention to provide a kind of super abrasive static-free glue band, with asking for solving to propose in above-mentioned background technology Topic.
To achieve the above object, the present invention provides following technical scheme：
A kind of super abrasive static-free glue band, be according to the primary raw material of weight portion：Natural resin 25-37 parts, phenolic resin 13-20 Part, ammonium persulfate 2-4 parts, Graphene 5-10 parts, polyester fiber 8-10 parts, barium sulfate 4-8 parts, 2-6 parts of 1,3- propane sultones, 2-7 parts, methyl acrylate 2-4 parts, EDTA 1-2 parts of 2- chloro-3-pyridyl carboxylic acids.As further scheme of the invention：According to weight Measure part raw material be：Natural resin 29-33 parts, phenolic resin 15-18 parts, ammonium persulfate 2-4 parts, Graphene 7-9 parts, polyester fibre Dimension 8-10 parts, barium sulfate 4-8 parts, 2-6 parts of 1,3- propane sultones, 2-7 parts of 2- chloro-3-pyridyl carboxylic acids, methyl acrylate 2-4 Part, EDTA 1-2 parts.
As further scheme of the invention：Raw material according to weight portion is：32 parts of natural resin, 17 parts of phenolic resin, 3 parts of ammonium persulfate, 8 parts of Graphene, 9 parts of polyester fiber, 6 parts of barium sulfate, 4 parts of 1,3- propane sultones, 2- chloro-3-pyridyl carboxylic acids 5 parts, 3 parts of methyl acrylate, 2 parts of EDTA.
A kind of preparation method of super abrasive static-free glue band, preparation method is specific as follows：
Weigh in proportion in natural resin, phenolic resin, ammonium persulfate, Graphene, polyester fiber, barium sulfate, 1,3- propane sulphurs Ester, 2- chloro-3-pyridyls carboxylic acid, methyl acrylate, EDTA, stir and evenly mix rear microwave treatment, and the power of microwave treatment is 200- 300W, microwave treatment time is 10-20min, and microwave treatment is put into reactor after terminating, and pressure is set to 7-10MPa, in platinum Reacted under the catalysis of silk, reaction terminates rear extrusion molding and obtains final product.
As further scheme of the invention：The power of microwave treatment is 250W, and microwave treatment time is 15min.
As further scheme of the invention：Pressure is set to 9MPa.
Compared with prior art, the beneficial effects of the invention are as follows：
Super abrasive static-free glue band prepared by the present invention has wear-resisting and antistatic function concurrently, and antistatic performance persistently, can be each Used under kind Different climate damp condition, high financial profit, low cost, long service life.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, Obviously, described embodiment is only a part of embodiment of the invention, rather than whole embodiments.Based in the present invention Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, all Belong to the scope of protection of the invention.
Embodiment 1
A kind of super abrasive static-free glue band, be according to the primary raw material of weight portion：25 parts of natural resin, 13 parts of phenolic resin, mistake 2 parts of ammonium sulfate, 5 parts of Graphene, 8 parts of polyester fiber, 4 parts of barium sulfate, 2 parts of 1,3- propane sultones, 2- chloro-3-pyridyls carboxylic acid 2 Part, 2 parts of methyl acrylate, 1 part of EDTA.A kind of preparation method of super abrasive static-free glue band, preparation method is specific as follows：
Weigh in proportion in natural resin, phenolic resin, ammonium persulfate, Graphene, polyester fiber, barium sulfate, 1,3- propane sulphurs Ester, 2- chloro-3-pyridyls carboxylic acid, methyl acrylate, EDTA, stir and evenly mix rear microwave treatment, and the power of microwave treatment is 200W, micro- Ripple process time is 10min, and microwave treatment is put into reactor after terminating, and pressure is set to 7MPa, anti-under the catalysis of platinum filament Should, reaction terminates rear extrusion molding and obtains final product.
Embodiment 2
A kind of super abrasive static-free glue band, be according to the primary raw material of weight portion：29 parts of natural resin, 15 parts of phenolic resin, mistake 2 parts of ammonium sulfate, 7 parts of Graphene, 8 parts of polyester fiber, 4 parts of barium sulfate, 2 parts of 1,3- propane sultones, 2- chloro-3-pyridyls carboxylic acid 2 Part, 2 parts of methyl acrylate, 1 part of EDTA.
A kind of preparation method of super abrasive static-free glue band, preparation method is specific as follows：
Weigh in proportion in natural resin, phenolic resin, ammonium persulfate, Graphene, polyester fiber, barium sulfate, 1,3- propane sulphurs Ester, 2- chloro-3-pyridyls carboxylic acid, methyl acrylate, EDTA, stir and evenly mix rear microwave treatment, and the power of microwave treatment is 200W, micro- Ripple process time is 10min, and microwave treatment is put into reactor after terminating, and pressure is set to 7MPa, anti-under the catalysis of platinum filament Should, reaction terminates rear extrusion molding and obtains final product.
Embodiment 3
A kind of super abrasive static-free glue band, be according to the primary raw material of weight portion：32 parts of natural resin, 17 parts of phenolic resin, mistake 3 parts of ammonium sulfate, 8 parts of Graphene, 9 parts of polyester fiber, 6 parts of barium sulfate, 4 parts of 1,3- propane sultones, 2- chloro-3-pyridyls carboxylic acid 5 Part, 3 parts of methyl acrylate, 2 parts of EDTA.
A kind of preparation method of super abrasive static-free glue band, preparation method is specific as follows：
Weigh in proportion in natural resin, phenolic resin, ammonium persulfate, Graphene, polyester fiber, barium sulfate, 1,3- propane sulphurs Ester, 2- chloro-3-pyridyls carboxylic acid, methyl acrylate, EDTA, stir and evenly mix rear microwave treatment, and the power of microwave treatment is 250W, micro- Ripple process time is 15min, and microwave treatment is put into reactor after terminating, and pressure is set to 9MPa, anti-under the catalysis of platinum filament Should, reaction terminates rear extrusion molding and obtains final product.
Embodiment 4
A kind of super abrasive static-free glue band, be according to the primary raw material of weight portion：33 parts of natural resin, 18 parts of phenolic resin, mistake 4 parts of ammonium sulfate, 9 parts of Graphene, 10 parts of polyester fiber, 8 parts of barium sulfate, 6 parts of 1,3- propane sultones, 2- chloro-3-pyridyls carboxylic acid 7 Part, 4 parts of methyl acrylate, 2 parts of EDTA.
A kind of preparation method of super abrasive static-free glue band, preparation method is specific as follows：
Weigh in proportion in natural resin, phenolic resin, ammonium persulfate, Graphene, polyester fiber, barium sulfate, 1,3- propane sulphurs Ester, 2- chloro-3-pyridyls carboxylic acid, methyl acrylate, EDTA, stir and evenly mix rear microwave treatment, and the power of microwave treatment is 300W, micro- Ripple process time is 20min, and microwave treatment is put into reactor after terminating, and pressure is set to 10MPa, anti-under the catalysis of platinum filament Should, reaction terminates rear extrusion molding and obtains final product.
Embodiment 5
A kind of super abrasive static-free glue band, be according to the primary raw material of weight portion：37 parts of natural resin, 20 parts of phenolic resin, mistake 4 parts of ammonium sulfate, 10 parts of Graphene, 10 parts of polyester fiber, 8 parts of barium sulfate, 6 parts of 1,3- propane sultones, 2- chloro-3-pyridyl carboxylic acids 7 parts, 4 parts of methyl acrylate, 2 parts of EDTA.A kind of preparation method of super abrasive static-free glue band, preparation method is specific as follows：
Weigh in proportion in natural resin, phenolic resin, ammonium persulfate, Graphene, polyester fiber, barium sulfate, 1,3- propane sulphurs Ester, 2- chloro-3-pyridyls carboxylic acid, methyl acrylate, EDTA, stir and evenly mix rear microwave treatment, and the power of microwave treatment is 300W, micro- Ripple process time is 20min, and microwave treatment is put into reactor after terminating, and pressure is set to 10MPa, anti-under the catalysis of platinum filament Should, reaction terminates rear extrusion molding and obtains final product.
Comparative example 1
A kind of super abrasive static-free glue band, be according to the primary raw material of weight portion：32 parts of natural resin, 17 parts of phenolic resin, mistake 3 parts of ammonium sulfate, 8 parts of Graphene, 9 parts of polyester fiber, 6 parts of barium sulfate, 5 parts of 2- chloro-3-pyridyls carboxylic acid, 3 parts of methyl acrylate, 2 parts of EDTA.
A kind of preparation method of super abrasive static-free glue band, preparation method is specific as follows：
Natural resin, phenolic resin, ammonium persulfate, Graphene, polyester fiber, barium sulfate, 2- chloro-3-pyridyl carboxylics are weighed in proportion Acid, methyl acrylate, EDTA, stir and evenly mix rear microwave treatment, and the power of microwave treatment is 250W, and microwave treatment time is 15min, microwave treatment is put into reactor after terminating, and pressure is set to 9MPa, is reacted under the catalysis of platinum filament, after reaction terminates Extrusion molding is obtained final product.
Comparative example 2
A kind of super abrasive static-free glue band, be according to the primary raw material of weight portion：32 parts of natural resin, 17 parts of phenolic resin, mistake 3 parts of ammonium sulfate, 8 parts of Graphene, 9 parts of polyester fiber, 6 parts of barium sulfate, 3 parts of methyl acrylate, 2 parts of EDTA.
A kind of preparation method of super abrasive static-free glue band, preparation method is specific as follows：
Weigh in proportion natural resin, phenolic resin, ammonium persulfate, Graphene, polyester fiber, barium sulfate, methyl acrylate, EDTA, stirs and evenly mixs rear microwave treatment, and the power of microwave treatment is 250W, and microwave treatment time is 15min, and microwave treatment terminates After put reactor into, pressure is set to 9MPa, is reacted under the catalysis of platinum filament, reaction terminates rear extrusion molding and obtains final product.
Comparative example 3
A kind of super abrasive static-free glue band, be according to the primary raw material of weight portion：32 parts of natural resin, 17 parts of phenolic resin, mistake 3 parts of ammonium sulfate, 8 parts of Graphene, 9 parts of polyester fiber, 6 parts of barium sulfate, 2 parts of EDTA.
A kind of preparation method of super abrasive static-free glue band, preparation method is specific as follows：
Natural resin, phenolic resin, ammonium persulfate, Graphene, polyester fiber, barium sulfate, EDTA are weighed in proportion, are stirred and evenly mixed Microwave treatment afterwards, the power of microwave treatment is 250W, and microwave treatment time is 15min, and microwave treatment puts reactor into after terminating In, pressure is set to 9MPa, is reacted under the catalysis of platinum filament, and reaction terminates rear extrusion molding and obtains final product.
Test
Embodiment 1, embodiment 2, embodiment 3, embodiment 4, embodiment 5 and comparative example 1, comparative example 2, comparative example 3 are made respectively Standby adhesive tape carries out wearability and antistatic test, and test result is as follows：
Adhesive tape prepared by embodiment 1-5, Akron abrasion volume 0.2cm3/ 1.61km, sheet resistance 2 × 102Ω；
Adhesive tape prepared by comparative example 1-3, Akron abrasion volume 1.1cm3/ 1.61km, the Ω of sheet resistance 95.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be in other specific forms realized.Therefore, no matter From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power Profit requires to be limited rather than described above, it is intended that all in the implication and scope of the equivalency of claim by falling Change is included in the present invention.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each implementation method is only wrapped Containing an independent technical scheme, this narrating mode of specification is only that for clarity, those skilled in the art should Specification an as entirety, the technical scheme in each embodiment can also be formed into those skilled in the art through appropriately combined May be appreciated other embodiment.

Claims (6)

1. a kind of super abrasive static-free glue band, it is characterised in that the primary raw material according to weight portion is：Natural resin 25-37 parts, Phenolic resin 13-20 parts, ammonium persulfate 2-4 parts, Graphene 5-10 parts, polyester fiber 8-10 parts, barium sulfate 4-8 parts, 1,3- third 2-6 parts of alkane sultone, 2-7 parts, methyl acrylate 2-4 parts, EDTA 1-2 parts of 2- chloro-3-pyridyl carboxylic acids.
2. super abrasive static-free glue band according to claim 1, it is characterised in that the raw material according to weight portion is：Naturally Resin 29-33 parts, phenolic resin 15-18 parts, ammonium persulfate 2-4 parts, Graphene 7-9 parts, polyester fiber 8-10 parts, barium sulfate 4- 8 parts, 2-6 parts of 1,3- propane sultones, 2-7 parts, methyl acrylate 2-4 parts, EDTA 1-2 parts of 2- chloro-3-pyridyl carboxylic acids.
3. super abrasive static-free glue band according to claim 1, it is characterised in that the raw material according to weight portion is：Naturally 32 parts of resin, 17 parts of phenolic resin, 3 parts of ammonium persulfate, 8 parts of Graphene, 9 parts of polyester fiber, 6 parts of barium sulfate, 1,3- propane sulphurs 4 parts of lactone, 5 parts of 2- chloro-3-pyridyls carboxylic acid, 3 parts of methyl acrylate, 2 parts of EDTA.
4. a kind of preparation method of super abrasive static-free glue band as described in claim 1-3 is any, it is characterised in that preparation side Method is specific as follows：
Weigh in proportion in natural resin, phenolic resin, ammonium persulfate, Graphene, polyester fiber, barium sulfate, 1,3- propane sulphurs Ester, 2- chloro-3-pyridyls carboxylic acid, methyl acrylate, EDTA, stir and evenly mix rear microwave treatment, and the power of microwave treatment is 200- 300W, microwave treatment time is 10-20min, and microwave treatment is put into reactor after terminating, and pressure is set to 7-10MPa, in platinum Reacted under the catalysis of silk, reaction terminates rear extrusion molding and obtains final product.
5. the preparation method of super abrasive static-free glue band according to claim 4, it is characterised in that the power of microwave treatment It is 250W, microwave treatment time is 15min.
6. the preparation method of super abrasive static-free glue band according to claim 4, it is characterised in that pressure is set to 9MPa。
CN201611094141.XA 2016-12-02 2016-12-02 A kind of super abrasive static-free glue band Withdrawn CN106751942A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107746684A (en) * 2017-11-06 2018-03-02 张永宏 Super abrasive static-free glue band

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102245727A (en) * 2008-12-17 2011-11-16 德莎欧洲公司 Pressure-sensitive adhesives based on natural rubber and polyacrylates
CN102746808A (en) * 2012-07-27 2012-10-24 清华大学深圳研究生院 High-conductivity graphene conducting resin and preparation method thereof
CN105315943A (en) * 2015-11-24 2016-02-10 苏州盖德精细材料有限公司 High-heat-conductivity epoxy resin conducting resin and preparing method thereof
CN106147665A (en) * 2016-07-01 2016-11-23 深圳市烯世传奇科技有限公司 A kind of durability heat-conducting glue based on graphene powder and preparation method thereof
CN106753090A (en) * 2016-12-02 2017-05-31 郑州源冉生物技术有限公司 A kind of wear-resisting static-free glue band

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102245727A (en) * 2008-12-17 2011-11-16 德莎欧洲公司 Pressure-sensitive adhesives based on natural rubber and polyacrylates
CN102746808A (en) * 2012-07-27 2012-10-24 清华大学深圳研究生院 High-conductivity graphene conducting resin and preparation method thereof
CN105315943A (en) * 2015-11-24 2016-02-10 苏州盖德精细材料有限公司 High-heat-conductivity epoxy resin conducting resin and preparing method thereof
CN106147665A (en) * 2016-07-01 2016-11-23 深圳市烯世传奇科技有限公司 A kind of durability heat-conducting glue based on graphene powder and preparation method thereof
CN106753090A (en) * 2016-12-02 2017-05-31 郑州源冉生物技术有限公司 A kind of wear-resisting static-free glue band

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107746684A (en) * 2017-11-06 2018-03-02 张永宏 Super abrasive static-free glue band

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Application publication date: 20170531