CN106693462A - Third-phase cleaning device with copper solvent extraction clarifying chamber - Google Patents
Third-phase cleaning device with copper solvent extraction clarifying chamber Download PDFInfo
- Publication number
- CN106693462A CN106693462A CN201611204670.0A CN201611204670A CN106693462A CN 106693462 A CN106693462 A CN 106693462A CN 201611204670 A CN201611204670 A CN 201611204670A CN 106693462 A CN106693462 A CN 106693462A
- Authority
- CN
- China
- Prior art keywords
- phase
- clarifying chamber
- pipe
- mutually
- solvent extraction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/24—Feed or discharge mechanisms for settling tanks
- B01D21/245—Discharge mechanisms for the sediments
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/0006—Settling tanks provided with means for cleaning and maintenance
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/02—Settling tanks with single outlets for the separated liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/087—Cleaning containers, e.g. tanks by methods involving the use of tools, e.g. brushes, scrapers
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Abstract
The invention discloses a third-phase cleaning device with a copper solvent extraction clarifying chamber. The third-phase cleaning device comprises the clarifying chamber, wherein a third-phase aggregation structure is arranged in the clarifying chamber and comprises a hollow phase guiding pipe, the lower end of the phase guiding pipe extends into a solution of the clarifying chamber, a phase guiding gap is reserved at the lower end of the phase guiding pipe and the bottom of the clarifying chamber, and a scrapping plate group is fixedly arranged at the lower end of the phase guiding pipe. The upper end of the phase guiding pipe extends out of the solution of the clarifying chamber, the upper end of the phase guiding pipe is connected with a hose pump through a guiding-out pipe, the hose pump of the guiding-out pipe is connected with a stirring tank, the lower portion of the stirring tank is connected with a third-phase storage tank through a discharging pipe, and the upper portion of the stirring tank is sequentially in serial connection with a filter pressing pump, a filter pressing machine and an organic phase storage tank through a treating pipe. A third phase deposing at the bottom of the clarifying chamber can be clarified under the condition that extracting operation is not affected.
Description
Technical field
A kind of third phase the invention belongs to copper solvent extraction technical field, more particularly to copper solvent extraction clarifying chamber is cleared up
Device.
Background technology
The not miscible Second Organic Phase formed between organic phase and water phase in third phase, i.e. solvent extraction process.
The formation of third phase has a many reasons, and such as Extraction Complexes solubility in diluent is small and separate out, and extractant is in diluent
Solubility is small, temperature reduction, forms various complexs etc..Third phase is inevitable during copper solvent extraction, and the of formation
Three-phase is deposited on depositing reservoir bottom, and the presence of third phase destroys extraction process, therefore to try to eliminate.Existing third phase is clear
Reason mode can influence to compare, influence split-phase, and can cause the entrainment caused by cleaning third phase, bring loss.
The content of the invention
It is an object of the invention to provide a kind of third phase cleaning plant of copper solvent extraction clarifying chamber, can not influence
Under extraction ruuning situation, cleaning is deposited on the third phase of clarifying chamber bottom.
In order to solve the above technical problems, the present invention is adopted the following technical scheme that：The third phase of copper solvent extraction clarifying chamber is clear
Reason device, including clarifying chamber, are provided with third phase aggregated structure in the clarifying chamber, third phase aggregated structure draws phase including hollow
Pipe, the lower end for drawing mutually pipe stretched into the solution of clarifying chamber, and drawn the mutually lower end of pipe and remained with clarifying chamber bottom and draw phase gap, is drawn
The lower end of phase pipe is installed with scraper plate group, and scraper plate group is made up of multiple along the scraper plate for drawing the mutually uniform spread configuration in pipe periphery, often
Individual scraper plate is along drawing the axial arranged of mutually pipe, and each scraper plate lower edge is towards the downward-sloping setting in clarifying chamber bottom, each
The outer end of scraper plate lower edge abuts with clarifying chamber bottom, and the inner end of each scraper plate lower edge is concordant with the lower end for drawing mutually pipe right
Connect；The solution of clarifying chamber is stretched out in the upper end for drawing mutually pipe, and draws the upper end of mutually pipe and be connected with peristaltic pump, peristaltic pump by outgoing line
Export pipeline be connected with tank diameter, the bottom of tank diameter is connected with third phase storage tank, the top of tank diameter by discharge line
Filter pressing pump, filter press and organic phase storage tank have been sequentially connected in series by processing pipeline.
It is described draw be provided with mutually pipe dragging rope, dragging rope extend out to outside clarifying chamber.
The dragging rope is provided with two, and two dragging ropes are separately positioned on the opposite sides for drawing mutually pipe.
The outgoing line is flexible pipe.
Third phase thickness of the distance for drawing phase gap less than clarifying chamber bottom.
The scraper plate is provided with four.
The filter press is plate and frame type filter-press.
Beneficial effects of the present invention：
Third phase aggregated structure is slowly at the uniform velocity in moving process in the present invention, can ensureing not influence to compare, do not influence point
In the case of phase, high-efficiency accumulation three-phase, while low-frequency start peristaltic pump extracts third phase, effectively reduces the entrainment caused by third phase
Bring loss.
The present invention realizes that cleaning is deposited on the third phase of clarifying chamber bottom, Er Qieqing in the case where extraction ruuning situation is not influenceed
The third phase managed is processed again, realizes resource reclaim, it is to avoid the wasting of resources, and handling process is as follows again：Extract
Third phase in the tank diameter after stirring precipitation, bottom material is directed to third phase storage tank, and top mixture is through overvoltage
Filter pump feeding filter press carries out separation of solid and liquid, and the organic phase after separation imported into organic phase storage tank.
It is described draw be provided with mutually pipe dragging rope, dragging rope extend out to outside clarifying chamber, dragging rope be provided with two,
Two dragging ropes are separately positioned on the opposite sides for drawing mutually pipe.Because the area of copper solvent extraction clarifying chamber is larger, what dragging was restricted sets
Put and be easy to the artificial traction outside clarifying chamber to draw mutually to manage, convenient working.The outgoing line selects flexible pipe, and mutually pipe traction is drawn in reduction
When obstruction, convenient operation.The distance for drawing phase gap is further ensured that not shadow less than the third phase thickness of clarifying chamber bottom
Sound is compared, does not influence split-phase.
Brief description of the drawings
Fig. 1 is process principle figure of the invention；
Fig. 2 is the structural representation at clarifying chamber position in the present invention
Fig. 3 is the structural representation of third phase aggregated structure in the present invention.
Specific embodiment
Specific embodiment of the invention is elaborated below in conjunction with accompanying drawing, the direction of arrow represents medium flow field in figure
To.
As shown in Figure 1 to Figure 3, the third phase cleaning plant of copper solvent extraction clarifying chamber of the invention, including clarifying chamber 1,
Third phase aggregated structure is provided with clarifying chamber 1, third phase aggregated structure draws mutually pipe 2 including hollow, and the lower end for drawing mutually pipe 2 is stretched into
In the solution of clarifying chamber 1, and draw the mutually lower end of pipe 2 and remained with the bottom of clarifying chamber 1 and draw phase gap, draw the lower end of mutually pipe 2
Scraper plate group is installed with, scraper plate group is made up of the scraper plate 3 that the mutually uniform spread configuration in the periphery of pipe 2 is drawn on four edges, four scraper plates 3 form X
Shape structure, each scraper plate 3 is along drawing the axial arranged of mutually pipe 2, and each lower edge of scraper plate 3 is downward towards the bottom of clarifying chamber 1
Be obliquely installed, the outer end of each lower edge of scraper plate 3 abuts with the bottom of clarifying chamber 1, the inner end of each lower edge of scraper plate 3 with draw
The lower end concordant docking of phase pipe 2；The solution of clarifying chamber 1 is stretched out in the upper end for drawing mutually pipe 2, and draws the upper end of mutually pipe 2 by delivery line
Road is connected with peristaltic pump 4, and the export pipeline of peristaltic pump 4 is connected with tank diameter 5, and the bottom of tank diameter 5 is connected by discharge line
The top for having third phase storage tank 6, tank diameter 5 has been sequentially connected in series filter pressing pump 7, filter press 8 and organic phase storage tank by processing pipeline
9。
It is described draw be provided with mutually pipe 2 dragging rope 10, dragging rope 10 is extended out to outside clarifying chamber 1.The dragging rope
10 are provided with two, and two dragging ropes 10 are separately positioned on the opposite sides for drawing mutually pipe 2.Because of the area of copper solvent extraction clarifying chamber
Larger, the setting of dragging rope 10 is easy to draw mutually pipe 2, convenient working in the outer artificial traction in clarifying chamber 1.
The distance for drawing phase gap less than the bottom of clarifying chamber 1 the thickness of third phase 11, be further ensured that do not influence compare,
Do not influence split-phase.
The outgoing line selects flexible pipe, and obstruction during the mutually traction of pipe 2, convenient operation are drawn in reduction.
The filter press selects plate and frame type filter-press.
In the present invention third phase aggregated structure under the traction of dragging rope 10 slowly at the uniform velocity moving, it is slow at the uniform velocity
High-efficiency accumulation three-phase is realized in moving process, and guarantee does not influence to compare, does not influence split-phase, while low-frequency start peristaltic pump 4
Third phase is extracted with mutually pipe is drawn through outgoing line, the entrainment caused by third phase is effectively reduced and is brought loss.
The present invention realizes that cleaning is deposited on the third phase of 1 Room bottom of clarification, Er Qieqing in the case where extraction ruuning situation is not influenceed
The third phase managed is processed again, realizes resource reclaim, it is to avoid the wasting of resources, and handling process is as follows again：Extract
Third phase in the tank diameter 5 after stirring precipitation, bottom material is directed to third phase storage tank 6, and top mixture passes through
The feeding filter press 8 of filter pressing pump 7 carries out separation of solid and liquid, and the organic phase after separation imported into organic phase storage tank 9.
Above example is only used to illustrative and not limiting technical scheme, although with reference to above-described embodiment to this hair
It is bright to be described in detail, it will be understood by those within the art that：Still the present invention can be modified or be waited
With replacement, any modification or partial replacement without departing from the spirit and scope of the present invention, it all should cover in power of the invention
In the middle of sharp claimed range.
Claims (7)
1. the third phase cleaning plant of copper solvent extraction clarifying chamber, including clarifying chamber, it is characterised in that：It is provided with the clarifying chamber
Third phase aggregated structure, third phase aggregated structure is mutually managed including hollow drawing, and the lower end for drawing mutually pipe is stretched into the solution of clarifying chamber,
And draw the mutually lower end of pipe and remained with clarifying chamber bottom and draw phase gap, the lower end for drawing mutually pipe is installed with scraper plate group, scraper plate group
It is made up of along the scraper plate for drawing the mutually uniform spread configuration in pipe periphery multiple, each scraper plate is along drawing the axial arranged of mutually pipe, and each
Towards the downward-sloping setting in clarifying chamber bottom, outer end and the clarifying chamber bottom of each scraper plate lower edge are supported for scraper plate lower edge
Connect, the inner end of each scraper plate lower edge and the lower end concordant docking for drawing mutually pipe；The solution of clarifying chamber is stretched out in the upper end for drawing mutually pipe,
And draw the upper end of mutually pipe peristaltic pump is connected with by outgoing line, the export pipeline of peristaltic pump is connected with tank diameter, tank diameter
Bottom is connected with third phase storage tank by discharge line, and the top of tank diameter has been sequentially connected in series filter pressing pump, pressure by processing pipeline
Filter and organic phase storage tank.
2. the third phase cleaning plant of copper solvent extraction clarifying chamber according to claim 1, it is characterised in that：It is described to draw phase
Dragging rope is provided with pipe, dragging rope is extended out to outside clarifying chamber.
3. the third phase cleaning plant of copper solvent extraction clarifying chamber according to claim 2, it is characterised in that：The dragging
Rope is provided with two, and two dragging ropes are separately positioned on the opposite sides for drawing mutually pipe.
4. the third phase cleaning plant of the copper solvent extraction clarifying chamber according to claim any one of 1-3, it is characterised in that：
The outgoing line is flexible pipe.
5. the third phase cleaning plant of copper solvent extraction clarifying chamber according to claim 4, it is characterised in that：It is described to draw phase
Third phase thickness of the distance in gap less than clarifying chamber bottom.
6. the third phase cleaning plant of copper solvent extraction clarifying chamber according to claim 5, it is characterised in that：The scraper plate
It is provided with four.
7. the third phase cleaning plant of copper solvent extraction clarifying chamber according to claim 5, it is characterised in that：The press filtration
Machine is plate and frame type filter-press.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611204670.0A CN106693462B (en) | 2016-12-23 | 2016-12-23 | Third phase cleaning device of copper solvent extraction clarification chamber |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611204670.0A CN106693462B (en) | 2016-12-23 | 2016-12-23 | Third phase cleaning device of copper solvent extraction clarification chamber |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106693462A true CN106693462A (en) | 2017-05-24 |
| CN106693462B CN106693462B (en) | 2022-07-08 |
Family
ID=58895841
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611204670.0A Active CN106693462B (en) | 2016-12-23 | 2016-12-23 | Third phase cleaning device of copper solvent extraction clarification chamber |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106693462B (en) |
Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040129636A1 (en) * | 2002-07-23 | 2004-07-08 | Monzyk Bruce F. | Metal removal and recovery by liquid-liquid extraction |
| CN1694751A (en) * | 2002-11-28 | 2005-11-09 | 技术重组股份有限公司 | Method and device used for mixing and sedimentation in solvent extraction processes for the recovery of highly-rupe products |
| US20100176061A1 (en) * | 2007-02-14 | 2010-07-15 | Monzyk Bruce F | Water purification |
| CN201648150U (en) * | 2010-01-04 | 2010-11-24 | 深圳市洁驰科技有限公司 | Alkaline copper etchant cyclic regeneration water washer |
| CN202207478U (en) * | 2011-09-02 | 2012-05-02 | 海南金亿新材料股份有限公司 | Solid-liquid separator of mixer-settler for extraction |
| CN102459662A (en) * | 2009-06-11 | 2012-05-16 | 奥图泰有限公司 | Method and apparatus for regeneration of extraction solution in metal extraction processes |
| CN204125497U (en) * | 2014-06-11 | 2015-01-28 | 天津市茂联科技有限公司 | A kind of process copper thired extracting phase equipment |
| CN204125502U (en) * | 2014-10-27 | 2015-01-28 | 赣州逸豪优美科实业有限公司 | A kind of third phase Automatic Extraction device for electrodeposited cobalt |
| CN204125538U (en) * | 2014-10-27 | 2015-01-28 | 赣州逸豪优美科实业有限公司 | A kind of third phase treatment system for cobaltous dihydroxycarbonate |
| CN206414818U (en) * | 2016-12-23 | 2017-08-18 | 灵宝金源矿业股份有限公司 | The third phase cleaning plant of copper solvent extraction clarifying chamber |
-
2016
- 2016-12-23 CN CN201611204670.0A patent/CN106693462B/en active Active
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040129636A1 (en) * | 2002-07-23 | 2004-07-08 | Monzyk Bruce F. | Metal removal and recovery by liquid-liquid extraction |
| CN1694751A (en) * | 2002-11-28 | 2005-11-09 | 技术重组股份有限公司 | Method and device used for mixing and sedimentation in solvent extraction processes for the recovery of highly-rupe products |
| US20100176061A1 (en) * | 2007-02-14 | 2010-07-15 | Monzyk Bruce F | Water purification |
| CN102459662A (en) * | 2009-06-11 | 2012-05-16 | 奥图泰有限公司 | Method and apparatus for regeneration of extraction solution in metal extraction processes |
| CN201648150U (en) * | 2010-01-04 | 2010-11-24 | 深圳市洁驰科技有限公司 | Alkaline copper etchant cyclic regeneration water washer |
| CN202207478U (en) * | 2011-09-02 | 2012-05-02 | 海南金亿新材料股份有限公司 | Solid-liquid separator of mixer-settler for extraction |
| CN204125497U (en) * | 2014-06-11 | 2015-01-28 | 天津市茂联科技有限公司 | A kind of process copper thired extracting phase equipment |
| CN204125502U (en) * | 2014-10-27 | 2015-01-28 | 赣州逸豪优美科实业有限公司 | A kind of third phase Automatic Extraction device for electrodeposited cobalt |
| CN204125538U (en) * | 2014-10-27 | 2015-01-28 | 赣州逸豪优美科实业有限公司 | A kind of third phase treatment system for cobaltous dihydroxycarbonate |
| CN206414818U (en) * | 2016-12-23 | 2017-08-18 | 灵宝金源矿业股份有限公司 | The third phase cleaning plant of copper solvent extraction clarifying chamber |
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| CN106693462B (en) | 2022-07-08 |
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