CN106730964A - A kind of distilling apparatus for producing high-purity germanium tetrachloride - Google Patents
A kind of distilling apparatus for producing high-purity germanium tetrachloride Download PDFInfo
- Publication number
- CN106730964A CN106730964A CN201510832115.1A CN201510832115A CN106730964A CN 106730964 A CN106730964 A CN 106730964A CN 201510832115 A CN201510832115 A CN 201510832115A CN 106730964 A CN106730964 A CN 106730964A
- Authority
- CN
- China
- Prior art keywords
- alembic
- infrared heating
- escaping pipe
- drainer
- distilling apparatus
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/02—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in boilers or stills
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G17/00—Compounds of germanium
- C01G17/04—Halides of germanium
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention discloses a kind of distilling apparatus for producing high-purity germanium tetrachloride,Including alembic and drainer,The alembic side is provided with charging aperture and the first air inlet,The alembic opposite side is provided with the second air inlet,The top of the alembic is provided with gas outlet,Helical axis is vertically arranged with the alembic inner axes,Multiple infrared heating blocks are provided with the helical axis,The multiple infrared heating block is vertically evenly arranged in the outer wall of the helical axis in the shape of a spiral,The bottom of the alembic is provided with infrared heating set,Temperature detector is provided with the infrared heating set,The top of the alembic is connected by the first escaping pipe and the drainer,Spiral cold-finger is provided with the drainer,The second escaping pipe and the 3rd escaping pipe are provided with the drainer,Second escaping pipe and second air inlet are connected.The distilling apparatus of the high-purity germanium tetrachloride of production that the present invention is provided, firing rate is fast, and temperature control effect is good.
Description
Technical field
The present invention relates to technical field of semiconductors, a kind of distilling apparatus for producing high-purity germanium tetrachloride is particularly related to.
Background technology
At present, when Chemical Manufacture, when running into a large amount of liquid phase separations, it is frequently necessary to use destilling tower to carry out separating-purifying, but the destilling tower for currently using is mostly to provide heat using alcohol or kerosene, coal burning heat release, such combustion heat supplying is very big to fuel consumption, while different raw materials must use different fuel, otherwise being easily destroyed the waste gas discharged after raw material, and fuel combustion can also cause environment pollution.Meanwhile, staff must stare at the temperature of each part of destilling tower the moment, and temperature control is very difficult.Therefore, it is necessary to be improved to existing destilling tower, can not use fuel carries out heat supply, also functions to the effect of environmental protection while energy saving, and with being easy to the function of temperature control.
The content of the invention
The invention aims to solve the problems, such as to be previously mentioned in above-mentioned background technology, there is provided a kind of firing rate is fast, the distilling apparatus of the good high-purity germanium tetrachloride of production of temperature control effect.
To achieve these goals, technical scheme is as follows：
A kind of distilling apparatus for producing high-purity germanium tetrachloride,Including alembic and drainer,The alembic side is provided with charging aperture and the first air inlet,The alembic opposite side is provided with the second air inlet,The top of the alembic is provided with gas outlet,Helical axis is vertically arranged with the alembic inner axes,Multiple infrared heating blocks are provided with the helical axis,The multiple infrared heating block is vertically evenly arranged in the outer wall of the helical axis in the shape of a spiral,The bottom of the alembic is provided with infrared heating set,Temperature detector is provided with the infrared heating set,The bottom of the alembic is provided with waste liquid port,The top of the alembic is connected by the first escaping pipe and the drainer,Spiral cold-finger is provided with the drainer,The second escaping pipe and the 3rd escaping pipe are provided with the drainer,Second escaping pipe and second air inlet are connected.
Preferably, the infrared heating block is to expose three pyrometric cones in face.
Preferably, the helical axis is fixedly connected with alembic top.
Preferably, being provided with upper end immediately below the alembic has the waste liquid box of opening, and drawer type waste liquid chamber is provided with the waste liquid box.
Preferably, the first solenoid electric valve is provided with first escaping pipe, the second solenoid electric valve is provided with second escaping pipe, the waste liquid box side wall is provided with the controller for controlling first solenoid electric valve and second solenoid electric valve.
Compared with prior art, the distilling apparatus of the high-purity germanium tetrachloride of production that the present invention is provided, firing rate is fast, and temperature control effect is good.
Brief description of the drawings
Technical scheme in order to illustrate more clearly the embodiments of the present invention, the accompanying drawing to be used needed for being described to embodiment below is briefly described, apparently, drawings in the following description are only some embodiments of the present invention, for those of ordinary skill in the art, without having to pay creative labor, other accompanying drawings can also be obtained according to these accompanying drawings.
Fig. 1 is the structural representation in the present embodiment.
1st, alembic, 2, charging aperture, the 3, first air inlet, 4th, temperature detector, the 5, first escaping pipe, the 6, first solenoid electric valve, 7th, drainer, 8, infrared heating block, the 9, second solenoid electric valve, 10th, the 3rd escaping pipe, the 11, second escaping pipe, 12, infrared heating set, 13rd, waste liquid box, 14, waste liquid port, 15, controller, 16th, the second air inlet, 17, helical axis.
Specific embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment is only a part of embodiment of the invention, rather than whole embodiments.Based on the embodiment in the present invention, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made belongs to the scope of protection of the invention.
Specific embodiment：
A kind of distilling apparatus for producing high-purity germanium tetrachloride with reference to shown in Fig. 1,Including alembic 1 and drainer 7,The side of alembic 1 is provided with the air inlet 3 of charging aperture 2 and first,The opposite side of alembic 1 is provided with the second air inlet 16,The top of alembic 1 is provided with gas outlet,Helical axis 17 is vertically arranged with the inner axes of alembic 1,Multiple infrared heating blocks 8 are provided with helical axis 17,Multiple infrared heating blocks 8 are vertically evenly arranged in the outer wall of helical axis 17 in the shape of a spiral,The bottom of alembic 1 is provided with infrared heating set 12,Temperature detector 4 is provided with infrared heating set 12,The bottom of alembic 1 is provided with waste liquid port 14,The top of alembic 1 is connected by the first escaping pipe 5 and drainer 7,Spiral cold-finger is provided with drainer 7,The second escaping pipe 11 and the 3rd escaping pipe 10 are provided with drainer 7,Second escaping pipe 11 and the second air inlet 16 are connected.
In the present embodiment, infrared heating block 8 is to expose three pyrometric cones in face.
In the present embodiment, helical axis 17 is fixedly connected with the top of alembic 1.
In the present embodiment, upper end is provided with immediately below alembic 1 has the waste liquid box 13 of opening, and waste liquid box 13 is interior to be provided with drawer type waste liquid chamber, and the waste liquid of discharge enters waste liquid box 13 from waste liquid port 14, through being extracted out by drawer type waste liquid chamber after a period of time, then it is collected.
In the present embodiment, the first solenoid electric valve 6 is provided with the first escaping pipe 5, the second solenoid electric valve 9 is provided with the second escaping pipe 11, the side wall of waste liquid box 13 is provided with the controller 15 of the first solenoid electric valve 6 of control and the second solenoid electric valve 9.
The course of work of the present embodiment：When distillation work is carried out using this equipment,The temperature on infrared heating set 12 and infrared heating block 8 is set on temperature detector 4,Then raw material is entered into alembic 1 from charging aperture 2,Start distillation work,After distillation work terminates,Product after distillation from gas outlet out,Enter drainer 7 by the first escaping pipe 5,By after spiral cold-finger condensation,Qualified product discharge,Underproof product enters continuation in alembic 1 and distills by the second escaping pipe 11,Until meeting the requirements,Temperature in the real-time detection alembic 1 of temperature detector 4,And the temperature to infrared heating set 12 and infrared heating block 8 is controlled,And outgassing rate is controlled by the first solenoid electric valve 6 and the second solenoid electric valve 9,Grasp whole still-process,Last closing control device 15,Infrared heating covers 12 and infrared heating block 8,Terminate still-process.
Presently preferred embodiments of the present invention is the foregoing is only, is not intended to limit the invention, all any modification, equivalents made within the scope of the present invention etc. should be included within the scope of the present invention.
Claims (5)
1. a kind of distilling apparatus for producing high-purity germanium tetrachloride,It is characterized in that,Including alembic and drainer,The alembic side is provided with charging aperture and the first air inlet,The alembic opposite side is provided with the second air inlet,The top of the alembic is provided with gas outlet,Helical axis is vertically arranged with the alembic inner axes,Multiple infrared heating blocks are provided with the helical axis,The multiple infrared heating block is vertically evenly arranged in the outer wall of the helical axis in the shape of a spiral,The bottom of the alembic is provided with infrared heating set,Temperature detector is provided with the infrared heating set,The bottom of the alembic is provided with waste liquid port,The top of the alembic is connected by the first escaping pipe and the drainer,Spiral cold-finger is provided with the drainer,The second escaping pipe and the 3rd escaping pipe are provided with the drainer,Second escaping pipe and second air inlet are connected.
2. a kind of distilling apparatus for producing high-purity germanium tetrachloride according to claim 1, it is characterised in that：The infrared heating block is to expose three pyrometric cones in face.
3. a kind of distilling apparatus for producing high-purity germanium tetrachloride according to claim 1, it is characterised in that：The helical axis is fixedly connected with alembic top.
4. a kind of distilling apparatus for producing high-purity germanium tetrachloride according to claim 1, it is characterised in that：Being provided with upper end immediately below the alembic has the waste liquid box of opening, and drawer type waste liquid chamber is provided with the waste liquid box.
5. a kind of distilling apparatus for producing high-purity germanium tetrachloride according to claim 4, it is characterised in that：The first solenoid electric valve is provided with first escaping pipe, the second solenoid electric valve is provided with second escaping pipe, the waste liquid box side wall is provided with the controller for controlling first solenoid electric valve and second solenoid electric valve.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510832115.1A CN106730964A (en) | 2015-11-25 | 2015-11-25 | A kind of distilling apparatus for producing high-purity germanium tetrachloride |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510832115.1A CN106730964A (en) | 2015-11-25 | 2015-11-25 | A kind of distilling apparatus for producing high-purity germanium tetrachloride |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106730964A true CN106730964A (en) | 2017-05-31 |
Family
ID=58964835
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510832115.1A Pending CN106730964A (en) | 2015-11-25 | 2015-11-25 | A kind of distilling apparatus for producing high-purity germanium tetrachloride |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106730964A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107326199A (en) * | 2017-05-25 | 2017-11-07 | 广东省稀有金属研究所 | The continuous producing method of impurity zinc-mercury in a kind of removing gallium |
| CN107320990A (en) * | 2017-07-24 | 2017-11-07 | 江苏新化化工有限公司 | Negative pressure continuous rectification apparatus |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU1575379A1 (en) * | 1988-05-24 | 1992-04-30 | Институт химии АН СССР | Method of dispensing high-purity substances |
| WO2003059808A1 (en) * | 2001-11-15 | 2003-07-24 | Draka Fibre Technology B.V. | Method of preparing very pure silicon chloride and/or germanium chloride |
| CN1842491A (en) * | 2004-08-04 | 2006-10-04 | 德古萨公司 | Method and device for purifying silicon tetrachloride or germanium tetrachloride containing hydride |
| CN101269836A (en) * | 2008-05-07 | 2008-09-24 | 云南驰宏锌锗股份有限公司 | Rectification column for removing hydrogen containing foreign matter in germanic chloride |
| CN201208516Y (en) * | 2008-05-07 | 2009-03-18 | 云南驰宏锌锗股份有限公司 | Fractionating tower capable of removing hydrogen-containing purity in germanic chloride |
| CN102328951A (en) * | 2011-07-13 | 2012-01-25 | 云南驰宏锌锗股份有限公司 | Method and device for removing hydrogen-containing impurities from germanium tetrachloride |
| CN102976395A (en) * | 2012-11-19 | 2013-03-20 | 云南驰宏锌锗股份有限公司 | Production system of germanium tetrachloride for optical fiber |
| CN103183375A (en) * | 2011-12-29 | 2013-07-03 | 北京有色金属研究总院 | Preparation purification method of germanium tetrachloride for optical fiber |
| CN103657127A (en) * | 2012-09-13 | 2014-03-26 | 天津市港马防水材料工程有限公司 | Infrared heating distillation tower |
-
2015
- 2015-11-25 CN CN201510832115.1A patent/CN106730964A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU1575379A1 (en) * | 1988-05-24 | 1992-04-30 | Институт химии АН СССР | Method of dispensing high-purity substances |
| WO2003059808A1 (en) * | 2001-11-15 | 2003-07-24 | Draka Fibre Technology B.V. | Method of preparing very pure silicon chloride and/or germanium chloride |
| CN1842491A (en) * | 2004-08-04 | 2006-10-04 | 德古萨公司 | Method and device for purifying silicon tetrachloride or germanium tetrachloride containing hydride |
| CN101269836A (en) * | 2008-05-07 | 2008-09-24 | 云南驰宏锌锗股份有限公司 | Rectification column for removing hydrogen containing foreign matter in germanic chloride |
| CN201208516Y (en) * | 2008-05-07 | 2009-03-18 | 云南驰宏锌锗股份有限公司 | Fractionating tower capable of removing hydrogen-containing purity in germanic chloride |
| CN102328951A (en) * | 2011-07-13 | 2012-01-25 | 云南驰宏锌锗股份有限公司 | Method and device for removing hydrogen-containing impurities from germanium tetrachloride |
| CN103183375A (en) * | 2011-12-29 | 2013-07-03 | 北京有色金属研究总院 | Preparation purification method of germanium tetrachloride for optical fiber |
| CN103657127A (en) * | 2012-09-13 | 2014-03-26 | 天津市港马防水材料工程有限公司 | Infrared heating distillation tower |
| CN102976395A (en) * | 2012-11-19 | 2013-03-20 | 云南驰宏锌锗股份有限公司 | Production system of germanium tetrachloride for optical fiber |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107326199A (en) * | 2017-05-25 | 2017-11-07 | 广东省稀有金属研究所 | The continuous producing method of impurity zinc-mercury in a kind of removing gallium |
| CN107320990A (en) * | 2017-07-24 | 2017-11-07 | 江苏新化化工有限公司 | Negative pressure continuous rectification apparatus |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105132028A (en) | Crop straw continuous segmented pyrolysis circulation system | |
| CN106730964A (en) | A kind of distilling apparatus for producing high-purity germanium tetrachloride | |
| CN103469160B (en) | Far-infrared ray power heat-generating pipe production equipment special | |
| CN102964884B (en) | Hot cracking method process for preparing carbon black by using co-production of tail gas | |
| CN107446609A (en) | A kind of continous way plastic garbage thermal cracking refining equipment of efficient energy-saving | |
| CN205222977U (en) | Sludge drying tower | |
| CN104386686A (en) | Activated carbon production facility | |
| CN206385088U (en) | A kind of lock gas row's charcoal cooling device of reduction and gaseous charcoal technique processed | |
| CN205099379U (en) | Energy -conserving oxidation furnace of red lead | |
| CN104628004A (en) | Preparation tank, preparation furnace kiln and preparation method of silicon-based negative electrode material for batteries | |
| CN204079885U (en) | Low Water Consumption Coke Quenching case and the coke quenching device based on this quenching case | |
| CN103469159A (en) | Special production equipment for far infrared energy heating panel | |
| CN102865741B (en) | Metal magnesium and calcium reduction furnace thermal storage combustion system and control method thereof | |
| CN204324901U (en) | Active carbon production equipment | |
| CN207991243U (en) | A kind of all-oxygen combustion melting furnace of rock wool production | |
| CN207313527U (en) | A kind of automatic reallocation, automatic heating, automatic cooling and automatic negative-pressure gas gathering system | |
| CN204080052U (en) | A kind of waste aluminum retrieving arrangement | |
| CN104266511B (en) | A kind of durable flue gas waste heat recovery apparatus | |
| CN208260236U (en) | A kind of extractor | |
| CN203540108U (en) | Device for recycling light components by using flash tank | |
| CN220951200U (en) | Temperature control device for low-temperature chlorination and low-temperature chlorination system | |
| CN108240625A (en) | A kind of fixed-end forces pyrolysis installation | |
| CN204412233U (en) | 16 quartz plate photolysis devices | |
| CN204717696U (en) | A kind of intelligent destroyer | |
| CN202145088U (en) | Caprolactam automatic temperature control melting furnace |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170531 |
|
| RJ01 | Rejection of invention patent application after publication |