CN106721892A - Propionic acid propionic acid sodium form Midew preventive for feed - Google Patents
Propionic acid propionic acid sodium form Midew preventive for feed Download PDFInfo
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- CN106721892A CN106721892A CN201710051568.XA CN201710051568A CN106721892A CN 106721892 A CN106721892 A CN 106721892A CN 201710051568 A CN201710051568 A CN 201710051568A CN 106721892 A CN106721892 A CN 106721892A
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- Prior art keywords
- propionic acid
- feed
- sodium
- midew preventive
- midew
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3481—Organic compounds containing oxygen
- A23L3/3499—Organic compounds containing oxygen with doubly-bound oxygen
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3472—Compounds of undetermined constitution obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3481—Organic compounds containing oxygen
- A23L3/3508—Organic compounds containing oxygen containing carboxyl groups
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/358—Inorganic compounds
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Nutrition Science (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
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- Inorganic Chemistry (AREA)
- Fodder In General (AREA)
Abstract
Propionic acid propionic acid sodium form Midew preventive for feed of the present invention, including propionic acid and sodium propionate, wherein, the mass ratio of propionic acid and sodium propionate is：20‑75:3‑30.The present invention also provides another propionic acid propionic acid sodium form Midew preventive for feed, and the Midew preventive for feed is made up of each component of following mass parts, one or more combination 1 20 in NaOH, sodium carbonate and sodium acid carbonate, propionic acid 22 80, white carbon 0 35, inserts 0 50.Propionic acid propionic acid sodium form Midew preventive for feed of the present invention has the advantages that stability is high, controlled release ability strong, good palatability, cost performance are high.
Description
Technical field
The invention belongs to feedstuff mildew technical field, more particularly to a kind of propionic acid-propionic acid sodium form Midew preventive for feed.
Background technology
Feed mold is a great problem for perplexing aquaculture.Feed mold can cause following massive losses：Seriously go mouldy
Raw material should not be used to produce feed, causes feed resource to waste；Livestock and poultry ingest after moldy feed, show anorexia and stop eating,
, there are various severe complications in growth inhibition, egg drop reduction, weak, anaemia, or even cause death, influence Animal husbandry production effect
Benefit；Mycotoxin is accumulated in animal body, causes mycotoxin content in human body to raise by food chain, serious to threaten the mankind to be good for
Health.
To prevent feed from being gone mouldy during storage, feed factory needs to add a certain amount of feed to prevent in feed
Mould dose.What consumption was maximum now is propionic acid type mould inhibitor, and its formula composition is propionic acid, propionic acid ammonium, adsorbent, diluent.
Propionic acid is a kind of volatile fatty acid, is colourless transparent liquid, with penetrating odor, soluble in water, ethanol etc.
Solvent.Because the volatility of propionic acid is stronger, individually addition propionic acid when, its mould proof time is short, thus in Midew preventive for feed often with
Propionic acid is added with the mode of the mixture of propionic acid ammonium.Propionic acid ammonium persistently can dissociate propionic acid to play mould proof work in acid condition
With.
On the one hand propionic acid ammonium can play mildew-proof function with hydrolysis propionic acid, and on the other hand, propionic acid ammonium can slow down free third
The volatilization of acid, extends the action time of propionic acid.But, there are following two aspects using propionic acid-propionic acid ammonium type Midew preventive for feed
Defect：
1st, pellet in process of production, can be by quenched granulation link, and temperature needed for this link is 70-90 DEG C.Third
45 DEG C of sour ammonium fusing point, starts to decompose when being heated to 70 DEG C.Therefore, propionic acid ammonium can be lost in quenched pelletization.Third
After sour ammonium loss, the ability for slowing down free propionic acid volatilization dies down, and causes mould proof less able.
2nd, ammonia is discharged when propionic acid ammonium is decomposed, there is ammonia stink, influence the palatability of feed.
The content of the invention
To solve the problem above that existing propionic acid-propionic acid ammonium type Midew preventive for feed is present, the present invention proposes a kind of propionic acid-the third
Sour sodium form Midew preventive for feed.
Propionic acid of the present invention-propionic acid sodium form Midew preventive for feed, including propionic acid and sodium propionate, wherein, the matter of propionic acid and sodium propionate
Measuring ratio is：20-75:3-30.
Preferably, propionic acid of the present invention-propionic acid sodium form Midew preventive for feed also includes white carbon.
Preferably, propionic acid of the present invention-propionic acid sodium form Midew preventive for feed is made up of each component of following mass parts, propionic acid 20-
75, sodium propionate 3-30, white carbon 0-35, inserts 0-50.
Preferably, the inserts in propionic acid of the present invention-propionic acid sodium form Midew preventive for feed is water, sodium sulphate, sodium chloride, wheat meal
One or more combination in stone, zeolite powder, montmorillonite, chaff powder.
Preferably, propionic acid of the present invention-propionic acid sodium form Midew preventive for feed is made up of each component of following mass parts, propionic acid 50,
Sodium propionate 10, white carbon 30, zeolite powder 10.
In actual production, sodium propionate can be obtained by raw material reactions such as propionic acid and NaOH, sodium carbonate or sodium acid carbonates.Cause
This, the present invention also provides another propionic acid-propionic acid sodium form Midew preventive for feed, the Midew preventive for feed by following mass parts each component
Constitute, one or more combination 1-20, propionic acid 22-80, white carbon 0-35 in NaOH, sodium carbonate and sodium acid carbonate are filled out
Charge 0-50.
Preferably, the inserts in propionic acid of the present invention-propionic acid sodium form Midew preventive for feed is water, sodium sulphate, sodium chloride, wheat meal
One or more in stone, zeolite powder, montmorillonite, chaff powder.
Preferably, propionic acid of the present invention-propionic acid sodium form Midew preventive for feed is made up of each component of following mass parts, propionic acid 45,
NaOH 5, white carbon 25, sodium chloride 25.
Propionic acid of the present invention-propionic acid sodium form Midew preventive for feed has the following advantages that：
1st, stability is high.After replacing propionic acid ammonium using sodium propionate, the propionic acid ammonium thermal instability of itself is overcome, made whole
The heat endurance of product is higher.
2nd, controlled release ability is strong.Sodium propionate is dissolved among propionic acid, can form double sodium propionate structures.This kind of structure can have
Effect slows down the volatilization of propionic acid itself.By adjusting the ratio between sodium propionate and propionic acid, it is possible to achieve speed of being volatilized to propionic acid
The regulation of rate.
3rd, good palatability.Propionic acid-propionic acid sodium form mould inhibitor does not have ammonia stink, improves palatability.Sodium propionate is to propionic acid simultaneously
Slow-release capability more preferably, when the mass ratio of sodium propionate and propionic acid is higher, product only has faint tart flavour.
4th, cost performance is high.Propionic acid-propionic acid sodium form mould inhibitor improve propionic acid-propionic acid ammonium type mould inhibitor stability while not
Increase cost, still there is propionic acid-propionic acid ammonium type high performance-price ratio.
Specific embodiment
Embodiment 1
A kind of propionic acid-propionic acid sodium form Midew preventive for feed, is made up of, propionic acid 75, sodium propionate 30 each component of following mass parts.
The anti-mold effect ratio of embodiment 1 improves 22% by propionic acid 75, the mould inhibitor of the composition of propionic acid ammonium 30.
Embodiment 2
A kind of propionic acid-propionic acid sodium form Midew preventive for feed, is made up of, propionic acid 20, sodium propionate 3 each component of following mass parts.
The anti-mold effect ratio of embodiment 2 improves 20% by propionic acid 20, the mould inhibitor of the composition of propionic acid ammonium 3.
Embodiment 3
A kind of propionic acid-propionic acid sodium form Midew preventive for feed, is made up of, propionic acid 50, sodium propionate 15 each component of following mass parts.
The anti-mold effect ratio of embodiment 3 improves 32% by propionic acid 50, the mould inhibitor of the composition of propionic acid ammonium 15.
Embodiment 4
A kind of propionic acid-propionic acid sodium form Midew preventive for feed, is made up of, propionic acid 55, sodium propionate 10 each component of following mass parts,
White carbon 35.The anti-mold effect ratio of embodiment 4 is improved by propionic acid 55, propionic acid ammonium 10, the mould inhibitor effect of the composition of white carbon 35
25%.
Embodiment 5
A kind of propionic acid-propionic acid sodium form Midew preventive for feed, is made up of, propionic acid 30, sodium propionate 5 each component of following mass parts,
White carbon 15, sodium chloride 50.
Embodiment 6
A kind of propionic acid-propionic acid sodium form Midew preventive for feed, is made up of, propionic acid 40, sodium propionate 10 each component of following mass parts,
White carbon 25, medical stone 25.
Embodiment 7
A kind of propionic acid-propionic acid sodium form Midew preventive for feed, is made up of, propionic acid 45, NaOH each component of following mass parts
5, white carbon 25, sodium chloride 25.
Embodiment 8
A kind of propionic acid-propionic acid sodium form Midew preventive for feed, is made up of, propionic acid 60, sodium carbonate 10 each component of following mass parts,
White carbon 30, montmorillonite 5.
Embodiment 9
A kind of propionic acid-propionic acid sodium form Midew preventive for feed, is made up of, propionic acid 35, sodium acid carbonate each component of following mass parts
10, white carbon 20, chaff powder 40.
Embodiment 5- embodiments 9, on the basis of preferable anti-mold effect is ensured, can preferable reduces cost, cost performance is high.
Contrast test (one)：
1. experimental program
Propionic acid group, propionic acid-propionic acid ammonium group, propionic acid-sodium propionate group (embodiment 4) are set up in experiment.
The Midew preventive for feed of propionic acid group, is made up of each component of following mass parts, propionic acid 55, sodium sulphate 10, white carbon 35.
The Midew preventive for feed of propionic acid-propionic acid ammonium group, is made up of, propionic acid 55, propionic acid ammonium 10, in vain each component of following mass parts
Carbon black 35.
The Midew preventive for feed of propionic acid-sodium propionate group (embodiment 4), is made up of, propionic acid 55, third each component of following mass parts
Sour sodium 10, white carbon 35.
Every group weighs the sample of identical weight in the measuring cup of same size.Measuring cup is placed in 40 DEG C, 80 DEG C of baking
In case, weigh at regular intervals, calculate each group weight loss percentage.
2. experimental data
(1) 40 DEG C, weighed once per 30min.
(2) 80 DEG C, weighed once per 5min.
3. experimental result
A. weight loss percentage：Propionic acid-sodium propionate group ＜ propionic acid-propionic acid ammonium group ＜ propionic acid groups.
B. what weight loss percentage reacted is the speed of propionic acid volatilization, and loss late is smaller, illustrates the controlled release energy to propionic acid
Power is stronger.This description of test sodium propionate is better than propionic acid ammonium to the controlled release ability of propionic acid.
Contrast test (two)：
1. propionic acid group, propionic acid-propionic acid ammonium group, propionic acid-sodium propionate group (embodiment 4) are set up in experiment.The feed of propionic acid group is prevented
Mould dose, it is made up of each component of following mass parts, propionic acid 65, white carbon 35.
The Midew preventive for feed of propionic acid-propionic acid ammonium group, is made up of, propionic acid 55, propionic acid ammonium 10, in vain each component of following mass parts
Carbon black 35.
The Midew preventive for feed of propionic acid-sodium propionate group (embodiment 4), is made up of, propionic acid 55, third each component of following mass parts
Sour sodium 10, white carbon 35.
2. experimental program
(1) material prepares
The feedstuff mildew of feed corn flour (moisture 12.67%), the Midew preventive for feed of propionic acid group, propionic acid-propionic acid ammonium group
Agent, propionic acid-sodium propionate group (embodiment 4).
(2) experiment process
(3) experimental technique is quick, accurately weigh 0.2g (being accurate to 0.001g) mould inhibitors in clean valve bag, adds
200g corn flour, is all transferred in the transparent wide-mouth bottles of 500ml after mixing.Wide-mouth bottle is sealed with identical napkin paper, and rubber band is pricked
Tightly, label.Five repetitions are done in each treatment.
In mold incubator by all wide-mouth bottles as 33 ± 2 DEG C.Incubator middle berth wet towel, keeps air relatively wet
Degree ＞ 80%.Situation in wide-mouth bottle is observed daily, and is recorded.
2. Germicidal efficacy record sheet
Chart example：√ --- normal, O --- caking ,+--- it is mouldy.Quantity is more, represents that degree is more serious.
3rd, experimental result
By data above it can be seen that：There is caking at the 7th day in blank group, Signs of Mould occurred within the 9th day, and the 12nd day
Seriously go mouldy；There is caking and Signs of Mould at the 12nd day in propionic acid group, seriously went mouldy within the 13rd day；Propionic acid-propionic acid ammonium group is
There is caking and Signs of Mould within 13 days, seriously go mouldy within the 14th day；Propionic acid-sodium propionate group (embodiment 4) occurred light at the 16th day
Micro- caking and Signs of Mould.It can be seen that, mould proof ability：Propionic acid-sodium propionate group ＞ propionic acid-propionic acid ammonium group ＞ propionic acid ammonium group ＞ blank
Group.
The above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted, although with reference to preferred embodiment to this hair
It is bright to be described in detail, it will be understood by those within the art that, technical scheme can be modified
Or equivalent, without deviating from the objective and scope of technical solution of the present invention, it all should cover in claim of the invention
In the middle of scope.
Claims (8)
1. propionic acid-propionic acid sodium form Midew preventive for feed, it is characterised in that the Midew preventive for feed includes propionic acid and sodium propionate, also, third
Acid and the mass ratio of sodium propionate are：20-75:3-30.
2. Midew preventive for feed according to claim 1, it is characterised in that the Midew preventive for feed also includes white carbon.
3. Midew preventive for feed according to claim 2, it is characterised in that the Midew preventive for feed is each by following mass parts
Component is constituted, propionic acid 20-75, sodium propionate 3-30, white carbon 0-35, inserts 0-50.
4. Midew preventive for feed according to any one of claim 1 to 3, it is characterised in that the inserts is water, sulfuric acid
One or more combination in sodium, sodium chloride, medical stone, zeolite powder, montmorillonite, chaff powder.
5. Midew preventive for feed according to claim 4, it is characterised in that the Midew preventive for feed is each by following mass parts
Component is constituted, propionic acid 50, sodium propionate 10, white carbon 30, zeolite powder 10.
6. propionic acid-propionic acid sodium form Midew preventive for feed, it is characterised in that the Midew preventive for feed by following mass parts each component structure
Into one or more combination 1-20, propionic acid 22-80, white carbon 0-35 in NaOH, sodium carbonate and sodium acid carbonate, filling
Material 0-50.
7. the Midew preventive for feed described in claim 6, it is characterised in that the inserts is water, sodium sulphate, sodium chloride, wheat
One or more in meal stone, zeolite powder, montmorillonite, chaff powder.
8. Midew preventive for feed according to claim 7, it is characterised in that the Midew preventive for feed is each by following mass parts
Component is constituted, propionic acid 45, NaOH 5, white carbon 25, sodium chloride 25.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710051568.XA CN106721892A (en) | 2017-01-20 | 2017-01-20 | Propionic acid propionic acid sodium form Midew preventive for feed |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710051568.XA CN106721892A (en) | 2017-01-20 | 2017-01-20 | Propionic acid propionic acid sodium form Midew preventive for feed |
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| Publication Number | Publication Date |
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| CN106721892A true CN106721892A (en) | 2017-05-31 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201710051568.XA Pending CN106721892A (en) | 2017-01-20 | 2017-01-20 | Propionic acid propionic acid sodium form Midew preventive for feed |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110973443A (en) * | 2019-12-23 | 2020-04-10 | 宜兴市天石饲料有限公司 | Propionic acid and sodium propionate type Chinese herbal medicine mildew preventive and preparation method thereof |
| CN112106917A (en) * | 2020-09-25 | 2020-12-22 | 重庆民泰新农业科技发展集团有限公司 | Feed slow-release mildew inhibitor and using method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1656945A (en) * | 2004-12-16 | 2005-08-24 | 国龙科技饲料(上海)有限公司 | Liquid feed additive coating technology |
| CN1961720A (en) * | 2006-11-30 | 2007-05-16 | 上海交通大学 | Mold-proof oxidation-resistant compound additive |
| CN101731451A (en) * | 2010-01-21 | 2010-06-16 | 鲁昊 | Compound mouldproof agent with acidizing effect and preparation method thereof |
| CN105341360A (en) * | 2015-12-07 | 2016-02-24 | 重庆华睿隆生物科技有限公司 | Carrier-free propionic acid solid feed mildew preventive and preparation and use thereof |
| CN106036034A (en) * | 2016-05-20 | 2016-10-26 | 四川爱客信生物科技有限公司 | Mixed liquid additive for feed and preparation method of mixed liquid additive |
-
2017
- 2017-01-20 CN CN201710051568.XA patent/CN106721892A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1656945A (en) * | 2004-12-16 | 2005-08-24 | 国龙科技饲料(上海)有限公司 | Liquid feed additive coating technology |
| CN1961720A (en) * | 2006-11-30 | 2007-05-16 | 上海交通大学 | Mold-proof oxidation-resistant compound additive |
| CN101731451A (en) * | 2010-01-21 | 2010-06-16 | 鲁昊 | Compound mouldproof agent with acidizing effect and preparation method thereof |
| CN105341360A (en) * | 2015-12-07 | 2016-02-24 | 重庆华睿隆生物科技有限公司 | Carrier-free propionic acid solid feed mildew preventive and preparation and use thereof |
| CN106036034A (en) * | 2016-05-20 | 2016-10-26 | 四川爱客信生物科技有限公司 | Mixed liquid additive for feed and preparation method of mixed liquid additive |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110973443A (en) * | 2019-12-23 | 2020-04-10 | 宜兴市天石饲料有限公司 | Propionic acid and sodium propionate type Chinese herbal medicine mildew preventive and preparation method thereof |
| CN112106917A (en) * | 2020-09-25 | 2020-12-22 | 重庆民泰新农业科技发展集团有限公司 | Feed slow-release mildew inhibitor and using method thereof |
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Application publication date: 20170531 |