CN106724471A - A kind of high temperature resistant refreshing health-care straw mat - Google Patents

A kind of high temperature resistant refreshing health-care straw mat Download PDF

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Publication number
CN106724471A
CN106724471A CN201611199935.2A CN201611199935A CN106724471A CN 106724471 A CN106724471 A CN 106724471A CN 201611199935 A CN201611199935 A CN 201611199935A CN 106724471 A CN106724471 A CN 106724471A
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parts
temperature
resistant layer
modified
resistant
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耿俊虎
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ANHUI AGRICULTURE GRASS Co Ltd
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ANHUI AGRICULTURE GRASS Co Ltd
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    • AHUMAN NECESSITIES
    • A47FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
    • A47GHOUSEHOLD OR TABLE EQUIPMENT
    • A47G9/00Bed-covers; Counterpanes; Travelling rugs; Sleeping rugs; Sleeping bags; Pillows
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L23/00Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • C08L23/02Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
    • C08L23/16Elastomeric ethene-propene or ethene-propene-diene copolymers, e.g. EPR and EPDM rubbers
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/011Nanostructured additives
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00Properties
    • C08L2201/08Stabilised against heat, light or radiation or oxydation
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/02Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/54Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids

Abstract

The invention discloses a kind of high temperature resistant refreshing health-care straw mat, including mat body, the high-temperature-resistant layer of mat body lower surface is arranged at, the Chinese medicine for being arranged at mat body upper surface is refreshed oneself and coating and is arranged at the skid resistant course of high-temperature-resistant layer lower surface;The raw material of high-temperature-resistant layer includes ethylene propylene diene rubber, epoxy resin, melamine resin, phenolic resin, APP, polytetrafluoroethylene (PTFE), PCDL, IPDI, tricarboxylic propane tri, butyl titanate, MTES, toluene di-iso-cyanide ester, acrylic emulsion, sodium pyrophosphate, lauryl sodium sulfate, attapulgite, modified asbestos powder, nanometer alchlor, mica powder, nano titanium oxide, modified additive, zinc stearate, hydroxyethyl cellulose, silane coupler KH 560, dispersant, diluent and deionized water.Health care straw mat of the invention has functions that excellent resistance to elevated temperatures and refreshes oneself.

Description

A kind of high temperature resistant refreshing health-care straw mat
Technical field
The present invention relates to straw mat field, more particularly to a kind of high temperature resistant refreshing health-care straw mat.
Background technology
Straw mat in the market is formed using seat straw plaited mostly, and relatively dry, resistance to elevated temperatures is poor, and existing market On straw mat health properties it is single, only used as straw mat mostly, and lack health-care efficacy, with carrying for people's living standard Height, for the health-care efficacy requirement more and more higher of straw mat, the straw mat of in the market cannot meet the demand of people to people, therefore need badly A kind of high temperature resistant refreshing health-care straw mat is designed to solve the problems of the prior art.
The content of the invention
To solve technical problem present in background technology, the present invention proposes a kind of high temperature resistant refreshing health-care straw mat, has Excellent resistance to elevated temperatures and the effect refreshed oneself.
A kind of high temperature resistant refreshing health-care straw mat proposed by the present invention, including mat body, are arranged at mat body lower surface High-temperature-resistant layer, the Chinese medicine for being arranged at mat body upper surface refreshes oneself and coating and is arranged at the skid resistant course of high-temperature-resistant layer lower surface;
Mat body is that straw mat, rattan seat, bamboo mat, the mat make of thin bamboo strips, one or more braiding of Lin Xizhong are formed;
The raw material of high-temperature-resistant layer includes by weight:Ethylene propylene diene rubber 80-120 parts, epoxy resin 35-45 parts, melamine Resin 15-25 parts, phenolic resin 8-16 parts, APP 15-35 parts, polytetrafluoroethylene (PTFE) 12-24 parts, PCDL 13- 26 parts, IPDI 8-16 parts, 4-8 parts of tricarboxylic propane tri, butyl titanate 2-5 parts, first 2-5 parts of ethyl triethoxy silicane alkane, toluene di-iso-cyanide ester 1-8 parts, acrylic emulsion 2-6 parts, sodium pyrophosphate 2-5 parts, dodecyl Sodium sulphate 3-6 parts, attapulgite 3-9 parts, 1-6 parts of modified asbestos powder, 2-5 parts of nanometer alchlor, mica powder 2-4 parts, nanometer Titanium dioxide 3-6 parts, modified additive 8-16 parts, zinc stearate 2-5 parts, hydroxyethyl cellulose 3-9 parts, silane coupler KH-560 2-6 parts, dispersant 2-8 parts, diluent 2-5 parts, deionized water 12-26 parts;
The refresh oneself raw material of coating of Chinese medicine includes by weight:Radix Astragali 5-15 parts, Radix Codonopsis 2-5 parts, rattletop 3-6 parts, bavin root 1-4 Part, even 2-5 parts of rice, Gorgon fruit 1-4 parts, Chinese yam 3-6 parts, chrysanthemum indicum 2-5 parts, cassia seed 1-3 parts, Jasmine 4-8 parts, dried peppermint leaf 2- 5 parts, Verbena officinalis 1-3 parts, rosemary 2-5 parts, lemon grass (Cymbopogon citratus) 3-6 parts, dried orange peel 2-4 parts, grape-fruit 1-5 parts, borneol 2-5 parts, camphor 4-6 parts, galingal 4-8 parts, cassia bark 1-3 parts, Ligusticum wallichii 2-5 parts, root of Dahurain angelica 3-6 parts, rhizoma atractylodis 1-3 parts, kaempferia galamga 2-5 parts, realgar 4-8 parts, Cloves 3-6 parts, fruit of Chinese wolfberry 2-5 parts, mulberry leaf branch 4-8 parts, red sage root 3-6 parts, safflower 1-3 parts, reticulate millettia 2-5 parts, caulis trachelospermi 4-8 Part, 5-15 parts of natural rubber glue;
Skid resistant course is silica-gel antiskid pad.
Preferably, in the raw material of high-temperature-resistant layer, the raw material of modified additive includes by weight:Sepiolite powder 2-5 parts, expansion Graphite 3-6 parts, vermiculite 1-3 parts, mass percent be hydrochloric acid solution 2-5 parts of 4-6%, carbamate 3-5 parts, acrylic acid it is different Propyl ester 4-6 parts, nano-sized magnesium hydroxide 2-5 parts, modified silicon oil 3-8 parts, Firebrake ZB 4-6 parts, talcum powder 2-5 parts, montmorillonite 3-6 Part, alumina fibre 1-4 parts.
Preferably, in the raw material of high-temperature-resistant layer, modified additive is prepared by following technique:By sepiolite powder, expansion stone Ink and vermiculite calcine 2-5h in being put into calcining furnace at 820-920 DEG C, cool down, and are put into the hydrochloric acid that mass percent is 4-6% molten 1-3h is soaked in liquid, filtering is taken out, drying is cleaned with clear water, crushing obtains material a, then by material a, carbamate, third Isopropyl gadoleate, nano-sized magnesium hydroxide, modified silicon oil, Firebrake ZB, talcum powder, montmorillonite and alumina fibre are well mixed, and grind Mill is uniformly dispersed, and obtains final product modified additive.
Preferably, in the raw material of high-temperature-resistant layer, in the preparation technology of modified additive, modified silicon oil is by following technique system It is standby:By containing hydrogen silicone oil, 16 dilute and VTES is well mixed, 85-95 DEG C is warming up to, is subsequently adding chlorine platinum Acid, is continuously heating to 100-120 DEG C, is incubated 1-3h, is cooled to room temperature and obtains modified silicon oil.
Preferably, in the raw material of high-temperature-resistant layer, in the preparation technology of modified additive, in the preparation technology of modified silicon oil, contain The weight ratio of hydrogen silicone oil, 16 dilute, VTESs and chloroplatinic acid is 2-5:1-3:3-5:4-8.
Preferably, Chinese medicine coating of refreshing oneself is prepared by following technique:By the Radix Astragali, Radix Codonopsis, rattletop, even Chai Gen, rice, Gorgon euryale Reality, Chinese yam, chrysanthemum indicum, cassia seed, Jasmine, dried peppermint leaf, Verbena officinalis, rosemary, lemon grass (Cymbopogon citratus), dried orange peel, grape-fruit, borneol, camphor tree Brain, galingal, cassia bark, Ligusticum wallichii, the root of Dahurain angelica, rhizoma atractylodis, kaempferia galamga, realgar, cloves, the fruit of Chinese wolfberry, mulberry leaf branch, the red sage root, safflower, reticulate millettia and network Stone rattan is put into barrel after being ground into 20-40 mesh, and then barrel is put into extraction kettle, installs sealing ring, then tightens extraction The end socket of kettle, then opens carbon dioxide steel cylinder, and carbon dioxide enters in constant temperature control box by filtering, constant temperature control box cooling Co 2 liquefaction is caused to 3-5 DEG C, it is super that the carbon dioxide after liquefaction enters formation in extraction heat exchanger through high-pressure pump pressurization Critical condition, it is dense then to adding green salt to be well mixed in extract subsequently into carrying out that extract is obtained by extraction in extractor Dried after contracting, be cooled to room temperature, be subsequently adding natural rubber glue and be well mixed, obtained Chinese medicine and refresh oneself coating.
Preferably, high-temperature-resistant layer is prepared by following technique:By ethylene propylene diene rubber, epoxy resin, melamine resin, phenol Urea formaldehyde, APP, polytetrafluoroethylene (PTFE), PCDL, IPDI, the propylene of tricarboxylic methylpropane three Acid esters, butyl titanate, MTES, toluene di-iso-cyanide ester, acrylic emulsion, sodium pyrophosphate, dodecyl sulphur Sour sodium and deionized water are added in mixer, and 25-40min is stirred under low whipping speed 180-220r/min, are subsequently adding concavo-convex Rod soil, modified asbestos powder, nanometer alchlor, mica powder, nano titanium oxide, modified additive, zinc stearate, hydroxy ethyl fiber Element, silane coupler KH-560, dispersant and diluent, 50-70min is stirred under low whipping speed 450-550r/min, uses mesh The silk screen filter of the number mesh of > 120, barrelling obtains high-temperature-resistant layer.
A kind of high temperature resistant refreshing health-care straw mat of the invention, including mat body, are arranged at the resistance to of mat body lower surface Heat zone, the Chinese medicine for being arranged at mat body upper surface is refreshed oneself and coating and is arranged at the skid resistant course of high-temperature-resistant layer lower surface;Resistance to height The raw material of warm layer includes ethylene propylene diene rubber, epoxy resin, melamine resin, phenolic resin, APP, polytetrafluoroethylene (PTFE), poly- Carbonate diol, IPDI, tricarboxylic propane tri, butyl titanate, methyl triethoxy Silane, toluene di-iso-cyanide ester, acrylic emulsion, sodium pyrophosphate, lauryl sodium sulfate, attapulgite, modified asbestos powder, nanometer Alchlor, mica powder, nano titanium oxide, modified additive, zinc stearate, hydroxyethyl cellulose, silane coupler KH-560, Dispersant, diluent and deionized water.In the raw material of high-temperature-resistant layer, modified additive is prepared by following technique:By sepiolite Powder, expanded graphite and vermiculite are calcined in being put into calcining furnace, cooling, are put into immersion in hydrochloric acid solution, and filtering is taken out, and is cleaned with clear water Drying, crushing obtain material a, then by material a, carbamate, isopropyl acrylate, nano-sized magnesium hydroxide, modified silicon oil, Firebrake ZB, talcum powder, montmorillonite and alumina fibre are well mixed, and grinding distribution is uniform, obtains final product modified additive, applies to resistance to height In the preparation of warm layer, the resistance to elevated temperatures of high-temperature-resistant layer is effectively increased, further increase the resistance to height of health care straw mat of the present invention Warm nature energy.In the raw material of high-temperature-resistant layer, in the preparation technology of modified additive, modified silicon oil is prepared by following technique:To contain Hydrogen silicone oil, 16 is dilute and VTES well mixed, heats up, and is subsequently adding chloroplatinic acid, continues to heat up, insulation, It is cooled to room temperature and obtains modified silicon oil, apply in the preparation of high-temperature-resistant layer, effectively increases the resistance to elevated temperatures of high-temperature-resistant layer, Further increase the resistance to elevated temperatures of health care straw mat of the present invention.Chinese medicine coating of refreshing oneself is prepared by following technique:By the Radix Astragali, Radix Codonopsis, rattletop, even Chai Gen, rice, Gorgon fruit, Chinese yam, chrysanthemum indicum, cassia seed, Jasmine, dried peppermint leaf, Verbena officinalis, rosemary, lemon Grass, dried orange peel, grape-fruit, borneol, camphor, galingal, cassia bark, Ligusticum wallichii, the root of Dahurain angelica, rhizoma atractylodis, kaempferia galamga, realgar, cloves, the fruit of Chinese wolfberry, mulberry leaf Branch, the red sage root, safflower, reticulate millettia and caulis trachelospermi are put into barrel after crushing, and then barrel is put into extraction kettle, install sealing Circle, then tightens the end socket of extraction kettle, then opens carbon dioxide steel cylinder, and carbon dioxide enters constant temperature control box by filtering Interior, constant temperature control box is lowered the temperature and causes co 2 liquefaction, and the carbon dioxide after liquefaction enters extraction heat exchange through high-pressure pump pressurization Supercriticality is formed in device, subsequently into carrying out that extract is obtained by extraction in extractor, then to adding green salt in extract It is well mixed, dried after concentration, room temperature is cooled to, it is subsequently adding natural rubber glue and is well mixed, obtain Chinese medicine and refresh oneself coating, Effectively increase the refreshing effect of health care straw mat of the present invention.Health care straw mat of the invention has excellent resistance to elevated temperatures and refreshes oneself Effect.
Specific embodiment
The present invention is described in detail with reference to specific embodiment, it should be appreciated that embodiment is served only for illustrating this hair Bright, rather than for limiting the invention, any modification made on the basis of the present invention, equivalent etc. are in this hair In bright protection domain.
Embodiment 1
A kind of high temperature resistant refreshing health-care straw mat proposed by the present invention, including mat body, are arranged at mat body lower surface High-temperature-resistant layer, the Chinese medicine for being arranged at mat body upper surface refreshes oneself and coating and is arranged at the skid resistant course of high-temperature-resistant layer lower surface.
Mat body is that straw mat braiding is formed.
High-temperature-resistant layer is prepared by following technique:By weight by 100 parts of ethylene propylene diene rubbers, 40 parts of epoxy resin, 20 parts of melamine resins, 12 parts of phenolic resin, 25 parts of APPs, 18 parts of polytetrafluoroethylene (PTFE), 19.5 parts of PCDLs, 12 parts IPDI, 6 parts of tricarboxylic propane tris, 3.5 parts of butyl titanates, 3.5 parts of ethoxies of methyl three Base silane, 4.5 parts of toluene di-iso-cyanide esters, 4 parts of acrylic emulsions, 3.5 parts of sodium pyrophosphates, 4.5 parts of lauryl sodium sulfate and 19 Part deionized water is added in mixer, and 32.5min is stirred under low whipping speed 200r/min, be subsequently adding 6 parts of attapulgites, 3.5 parts of modified asbestos powder, 3.5 parts of nanometer alchlors, 3 parts of mica powders, 4.5 parts of nano titanium oxides, 12 parts of modified additives, 3.5 parts of zinc stearates, 6 parts of hydroxyethyl celluloses, 4 parts of silane coupler KH-560,5 parts of dispersants and 3.5 parts of diluents, are stirring Mix and stir 60min under speed 500r/min, with the silk screen filter of the mesh of mesh number 130, barrelling obtains high-temperature-resistant layer.
Chinese medicine coating of refreshing oneself is prepared by following technique:10 parts of Radixs Astragali, 3.5 parts of Radix Codonopsis, 4.5 parts are risen by weight Fiber crops, 2.5 parts of bavin roots, 3.5 portions of company's rice, 2.5 portions of Gorgon fruits, 4.5 parts of Chinese yams, 3.5 parts of chrysanthemum indicums, 2 parts of cassia seeds, 6 parts of Jasmines, 3.5 parts of dried peppermint leaves, 2 portions of Verbena officinalis, 3.5 parts of rosemary, 4.5 parts of lemon grass (Cymbopogon citratus)s, 3 parts of dried orange peels, 3 parts of grape-fruits, 3.5 parts of borneols, 5 parts Camphor, 6 parts of galingals, 2 parts of cassia barks, 3.5 parts of Ligusticum wallichiis, 4.5 parts of roots of Dahurain angelica, 2 parts of rhizoma atractylodis, 3.5 parts of kaempferia galamgas, 6 portions of realgars, 4.5 portions of cloves, 3.5 portions of fruits of Chinese wolfberry, 6 portions of mulberry leaf branches, 4.5 portions of reds sage root, 2 portions of safflowers, 3.5 portions of reticulate millettias and 6 portions of caulis trachelospermis are put after being ground into 30 mesh In feeding cylinder, then barrel is put into extraction kettle, installs sealing ring, then tighten the end socket of extraction kettle, then open dioxy Change carbon steel bottle, carbon dioxide enters in constant temperature control box by filtering, constant temperature control box is cooled to 4 DEG C and causes carbon dioxide liquid Change, the carbon dioxide after liquefaction pressurizes to enter in extraction heat exchanger through high-pressure pump and forms supercriticality, subsequently into extraction Carry out that extract is obtained by extraction in device, then to adding green salt to be well mixed in extract, dried after concentration, be cooled to room temperature, It is subsequently adding 10 parts of natural rubber glue to be well mixed, obtains Chinese medicine and refresh oneself coating.
Skid resistant course is silica-gel antiskid pad.
In the raw material of high-temperature-resistant layer, modified additive is prepared by following technique:By weight by 3.5 parts of sepiolite powders, 4.5 parts of expanded graphites and 2 parts of vermiculites calcine 3.5h in being put into calcining furnace at 870 DEG C, cooling, are put into 3.5 parts of mass percents To soak 2h in 5% hydrochloric acid solution, filtering is taken out, and drying is cleaned with clear water, and crushing obtains material a, then by material a, 4 parts Carbamate, 5 parts of isopropyl acrylates, 3.5 parts of nano-sized magnesium hydroxides, 5.5 parts of modified silicon oils, 5 parts of Firebrake ZBs, 3.5 parts of cunnings Stone flour, 4.5 parts of montmorillonites and 2.5 parts of alumina fibres are well mixed, and grinding distribution is uniform, obtains final product modified additive.
In the raw material of high-temperature-resistant layer, in the preparation technology of modified additive, modified silicon oil is prepared by following technique:By weight Amount part by 3.5 parts of containing hydrogen silicone oils, 2 part 16 it is dilute and 4 parts of VTESs are well mixed, be warming up to 90 DEG C, then 6 parts of chloroplatinic acids are added, 110 DEG C are continuously heating to, 2h is incubated, room temperature is cooled to and is obtained modified silicon oil.
Embodiment 2
A kind of high temperature resistant refreshing health-care straw mat proposed by the present invention, including mat body, are arranged at mat body lower surface High-temperature-resistant layer, the Chinese medicine for being arranged at mat body upper surface refreshes oneself and coating and is arranged at the skid resistant course of high-temperature-resistant layer lower surface.
Mat body is that the braiding of rattan seat is formed.
High-temperature-resistant layer is prepared by following technique:By weight by 80 parts of ethylene propylene diene rubbers, 45 parts of epoxy resin, 15 Part melamine resin, 16 parts of phenolic resin, 15 parts of APPs, 24 parts of polytetrafluoroethylene (PTFE), 13 parts of PCDLs, 16 parts of different Buddhists That ketone diisocyanate, 4 parts of tricarboxylic propane tris, 5 parts of butyl titanates, 2 parts of MTESs, 8 Part toluene di-iso-cyanide ester, 2 parts of acrylic emulsions, 5 parts of sodium pyrophosphates, 3 parts of lauryl sodium sulfate and 26 parts of deionized waters are added In mixer, 40min is stirred under low whipping speed 180r/min, be subsequently adding 3 parts of attapulgites, 6 parts of modified asbestos powder, 2 parts Nanometer alchlor, 4 parts of mica powders, 3 parts of nano titanium oxides, 16 parts of modified additives, 2 parts of zinc stearates, 9 parts of hydroxy ethyl fibers Element, 2 parts of silane coupler KH-560,8 parts of dispersants and 2 parts of diluents, stir 50min under low whipping speed 550r/min, use Mesh number is the silk screen filter of 130 mesh, and barrelling obtains high-temperature-resistant layer.
Chinese medicine coating of refreshing oneself is prepared by following technique:By weight by 5 parts of Radixs Astragali, 5 parts of Radix Codonopsis, 3 parts of rattletops, 4 parts Chai Gen, 2 parts of company's rice, 4 parts of Gorgon fruits, 3 parts of Chinese yams, 5 parts of chrysanthemum indicums, 1 part of cassia seed, 8 parts of Jasmines, 2 parts of dried peppermint leaves, 3 parts of horsewhips Grass, 2 parts of rosemary, 6 parts of lemon grass (Cymbopogon citratus)s, 2 parts of dried orange peels, 5 parts of grape-fruits, 2 parts of borneols, 6 parts of camphor, 4 parts of galingals, 3 parts of cassia barks, 2 parts Ligusticum wallichii, 6 parts of roots of Dahurain angelica, 1 part of rhizoma atractylodis, 5 parts of kaempferia galamgas, 4 portions of realgars, 6 portions of cloves, 2 portions of fruits of Chinese wolfberry, 8 parts of mulberry leaf branches, 3 parts of reds sage root, 3 parts Safflower, 2 portions of reticulate millettias and 8 portions of caulis trachelospermis are put into barrel after being ground into 20 mesh, and then barrel is put into extraction kettle, are installed close Seal, then tightens the end socket of extraction kettle, then opens carbon dioxide steel cylinder, and carbon dioxide enters constant temperature control box by filtering Interior, constant temperature control box is cooled to 5 DEG C and causes co 2 liquefaction, and the carbon dioxide after liquefaction enters extraction heat through high-pressure pump pressurization Supercriticality is formed in exchanger, subsequently into carrying out that extract is obtained by extraction in extractor, is then added in extract Green salt is well mixed, and is dried after concentration, is cooled to room temperature, is subsequently adding 5 parts of natural rubber glue and is well mixed, and obtains Chinese medicine and carries Refreshing coating.
Skid resistant course is silica-gel antiskid pad.
In the raw material of high-temperature-resistant layer, modified additive is prepared by following technique:By weight by 2 parts of sepiolite powders, 6 parts Expanded graphite and 1 part of vermiculite calcine 2h in being put into calcining furnace at 920 DEG C, cooling, are put into the salt that 5 parts of mass percents are 4% 3h is soaked in acid solution, filtering is taken out, drying is cleaned with clear water, crushing obtains material a, then by material a, 3 parts of carbamic acids Ester, 6 parts of isopropyl acrylates, 2 parts of nano-sized magnesium hydroxides, 8 parts of modified silicon oils, 4 parts of Firebrake ZBs, 5 parts of talcum powder, 3 parts of montmorillonites Well mixed with 4 parts of alumina fibres, grinding distribution is uniform, obtains final product modified additive.
In the raw material of high-temperature-resistant layer, in the preparation technology of modified additive, modified silicon oil is prepared by following technique:By weight Amount part by 2 parts of containing hydrogen silicone oils, 3 part 16 it is dilute and 3 parts of VTESs are well mixed, be warming up to 95 DEG C, Ran Houjia Enter 4 parts of chloroplatinic acids, be continuously heating to 120 DEG C, be incubated 1h, be cooled to room temperature and obtain modified silicon oil.
Embodiment 3
A kind of high temperature resistant refreshing health-care straw mat proposed by the present invention, including mat body, are arranged at mat body lower surface High-temperature-resistant layer, the Chinese medicine for being arranged at mat body upper surface refreshes oneself and coating and is arranged at the skid resistant course of high-temperature-resistant layer lower surface.
Mat body is that bamboo mat braiding is formed.
High-temperature-resistant layer is prepared by following technique:By weight by 120 parts of ethylene propylene diene rubbers, 35 parts of epoxy resin, 25 parts of melamine resins, 8 parts of phenolic resin, 35 parts of APPs, 12 parts of polytetrafluoroethylene (PTFE), 26 parts of PCDLs, 8 parts of different Buddhists That ketone diisocyanate, 8 parts of tricarboxylic propane tris, 2 parts of butyl titanates, 5 parts of MTESs, 1 Part toluene di-iso-cyanide ester, 6 parts of acrylic emulsions, 2 parts of sodium pyrophosphates, 6 parts of lauryl sodium sulfate and 12 parts of deionized waters are added In mixer, 25min is stirred under low whipping speed 220r/min, be subsequently adding 9 parts of attapulgites, 1 part of modified asbestos powder, 5 parts Nanometer alchlor, 2 parts of mica powders, 6 parts of nano titanium oxides, 8 parts of modified additives, 5 parts of zinc stearates, 3 parts of hydroxy ethyl fibers Element, 6 parts of silane coupler KH-560,2 parts of dispersants and 5 parts of diluents, stir 70min under low whipping speed 450r/min, use Mesh number is the silk screen filter of 130 mesh, and barrelling obtains high-temperature-resistant layer.
Chinese medicine coating of refreshing oneself is prepared by following technique:By weight by 15 parts of Radixs Astragali, 2 parts of Radix Codonopsis, 6 parts of rattletops, 1 part Chai Gen, 5 parts of company's rice, 1 part of Gorgon fruit, 6 parts of Chinese yams, 2 parts of chrysanthemum indicums, 3 parts of cassia seeds, 4 parts of Jasmines, 5 parts of dried peppermint leaves, 1 part of horsewhip Grass, 5 parts of rosemary, 3 parts of lemon grass (Cymbopogon citratus)s, 4 parts of dried orange peels, 1 part of grape-fruit, 5 parts of borneols, 4 parts of camphor, 8 parts of galingals, 1 part of cassia bark, 5 parts Ligusticum wallichii, 3 parts of roots of Dahurain angelica, 3 parts of rhizoma atractylodis, 2 parts of kaempferia galamgas, 8 portions of realgars, 3 portions of cloves, 5 portions of fruits of Chinese wolfberry, 4 parts of mulberry leaf branches, 6 parts of reds sage root, 1 part Safflower, 5 portions of reticulate millettias and 4 portions of caulis trachelospermis are put into barrel after being ground into 40 mesh, and then barrel is put into extraction kettle, are installed close Seal, then tightens the end socket of extraction kettle, then opens carbon dioxide steel cylinder, and carbon dioxide enters constant temperature control box by filtering Interior, constant temperature control box is cooled to 3 DEG C and causes co 2 liquefaction, and the carbon dioxide after liquefaction enters extraction heat through high-pressure pump pressurization Supercriticality is formed in exchanger, subsequently into carrying out that extract is obtained by extraction in extractor, is then added in extract Green salt is well mixed, and is dried after concentration, is cooled to room temperature, is subsequently adding 15 parts of natural rubber glue and is well mixed, and obtains Chinese medicine Refresh oneself coating.
Skid resistant course is silica-gel antiskid pad.
In the raw material of high-temperature-resistant layer, modified additive is prepared by following technique:By weight by 5 parts of sepiolite powders, 3 parts Expanded graphite and 3 parts of vermiculites calcine 5h in being put into calcining furnace at 820 DEG C, cooling, are put into the salt that 2 parts of mass percents are 6% 1h is soaked in acid solution, filtering is taken out, drying is cleaned with clear water, crushing obtains material a, then by material a, 5 parts of carbamic acids Ester, 4 parts of isopropyl acrylates, 5 parts of nano-sized magnesium hydroxides, 3 parts of modified silicon oils, 6 parts of Firebrake ZBs, 2 parts of talcum powder, 6 parts of montmorillonites Well mixed with 1 part of alumina fibre, grinding distribution is uniform, obtains final product modified additive.
In the raw material of high-temperature-resistant layer, in the preparation technology of modified additive, modified silicon oil is prepared by following technique:By weight Amount part by 5 parts of containing hydrogen silicone oils, 1 part 16 it is dilute and 5 parts of VTESs are well mixed, be warming up to 85 DEG C, Ran Houjia Enter 8 parts of chloroplatinic acids, be continuously heating to 100 DEG C, be incubated 3h, be cooled to room temperature and obtain modified silicon oil.
Embodiment 4
A kind of high temperature resistant refreshing health-care straw mat proposed by the present invention, including mat body, are arranged at mat body lower surface High-temperature-resistant layer, the Chinese medicine for being arranged at mat body upper surface refreshes oneself and coating and is arranged at the skid resistant course of high-temperature-resistant layer lower surface.
Mat body is that mat make of thin bamboo strips braiding is formed.
High-temperature-resistant layer is prepared by following technique:By weight by 85 parts of ethylene propylene diene rubbers, 42 parts of epoxy resin, 18 Part melamine resin, 15 parts of phenolic resin, 18 parts of APPs, 22 parts of polytetrafluoroethylene (PTFE), 14 parts of PCDLs, 15 parts of different Buddhists That ketone diisocyanate, 5 parts of tricarboxylic propane tris, 4 parts of butyl titanates, 3 parts of MTESs, 7 Part toluene di-iso-cyanide ester, 3 parts of acrylic emulsions, 4 parts of sodium pyrophosphates, 4 parts of lauryl sodium sulfate and 24 parts of deionized waters are added In mixer, 39min is stirred under low whipping speed 190r/min, be subsequently adding 4 parts of attapulgites, 5 parts of modified asbestos powder, 3 parts Nanometer alchlor, 3.5 parts of mica powders, 4 parts of nano titanium oxides, 15 parts of modified additives, 3 parts of zinc stearates, 8 parts of ethoxy fibres Dimension element, 3 parts of silane coupler KH-560,7 parts of dispersants and 3 parts of diluents, 55min is stirred under low whipping speed 520r/min, With the silk screen filter that mesh number is 145 mesh, barrelling obtains high-temperature-resistant layer.
Chinese medicine coating of refreshing oneself is prepared by following technique:By weight by 8 parts of Radixs Astragali, 4 parts of Radix Codonopsis, 4 parts of rattletops, 3 parts Chai Gen, 3 portions of company's rice, 3 portions of Gorgon fruits, 4 parts of Chinese yams, 4 parts of chrysanthemum indicums, 1.5 parts of cassia seeds, 7 parts of Jasmines, 3 parts of dried peppermint leaves, 2.5 parts Verbena officinalis, 3 parts of rosemary, 5 parts of lemon grass (Cymbopogon citratus)s, 2.5 parts of dried orange peels, 4 parts of grape-fruits, 3 parts of borneols, 5.5 parts of camphors, 5 parts of galingals, 2.5 Part cassia bark, 3 parts of Ligusticum wallichiis, 5 parts of roots of Dahurain angelica, 1.5 parts of rhizoma atractylodis, 4 parts of kaempferia galamgas, 5 portions of realgars, 5 portions of cloves, 3 portions of fruits of Chinese wolfberry, 7 parts of mulberry leaf branches, 4 portions of reds sage root, 2.5 portions of safflowers, 3 portions of reticulate millettias and 7 portions of caulis trachelospermis are put into barrel after being ground into 25 mesh, and barrel then is put into extraction Take in kettle, install sealing ring, then tighten the end socket of extraction kettle, then open carbon dioxide steel cylinder, carbon dioxide is by filtering Into in constant temperature control box, constant temperature control box is cooled to 4.5 DEG C and causes co 2 liquefaction, and the carbon dioxide after liquefaction is through high pressure Pump pressurization enters in extraction heat exchanger and forms supercriticality, subsequently into carrying out that extract is obtained by extraction in extractor, so Add green salt to be well mixed in backward extract, dried after concentration, be cooled to room temperature, be subsequently adding 8 parts of natural rubber glue and mix Close uniform, obtain Chinese medicine and refresh oneself coating.
Skid resistant course is silica-gel antiskid pad.
In the raw material of high-temperature-resistant layer, modified additive is prepared by following technique:By weight by 3 parts of sepiolite powders, 5 parts Expanded graphite and 1.5 parts of vermiculites calcine 3h in being put into calcining furnace at 900 DEG C, cooling, and it is 4.5% to be put into 4 parts of mass percents Hydrochloric acid solution in soak 2.5h, filtering is taken out, and drying is cleaned with clear water, and crushing obtains material a, then by material a, 3.5 parts Carbamate, 5.5 parts of isopropyl acrylates, 3 parts of nano-sized magnesium hydroxides, 7 parts of modified silicon oils, 4.5 parts of Firebrake ZBs, 4 parts of talcums Powder, 4 parts of montmorillonites and 3 parts of alumina fibres are well mixed, and grinding distribution is uniform, obtains final product modified additive.
In the raw material of high-temperature-resistant layer, in the preparation technology of modified additive, modified silicon oil is prepared by following technique:By weight Amount part by 3 parts of containing hydrogen silicone oils, 2.5 part 16 it is dilute and 3.5 parts of VTESs are well mixed, be warming up to 92 DEG C, so 5 parts of chloroplatinic acids are added afterwards, 115 DEG C are continuously heating to, 1.5h is incubated, and are cooled to room temperature and are obtained modified silicon oil.
Embodiment 5
A kind of high temperature resistant refreshing health-care straw mat proposed by the present invention, including mat body, are arranged at mat body lower surface High-temperature-resistant layer, the Chinese medicine for being arranged at mat body upper surface refreshes oneself and coating and is arranged at the skid resistant course of high-temperature-resistant layer lower surface.
Mat body is that the braiding of Lin's seat is formed.
High-temperature-resistant layer is prepared by following technique:By weight by 115 parts of ethylene propylene diene rubbers, 38 parts of epoxy resin, 22 parts of melamine resins, 9 parts of phenolic resin, 32 parts of APPs, 14 parts of polytetrafluoroethylene (PTFE), 25 parts of PCDLs, 9 parts of different Buddhists That ketone diisocyanate, 7 parts of tricarboxylic propane tris, 3 parts of butyl titanates, 4 parts of MTESs, 2 Part toluene di-iso-cyanide ester, 5 parts of acrylic emulsions, 3 parts of sodium pyrophosphates, 5 parts of lauryl sodium sulfate and 14 parts of deionized waters are added In mixer, 26min is stirred under low whipping speed 210r/min, be subsequently adding 8 parts of attapulgites, 2 parts of modified asbestos powder, 4 parts Nanometer alchlor, 2.5 parts of mica powders, 5 parts of nano titanium oxides, 9 parts of modified additives, 4 parts of zinc stearates, 4 parts of ethoxy fibres Dimension element, 5 parts of silane coupler KH-560,3 parts of dispersants and 4 parts of diluents, 65min is stirred under low whipping speed 480r/min, With the silk screen filter of the mesh of mesh number 135, barrelling obtains high-temperature-resistant layer.
Chinese medicine coating of refreshing oneself is prepared by following technique:By weight by 12 parts of Radixs Astragali, 3 parts of Radix Codonopsis, 5 parts of rattletops, 2 parts Chai Gen, 4 portions of company's rice, 2 portions of Gorgon fruits, 5 parts of Chinese yams, 3 parts of chrysanthemum indicums, 2.5 parts of cassia seeds, 5 parts of Jasmines, 4 parts of dried peppermint leaves, 1.5 parts Verbena officinalis, 4 parts of rosemary, 4 parts of lemon grass (Cymbopogon citratus)s, 3.5 parts of dried orange peels, 2 parts of grape-fruits, 4 parts of borneols, 4.5 parts of camphors, 7 parts of galingals, 1.5 Part cassia bark, 4 parts of Ligusticum wallichiis, 4 parts of roots of Dahurain angelica, 2.5 parts of rhizoma atractylodis, 3 parts of kaempferia galamgas, 7 portions of realgars, 4 portions of cloves, 4 portions of fruits of Chinese wolfberry, 5 parts of mulberry leaf branches, 5 portions of reds sage root, 1.5 portions of safflowers, 4 portions of reticulate millettias and 5 portions of caulis trachelospermis are put into barrel after being ground into 35 mesh, and barrel then is put into extraction Take in kettle, install sealing ring, then tighten the end socket of extraction kettle, then open carbon dioxide steel cylinder, carbon dioxide is by filtering Into in constant temperature control box, constant temperature control box is cooled to 3.5 DEG C and causes co 2 liquefaction, and the carbon dioxide after liquefaction is through high pressure Pump pressurization enters in extraction heat exchanger and forms supercriticality, subsequently into carrying out that extract is obtained by extraction in extractor, so Add green salt to be well mixed in backward extract, dried after concentration, be cooled to room temperature, be subsequently adding 12 parts of natural rubber glue and mix Close uniform, obtain Chinese medicine and refresh oneself coating.
Skid resistant course is silica-gel antiskid pad.
In the raw material of high-temperature-resistant layer, modified additive is prepared by following technique:By weight by 4 parts of sepiolite powders, 4 parts Expanded graphite and 2.5 parts of vermiculites calcine 4h in being put into calcining furnace at 840 DEG C, cooling, and it is 5.5% to be put into 3 parts of mass percents Hydrochloric acid solution in soak 1.5h, filtering is taken out, and drying is cleaned with clear water, and crushing obtains material a, then by material a, 4.5 parts Carbamate, 4.5 parts of isopropyl acrylates, 4 parts of nano-sized magnesium hydroxides, 4 parts of modified silicon oils, 5.5 parts of Firebrake ZBs, 3 parts of talcums Powder, 5 parts of montmorillonites and 2 parts of alumina fibres are well mixed, and grinding distribution is uniform, obtains final product modified additive.
In the raw material of high-temperature-resistant layer, in the preparation technology of modified additive, modified silicon oil is prepared by following technique:By weight Amount part by 4 parts of containing hydrogen silicone oils, 1.5 part 16 it is dilute and 4.5 parts of VTESs are well mixed, be warming up to 88 DEG C, so 7 parts of chloroplatinic acids are added afterwards, 105 DEG C are continuously heating to, 2.5h is incubated, and are cooled to room temperature and are obtained modified silicon oil.
The above, the only present invention preferably specific embodiment, but protection scope of the present invention is not limited thereto, Any one skilled in the art the invention discloses technical scope in, technology according to the present invention scheme and its Inventive concept is subject to equivalent or change, should all be included within the scope of the present invention.

Claims (7)

1. a kind of high temperature resistant refreshing health-care straw mat, it is characterised in that including mat body, be arranged at the resistance to of mat body lower surface Heat zone, the Chinese medicine for being arranged at mat body upper surface is refreshed oneself and coating and is arranged at the skid resistant course of high-temperature-resistant layer lower surface;
Mat body is that straw mat, rattan seat, bamboo mat, the mat make of thin bamboo strips, one or more braiding of Lin Xizhong are formed;
The raw material of high-temperature-resistant layer includes by weight:Ethylene propylene diene rubber 80-120 parts, epoxy resin 35-45 parts, melamine resin 15-25 parts, phenolic resin 8-16 parts, APP 15-35 parts, polytetrafluoroethylene (PTFE) 12-24 parts, PCDL 13-26 parts, IPDI 8-16 parts, 4-8 parts of tricarboxylic propane tri, butyl titanate 2-5 parts, the second of methyl three TMOS 2-5 parts, toluene di-iso-cyanide ester 1-8 parts, acrylic emulsion 2-6 parts, sodium pyrophosphate 2-5 parts, lauryl sodium sulfate 3-6 parts, attapulgite 3-9 parts, 1-6 parts of modified asbestos powder, 2-5 parts of nanometer alchlor, mica powder 2-4 parts, nanometer titanium dioxide Titanium 3-6 parts, modified additive 8-16 parts, zinc stearate 2-5 parts, hydroxyethyl cellulose 3-9 parts, silane coupler KH-560 2-6 Part, dispersant 2-8 parts, diluent 2-5 parts, deionized water 12-26 parts;
The refresh oneself raw material of coating of Chinese medicine includes by weight:Radix Astragali 5-15 parts, Radix Codonopsis 2-5 parts, rattletop 3-6 parts, 1-4 parts of bavin root, Connect 2-5 parts of rice, Gorgon fruit 1-4 parts, Chinese yam 3-6 parts, chrysanthemum indicum 2-5 parts, cassia seed 1-3 parts, Jasmine 4-8 parts, dried peppermint leaf 2-5 Part, Verbena officinalis 1-3 parts, rosemary 2-5 parts, lemon grass (Cymbopogon citratus) 3-6 parts, dried orange peel 2-4 parts, grape-fruit 1-5 parts, borneol 2-5 parts, camphor 4- 6 parts, galingal 4-8 parts, cassia bark 1-3 parts, Ligusticum wallichii 2-5 parts, root of Dahurain angelica 3-6 parts, rhizoma atractylodis 1-3 parts, kaempferia galamga 2-5 parts, realgar 4-8 parts, fourth It is fragrant 3-6 parts, fruit of Chinese wolfberry 2-5 parts, mulberry leaf branch 4-8 parts, red sage root 3-6 parts, safflower 1-3 parts, reticulate millettia 2-5 parts, caulis trachelospermi 4-8 parts, 5-15 parts of natural rubber glue;
Skid resistant course is silica-gel antiskid pad.
2. high temperature resistant refreshing health-care straw mat according to claim 1, it is characterised in that in the raw material of high-temperature-resistant layer, is modified The raw material of auxiliary agent includes by weight:Sepiolite powder 2-5 parts, expanded graphite 3-6 parts, vermiculite 1-3 parts, mass percent be 4- 6% hydrochloric acid solution 2-5 parts, carbamate 3-5 parts, isopropyl acrylate 4-6 parts, nano-sized magnesium hydroxide 2-5 parts, modified silicon It is oily 3-8 parts, Firebrake ZB 4-6 parts, talcum powder 2-5 parts, montmorillonite 3-6 parts, alumina fibre 1-4 parts.
3. high temperature resistant refreshing health-care straw mat according to claim 1 and 2, it is characterised in that in the raw material of high-temperature-resistant layer, change Property auxiliary agent is prepared by following technique:Sepiolite powder, expanded graphite and vermiculite are put into calcining furnace and are forged at 820-920 DEG C 2-5h is burnt, cooling is put into mass percent to soak 1-3h in the hydrochloric acid solution of 4-6%, and filtering is taken out, and is cleaned with clear water and dried Dry, crushing obtains material a, then by material a, carbamate, isopropyl acrylate, nano-sized magnesium hydroxide, modified silicon oil, boron Sour zinc, talcum powder, montmorillonite and alumina fibre are well mixed, and grinding distribution is uniform, obtains final product modified additive.
4. the high temperature resistant refreshing health-care straw mat according to claim any one of 1-3, it is characterised in that the raw material of high-temperature-resistant layer In, in the preparation technology of modified additive, modified silicon oil is prepared by following technique:By containing hydrogen silicone oil, 16 dilute and vinyl Triethoxysilane is well mixed, and is warming up to 85-95 DEG C, is subsequently adding chloroplatinic acid, is continuously heating to 100-120 DEG C, is incubated 1- 3h, is cooled to room temperature and obtains modified silicon oil.
5. the high temperature resistant refreshing health-care straw mat according to claim any one of 1-4, it is characterised in that the raw material of high-temperature-resistant layer In, in the preparation technology of modified additive, in the preparation technology of modified silicon oil, containing hydrogen silicone oil, 16 dilute, vinyl triethoxyl silicon The weight ratio of alkane and chloroplatinic acid is 2-5:1-3:3-5:4-8.
6. the high temperature resistant refreshing health-care straw mat according to claim any one of 1-5, it is characterised in that Chinese medicine refresh oneself coating by Following technique is prepared:By the Radix Astragali, Radix Codonopsis, rattletop, even Chai Gen, rice, Gorgon fruit, Chinese yam, chrysanthemum indicum, cassia seed, Jasmine, thin Lotus leaf, Verbena officinalis, rosemary, lemon grass (Cymbopogon citratus), dried orange peel, grape-fruit, borneol, camphor, galingal, cassia bark, Ligusticum wallichii, the root of Dahurain angelica, rhizoma atractylodis, mountain How, realgar, cloves, the fruit of Chinese wolfberry, mulberry leaf branch, the red sage root, safflower, reticulate millettia and caulis trachelospermi be put into barrel after being ground into 20-40 mesh, Then barrel is put into extraction kettle, installs sealing ring, then tighten the end socket of extraction kettle, then open carbon dioxide steel cylinder, Carbon dioxide enters in constant temperature control box by filtering, and constant temperature control box is cooled to 3-5 DEG C and causes co 2 liquefaction, after liquefaction Carbon dioxide enter in extraction heat exchanger through high-pressure pump pressurization and form supercriticality, subsequently into being extracted in extractor Extract is obtained, then to adding green salt to be well mixed in extract, is dried after concentration, be cooled to room temperature, be subsequently adding day Right rubber cement is well mixed, and obtains Chinese medicine and refreshes oneself coating.
7. the preparation method of the high temperature resistant refreshing health-care straw mat according to claim any one of 1-6, it is characterised in that resistance to height Warm layer is prepared by following technique:By ethylene propylene diene rubber, epoxy resin, melamine resin, phenolic resin, APP, poly- Tetrafluoroethene, PCDL, IPDI, tricarboxylic propane tri, butyl titanate, first Ethyl triethoxy silicane alkane, toluene di-iso-cyanide ester, acrylic emulsion, sodium pyrophosphate, lauryl sodium sulfate and deionized water are added In mixer, 25-40min is stirred under low whipping speed 180-220r/min, be subsequently adding attapulgite, modified asbestos powder, receive Rice alchlor, mica powder, nano titanium oxide, modified additive, zinc stearate, hydroxyethyl cellulose, silane coupler KH- 560th, dispersant and diluent, 50-70min is stirred under low whipping speed 450-550r/min, with the silk screen mistake of the mesh of mesh number > 120 Filter, barrelling obtains high-temperature-resistant layer.
CN201611199935.2A 2016-12-22 2016-12-22 A kind of high temperature resistant refreshing health-care straw mat Pending CN106724471A (en)

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Application publication date: 20170531