CN106727742A - A kind of charred CACUMEN PLATYCLADI produces processing procedure - Google Patents
A kind of charred CACUMEN PLATYCLADI produces processing procedure Download PDFInfo
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- A61K36/13—Coniferophyta (gymnosperms)
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Abstract
The present invention relates to technical field of traditional Chinese medicine pharmacy, a kind of charred CACUMEN PLATYCLADI production processing procedure is specifically disclosed, including：1. receive and adopt fresh arbor-vitae branch and leaf；2. cutting；3. charcoal is fried；4. screen；The present invention is using moderate heat middling speed frying after fresh arbor-vitae leaf segment, the charred CACUMEN PLATYCLADI medicine materical crude slice manufactured after the processing procedure for weeding out its powder and old branch is above other concocting methods on crucial Testing index of the appearance character with setting, has been really achieved the purpose of stir-baked the crude drugs into black on outside and brown in inside in traditional Chinese medicine theory.Charred CACUMEN PLATYCLADI production processing procedure of the invention is applied to modern and following prepared slices of Chinese crude drugs enterprise charred CACUMEN PLATYCLADI production processing procedure production overall process, and be conducive to before national future portion herbal species that the development of circle is formulated with production technology after factory, reduce crude drug middle flow link, ensure drug quality, shorten the production cycle, human input is reduced, production cost is reduced.
Description
Technical field
The present invention relates to technical field of traditional Chinese medicine pharmacy, and in particular to a kind of charred CACUMEN PLATYCLADI produces processing procedure.
Background technology
Charred CACUMEN PLATYCLADI is the common drug of tcm clinical practice controlling of bleeding with astringents, is cupressaceae plant arbor-vitae
Dry branch and the Ye Jing of Platycladusorientalis (L.) Franco are processed and formed.Cacumen biotae begins to be loaded into history medicine
Books are Han dynastys《Sheng Nong's herbal classic》, concocting method comes across the Northern and Southern Dynasties earliest《Thunder God processes opinion》In " sealwort system ", to Tang
In generation, has increased net system, cutting, steaming method, roasting method etc. newly, the Song dynasty increased newly micro- stir-fry, it is micro- process, Jin and Yuan dynasty increased newly cooking method, stir-bake to yellowish,
Ashing method etc., the Ming Dynasty has increased salt solution stir-fry newly, has fried black etc., and the Qing Dynasty has increased withered etc. the concocting method of vinegar system, stir-bake to brown newly, in modern age industry
During professional is to the research of charred CACUMEN PLATYCLADI, occur in that drying method with the method for forging again.Chinese Pharmacopoeia version in 2015 one and place process rule
The concocting method of the cacumen biotae that model is recorded is selected on the basis of ancient method processing is inherited, and mainly records Biotae orientalise
With two kinds of methods of charred CACUMEN PLATYCLADI, in the control of its prepared slice quality, cacumen biotae predominantly detects moisture, total ash, acid-insoluble ash, leaching
Go out thing, assay, charred CACUMEN PLATYCLADI is predominantly detected：Extract.
At present,《Chinese Pharmacopoeia》The traditional charred CACUMEN PLATYCLADI big gun recorded in version in 2015 and local latest edition concocted specification
Technique processed is limited, simple described in its processing procedure content word, processes operation without clear and definite technical parameter, quality assurance
Detection it is single.Therefore, charred CACUMEN PLATYCLADI technical data in actual production process quotes difficult, does not have to kind quantity-produced quality
It is secure.The charred CACUMEN PLATYCLADI production cycle is long, and concocted quality is unstable, product heterogeneity, and human input is big, and production cost is high, product
Can neither inheriting tradition well concocting method, do not catch up with current Good growth requirement yet, add each Manufacture of medicinal slices of TCM enterprise
Industry processes professional and occurs in that serious fault-layer-phenomenon, causes the charred CACUMEN PLATYCLADI quality of each Manufacture of medicinal slices of TCM enterprise production at present
The requirement of pharmacopeia detection, traditional stir-baked the crude drugs into black on outside and brown in inside and " homogeneity of the continuous quality of production of product " specified in GMP is extremely difficult to,
It is unfavorable for Dispensing on tcm clinical practice, it is not good using drug effect.
The content of the invention
In view of this, it is necessary to for above-mentioned problem, provide a kind of new in inheriting tradition charred CACUMEN PLATYCLADI concocting method
Charred CACUMEN PLATYCLADI produces processing procedure.
The present invention helps to solve the problems such as charred CACUMEN PLATYCLADI production cycle is long, and quality is unstable, product cost is high, and can be convenient
Production operation personnel quickly grasp the concocting method of cacumen biotae charcoal in Manufacture of medicinal slices of TCM enterprise.
To achieve the above object, the present invention takes following technical scheme：
Charred CACUMEN PLATYCLADI of the invention produces processing procedure, comprises the following steps：
Step 1) raw material receive adopt：Fresh branch and leaf are harvested, debris are removed, deposited standby；
Step 2) cutting：Take step 1) obtained by fresh raw material, fresh raw material is placed on medicine cutter and is cut into 0.8-1.2cm's
Section long, deposits standby；
Step 3) fry charcoal：Take step 2) obtained by fresh-cut section raw material, it is 355-365 DEG C to set machine for stir-frying Chinese medicine instrument temperature, if
Instrument rotating speed is 30 ± 2rpm, when instrument temperature is raised to 328-332 DEG C, the segment raw material is put into pot, fries 28-33 points
Clock, to medicinal material surface dark brown, during internal coke yellow, sprinkling drinking water is a little, extinguishes Mars, takes out, and airing overnight, obtains final product side
Cypress charcoal；
Step 4) screening：By step 3) obtained by charred CACUMEN PLATYCLADI, screened in input upper sieve, remove powder and branch bar,
Obtain final product net charred CACUMEN PLATYCLADI.
Further, step 1) harvesting fresh branch and Ye Weixia, season in autumn two harvesting fresh arbor-vitae branch and leaf.
Further, step 2) the fresh raw material staple fiber ppd be 1cm.
Further, step 3) the machine for stir-frying Chinese medicine instrument temperature is set to 360 DEG C, and instrument rotating speed is 30rpm.
Further, step 3) instrument temperature when being raised to 330 DEG C, will fry 30 minutes in fresh cacumen biotae section input pot.
Further, step 4) in, arbor-vitae carbon is screened using ZSX types spin vibration sieve, lower screen is 18 mesh, and upper strata is
10 mesh are sieved, the mesh sieve of lower floor 18 removes powder, and the mesh sieve of upper strata 10 removes debranching bar.
Beneficial effects of the present invention are：
Charred CACUMEN PLATYCLADI of the invention produces processing procedure, the processing procedure of inheriting tradition in whole production process, using existing
For production equipment, set feasible technological parameter and production operation flow, to quality control Chinese Pharmacopoeia examination criteria
On increased detection, it is ensured that the stability and controllability of quality in process of producing product.The present invention can be suitably used for it is modern with
Following prepared slices of Chinese crude drugs enterprise charred CACUMEN PLATYCLADI production processing procedure production overall process, and be conducive to national future traditional Chinese medicine enterprise production technology
Formulate, reduce crude drug middle flow link, it is ensured that drug quality, shorten the production cycle, reduce human input, reduction is produced into
This.
Specific embodiment
To make the object, technical solutions and advantages of the present invention clearer, below in conjunction with the embodiment of the present invention, to this hair
Bright technical scheme is made further clearly and completely to describe.It should be noted that described embodiment is only the present invention one
Section Example, rather than whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art are not doing
Go out the every other embodiment obtained under the premise of creative work, belong to the scope of protection of the invention.
Embodiment 1
The charred CACUMEN PLATYCLADI production processing procedure of the present embodiment includes：
Step 1) raw material receive adopt：Summer, season in autumn two harvest fresh branch and leaf, remove debris, and bamboo basket storage is standby；
It is of the invention that fresh branch is directly harvested from arbor vitae with leaf as raw materials for production, matter when being conducive to being processed further
Amount guarantee, saves the drying of arbor-vitae crude drug and the time of middle flow and expense, while also directly controlling raw material dry
Contaminated possibility in the dry and process of circulation, and reduce product cost, it is ensured that product quality.
Step 2) cutting：Take the fresh raw material obtained by step (1), if OY-300 types at a high speed block reciprocating medicine cutter knife away from for
1cm, fresh raw material is placed on medicine cutter the section for being cut into 1cm, is deposited standby；
The present invention directly carries out segment to fresh raw material, is conducive to that fresh raw material can be increased in pot during next step stir-fry charcoal
The contact frequency of mobility and pot inwall, reach pot inwall uniformly carries out heat transfer to fresh cacumen biotae, and realizes processing design
Purpose.
Step 3) fry charcoal：The fresh-cut section raw material obtained by step (2) is taken, if XCYQ-75 type automatic control high-temperature fuel gas machine for stir-frying Chinese medicine instrument
Table temperature is 360 DEG C, if instrument rotating speed is 30rpm, when instrument temperature is raised to 330 DEG C, by the fresh arbor-vitae raw material section inputs of 15kg
In pot, fry about 30 minutes, to medicinal material surface dark brown, during internal coke yellow, sprinkling drinking water is a little, extinguishes Mars, takes out, stand
Dry in the air overnight, obtain final product charred CACUMEN PLATYCLADI.
With modern machinery and equipment be combined traditional charred CACUMEN PLATYCLADI processing procedure by the present invention, can be quickly right during charcoal is fried
Processed product is uniformly stir-fried, and can accurately control the processing temperature and time of design, it is ensured that continuous production product can reach
The mass uniformity of GMP requirements.
The present invention is processed using fresh arbor-vitae branch and leaf as raw material, moderate heat is processed.Its main cause is, fresh arbor-vitae branch
Moisture and volatile oil higher is contained within leaf, heat conduction velocity can be reduced during moderate heat fries charcoal, cacumen biotae can be protected again
Internal new beneficiating ingredient is heated and is converted into, and can the original composition of member-retaining portion.The finished product charcoal end of frying in production is few, finished product
Extracting rate is high, while can reach the purpose of traditional stir-baked the crude drugs into black on outside and brown in inside again.
Step 4) screening：Take step 3) obtained by charred CACUMEN PLATYCLADI, if ZSX type spin vibration sieves lower screen be 18 mesh, upper strata for sieve 10
Mesh, charred CACUMEN PLATYCLADI is put into upper sieve and is screened, and removes 18 mesh sieve low-grades powder and 10 mesh sieve top grade old branch, it is ensured that product matter
Amount, obtains final product net charred CACUMEN PLATYCLADI.
The present invention sieves to charred CACUMEN PLATYCLADI, removes powder and old branch, its purpose is to preferably ensure charred CACUMEN PLATYCLADI
Quality.
Comparative example 1
《Chinese Pharmacopoeia》One modern comfort of version in 2015 fries charred CACUMEN PLATYCLADI production processing procedure, comprises the following steps：
Step 1) cacumen biotae：Take (dry) cacumen biotae and remove hard stalk and debris, deposit standby.
Step 2) fry charcoal：Take step 1) obtained by cacumen biotae, if XCYQ-75 type automatic control high-temperature fuel gas machine for stir-frying Chinese medicine instrument temperatures
It is 480 DEG C, if instrument rotating speed is 30rpm, when instrument temperature is raised to 450 DEG C, takes in fresh cacumen biotae section 10kg input pots, fries about
8 minutes, during to medicinal material surface coke black, internal Jiao's brown or to specified degree, spray clear water was a little, extinguishes Mars, takes out, and dries in the air
It is dry.Obtain final product charred CACUMEN PLATYCLADI.
Comparative example 2
《Chinese Pharmacopoeia》One traditional-handwork of version in 2015 fries charred CACUMEN PLATYCLADI production processing procedure, comprises the following steps：
Step 1) cacumen biotae：Take (dry) cacumen biotae and remove hard stalk and debris, deposit standby.
Step 2) fry charcoal：Take step 1) obtained by cacumen biotae 1Kg put in hot pot, fry with high heat to surface coke black, inside
Burnt brown, spray clear water is a little, extinguishes Mars, takes out, and dries.Obtain final product charred CACUMEN PLATYCLADI.
Comparative example 3
This comparative example is differed only in embodiment 1, uses dry side CedarLeaves to carry out processing charred CACUMEN PLATYCLADI for raw material, remaining behaviour
Make process and state modulator is same as Example 1.
1. it was verified that substantial amounts of powder can be produced during using dry side CedarLeaves cutting, and the waste of raw material is increased.If
Do not cut, crude drug poor fluidity, it is impossible to contacted well with pot and can directly influence concocted quality.
2. it was verified that pressing the technological parameter of comparative example 3 and operating method, dry side CedarLeaves are used for raw material is processed, into
In product carbonize product substantially increase with the amount of ashes product, finished color Cheng Jiao color to black, finished product extracting rate bottom, ashes after sieving
Many, the appearance character difference with pharmacopoeial requirements is obvious.
Comparative example 4
This comparative example is differed only in embodiment 1, and it is raw material to use complete fresh cacumen biotae, does not carry out segment, its
Remaining operating process and state modulator are same as Example 1.
Facts have proved：The not segment of fresh cacumen biotae carries out stir-fry charcoal, and because raw material is long, poor fluidity contacts pot in frying
Again less than stirring well, raw material can not be contacted uniformly body portion with pot, and the partial material contacted with pot when long
It is most of to carbonize, then into ashes, pot is not contacted partially due to temperature not enough, can only become yellow green to yellowish-brown.Cross
Finished product extracting rate is low after sieve, and proterties difficulty reaches pharmacopoeial requirements.
Comparative example 5
This comparative example is differed only in embodiment 1, and the step 2 employed in comparative example 1 carries out charcoal stir-fry, to substitute reality
The stir-fry of the charcoal in example 1 step is applied to be processed.
Facts have proved：If frying, charcoal temperature is high, the time is too short, and the raw material of part contact pot can fast charring, major part
Raw material has little time to stir, and is heated irregular, between the finished product proterties brownish black and lark produced, section brown color and primary colors
Between, it is big with pharmacopeia character description gap.
The various embodiments of the present invention processing procedure finished product detection data of table one
Explanation：Because fresh goods raw material is inconvenient to be detected, so without fresh goods raw material detection data.Fresh raw material feed intake into
Product yield is the finished product extracting rate after being converted by dry raw material.
Table 2 2015 editions《Chinese Pharmacopoeia》Detection data
Data in table one, are comprehensive finished product detection average data, finished product extracting rate and the aesthetic appearance of each embodiment stir-fry five batches
Shape.Wherein selected raw material：Embodiment 1, comparative example 5 are fresh arbor-vitae cutting product raw material, and comparative example 4 is complete fresh cacumen biotae
It is raw material, comparative example 1, comparative example 2, comparative example 3 are dry side CedarLeaves raw material.It uses concocting method：Embodiment 1 is of the invention
Concocting method, uses modern comfort moderate heat frying on traditional Process ba- sis.Comparative example 1 is with comparative example 2 as described by pharmacopeia
Operated, wherein the concocting method of comparative example 1 is equipment intense fire frying, the concocting method of comparative example 2 is the craft frying of iron pan intense fire.
Comparative example 3 uses dry side CedarLeaves to carry out processing charred CACUMEN PLATYCLADI for raw material on the basis of embodiment 1.Comparative example 4 is using complete fresh
Cacumen biotae is raw material, does not carry out segment, and remaining operating process and state modulator are same as Example 1.It is right that comparative example 5 is employed
Step 2 in ratio 1 carries out charcoal stir-fry, and frying step with the charcoal in alternate embodiment 1 is processed.
To sum up, charred CACUMEN PLATYCLADI fry charcoal during because raw material, technological parameter it is different from equipment, the detection data of each finished product, into
Product extracting rate is also differed with appearance character.Press《Chinese Pharmacopoeia》Detection requirement of 2015 editions cacumen biotaes with charred CACUMEN PLATYCLADI and finished product proterties
It is required that, the final product quality to each embodiment is contrasted, and the comprehensive quality index that charred CACUMEN PLATYCLADI of the invention processes finished product is optimal, reaches
The requirement of " stir-baked the crude drugs into black on outside and brown in inside " described in successive dynasties traditional Chinese medicine books.
Charred CACUMEN PLATYCLADI of the invention produces processing procedure, and Historic Evolution exploration, name among the people doctor's big gun are carried out charcoal is fried to cacumen biotae
Method processed is investigated and modern Chinese herbal medicine is processed in the research of equipment, in order to ensure the technique of traditional charred CACUMEN PLATYCLADI, makes full use of the modern times
Scientific equipment, the principle of comprehensive improve product quality, our company researcher according to cacumen biotae fry charcoal during, by water, temperature,
Physics and chemical change produced by the influence of operating method and frying time, have invented " charred CACUMEN PLATYCLADI production processing procedure ", and build
Reliable variety production technological process is stood with manufacturing parameter to control each production link, the comprehensive quality of product has been carried
Definite guarantee is risen to.
Traditional Chinese medicine frying charcoal, it is important to " stir-baked the crude drugs into black on outside and brown in inside ", during actual charred CACUMEN PLATYCLADI frying, to " frying charcoal to deposit in successive dynasties bookcase
Property " quality hold the more definite standard of neither one, being operating personnel scene judges, its continuous production processes product matter
The homogeneity of amount is difficult control, and finished product difference is big, is unfavorable for that tcm clinical practice is adjusted.Our company researcher is in recent two decades offside
The clinical verification tracking of cypress charcoal drug effect, sums up with extract, content and finished product proterties to judge finished product standard, quality requirement
For：Extract should preserve the 70-80% of raw material detection limit, and content should preserve the 20-30% of raw material detection limit, and appearance character meets
Pharmacopeia is described." the charred CACUMEN PLATYCLADI production processing procedure " that our company is invented uses fresh goods Raw material processing, there is reliable production technology
Flow and manufacturing parameter, the homogeneity of product quality, processes for common Chinese and operates in can guarantee that production in continuous production
Personnel also can quickly grasp this technology.
Embodiment described above only expresses several embodiments of the invention, and its description is more specific and detailed, but simultaneously
Therefore the limitation to the scope of the claims of the present invention can not be interpreted as.It should be pointed out that for one of ordinary skill in the art
For, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to guarantor of the invention
Shield scope.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.
Claims (6)
1. a kind of charred CACUMEN PLATYCLADI produces processing procedure, it is characterised in that comprise the following steps：
Step 1) raw material receive adopt：Fresh branch and leaf are harvested, debris are removed, deposited standby；
Step 2) cutting：Take step 1) obtained by fresh raw material, fresh raw material is placed on medicine cutter the length for being cut into 0.8-1.2cm
Section, deposits standby；
Step 3) fry charcoal：Take step 2) obtained by fresh-cut section raw material, it is 355-365 DEG C to set machine for stir-frying Chinese medicine instrument temperature, if instrument
Rotating speed is 30 ± 2rpm, when instrument temperature is raised to 328-332 DEG C, the segment raw material is put into pot, stir-fry 28-33 minutes, extremely
Medicinal material surface dark brown, during internal coke yellow, sprinkling drinking water is a little, extinguishes Mars, takes out, and airing overnight, obtains final product charred CACUMEN PLATYCLADI；
Step 4) screening：By step 3) obtained by charred CACUMEN PLATYCLADI, screened in input upper sieve, remove powder and branch bar, obtain final product
Net charred CACUMEN PLATYCLADI.
2. charred CACUMEN PLATYCLADI according to claim 1 production processing procedure, it is characterised in that step 1) harvesting fresh branch
The fresh arbor-vitae branch and leaf harvested with Ye Weixia, season in autumn two.
3. charred CACUMEN PLATYCLADI according to claim 1 production processing procedure, it is characterised in that step 2) the fresh raw material segment is long
It is 1cm to spend.
4. charred CACUMEN PLATYCLADI according to claim 1 produces processing procedure, it is characterised in that step 3) the machine for stir-frying Chinese medicine instrument temperature
Degree is set to 360 DEG C, and instrument rotating speed is 30rpm.
5. charred CACUMEN PLATYCLADI according to claim 1 production processing procedure, it is characterised in that step 3) instrument temperature is raised to
At 330 DEG C, will be fried 30 minutes in fresh cacumen biotae section input pot.
6. charred CACUMEN PLATYCLADI according to claim 1 produces processing procedure, it is characterised in that step 4) in, shaken using the rotation of ZSX types
Sieve is screened to charred CACUMEN PLATYCLADI, and lower screen is 18 mesh, and upper strata is 10 mesh of sieve, and the mesh sieve of lower floor 18 removes powder, and the mesh sieve of upper strata 10 is removed
Go old branch.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116327865A (en) * | 2022-11-23 | 2023-06-27 | 荃豆数字科技有限公司 | Novel method for preparing charcoal from palm charcoal in traditional Chinese medicine decoction piece |
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| CN101926854A (en) * | 2010-04-15 | 2010-12-29 | 苏州卫生职业技术学院 | Method for processing charred lotus leaves |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101926854A (en) * | 2010-04-15 | 2010-12-29 | 苏州卫生职业技术学院 | Method for processing charred lotus leaves |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116327865A (en) * | 2022-11-23 | 2023-06-27 | 荃豆数字科技有限公司 | Novel method for preparing charcoal from palm charcoal in traditional Chinese medicine decoction piece |
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