CN106706069A - Ammonia mother liquid barrel liquid level measuring system - Google Patents

Ammonia mother liquid barrel liquid level measuring system Download PDF

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Publication number
CN106706069A
CN106706069A CN201510794867.3A CN201510794867A CN106706069A CN 106706069 A CN106706069 A CN 106706069A CN 201510794867 A CN201510794867 A CN 201510794867A CN 106706069 A CN106706069 A CN 106706069A
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CN
China
Prior art keywords
liquid level
ammonia mother
measuring system
heating tube
level measuring
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510794867.3A
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Chinese (zh)
Inventor
于勇
余科
刘庆庆
朱松明
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zigong Innovation Center of Zhejiang University
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Zigong Innovation Center of Zhejiang University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zigong Innovation Center of Zhejiang University filed Critical Zigong Innovation Center of Zhejiang University
Priority to CN201510794867.3A priority Critical patent/CN106706069A/en
Publication of CN106706069A publication Critical patent/CN106706069A/en
Pending legal-status Critical Current

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Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01FMEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F23/00Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm
    • G01F23/14Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measurement of pressure

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  • Physics & Mathematics (AREA)
  • Fluid Mechanics (AREA)
  • General Physics & Mathematics (AREA)
  • Investigating Or Analyzing Materials Using Thermal Means (AREA)

Abstract

An ammonia mother liquid barrel liquid level measuring system comprises a single-flange liquid level transmitter and is characterized by further comprising a DCS control system and a heating device. An output end of the DCS control system is connected with the heating device, an input end of the DCS control system is connected with a thermal resistor, and the thermal resistor is arranged on the outer side of a connection pipe connected with the single-flange liquid level transmitter. By the heating device for heating the connection pipe, a non-frozen state of ammonia mother liquid is guaranteed, frosting of the ammonia mother liquid at a diaphragm of the single-flange liquid level transmitter at a low temperature is avoided, effectiveness of the single-flange liquid level transmitter in liquid level measurement of the ammonia mother liquid is guaranteed, mother liquid leakage is avoided, and accordingly harms to personnel and equipment are avoided. Starting and stopping of the heating device are controlled by the DCS control system, automatic control in heating of the connection pipe is realized, and equipment can be maintained by workers conveniently.

Description

Ammonia mother vat liquid level measuring system
Technical field
The present invention relates to liquid level emasuring device in a kind of soda manufacture, more particularly to a kind of ammonia mother vat liquid level is surveyed Amount protection system.
Background technology
Fluid level transmitter is a kind of in-situ transducer being directly installed on pipeline or container.Due to isolation diaphragm Directly it is in contact with liquid medium, is drawn with connecting pipe without by positive pressure side, therefore high temperature, height can be measured Viscosity, easily crystallization, the easily liquid level of precipitation and the medium such as deep-etching, pressure and density, it is then converted into 4~ 20mA.DC signal outputs.
During soda manufacture, the mother liquor in ammonia mother vat once leaks, and will cause the damage of personnel and equipment. The current measurement to liquid level commonly uses single flange liquid level transmission device and measures.Single flange liquid level transmission device is According to pressure sensitive principle, the height of current liquid is calculated by the change of the densitometer pressure of liquid, But when running in winter, due to mother liquor, usually frosting at transducer diaphragm, causes the liquid level cannot to this kind of transmitter Measurement, can carry out great hidden danger to the continuous operation of production and safety belt.
In order to solve this problem, when designing a kind of low temperature can normal work liquid level emasuring device, it is ensured that it is raw The normal operation and equipment, personal safety produced.
The content of the invention
The present invention provides a kind of ammonia mother vat liquid level measuring system, it is therefore an objective to solve prior art problem, there is provided It is a kind of will not frosting causes what liquid level cannot be measured at the diaphragm of fluid level transmitter due to mother liquor when temperature is low Liquid level measuring system, the system solves problem of the prior art well.
The technical scheme that solve problem of the present invention is used is:
Ammonia mother vat liquid level measuring system, comprising single flange liquid level transmission device, also including DCS control systems and plus Thermal.The DCS control systems output end connects heater, input connection thermal resistor, thermal resistance It is arranged on the adapter outside being connected with single flange liquid level transmission device.
The heater is heater strip, and heater strip is arranged on adapter outside or is taken over around being located at.
The heater is heating tube, and steam electromagnetic valve is arranged on the admission end of heating tube, heating tube Exhaust steam end is provided with condensate drain valve, and wherein steam electromagnetic valve is connected with DCS control system output ends, and steam electricity Heating tube portion between magnet valve and condensate drain valve is arranged on the adapter outside being connected with single flange liquid level transmission device Or in adapter.
Two branch roads of the heating tube of parallel connection, two friendships of branch road are provided between steam electromagnetic valve and condensate drain valve Connect position and be provided with threeway or triple valve, at least one branch road is arranged in adapter outside or adapter.
One of branch road around be located at adapter on.
The heating tube is carbon steel pipe.
Beneficial effects of the present invention:
1. firing equipment is provided with (as passed through heating tube or electrical heating using high steam in adapter in the present invention Silk) butt tube heated, it is ensured that and ammonia mother liquor is in non-frozen state, it is to avoid ammonia mother liquor exists when temperature is low Frosting at the diaphragm of single flange liquid level transmission device, it is ensured that it is female that single flange liquid level transmission device can effectively measure ammonia The liquid level of liquid, it is to avoid mother liquor leaks, and then avoids causing the damage of personnel and equipment.
2. the unlatching of firing equipment controlled by DCS control systems in the present invention, closed, realize butt tube The Automated condtrol of heating, while facilitating staff to repair equipment.
Brief description of the drawings
Fig. 1 is structural representation of the invention;
Fig. 2 is structural representation of the invention two.
In figure:100. ammonia mother vats, 1. single flange liquid level transmission device, 2.DCS control systems, 3. heater strip, 5. thermal resistance, 6. adapter;30. steam electromagnetic valves, 40. heating tubes, 41. heating tube branch roads, 50. condensate drain valves, 60. threeways, 70. triple valves.
Specific embodiment
The present invention is described in further details below in conjunction with the drawings and specific embodiments.
Embodiment 1
Ammonia mother vat liquid level measuring system as shown in Figure 1, comprising single flange liquid level transmission device 1, DCS Control system 2 and heater, the heater used in the present embodiment are heater strip 3, are a kind of electrical heating Device.The output end of DCS control systems 2 connects heater strip 3, input connection thermal resistor 5.Due to this The purpose of measuring system is to ensure that the low temperature condition flange liquid level transmission device 1 that places an order can also work, i.e., to ensure Ammonia mother liquor is in non-frozen state, and single flange liquid level transmission device 1 is by adapter 6 and ammonia mother liquor when using Bucket 100 is connected with each other, therefore thermal resistance 5 is arranged on the outside of adapter 6, is used to detect ammonia mother liquor peripheral environment Temperature, it is ensured that ammonia mother liquor does not freeze.
The effect of above-mentioned heater in order to be heated to ammonia mother liquor, to avoid ammonia mother liquor from freezing, Ke Yishe Put in the outside of adapter 6, it is also possible to be set directly in adapter 6, how to set depending on using which kind of heating Device.Electric heater unit is except the heater strip in the present embodiment, it is also possible to according to circumstances using any applicable Electric heater unit.It is heater that heating wire 3 is used in the present embodiment, one be it is with low cost, two be can It is wrapped in adapter 6 with by heater strip, effectively ammonia mother liquor is heated.
Specific work process is as described below:Thermal resistance 5 detects the environment temperature of adapter 6, and temperature data is transmitted To in DCS control systems, what a temperature value is previously set in DCS control systems, when less than setting During temperature value, i.e., when ammonia mother liquor will freeze, DCS control systems control heater strip 3 is heated, ammonia mother liquor Liquid body is maintained at, single flange liquid level transmission device 1 being capable of normal work.When the temperature value higher than setting, When there is accident to avoid ammonia mother liquor temperature too high, DCS control systems control heater strip 3 stops heating.It is whole Individual system is automatically controlled by DCS control systems, not only effectively solves single flange liquid level transmission device in the winter The problem of cisco unity malfunction, also achieves automated production under the low temperature conditions such as season.
Embodiment 2
Ammonia mother vat liquid level measuring system as shown in Figure 2, in addition to heater difference, miscellaneous part is equal Identical, the heater in the present embodiment is heating tube, concrete structure:Comprising single flange liquid level transmission device 1, DCS control systems 2, the one end of DCS control systems 2 connection steam electromagnetic valve 30, other end connection thermal resistor 5. The steam electromagnetic valve 30 is arranged on the admission end of heating tube 40, and the exhaust steam end of heating tube 40 is provided with condensate drain Valve 50, being arranged on for heating tube portion between steam electromagnetic valve 30 and condensate drain valve 50 becomes with single flange liquid level Send on the outside of adapter 6 or adapter 6 that device 1 is connected, thermal resistance 5 is arranged on the outside of adapter 6.
In order to preferably be heated to ammonia mother liquor, in steam electromagnetic valve 30 and condensate drain valve 50 in the present embodiment Between be provided with two branch roads of the heating tube of parallel connection 41, one of branch road 41 is another around being located in adapter 6 Individual branch road 41 is arranged on the outside of adapter 6, and threeway 60 is provided with two delivery positions of heating tube branch road 41 one, Another place is provided with triple valve 70.
Due to being heated to ammonia mother liquor using high-temperature steam in the present embodiment, and in order to preferably by heating tube Around being located in adapter 6, heating tube uses carbon steel pipe.
Thermal resistance 5 and the composition thermostat unit of steam electromagnetic valve 30, high-temperature steam pass through thermostat unit It is connected with DCS control systems 2 by communication line, through the good humidity control system of DCS set-up of control system After open or close steam electromagnetic valve 30, heat tracing is carried out to flange liquid level transmission device 1 and adapter 6, it is ensured that ammonia Mother liquor is in non-frozen state, flange liquid level transmission device 1 is measured liquid level.
During initial launch, the condensate liquid in the discharge line of condensate drain valve 50 is opened, be then shut off condensate drain valve 50.Heat The temperature that resistance 5 is detected is less than the setting value of DCS control systems 2, is controlled automatically by DCS control systems 2 Steam electromagnetic valve 30 is opened in system output, and high-temperature steam is conveyed in the pipeline to heating tube 40, and flange liquid level is become Device 1, ammonia mother liquor, adapter 6 is sent to be heated, after thermal resistance 5 detects temperature reaches setting value, by DCS control systems 2 automatically control steam off magnetic valve 30, are carried out by the high-temperature steam retained in heating tube Heat tracing.When below temperature drop to setting value, DCS control systems controlled output opens steam electromagnetic valve 30 Setting value is heated to heating tube conveying steam, is carried out with this rule later.
The advantage of this scheme is to be capable of achieving the automatic heating to pipeline, it is ensured that transmitter can accurately be determined Level value;Personnel can be maintained easily to safeguard faulty meter (transmitter).When needing to safeguard, only Need to by operating DCS control system steam off magnetic valves, after just operable after temperature drop, it is to avoid length Pipeline of the phase after steam is heated easily scalds attendant in the condition of high temperature.Meanwhile, it is automatic right to be capable of achieving The heat tracing of pipeline and instrument, thermal resistance is detected after temperature is less than setting value and just can set by DCS control systems Put and automatically open up steam electromagnetic valve heating, heating is just stopped after reaching setting value, treat temperature drop to setting value After be again started up steam heating.

Claims (6)

1. ammonia mother vat liquid level measuring system, comprising single flange liquid level transmission device, it is characterised in that:Also include DCS Control system and heater;The DCS control systems output end connects heater, input connection heat Resistance, thermal resistance is arranged on the adapter outside being connected with single flange liquid level transmission device.
2. ammonia mother vat liquid level measuring system as described in claim 1, it is characterised in that:The heater It is heater strip, heater strip is arranged on adapter outside or is taken over around being located at.
3. ammonia mother vat liquid level measuring system as described in claim 1, it is characterised in that:The heater It is heating tube, steam electromagnetic valve is arranged on the admission end of heating tube, the exhaust steam end of heating tube is provided with condensate drain valve, Wherein steam electromagnetic valve is connected with DCS control system output ends, and between steam electromagnetic valve and condensate drain valve Heating tube portion be arranged on be connected with single flange liquid level transmission device adapter outside or take on.
4. ammonia mother vat liquid level measuring system as described in claim 3, it is characterised in that:In steam electromagnetic valve Be provided with two branch roads of the heating tube of parallel connection and condensate drain valve between, the delivery position of two branch roads be provided with threeway or Triple valve, at least one branch road is arranged in adapter outside or adapter.
5. ammonia mother vat liquid level measuring system as described in claim 4, it is characterised in that:One of branch road Taken over around being located at.
6. ammonia mother vat liquid level measuring system as described in claim 3, it is characterised in that:The heating tube is Carbon steel pipe.
CN201510794867.3A 2015-11-18 2015-11-18 Ammonia mother liquid barrel liquid level measuring system Pending CN106706069A (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
CN201510794867.3A CN106706069A (en) 2015-11-18 2015-11-18 Ammonia mother liquid barrel liquid level measuring system

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CN106706069A true CN106706069A (en) 2017-05-24

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109253775A (en) * 2018-11-22 2019-01-22 佛山高富中石油燃料沥青有限责任公司 A kind of transition apparatus of high-viscosity high-elasticity chemical liquor and easy coking level gauging

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CN101441485A (en) * 2007-11-19 2009-05-27 中国石化扬子石油化工有限公司 Temperature control method of mother liquor pipeline conveying of slurry method HDPE apparatus
DE102008031645A1 (en) * 2008-07-04 2010-01-14 Continental Automotive Gmbh Liquid level sensor for sensing liquid level sensor of tank, has withdrawal pipe for withdrawing fluid from tank, and has controlling and evaluating device
CN201574089U (en) * 2009-11-20 2010-09-08 重庆泰丰泰兴化工有限责任公司 Ammonia recovery reboiler
CN102564514A (en) * 2012-02-10 2012-07-11 北京中油联自动化技术开发有限公司 Electronic fusion measurement liquid level transmitter and measurement method thereof
CN203061028U (en) * 2012-07-23 2013-07-17 江苏晋煤恒盛化工股份有限公司 Liquid level measurement device for decarburization tower
CN203090744U (en) * 2013-03-28 2013-07-31 成都锐思环保技术有限责任公司 Steam direct-heating liquid ammonia evaporation process control system for flue gas denitration
CN203346361U (en) * 2013-05-21 2013-12-18 河北钢铁股份有限公司唐山分公司 Device for extracting desulfuration foam with coking wet method
CN103979575A (en) * 2014-05-16 2014-08-13 北京博智伟德环保科技有限公司 System and control method for producing ammonia gas by hydrolyzing urea solution
CN203811232U (en) * 2014-02-25 2014-09-03 重庆华彩化工有限责任公司 Ammonia water level measuring device
CN205176695U (en) * 2015-11-18 2016-04-20 浙江大学自贡创新中心 Ammonia mother vat liquid level measurement system

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CN101441485A (en) * 2007-11-19 2009-05-27 中国石化扬子石油化工有限公司 Temperature control method of mother liquor pipeline conveying of slurry method HDPE apparatus
DE102008031645A1 (en) * 2008-07-04 2010-01-14 Continental Automotive Gmbh Liquid level sensor for sensing liquid level sensor of tank, has withdrawal pipe for withdrawing fluid from tank, and has controlling and evaluating device
CN201574089U (en) * 2009-11-20 2010-09-08 重庆泰丰泰兴化工有限责任公司 Ammonia recovery reboiler
CN102564514A (en) * 2012-02-10 2012-07-11 北京中油联自动化技术开发有限公司 Electronic fusion measurement liquid level transmitter and measurement method thereof
CN203061028U (en) * 2012-07-23 2013-07-17 江苏晋煤恒盛化工股份有限公司 Liquid level measurement device for decarburization tower
CN203090744U (en) * 2013-03-28 2013-07-31 成都锐思环保技术有限责任公司 Steam direct-heating liquid ammonia evaporation process control system for flue gas denitration
CN203346361U (en) * 2013-05-21 2013-12-18 河北钢铁股份有限公司唐山分公司 Device for extracting desulfuration foam with coking wet method
CN203811232U (en) * 2014-02-25 2014-09-03 重庆华彩化工有限责任公司 Ammonia water level measuring device
CN103979575A (en) * 2014-05-16 2014-08-13 北京博智伟德环保科技有限公司 System and control method for producing ammonia gas by hydrolyzing urea solution
CN205176695U (en) * 2015-11-18 2016-04-20 浙江大学自贡创新中心 Ammonia mother vat liquid level measurement system

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109253775A (en) * 2018-11-22 2019-01-22 佛山高富中石油燃料沥青有限责任公司 A kind of transition apparatus of high-viscosity high-elasticity chemical liquor and easy coking level gauging

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Application publication date: 20170524

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