CN106727256A - A kind of preparation method of the non-stimulated suncream of natural plants composite essential oil - Google Patents

A kind of preparation method of the non-stimulated suncream of natural plants composite essential oil Download PDF

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CN106727256A
CN106727256A CN201710128232.9A CN201710128232A CN106727256A CN 106727256 A CN106727256 A CN 106727256A CN 201710128232 A CN201710128232 A CN 201710128232A CN 106727256 A CN106727256 A CN 106727256A
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essential oil
suncream
stimulated
natural plants
propolis
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李慧芝
宋桂兰
韩斌
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University of Jinan
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4973Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
    • A61K8/498Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86Polyethers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • A61K8/988Honey; Royal jelly, Propolis
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/04Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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  • Health & Medical Sciences (AREA)
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  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
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  • Oil, Petroleum & Natural Gas (AREA)
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  • Cosmetics (AREA)

Abstract

The invention discloses a kind of preparation method of the non-stimulated suncream of natural plants composite essential oil, characterized in that, with use root of Dahurain angelica essential oil, sweet yellow grass ketone, fennel essential oil, ginger essential oil, honeysuckle essential oil, propolis saturated solution prepare composite essential oil be main optical absorbing agent;Then in the reactor, added by mass percentage concentration, xanthans:0.1 ~ 0.2%, deionized water:20 ~ 25%, after dissolving, add composite essential oil:35 ~ 40%, octadecyl alcolol:8 ~ 12%, fibroin albumen:2 ~ 6%, vaseline:The emulsifying agent of 2 ~ 4%, EM 90:20 ~ 28%, absolutely, to stir and evenly mix, it is 7.0 or so to add triethanolamine regulation pH to each component sum, temperature at 50 ± 3 DEG C, lumped together by high-speed stirred, then temperature is risen into 78 ± 2 DEG C, constant temperature 6 hours, it is cooled to room temperature, places one week, obtains the non-stimulated suncream of natural plants composite essential oil.The suncream distributes nature fragrance, and with antibacterial, moisturizing, whitening, anti-sunlight function, non-stimulated to human body, easy to use, sun-proof result is averagely more than 90%.

Description

A kind of preparation method of the non-stimulated suncream of natural plants composite essential oil
Technical field
The present invention relates to cosmetic technical field, and in particular to a kind of system of the non-stimulated suncream of natural plants composite essential oil Preparation Method, has good sun-proof, moisturizing effect to skin.
Background technology
As the increasingly serious ozone layer of environmental pollution is also gradually thinning, the ultraviolet for reaching ground is continuously increased, and this is Cause the extensive concern of people.If in the case of any safeguard procedures, skin is by prolonged solar radiation, surface There is redness, cusalgia, bubble, flexibility decrease, wrinkle occur, aging, severe patient can also be suppressed immune system, cause certainly Body immunity disease such as lupus erythematosus disease, idiopathic photodermatosis such as polymorphous light eruption or urticaria solaris, or even Cause cutaneum carcinoma.Although ultraviolet has so harm to skin, like that the people of outdoor activities are more and more.Therefore, in order to The harm that ultraviolet radiation causes is reduced, it is sun-proof to be particularly important.So selection sun-screening agent and sunlight screening skin-protecting product are directly affected Effect to sun-proof result and sunlight screening skin-protecting product to skin, and sun protection factor sun-screening agent higher to the shielding of solar UV and Assimilation effect is better, but the organic uv absorbers concentration for adding is higher, causes allergic possibility bigger.With natural The plants essential oil refined based on plant not only has and absorbs the sun-proof function of ultraviolet, and with antibacterial, whitening, skin care, disappear Inflammation etc. act on, its plant extracts as cosmetic material have effect stability, persistently, and to skin action temperature and, excitant It is small, safe, while also having whitening, moisturizing to act on.Therefore plant extracts is developed as in sun care preparations Sun-screening agent, as focus of concern.
Suncream refers to that with the addition of to intercept or absorb the sun-screening agent of ultraviolet and prevent skin by tanned, sunburn reaching Cosmetics.Suncream is to play anti-sunlight function by inorganic and organic active ingredients.According to sun-proof principle, can be by suncream point It is physical sunscreen frost, chemical sunscreen frost.But chemical sun is in skin sense and good visual effect, but some sensitive skins crowd can be right Chemical sun Guo Min.It is using thin particulate matter light reflection ultraviolet, such as conventional titanium dioxide, zinc oxide in physical sunscreen frost Deng thin particulate matter.But the suncream of existing various brands with the addition of more chemical composition, have damage to skin.
Ultraviolet wavelength is divided into tri- sections of UVA, UVB, UVC, and wherein UVB is medium wave band ultraviolet range, and wave-length coverage is 280 ~ 320nm, it is most strong to skin ability to function, corium can be entered, it is sunburnt that acute dermatitis occurs(Erythema is burnt). UVA is long-wave band ultraviolet range, and wave-length coverage is 320 ~ 400nm, may pass through corium, and effect is slow, lasting, with accumulation property, With the passing of time skin aging can be caused, while increasing infringements of the UVB to skin.UVC be short-wave band ultraviolet range, wave-length coverage be 200 ~ 280nm, as sterilizing area, its penetration capacity is weak, and transmission capacity can only achieve the cuticula of skin, will not produce danger to skin Evil.Therefore the absorbability in the range of 280 ~ 400nm is mainly considered when sun-screening agent is selected.
Plant extracts is applied in suncream it has been reported that Chinese Patent Application No. is:2015107768581 A kind of turmeric skin care suncream is disclosed in patent;Chinese Patent Application No. is:Disclosed in 2015105087909 patent A kind of convex-concave rod Chinese medicinal herb sun protection cream;Chinese Patent Application No. is:A kind of rutin is disclosed in the patent of 201610487550X Plant sun frost.
There is the active material difference contained by different types of plants essential oil, the sun-proof result of single plant essential oil is undesirable, And duration is short, the application adds the means such as corrosion inhibiter by the compounding to plants essential oil, obtains a kind of composite plant Essential oil suncream, the essential oil after compounding has complementation with the absorption in ultra-violet (UV) band to light, also with sterilization, whitening function, Preservative need not be added can be preserved for a long time, it is not necessary to added essence and had good fragrance, while having moisturizing, suppression Bacterium and other effects.
The content of the invention
It is to solve it is an object of the invention to provide a kind of preparation method of the non-stimulated suncream of natural plants composite essential oil There is addition chemical sun in existing suncream and easily easily cause allergic problem.There is provided a kind of raw material sources extensively, low cost Honest and clean, sun-proof result is notable, non-stimulated, be combined suncream with antibacterial, moisturizing natural plants.
The purpose of the present invention is achieved through the following technical solutions.
A kind of preparation method of the non-stimulated suncream of natural plants composite essential oil, it is characterised in that the method has following Processing step:
(1)Propolis saturated solution:Propolis is put into low temperature refrigerator freezing a few hours, crushing is carried out after taking-up immediately and is made powder, By in powdered propolis immersion ethanol, stirring and dissolving is placed 48 hours, and solution reaches saturation, takes supernatant for propolis saturation is molten Liquid, it is standby;
(2)Composite essential oil is prepared:In the reactor, added by following composition mass percentage concentration, root of Dahurain angelica essential oil:10 ~ 15%, it is sweet Yellow grass ketone:10 ~ 15%, fennel essential oil:6 ~ 10%, ginger essential oil:6 ~ 10%, honeysuckle essential oil:10 ~ 15%, propolis saturated solution:4~ 6%, ethoxylated dodecyl alcohol AEO-3:38 ~ 48%, each component sum is for absolutely, high-speed stirred is lumped together, answered Close essential oil;
(3)It is prepared by the non-stimulated suncream of natural plants composite essential oil:In the reactor, by following composition mass percentage concentration and suitable Sequence is added, xanthans:0.1 ~ 0.2%, deionized water:20 ~ 25%, after dissolving, add composite essential oil:35 ~ 40%, octadecyl alcolol:8~ 12%, fibroin albumen:2 ~ 6%, vaseline:2 ~ 4%, EM-90 emulsifying agent:20 ~ 28%, each component sum is for absolutely, stirring is mixed Even, it is 7.0 or so to add triethanolamine regulation pH, and temperature at 50 ± 3 DEG C, lumped together, then temperature is risen to by high-speed stirred 78 ± 2 DEG C, constant temperature 6 hours is cooled to room temperature, places one week, obtains the non-stimulated suncream of natural plants composite essential oil, is distributed into appearance In device.
In step(1)Described propolis is natural original propolis.
In step(2)Described licoflavone is oil soluble licorice flavones.
In step(3)Described root of Dahurain angelica essential oil, sweet yellow grass ketone, fennel essential oil, ginger essential oil, honeysuckle essential oil are plant Extract.
UV Absorption situation is measured using ultraviolet spectrophotometry.
Application method:The non-stimulated suncream of natural plants composite essential oil directly can be applied on human body skin.
The present invention compared with the prior art, has the following advantages that and beneficial effect:
(1)The present invention obtain the non-stimulated suncream of natural plants composite essential oil be using extracted form natural plant root of Dahurain angelica essential oil, Sweet yellow grass ketone, fennel essential oil, ginger essential oil, honeysuckle essential oil are main optical absorbing agent composition, and these natural materials are contained by it There is component conjugated structure to have obvious absorption in ultra-violet (UV) band, not contain chemical sun, environmental protection, safety non-toxic, to skin Skin is non-stimulated;
(2)The natural plants composite essential oil non-stimulated suncream that the present invention is obtained directly can be applied on human body skin when using, Natural essential oil composition gives out nature fragrant, while containing several amino acids during fibroin albumen is with the addition of in this product, and has There is antibacterial, moisturizing etc. to act on, human body is had no side effect, it is easy to use;
(3)The non-stimulated suncream of natural plants composite essential oil that the present invention is obtained has flavonoids due to the addition of in propolis Compound, acid, alcohol, phenol, aldehyde, ester, ethers and alkene, terpene, steroid and several amino acids, aliphatic acid, enzyme, vitamin, Various trace elements have sustained release, moisturizing effect to plants essential oil, make that its sun-proof retention time is long, and the duration is small 10 to 12 When.
Using effect experience of the invention:
It is 120 people to participate in experiment number, is university student or other personnel, and the age was at 18 ~ 50 years old.Using described herein compound Plant whitening suncream, application method is:10 ~ 30min is wiped in face or other exposure portions before outdoor activities.Usage cycles are 2 months, averagely use 0.9 time for each person every day.Experimental result satisfaction is 93.6%;It is satisfied with standard:To no skin irritation, use Substantially feel comfortably cool afterwards, soft, non-greasy, moisturizing, with obvious sun-proof, whitening effect.
Root of Dahurain angelica essential oil mends the function of body, there is very strong healing power to body, particularly when treatment is just started, it is used for Reinforcing institutional framework.It assigns lymphatic system vigor, and catharsis is accelerated by the function of perspiring, especially after confined to bed for a long time, Body can be helped to discharge toxin.The generation of estrogen can be promoted, so in energy rule menstrual period, mitigate dysmenorrhoea, and help discharge born of the same parents Clothing.To the infertility of masculinity and femininity, curative effect is rather famous.Control uric acid, is beneficial to rheumatism, arthritis and gout and seat Osteoneuralgia.Rapid analgesic, either has a headache, has a toothache or antimigraine.In addition, it can also neutralize snake venom.Good skin care item, It is all helpful to various skin problems with inflammation-diminishing function, effect Zhuo for the treatment of mould parasitic problems.Scar can be treated Trace, wound and green grass or young crops of becoming silted up.Test discovery root of Dahurain angelica essential oil is carried out in 280 ~ 380nm scopes with stronger by being absorbed in ultra-violet (UV) band to it The absorption in broadband.240 ~ 280nm scopes absorb weaker.
Licoflavone is the natural whitening agent extracted from certain species Radix Glycyrrhizae, and it can suppress the activity of tyrosinase, and The activity of dopachrome change and DHICA oxidizing ferment can be suppressed, be that a kind of quick, efficiently, green whitening cosmetics add Plus agent.Liquorice flavonoids compound liquiritin, liquiritigenin and asparagus fern phthalein amine, mannitol etc., and the chemical combination extracted from Radix Glycyrrhizae Thing -- licoflavone has multiple efficacies in cosmetics, meanwhile, licoflavone also has suppression tyrosinase activity, removes oxygen Free radical, its oxidation resistance and vitamin E relatively, the effect with anti-inflammatory, antiallergic action, this mostlys come from sweet Oxalic acid iridium -- glycyrrhizic acid and glycyrrhetate, moreover it is possible to suppress capillary permeability.Licoflavone in view of Radix Glycyrrhizae be traditional tonic medicine, Tonic class contains protein and several amino acids, refers to class, polysaccharide, tartaric acid, vitamins, trace element etc., wherein albumen Amino acid after matter and its hydrolysis is used for cosmetics, to skin, the nutritious moisture-keeping function of hair, and skin, hair to damaging There is repair, so under the theory of this traditional Chinese medical science, during licoflavone addition compound skin-whitening generally taken off into spot liquid.By to its Ultra-violet (UV) band absorbs carries out test discovery licoflavone essential oil in absorption of 200 ~ 420nm scopes with stronger broadband.
The bioactivity of chlorogenic acid contained by honeysuckle, can promote human metabolism, regulation bodily fuctions, improve immune Power, with antibacterial, anti-inflammatory, adjusts the effect such as immune.Honeysuckle essential oil has moistening skin and eliminating spot, and anti-aging balances sebum and water Part secretion, drains moisture content.Find that honeysuckle essential oil has in 200 ~ 380nm scopes by absorbing test in ultra-violet (UV) band to it The absorption in stronger broadband.
Fennel essential oil is the indispensable weapon of women chest enlarge, improves that skin is slack and undisciplined and pore is thick, has consolidation skin, except microgroove Effect;Moistening effect is very well, also very helpful to preventing wrinkle and tangerine hull constitution etc..Dispel flatulence, appetizing, sharp stomach, decorporation is just. Fat-reducing, diuresis, help fat-reducing.Belong to potent essential oil, excessive use can trigger toxicity.Pregnant woman, children, epileptic should avoid making With.With strong fennel fragrance.The golden fennel essential oil of test discovery is carried out in 280 ~ 350nm models by being absorbed in ultra-violet (UV) band to it Enclose the absorption with stronger broadband.
Ginger essential oil contributes to dissipation hemostasis, controls wound;Conditioning oily skin, pale skin quality uses also effective.Promote the sexual maturity, Go ventosity, be particularly helpful to improve internal moisture, such as influenza, many phlegm and rhinorrhea.Resolving sputum, bring down a fever, hypocatharsis, make body Body temperature is warmed up.Find that ginger essential oil has stronger broadband in 200 ~ 410nm scopes by absorbing test in ultra-violet (UV) band to it Absorb.
Propolis is the resin that honeybee gathers from plant gemma or trunk, is mixed into the secretion of palatine gland, wax gland thereon A kind of colloidal solid thing with aromatic odor for processing.It is secreted by the repairing honeycomb such as Apidae animal apis cerana The stickum of yellowish-brown or dark brown, can be used as medicine.Its is mild-natured, bitter, pungent, micro-sweet, there is moisturizing myogenic, the work(of anti-inflammatory analgetic Effect, can treat the illnesss such as gastric ulcer, canker sore, burn and scald, skin Tearing Pain, radiation proof.Contained acid compounds in propolis There is caffeic acid, anisic acid, p-Coumaric Acid, forulic acid, isoferulic acid, cinnamic acid, 3,4- dimethoxys cinnamic acid, benzoic acid, right Hydroxybenzoic acid etc..Propolis ingredient is extremely complex, have flavone compound, acid, alcohol, phenol, aldehyde, ester, ethers and alkene, Terpene, steroid and several amino acids, aliphatic acid, enzyme, vitamin, various trace elements etc., its is mild-natured, bitter, pungent, micro- Sweet, the effect for having moisturizing myogenic, anti-inflammatory analgetic carries out test discovery propolis ethanol solution 200 by being absorbed in ultra-violet (UV) band to it ~ 400nm scopes have the absorption in stronger broadband.
Specific embodiment
Embodiment 1
(1)Propolis saturated solution:The powdered propolis of 20g is immersed in 100mL ethanol, stirring and dissolving, placed 48 hours, solution Saturation is reached, supernatant is taken for propolis saturated solution;
(2)Composite essential oil is prepared:In the reactor, it is separately added into, root of Dahurain angelica essential oil:12mL, sweet yellow grass ketone:12mL, fennel essential oil: 8mL, ginger essential oil:8mL, honeysuckle essential oil:12mL, propolis saturated solution:5mL, ethoxylated dodecyl alcohol AEO-3:43g, High-speed stirred is lumped together, obtains composite essential oil;
(3)It is prepared by the non-stimulated suncream of natural plants composite essential oil:In the reactor, it is separately added into, xanthans:0.1g, go from Sub- water:22mL, after dissolving, adds composite essential oil:40g, octadecyl alcolol:10g, fibroin albumen:4g, vaseline:2g, EM-90 breast Agent:22g, stirs and evenly mixs, and it is 7.0 or so to add triethanolamine regulation pH, and at 50 ± 3 DEG C, it is one that high-speed stirred is mixed to temperature Body, then temperature is risen to 78 ± 2 DEG C, constant temperature 6 hours is cooled to room temperature, places one week, obtains natural plants composite essential oil non-stimulated Suncream, is distributed into container.
Embodiment 2
(1)Propolis saturated solution:The powdered propolis of 50g is immersed in 200mL ethanol, stirring and dissolving, placed 48 hours, solution Saturation is reached, supernatant is taken for propolis saturated solution;
(2)Composite essential oil is prepared:In the reactor, it is separately added into, root of Dahurain angelica essential oil:15mL, sweet yellow grass ketone:10mL, fennel essential oil: 10mL, ginger essential oil:10mL, honeysuckle essential oil:13mL, propolis saturated solution:4mL, ethoxylated dodecyl alcohol AEO-3: 38g, high-speed stirred is lumped together, obtains composite essential oil;
(3)It is prepared by the non-stimulated suncream of natural plants composite essential oil:In the reactor, it is separately added into, xanthans:0.1g, go from Sub- water:24mL, after dissolving, adds composite essential oil:35g, octadecyl alcolol:8g, fibroin albumen:2g, vaseline:3g, EM-90 are emulsified Agent:28g, stirs and evenly mixs, and it is 7.0 or so to add triethanolamine regulation pH, and temperature at 50 ± 3 DEG C, lump together by high-speed stirred, Temperature is risen to 78 ± 2 DEG C again, constant temperature 6 hours is cooled to room temperature, places one week, obtain natural plants composite essential oil non-stimulated anti- Frost is shone, is distributed into container.
Embodiment 3
(1)Propolis saturated solution:The powdered propolis of 20g is immersed in 100mL ethanol, stirring and dissolving, placed 48 hours, solution Saturation is reached, supernatant is taken for propolis saturated solution;
(2)Composite essential oil is prepared:In the reactor, it is separately added into, root of Dahurain angelica essential oil:10mL, sweet yellow grass ketone:15mL, fennel essential oil: 6mL, ginger essential oil:6mL, honeysuckle essential oil:15mL, propolis saturated solution:6mL, ethoxylated dodecyl alcohol AEO-3:42g, High-speed stirred is lumped together, obtains composite essential oil;
(3)It is prepared by the non-stimulated suncream of natural plants composite essential oil:In the reactor, it is separately added into, xanthans:0.15g, go from Sub- water:25mL, after dissolving, adds composite essential oil:36g, octadecyl alcolol:12g, fibroin albumen:3g, vaseline:4g, EM-90 breast Agent:20g, stirs and evenly mixs, and it is 7.0 or so to add triethanolamine regulation pH, and at 50 ± 3 DEG C, it is one that high-speed stirred is mixed to temperature Body, then temperature is risen to 78 ± 2 DEG C, constant temperature 6 hours is cooled to room temperature, places one week, obtains natural plants composite essential oil non-stimulated Suncream, is distributed into container.
Embodiment 4
(1)Propolis saturated solution:The powdered propolis of 20g is immersed in 100mL ethanol, stirring and dissolving, placed 48 hours, solution Saturation is reached, supernatant is taken for propolis saturated solution;
(2)Composite essential oil is prepared:In the reactor, it is separately added into, root of Dahurain angelica essential oil:11mL, sweet yellow grass ketone:13mL, fennel essential oil: 7mL, ginger essential oil:7mL, honeysuckle essential oil:10mL, propolis saturated solution:4mL, ethoxylated dodecyl alcohol AEO-3:48g, High-speed stirred is lumped together, obtains composite essential oil;
(3)It is prepared by the non-stimulated suncream of natural plants composite essential oil:In the reactor, it is separately added into, xanthans:0.1g, go from Sub- water:20mL, after dissolving, adds composite essential oil:39g, octadecyl alcolol:8g, fibroin albumen:6g, vaseline:2g, EM-90 are emulsified Agent:25g, stirs and evenly mixs, and it is 7.0 or so to add triethanolamine regulation pH, and temperature at 50 ± 3 DEG C, lump together by high-speed stirred, Temperature is risen to 78 ± 2 DEG C again, constant temperature 6 hours is cooled to room temperature, places one week, obtain natural plants composite essential oil non-stimulated anti- Frost is shone, is distributed into container.
Application method:Natural plants composite essential oil non-stimulated suncream directly can be applied on human body skin when using, day Right essential oil composition gives out nature fragrant, and with antibacterial, moisturizing, whitening, anti-sunlight function, it is non-stimulated to human body, use It is convenient;Duration, sun-proof result was averagely more than 90% at 10 to 12 hours.

Claims (5)

1. a kind of preparation method of the non-stimulated suncream of natural plants composite essential oil, it is characterised in that the method has following work Skill step:
(1)Propolis saturated solution:Propolis is put into low temperature refrigerator freezing a few hours, crushing is carried out after taking-up immediately and is made powder, By in powdered propolis immersion ethanol, stirring and dissolving is placed 48 hours, and solution reaches saturation, takes supernatant for propolis saturation is molten Liquid, it is standby;
(2)Composite essential oil is prepared:In the reactor, added by following composition mass percentage concentration, root of Dahurain angelica essential oil:10 ~ 15%, it is sweet Yellow grass ketone:10 ~ 15%, fennel essential oil:6 ~ 10%, ginger essential oil:6 ~ 10%, honeysuckle essential oil:10 ~ 15%, propolis saturated solution:4~ 6%, ethoxylated dodecyl alcohol AEO-3:38 ~ 48%, each component sum is for absolutely, high-speed stirred is lumped together, answered Close essential oil;
(3)It is prepared by the non-stimulated suncream of natural plants composite essential oil:In the reactor, by following composition mass percentage concentration and suitable Sequence is added, xanthans:0.1 ~ 0.2%, deionized water:20 ~ 25%, after dissolving, add composite essential oil:35 ~ 40%, octadecyl alcolol:8~ 12%, fibroin albumen:2 ~ 6%, vaseline:2 ~ 4%, EM-90 emulsifying agent:20 ~ 28%, each component sum is for absolutely, stirring is mixed Even, it is 7.0 or so to add triethanolamine regulation pH, and temperature at 50 ± 3 DEG C, lumped together, then temperature is risen to by high-speed stirred 78 ± 2 DEG C, constant temperature 6 hours is cooled to room temperature, places one week, obtains the non-stimulated suncream of natural plants composite essential oil, is distributed into appearance In device.
2. a kind of preparation method of the non-stimulated suncream of natural plants composite essential oil according to claim 1, its feature It is, step(1)Described propolis is natural original propolis.
3. a kind of preparation method of the non-stimulated suncream of natural plants composite essential oil according to claim 1, its feature It is, step(2)Described licoflavone is oil soluble licorice flavones.
4. a kind of preparation method of the non-stimulated suncream of natural plants composite essential oil according to claim 1, its feature It is, step(3)Described root of Dahurain angelica essential oil, sweet yellow grass ketone, fennel essential oil, ginger essential oil, honeysuckle essential oil are plant extract Thing.
5. prepared by a kind of preparation method of the non-stimulated suncream of natural plants composite essential oil according to claim 1 The non-stimulated suncream of natural plants composite essential oil.
CN201710128232.9A 2017-03-06 2017-03-06 A kind of preparation method of the non-stimulated suncream of natural plants composite essential oil Withdrawn CN106727256A (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113350225A (en) * 2020-03-04 2021-09-07 弘光科技大学 Sunscreen essential oil composition

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113350225A (en) * 2020-03-04 2021-09-07 弘光科技大学 Sunscreen essential oil composition

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Application publication date: 20170531