CN106640793B - Hydraulic station device and its method of work are supplied in a kind of carbon tetrachloride processing - Google Patents
Hydraulic station device and its method of work are supplied in a kind of carbon tetrachloride processing Download PDFInfo
- Publication number
- CN106640793B CN106640793B CN201611176123.6A CN201611176123A CN106640793B CN 106640793 B CN106640793 B CN 106640793B CN 201611176123 A CN201611176123 A CN 201611176123A CN 106640793 B CN106640793 B CN 106640793B
- Authority
- CN
- China
- Prior art keywords
- oil
- supply reservoir
- parts
- filter screen
- control system
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F15—FLUID-PRESSURE ACTUATORS; HYDRAULICS OR PNEUMATICS IN GENERAL
- F15B—SYSTEMS ACTING BY MEANS OF FLUIDS IN GENERAL; FLUID-PRESSURE ACTUATORS, e.g. SERVOMOTORS; DETAILS OF FLUID-PRESSURE SYSTEMS, NOT OTHERWISE PROVIDED FOR
- F15B11/00—Servomotor systems without provision for follow-up action; Circuits therefor
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F15—FLUID-PRESSURE ACTUATORS; HYDRAULICS OR PNEUMATICS IN GENERAL
- F15B—SYSTEMS ACTING BY MEANS OF FLUIDS IN GENERAL; FLUID-PRESSURE ACTUATORS, e.g. SERVOMOTORS; DETAILS OF FLUID-PRESSURE SYSTEMS, NOT OTHERWISE PROVIDED FOR
- F15B13/00—Details of servomotor systems ; Valves for servomotor systems
- F15B13/02—Fluid distribution or supply devices characterised by their adaptation to the control of servomotors
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F15—FLUID-PRESSURE ACTUATORS; HYDRAULICS OR PNEUMATICS IN GENERAL
- F15B—SYSTEMS ACTING BY MEANS OF FLUIDS IN GENERAL; FLUID-PRESSURE ACTUATORS, e.g. SERVOMOTORS; DETAILS OF FLUID-PRESSURE SYSTEMS, NOT OTHERWISE PROVIDED FOR
- F15B19/00—Testing; Calibrating; Fault detection or monitoring; Simulation or modelling of fluid-pressure systems or apparatus not otherwise provided for
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F15—FLUID-PRESSURE ACTUATORS; HYDRAULICS OR PNEUMATICS IN GENERAL
- F15B—SYSTEMS ACTING BY MEANS OF FLUIDS IN GENERAL; FLUID-PRESSURE ACTUATORS, e.g. SERVOMOTORS; DETAILS OF FLUID-PRESSURE SYSTEMS, NOT OTHERWISE PROVIDED FOR
- F15B20/00—Safety arrangements for fluid actuator systems; Applications of safety devices in fluid actuator systems; Emergency measures for fluid actuator systems
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F15—FLUID-PRESSURE ACTUATORS; HYDRAULICS OR PNEUMATICS IN GENERAL
- F15B—SYSTEMS ACTING BY MEANS OF FLUIDS IN GENERAL; FLUID-PRESSURE ACTUATORS, e.g. SERVOMOTORS; DETAILS OF FLUID-PRESSURE SYSTEMS, NOT OTHERWISE PROVIDED FOR
- F15B21/00—Common features of fluid actuator systems; Fluid-pressure actuator systems or details thereof, not covered by any other group of this subclass
- F15B21/02—Servomotor systems with programme control derived from a store or timing device; Control devices therefor
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F15—FLUID-PRESSURE ACTUATORS; HYDRAULICS OR PNEUMATICS IN GENERAL
- F15B—SYSTEMS ACTING BY MEANS OF FLUIDS IN GENERAL; FLUID-PRESSURE ACTUATORS, e.g. SERVOMOTORS; DETAILS OF FLUID-PRESSURE SYSTEMS, NOT OTHERWISE PROVIDED FOR
- F15B21/00—Common features of fluid actuator systems; Fluid-pressure actuator systems or details thereof, not covered by any other group of this subclass
- F15B21/04—Special measures taken in connection with the properties of the fluid
- F15B21/041—Removal or measurement of solid or liquid contamination, e.g. filtering
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F15—FLUID-PRESSURE ACTUATORS; HYDRAULICS OR PNEUMATICS IN GENERAL
- F15B—SYSTEMS ACTING BY MEANS OF FLUIDS IN GENERAL; FLUID-PRESSURE ACTUATORS, e.g. SERVOMOTORS; DETAILS OF FLUID-PRESSURE SYSTEMS, NOT OTHERWISE PROVIDED FOR
- F15B21/00—Common features of fluid actuator systems; Fluid-pressure actuator systems or details thereof, not covered by any other group of this subclass
- F15B21/04—Special measures taken in connection with the properties of the fluid
- F15B21/042—Controlling the temperature of the fluid
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F15—FLUID-PRESSURE ACTUATORS; HYDRAULICS OR PNEUMATICS IN GENERAL
- F15B—SYSTEMS ACTING BY MEANS OF FLUIDS IN GENERAL; FLUID-PRESSURE ACTUATORS, e.g. SERVOMOTORS; DETAILS OF FLUID-PRESSURE SYSTEMS, NOT OTHERWISE PROVIDED FOR
- F15B2211/00—Circuits for servomotor systems
- F15B2211/20—Fluid pressure source, e.g. accumulator or variable axial piston pump
- F15B2211/205—Systems with pumps
- F15B2211/20507—Type of prime mover
- F15B2211/20515—Electric motor
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F15—FLUID-PRESSURE ACTUATORS; HYDRAULICS OR PNEUMATICS IN GENERAL
- F15B—SYSTEMS ACTING BY MEANS OF FLUIDS IN GENERAL; FLUID-PRESSURE ACTUATORS, e.g. SERVOMOTORS; DETAILS OF FLUID-PRESSURE SYSTEMS, NOT OTHERWISE PROVIDED FOR
- F15B2211/00—Circuits for servomotor systems
- F15B2211/60—Circuit components or control therefor
- F15B2211/615—Filtering means
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F15—FLUID-PRESSURE ACTUATORS; HYDRAULICS OR PNEUMATICS IN GENERAL
- F15B—SYSTEMS ACTING BY MEANS OF FLUIDS IN GENERAL; FLUID-PRESSURE ACTUATORS, e.g. SERVOMOTORS; DETAILS OF FLUID-PRESSURE SYSTEMS, NOT OTHERWISE PROVIDED FOR
- F15B2211/00—Circuits for servomotor systems
- F15B2211/60—Circuit components or control therefor
- F15B2211/62—Cooling or heating means
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F15—FLUID-PRESSURE ACTUATORS; HYDRAULICS OR PNEUMATICS IN GENERAL
- F15B—SYSTEMS ACTING BY MEANS OF FLUIDS IN GENERAL; FLUID-PRESSURE ACTUATORS, e.g. SERVOMOTORS; DETAILS OF FLUID-PRESSURE SYSTEMS, NOT OTHERWISE PROVIDED FOR
- F15B2211/00—Circuits for servomotor systems
- F15B2211/80—Other types of control related to particular problems or conditions
- F15B2211/857—Monitoring of fluid pressure systems
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F15—FLUID-PRESSURE ACTUATORS; HYDRAULICS OR PNEUMATICS IN GENERAL
- F15B—SYSTEMS ACTING BY MEANS OF FLUIDS IN GENERAL; FLUID-PRESSURE ACTUATORS, e.g. SERVOMOTORS; DETAILS OF FLUID-PRESSURE SYSTEMS, NOT OTHERWISE PROVIDED FOR
- F15B2211/00—Circuits for servomotor systems
- F15B2211/80—Other types of control related to particular problems or conditions
- F15B2211/86—Control during or prevention of abnormal conditions
Abstract
The invention discloses supplying hydraulic station device and its method of work in a kind of processing of carbon tetrachloride, by pump oil motor, fan cooler, hydraulic lifting piston, injection pump, pressure detecting table, form than row flow speed control valve, oil return mechanism, supply reservoir, everything wheel, control system；Pump oil motor is fixedly mounted on centre position above supply reservoir；Injection pump is located at pump oil motor side；Oil return mechanism is positioned over front side above supply reservoir；Pressure detecting table through connection is on the pipeline on injection pump；Pressure detecting table side is arranged at than row flow speed control valve；Hydraulic lifting piston is located at pump oil motor opposite side；Fan cooler is positioned over rear side above supply reservoir.Hydraulic station device is supplied in a kind of carbon tetrachloride processing of the present invention, the device separates use with hydraulic pressure using equipment, device has the delicate electronic devices such as pressure gauge, flow speed control valve, it is precisely controlled oil pressure, fluid usage amount, efficiently, quickly, it is simple in construction, convenience in transport, suitable for various execution conditions.
Description
Technical field
The invention belongs to the application field of carbon tetrachloride processing equipment, and in particular to supply liquid in a kind of carbon tetrachloride processing
Press station arrangement and its method of work.
Background technology
It is required for one to provide power source for its hydraulic cylinder in the hydraulic station that carbon tetrachloride treatment industry uses
Hydraulic system, the Hydraulic Elements on hydraulic station under the control of electric elements, the program that is set according to people realize it is various not
Same pressure curve, to meet the requirement of a variety of products, raw material and production technology to pressure curve.
Hydraulic station production line is in one line due to the limitation of T fonts process layout using T fonts process layout
Hydraulic station is laid without unnecessary position by more hot presses, traditional hot press is that every press configures a hydraulic station,
So a melt pit have to be dug in the underground beside press, hydraulic station is placed in melt pit and built.Thus there is following ask
Topic：
1st, the heat dissipation problem of hydraulic station：Hydraulic station is placed in melt pit, be able to not can be radiated during work, high oil temperature can cause liquid
The viscosity of force feed reduces, and because the reduction of viscosity can reduce the sealing intensity of all sealing parts of hydraulic system, oozes
Oil, oil leakage phenomenon, can also aggravate the abrasion of oil pump and other Hydraulic Elements, increase the power consumption of Oil pump electrical machinery；
2nd, the regular job of hydraulic station, observation problem：Because hydraulic station is placed in melt pit, and cover plate is stamped, can not observed
To hydraulic station whether in normal work, also have, this hydraulic station is generally provided with manual/auto control form, if in work
Broken down suddenly when making, want promptly manually to carry out control device, be unlikely；
3rd, the cleaning of hydraulic station, maintenance problem：Routinely require, hydraulic oil will often be filtered, in hydraulic fluid tank body then
Thoroughly cleaned very much, also had, hydraulic station also will periodically be checked, repaired, and the melt pit for putting hydraulic station does not have too
Big space, so work brings no small difficulty more than giving.
The content of the invention
In order to solve the above-mentioned technical problem, the present invention provides in a kind of carbon tetrachloride processing and supplies hydraulic station device, including：
Pump oil motor 1, fan cooler 2, hydraulic lifting piston 3, injection pump 4, pressure detecting table 5, than row flow speed control valve 6, oil return mechanism
7, supply reservoir 8, everything wheel 9, control system 10；The supply reservoir 8 is rectangular configuration, and it is galvanized steel plain sheet material that it is internal,
PVC material is coated with outside it；The pump oil motor 1 is fixedly mounted on the top centre position of supply reservoir 8；The injection pump 4
In the side of pump oil motor 1, injection pump 4 and the drive connection of pump oil motor 1；Before the oil return mechanism 7 is positioned over the top of supply reservoir 8
Side, oil return mechanism 7 pass through oil pipe and the through connection of injection pump 4；Pipe of the through connection of pressure detecting table 5 on injection pump 4
Lu Shang；It is described to be arranged at the side of pressure detecting table 5 than row flow speed control valve 6, penetrate and connect than the pipeline on row flow speed control valve 6 and injection pump 4
Connect；The hydraulic lifting piston 3 is located at the opposite side of pump oil motor 1, hydraulic lifting piston 3 and the through connection of supply reservoir 8；It is described
Fan cooler 2 is positioned over the top of supply reservoir 8 rear side, and fan cooler 2 passes through airduct and the through connection of injection pump 4；It is described
The quantity of everything wheel 9 is 4, is fixedly welded on the bottom surrounding of supply reservoir 8 respectively；The control system 10 is positioned over supply reservoir
8 sides；
The pump oil motor 1, fan cooler 2, hydraulic lifting piston 3, injection pump 4 pass through wire and control system respectively
10 control connections；
The pressure detecting table 5, than row flow speed control valve 6 respectively pass through wire and control system 10 control connect.
Further, the oil return mechanism 7 includes：Return filter 7-1, flow control valve 7-2, oil return amount detector 7-
3, oil back chamber 7-4, return line 7-5；Wherein, the oil back chamber 7-4 is rectangle stainless steel structure, and oil back chamber 7-4 passes through fixation
Plate is fixedly welded on the top of supply reservoir 8；The return filter 7-1 is arranged above oil back chamber 7-4, return filter 7-1
Bottom and oil back chamber 7-4 through connections；The oil stream adjustable valve 7-2 is located at oil back chamber 7-4 upper ends, flow control valve 7-2 ends
Inside portion insertion return filter 7-1；The oil return amount detector 7-3 through connections are in return filter 7-1 sides；Described time
Oil pipe line 7-5 is corrosion-proof steel pipe, and return line 7-5 upper ends penetrate with oil back chamber 7-4；
The flow control valve 7-2, oil return amount detector 7-3 are connected by wire and the control of control system 10 respectively.
Further, the supply reservoir 8 includes：Pouring orifice 8-1, filter screen 8-2, filter screen glue viscosity detector 8-3, fluid
Liquid level detector 8-4, oil liquid temperature detector 8-5；Wherein, the pouring orifice 8-1 is located at the side of supply reservoir 8, pouring orifice 8-1
With the through connection of supply reservoir 8；The filter screen 8-2 is arranged and oil pipeline one end, and filter screen is provided with filter screen 8-2 and glues viscosity inspection
Survey device 8-3；The fluid liquid level detector 8-4 is fixedly mounted on the inwall side of supply reservoir 8, fluid liquid level detector 8-4 with
The distance of the bottom of supply reservoir 8 is between 10cm~15cm；The oil liquid temperature detector 8-5 is fixedly mounted on supply reservoir 8
The distance of another inwall side, oil liquid temperature detector 8-5 and the bottom of supply reservoir 8 is between 7cm~10cm；
The filter screen glues viscosity detector 8-3, fluid liquid level detector 8-4, oil liquid temperature detector 8-5 respectively by leading
Line connects with the control of control system 10.
Further, the filter screen 8-2 is molded by high polymer material pressing mold, filter screen 8-2 constituent and manufacturing process
It is as follows：
First, filter screen 8-2 constituents：
Count in parts by weight, 2- { [(tert-butoxy) carbonyl] amino } 64~124 parts of -4- methane sulfonyls methyl butyrate,
2- methyl -2- acrylic acid -4- [methyl (11 fluorine amyl group) sulfuryl amino] 54~154 parts of butyl ester, 2- acrylic acid -2- [[(ten
Seven fluoro octyl groups) sulfonyl] methylamino] 94~214 parts of ethyl ester, acrylic acid-2-ethyl caproite and methyl methacrylate, 2-
14~54 parts of the polymer of acrylamido -2- methyl propane sulfonic acids and methacrylic acid, 4- (chloro- 5, the 6- dihydros -7h- pyrroles of 4-
Cough up simultaneously [2,3-d] pyrimidin-7-yl)-N, 74~134 parts of N- dimethyl benzene sulfonamides, N- (9,10- dihydro -9,10- dioxo -1-
Anthryl) 34~74 parts of -7- oxo -7H- benzos [E] pyridine -4- formamides, concentration is that 24ppm~54ppm (S) -9,10- bis- is fluoro-
2,3- dihydro -3- methyl -7- oxo 54~114 parts of Benzoxazine -6- carboxylic acids of-(3S) -7H- pyridos [1,2,3-de]-Isosorbide-5-Nitrae -, 5,
34~74 parts of 6- dihydros -6- oxo -11H- pyridos [2,3-b] [Isosorbide-5-Nitrae] benzodiazepine, chloro- 5, the 10- dihydros -11- oxygen of 8-
114~144 parts of -11H- dibenzo [b, e] [Isosorbide-5-Nitrae] diaza of generation, 64~194 parts of crosslinking agent, dibenzo [b, f] [Isosorbide-5-Nitrae] sulphur nitrogen
Miscellaneous 44~114 parts of Zhuo -11- [10H] ketone, 11- piperazines -24~84 parts of dibenzo [B, F] [Isosorbide-5-Nitrae] sulphur azatropylidene hydrochloride, 4- ammonia
44~134 parts of base -2- methyl isophthalic acid 0H- thiophene [2,3-B] [1,5] benzodiazepine hydrochloride, 2- aryl -2,3- dihydro -1,
84~164 parts of 5- benzothiaheptylyins -4 (5H) -one；
The crosslinking agent is 4- isopentyl epoxides phenol, 6- butyl sulfonyl pyridine -3- alcohol, the bromo- 6- (cyclopropyl-methoxies of 5-
Base) any one in pyridine -3- alcohol；
2nd, filter screen 8-2 manufacturing process, is comprised the steps of：
1st step：1374~1644 parts of the ultra-pure water that electrical conductivity is the μ S/cm of 2.24 μ S/cm~4.24 is added in a kettle,
Start reactor in agitator, rotating speed be 64rpm~124rpm, startup heat pump, make reactor temperature rise to 44 DEG C~
74℃；Sequentially add 2- { [(tert-butoxy) carbonyl] amino } -4- methane sulfonyls methyl butyrate, 2- methyl -2- acrylic acid -4-
[methyl (11 fluorine amyl group) sulfuryl amino] butyl ester, 2- acrylic acid -2- [[(17 fluoro octyl group) sulfonyl] methylamino]
Ethyl ester, to being completely dissolved, regulation pH value is 3.4~6.4, agitator speed is adjusted into 134rpm~254rpm, temperature is for stirring
94 DEG C~134 DEG C, esterification 14~24 hours；
2nd step：Take acrylic acid-2-ethyl caproite and methyl methacrylate, 2- acrylamido -2- methyl propane sulfonic acids
Polymer, 4- (chloro- 5,6- dihydros -7h- pyrrolo-es [2,3-d] pyrimidin-7-yls of 4-)-N with methacrylic acid, N- dimethyl benzenes
Sulfonamide is crushed, and powder diameter is 524~1354 mesh；Add N- (9,10- dihydro -9,10- dioxo -1- anthryls) -7-
Oxo -7H- benzos [E] pyridine -4- formamides are well mixed, and are laid in pallet, and tiling thickness is 34mm~54mm, using dosage
The alpha ray for being 5.4MeV~14.4MeV for 3.4kGy~9.4kGy, energy irradiates 64~144 minutes, and the β of Isodose
X ray irradiation x 54~134 minutes；
3rd step：Through the 2nd step handle mixed-powder be dissolved in the fluoro- 2,3- dihydros -3- methyl -7- oxos of (S) -9,10- two -
In (3S) -7H- pyridos [1,2,3-de]-Isosorbide-5-Nitrae-Benzoxazine -6- carboxylic acids, add reactor, agitator speed be 74rpm~
184rpm, temperature are 84 DEG C~164 DEG C, and starting vavuum pump makes the vacuum of reactor reach 1.34MPa~1.84MPa, keeps
This state response 14~34 hours；Pressure release is simultaneously passed through radon gas, and it is 1.24MPa~1.64MPa to make reacting kettle inner pressure, and insulation is stood
24~34 hours；Agitator speed is promoted to 154rpm~294rpm, simultaneous reactions kettle pressure release to 0MPa；Sequentially add 5,6- bis-
Hydrogen -6- oxo -11H- pyridos [2,3-b] [1,4] benzodiazepine, the chloro- 5,10- dihydros -11- oxos -11H- dibenzo of 8-
After [b, e] [Isosorbide-5-Nitrae] diaza is completely dissolved, adds crosslinking agent and be stirred so that the hydrophilic lipophilic balance of reactor solution
For 5.4~8.4, insulation stands 24~44 hours；
4th step：When agitator speed is 144rpm~224rpm, dibenzo [b, f] [Isosorbide-5-Nitrae] sulphur azepine is sequentially added
Zhuo -11- [10H] ketone, 11- piperazines-dibenzo [B, F] [1,4] sulphur azatropylidene hydrochloride, 4- amino-2-methyl -10H- thiophene
[2,3-B] [1,5] benzodiazepine hydrochloride and (5H) -one of 2- aryl -2,3- dihydros -1,5- benzothiaheptylyin -4, lifting
Reactor pressure, 1.94MPa~2.74MPa is reached, temperature is 144 DEG C~264 DEG C, polymerisation 14~24 hours；Instead
Reacting kettle inner pressure is down to 0MPa after the completion of answering, 24 DEG C~44 DEG C is cooled to, discharging, enters molding press and can be prepared by filter screen 8-2.
Further, should the invention also discloses the method for work that hydraulic station device is supplied in a kind of processing of carbon tetrachloride
Method includes following steps：
1st step：Staff will supply hydraulic pressure oil inlet and the seamless socket connection of the oil-out of injection pump 4 of hydraulic station, together
When switch on power；
2nd step：Staff presses the start button in control system 10, starts pump oil motor 1, is driven in pump oil motor 1
Under dynamic, injection pump 4 pumps out the fluid in supply reservoir 8 by oil pipeline, there is provided is used to supply hydraulic station；
3rd step：During injection pump 4 pumps out fluid, pressure detecting table 5 monitors the oil pressure feelings in supply reservoir 8 in real time
Condition；When the oil pressure that pressure detecting table 5 is detected in supply reservoir 8 is higher than default value A, control system 10 controls hydraulic pressure liter
Drop piston 3 rises, and row pressure is carried out to supply reservoir 8；When pressure detecting table 5 detects that the oil pressure in supply reservoir 8 reaches system
During setting value A, control system 10 closes hydraulic lifting piston 3；
4th step：Than row flow speed control valve 6 to the real-time monitoring of fluid spray feed speed；When than row flow speed control valve 6 detect fluid spray feed speed
When rate is less than 10cm/ms, control system 10 increases than the aperture of row flow speed control valve 6；When detecting fluid spray feed speed than row flow speed control valve 6
During higher than 20cm/ms, control system 10 reduces than the aperture of row flow speed control valve 6；
5th step：During injection pump 4 pumps out fluid, part fluid is entered in oil return mechanism 7 by oil pipe；Oil return
Filter 7-1 carries out purification filtering to oil return, passes through through oil back chamber 7-4 in return line 7-5 oil returns to supply reservoir 8；
6th step：Oil return amount detector 7-3 is to the real-time monitoring of recirculating oil quantity；When oil return amount detector 7-3 detects recirculating oil quantity height
When 20ml, electric signal is sent to control system 10 by oil return amount detector 7-3, and the calculating storage element in control system 10 will
Recirculating oil quantity data storage simultaneously generates form, while increases flow control valve 7-2 apertures；
7th step：Filter screen 8-2 in supply reservoir 8 filters to fluid, and filter screen glues viscosity detector 8-3 to filter
Net 8-2 glues viscosity and monitored in real time, when filter screen, which glues viscosity detector 8-3, detects that filter screen 8-2 glues viscosity higher than 75%, control system
System 10 sends alarm signal, reminds staff to carry out cleaning process；
8th step：Fluid liquid level detector 8-4 is monitored in real time to the fluid liquid level in supply reservoir 8, when fluid level sensing
When device 8-4 detects that the fluid in supply reservoir 8 is less than 50ml, the warning lamp flicker in control system 10, staff is reminded
Carry out oiling process；
9th step：Oil liquid temperature detector 8-5 is monitored in real time to the oil liquid temperature in supply reservoir 8, when oil liquid temperature detects
When device 8-5 detects that the oil liquid temperature in supply reservoir 8 is higher than 98 DEG C, control system 10 starts fan cooler 2, fan coolling
Device 2 is cooled by airduct to fluid；When oil liquid temperature detector 8-5 detects that the oil liquid temperature in supply reservoir 8 is less than
At 25 DEG C, control system 10 stops fan cooler 2.
Hydraulic station device is supplied in a kind of carbon tetrachloride processing disclosed by the invention, the advantage is that：
(1) device separates use with hydraulic pressure using equipment, and device has the delicate electronic devices such as pressure gauge, flow speed control valve, essence
Quasi- control oil pressure, fluid usage amount, efficiently, quickly；
(2) the plant automation degree is high, computer control fluid input and output, facilitates employee to operate；
(3) apparatus structure is simple, convenience in transport, suitable for various execution conditions.
Hydraulic station device is supplied in a kind of carbon tetrachloride processing of the present invention, the device is separated with hydraulic pressure using equipment
Using, device has the delicate electronic devices such as pressure gauge, flow speed control valve, is precisely controlled oil pressure, fluid usage amount, efficiently, quickly, structure
Simply, convenience in transport, suitable for various execution conditions.
Brief description of the drawings
Fig. 1 is to supply hydraulic station device schematic diagram in a kind of heretofore described carbon tetrachloride processing.
Fig. 2 is heretofore described oil return mechanism structural representation.
Fig. 3 is heretofore described supply reservoir structural representation.
Fig. 4 is heretofore described screen material oxytolerant rate with usage time variation diagram.
In figure 1 above~Fig. 3, pump oil motor 1, fan cooler 2, hydraulic lifting piston 3, injection pump 4, pressure detecting table
5, than row flow speed control valve 6, oil return mechanism 7, return filter 7-1, flow control valve 7-2, oil return amount detector 7-3, oil back chamber 7-
4, return line 7-5, supply reservoir 8, pouring orifice 8-1, filter screen 8-2, filter screen glue viscosity detector 8-3, fluid liquid level detector
8-4, oil liquid temperature detector 8-5, everything wheel 9, control system 10.
Embodiment
Supply hydraulic station device in a kind of carbon tetrachloride processing provided by the invention is entered with reference to the accompanying drawings and examples
Row further illustrates.
As shown in figure 1, it is to supply hydraulic station device schematic diagram in a kind of heretofore described carbon tetrachloride processing.From figure
Find out in 1, including：Pump oil motor 1, fan cooler 2, hydraulic lifting piston 3, injection pump 4, pressure detecting table 5, than row speed governing
Valve 6, oil return mechanism 7, supply reservoir 8, everything wheel 9, control system 10；The supply reservoir 8 is rectangular configuration, and it is internal for plating
Zinc steel plate material, PVC material is coated with outside it；The pump oil motor 1 is fixedly mounted on the top centre position of supply reservoir 8；Institute
State injection pump 4 and be located at the side of pump oil motor 1, injection pump 4 and the drive connection of pump oil motor 1；The oil return mechanism 7 is positioned over fuel feeding
The top of fuel tank 8 front side, oil return mechanism 7 pass through oil pipe and the through connection of injection pump 4；The through connection of pressure detecting table 5 is being sprayed
On pipeline on oil pump 4；It is described to be arranged at the side of pressure detecting table 5 than row flow speed control valve 6, than on row flow speed control valve 6 and injection pump 4
Pipeline through connection；The hydraulic lifting piston 3 is located at the opposite side of pump oil motor 1, and hydraulic lifting piston 3 passes through with supply reservoir 8
Lead to and connect；The fan cooler 2 is positioned over the top of supply reservoir 8 rear side, and fan cooler 2 is passed through by airduct and injection pump 4
Lead to and connect；The quantity of everything wheel 9 is 4, is fixedly welded on the bottom surrounding of supply reservoir 8 respectively；The control system 10 is put
It is placed in the side of supply reservoir 8；
The pump oil motor 1, fan cooler 2, hydraulic lifting piston 3, injection pump 4 pass through wire and control system respectively
10 control connections；
The pressure detecting table 5, than row flow speed control valve 6 respectively pass through wire and control system 10 control connect.
As shown in Fig. 2 it is heretofore described oil return mechanism structural representation.Find out from Fig. 2 or Fig. 1, oil return machine
Structure 7 includes：Return filter 7-1, flow control valve 7-2, oil return amount detector 7-3, oil back chamber 7-4, return line 7-5；Its
In, the oil back chamber 7-4 is rectangle stainless steel structure, and oil back chamber 7-4 is fixedly welded on the top of supply reservoir 8 by fixed plate；
The return filter 7-1 is arranged above oil back chamber 7-4, return filter 7-1 bottoms and oil back chamber 7-4 through connections；Institute
State oil stream adjustable valve 7-2 and be located at oil back chamber 7-4 upper ends, flow control valve 7-2 ends are inserted inside return filter 7-1；Institute
Oil return amount detector 7-3 through connections are stated in return filter 7-1 sides；The return line 7-5 is corrosion-proof steel pipe, oil return
Pipeline 7-5 upper ends penetrate with oil back chamber 7-4；
The flow control valve 7-2, oil return amount detector 7-3 are connected by wire and the control of control system 10 respectively.
As shown in figure 3, it is heretofore described supply reservoir structural representation.Find out from Fig. 3 or Fig. 1, fuel feeding oil
Case 8 includes：Pouring orifice 8-1, filter screen 8-2, filter screen glue viscosity detector 8-3, fluid liquid level detector 8-4, oil liquid temperature detection
Device 8-5；Wherein, the pouring orifice 8-1 is located at the side of supply reservoir 8, pouring orifice 8-1 and the through connection of supply reservoir 8；The filter
8-2 arrangements and oil pipeline one end are netted, being provided with filter screen on filter screen 8-2 glues viscosity detector 8-3；The fluid liquid level detector
8-4 is fixedly mounted on the inwall side of supply reservoir 8, the distance of fluid liquid level detector 8-4 and the bottom of supply reservoir 8 10cm~
Between 15cm；The oil liquid temperature detector 8-5 is fixedly mounted on another inwall side of supply reservoir 8, oil liquid temperature detector
The distance of 8-5 and the bottom of supply reservoir 8 is between 7cm~10cm；
The filter screen glues viscosity detector 8-3, fluid liquid level detector 8-4, oil liquid temperature detector 8-5 respectively by leading
Line connects with the control of control system 10.
The course of work of hydraulic station device is supplied in a kind of carbon tetrachloride processing of the present invention is：
1st step：Staff will supply hydraulic pressure oil inlet and the seamless socket connection of the oil-out of injection pump 4 of hydraulic station, together
When switch on power；
2nd step：Staff presses the start button in control system 10, starts pump oil motor 1, is driven in pump oil motor 1
Under dynamic, injection pump 4 pumps out the fluid in supply reservoir 8 by oil pipeline, there is provided is used to supply hydraulic station；
3rd step：During injection pump 4 pumps out fluid, pressure detecting table 5 monitors the oil pressure feelings in supply reservoir 8 in real time
Condition；When the oil pressure that pressure detecting table 5 is detected in supply reservoir 8 is higher than default value A, control system 10 controls hydraulic pressure liter
Drop piston 3 rises, and row pressure is carried out to supply reservoir 8；When pressure detecting table 5 detects that the oil pressure in supply reservoir 8 reaches system
During setting value A, control system 10 closes hydraulic lifting piston 3；
4th step：Than row flow speed control valve 6 to the real-time monitoring of fluid spray feed speed；When than row flow speed control valve 6 detect fluid spray feed speed
When rate is less than 10cm/ms, control system 10 increases than the aperture of row flow speed control valve 6；When detecting fluid spray feed speed than row flow speed control valve 6
During higher than 20cm/ms, control system 10 reduces than the aperture of row flow speed control valve 6；
5th step：During injection pump 4 pumps out fluid, part fluid is entered in oil return mechanism 7 by oil pipe；Oil return
Filter 7-1 carries out purification filtering to oil return, passes through through oil back chamber 7-4 in return line 7-5 oil returns to supply reservoir 8；
6th step：Oil return amount detector 7-3 is to the real-time monitoring of recirculating oil quantity；When oil return amount detector 7-3 detects recirculating oil quantity height
When 20ml, electric signal is sent to control system 10 by oil return amount detector 7-3, and the calculating storage element in control system 10 will
Recirculating oil quantity data storage simultaneously generates form, while increases flow control valve 7-2 apertures；
7th step：Filter screen 8-2 in supply reservoir 8 filters to fluid, and filter screen glues viscosity detector 8-3 to filter
Net 8-2 glues viscosity and monitored in real time, when filter screen, which glues viscosity detector 8-3, detects that filter screen 8-2 glues viscosity higher than 75%, control system
System 10 sends alarm signal, reminds staff to carry out cleaning process；
8th step：Fluid liquid level detector 8-4 is monitored in real time to the fluid liquid level in supply reservoir 8, when fluid level sensing
When device 8-4 detects that the fluid in supply reservoir 8 is less than 50ml, the warning lamp flicker in control system 10, staff is reminded
Carry out oiling process；
9th step：Oil liquid temperature detector 8-5 is monitored in real time to the oil liquid temperature in supply reservoir 8, when oil liquid temperature detects
When device 8-5 detects that the oil liquid temperature in supply reservoir 8 is higher than 98 DEG C, control system 10 starts fan cooler 2, fan coolling
Device 2 is cooled by airduct to fluid；When oil liquid temperature detector 8-5 detects that the oil liquid temperature in supply reservoir 8 is less than
At 25 DEG C, control system 10 stops fan cooler 2.
Hydraulic station device is supplied in a kind of carbon tetrachloride processing of the present invention, the device is separated with hydraulic pressure using equipment
Using, device has the delicate electronic devices such as pressure gauge, flow speed control valve, is precisely controlled oil pressure, fluid usage amount, efficiently, quickly, structure
Simply, convenience in transport, suitable for various execution conditions.
It is the embodiment of filter screen 8-2 of the present invention manufacturing process below, embodiment is to further illustrate this hair
Bright content, but should not be construed as limiting the invention.Without departing from the spirit and substance of the case in the present invention, to the present invention
The modification and replacement that method, step or condition are made, belong to the scope of the present invention.
Unless otherwise specified, the conventional meanses that technological means used in embodiment is well known to those skilled in the art.
Embodiment 1
Filter screen 8-2 of the present invention is manufactured according to following steps, and is counted in parts by weight：
1st step：1374 parts of the ultra-pure water that electrical conductivity is 2.24 μ S/cm is added in a kettle, is started in reactor and is stirred
Device, rotating speed 64rpm, start heat pump, reactor temperature is risen to 44 DEG C；Sequentially add 2- { [(tert-butoxy) carbonyls
Base] amino 64 parts of -4- methane sulfonyls methyl butyrate, 2- methyl -2- acrylic acid -4- [methyl (11 fluorine amyl group) Herbicidal sulphonylaminos
Base] 54 parts of butyl ester, 2- acrylic acid -2- [[(17 fluoro octyl group) sulfonyl] methylamino] 94 parts of ethyl ester, stir to completely it is molten
Solution, regulation pH value are 3.4, agitator speed are adjusted into 134rpm, temperature is 94 DEG C, esterification 14 hours；
2nd step：Take acrylic acid-2-ethyl caproite and methyl methacrylate, 2- acrylamido -2- methyl propane sulfonic acids
14 parts of polymer, 4- (chloro- 5,6- dihydros -7h- pyrrolo-es [2,3-d] pyrimidin-7-yls of 4-)-N with methacrylic acid, N- diformazans
74 parts of base benzsulfamide is crushed, and powder diameter is 524 mesh；Addition N- (9,10- dihydro -9,10- dioxo -1- anthryls) -
34 parts of 7- oxo -7H- benzos [E] pyridine -4- formamides are well mixed, are laid in pallet, tiling thickness is 34mm, using dosage
The alpha ray for being 5.4MeV for 3.4kGy, energy irradiates 64 minutes, and the β x ray irradiation xs 54 minutes of Isodose；
3rd step：The fluoro- 2,3- dihydros -3- first of (S) -9,10- two is dissolved in through the mixed-powder that the 2nd step concentration for the treatment of is 24ppm
In base -7- oxos-(3S) -7H- pyridos [1,2,3-de]-Isosorbide-5-Nitrae -54 parts of Benzoxazine -6- carboxylic acids, reactor, agitator are added
Rotating speed is 74rpm, and temperature is 84 DEG C, and starting vavuum pump makes the vacuum of reactor reach 1.34MPa, keeps this state response 14
Hour；Pressure release is simultaneously passed through radon gas, and it is 1.24MPa to make reacting kettle inner pressure, and insulation stands 24 hours；Agitator speed is promoted to
154rpm, simultaneous reactions kettle pressure release to 0MPa；Sequentially add 5,6- dihydros -6- oxo -11H- pyridos [2,3-b] [1,4] benzene
And chloro- 114 parts of 5,10- dihydros -11- oxos -11H- dibenzo [b, e] [1,4] diaza of 34 parts of diaza, 8- is completely dissolved
Afterwards, add 64 parts of crosslinking agent to be stirred so that the hydrophilic lipophilic balance of reactor solution is 5.4, and insulation stands 24 hours；
4th step：When agitator speed is 144rpm, dibenzo [b, f] [Isosorbide-5-Nitrae] sulphur azatropylidene -11- is sequentially added
44 parts of [10H] ketone, 11- piperazines -24 parts of dibenzo [B, F] [1,4] sulphur azatropylidene hydrochloride, 4- amino-2-methyl -10H- thiophene
44 parts of [2,3-B] [1,5] benzodiazepine hydrochloride and (5H) -one 84 of 2- aryl -2,3- dihydro -1,5- benzothiaheptylyins -4
Part, reactor pressure is lifted, reaches 1.94MPa, temperature is 144 DEG C, polymerisation 14 hours；Will reaction after the completion of reaction
Pressure is down to 0MPa in kettle, is cooled to 24 DEG C, discharging, enters molding press and can be prepared by filter screen 8-2；
The crosslinking agent is 4- isopentyl epoxide phenol.
Embodiment 2
Filter screen 8-2 of the present invention is manufactured according to following steps, and is counted in parts by weight：
1st step：1644 parts of the ultra-pure water that electrical conductivity is 4.24 μ S/cm is added in a kettle, is started in reactor and is stirred
Device, rotating speed 124rpm, start heat pump, reactor temperature is risen to 74 DEG C；Sequentially add 2- { [(tert-butoxy) carbonyls
Base] amino 124 parts of -4- methane sulfonyls methyl butyrate, 2- methyl -2- acrylic acid -4- [methyl (11 fluorine amyl group) sulfonyls
Amino] 154 parts of butyl ester, 2- acrylic acid -2- [[(17 fluoro octyl group) sulfonyl] methylamino] 214 parts of ethyl ester, stir to complete
Fully dissolved, regulation pH value are 6.4, agitator speed are adjusted into 254rpm, temperature is 134 DEG C, esterification 24 hours；
2nd step：Take acrylic acid-2-ethyl caproite and methyl methacrylate, 2- acrylamido -2- methyl propane sulfonic acids
54 parts of polymer, 4- (chloro- 5,6- dihydros -7h- pyrrolo-es [2,3-d] pyrimidin-7-yls of 4-)-N with methacrylic acid, N- diformazans
134 parts of base benzsulfamide is crushed, and powder diameter is 1354 mesh；Add N- (9,10- dihydro -9,10- dioxo -1- anthracenes
Base) 74 parts of -7- oxo -7H- benzos [E] pyridine -4- formamides are well mixed, it are laid in pallet, tiling thickness is 54mm, use
Dosage is 9.4kGy, energy is 14.4MeV alpha ray irradiates 144 minutes, and the β x ray irradiation xs 134 minutes of Isodose；
3rd step：The fluoro- 2,3- dihydros -3- first of (S) -9,10- two is dissolved in through the mixed-powder that the 2nd step concentration for the treatment of is 54ppm
In base -7- oxos-(3S) -7H- pyridos [1,2,3-de]-Isosorbide-5-Nitrae -114 parts of Benzoxazine -6- carboxylic acids, reactor, agitator are added
Rotating speed is 184rpm, and temperature is 164 DEG C, and starting vavuum pump makes the vacuum of reactor reach 1.84MPa, keeps this state response
34 hours；Pressure release is simultaneously passed through radon gas, and it is 1.64MPa to make reacting kettle inner pressure, and insulation stands 34 hours；Agitator speed is promoted to
294rpm, simultaneous reactions kettle pressure release to 0MPa；Sequentially add 5,6- dihydros -6- oxo -11H- pyridos [2,3-b] [1,4] benzene
And chloro- 144 parts of 5,10- dihydros -11- oxos -11H- dibenzo [b, e] [1,4] diaza of 74 parts of diaza, 8- is completely dissolved
Afterwards, add 194 parts of crosslinking agent to be stirred so that the hydrophilic lipophilic balance of reactor solution is 8.4, and it is small that insulation stands 44
When；
4th step：When agitator speed is 224rpm, dibenzo [b, f] [Isosorbide-5-Nitrae] sulphur azatropylidene -11- is sequentially added
114 parts of [10H] ketone, 11- piperazines -84 parts of dibenzo [B, F] [1,4] sulphur azatropylidene hydrochloride, 4- amino-2-methyl -10H- thiophenes
134 parts of fen [2,3-B] [1,5] benzodiazepine hydrochloride and 2- aryl -2,3- dihydro -1,5- benzothiaheptylyins -4 (5H) -
164 parts of ketone, reactor pressure is lifted, reach 2.74MPa, temperature is 264 DEG C, polymerisation 24 hours；After the completion of reaction
Reacting kettle inner pressure is down to 0MPa, 44 DEG C is cooled to, discharging, enters molding press and can be prepared by filter screen 8-2；
The crosslinking agent is 6- butyl sulfonyl pyridine -3- alcohol.
Embodiment 3
Filter screen 8-2 of the present invention is manufactured according to following steps, and is counted in parts by weight：
1st step：1444 parts of the ultra-pure water that electrical conductivity is 3.24 μ S/cm is added in a kettle, is started in reactor and is stirred
Device, rotating speed 94rpm, start heat pump, reactor temperature is risen to 64 DEG C；Sequentially add 2- { [(tert-butoxy) carbonyls
Base] amino 84 parts of -4- methane sulfonyls methyl butyrate, 2- methyl -2- acrylic acid -4- [methyl (11 fluorine amyl group) Herbicidal sulphonylaminos
Base] 134 parts of butyl ester, 2- acrylic acid -2- [[(17 fluoro octyl group) sulfonyl] methylamino] 184 parts of ethyl ester, stir to complete
Dissolving, regulation pH value are 4.4, agitator speed are adjusted into 194rpm, temperature is 114 DEG C, esterification 19 hours；
2nd step：Take acrylic acid-2-ethyl caproite and methyl methacrylate, 2- acrylamido -2- methyl propane sulfonic acids
34 parts of polymer, 4- (chloro- 5,6- dihydros -7h- pyrrolo-es [2,3-d] pyrimidin-7-yls of 4-)-N with methacrylic acid, N- diformazans
84 parts of base benzsulfamide is crushed, and powder diameter is 954 mesh；Addition N- (9,10- dihydro -9,10- dioxo -1- anthryls) -
54 parts of 7- oxo -7H- benzos [E] pyridine -4- formamides are well mixed, are laid in pallet, tiling thickness is 44mm, using dosage
The alpha ray for being 9.4MeV for 6.4kGy, energy irradiates 114 minutes, and the β x ray irradiation xs 84 minutes of Isodose；
3rd step：The fluoro- 2,3- dihydros -3- first of (S) -9,10- two is dissolved in through the mixed-powder that the 2nd step concentration for the treatment of is 44ppm
In base -7- oxos-(3S) -7H- pyridos [1,2,3-de]-Isosorbide-5-Nitrae -74 parts of Benzoxazine -6- carboxylic acids, reactor, agitator are added
Rotating speed is 124rpm, and temperature is 134 DEG C, and starting vavuum pump makes the vacuum of reactor reach 1.14MPa, keeps this state response
24 hours；Pressure release is simultaneously passed through radon gas, and it is 1.44MPa to make reacting kettle inner pressure, and insulation stands 29 hours；Agitator speed is promoted to
194rpm, simultaneous reactions kettle pressure release to 0MPa；Sequentially add 5,6- dihydros -6- oxo -11H- pyridos [2,3-b] [1,4] benzene
And chloro- 124 parts of 5,10- dihydros -11- oxos -11H- dibenzo [b, e] [1,4] diaza of 54 parts of diaza, 8- is completely dissolved
Afterwards, add 134 parts of crosslinking agent to be stirred so that the hydrophilic lipophilic balance of reactor solution is 6.4, and it is small that insulation stands 34
When；
4th step：When agitator speed is 174rpm, dibenzo [b, f] [Isosorbide-5-Nitrae] sulphur azatropylidene -11- is sequentially added
84 parts of [10H] ketone, 11- piperazines -64 parts of dibenzo [B, F] [1,4] sulphur azatropylidene hydrochloride, 4- amino-2-methyl -10H- thiophene
114 parts of [2,3-B] [1,5] benzodiazepine hydrochloride and (5H) -one of 2- aryl -2,3- dihydro -1,5- benzothiaheptylyins -4
144 parts, reactor pressure is lifted, reaches 2.24MPa, temperature is 224 DEG C, polymerisation 20 hours；Will after the completion of reaction
Reacting kettle inner pressure is down to 0MPa, is cooled to 34 DEG C, discharging, enters molding press and can be prepared by filter screen 8-2；
The crosslinking agent is 5- bromo- 6- (cyclo propyl methoxy) pyridine -3- alcohol.
Reference examples
Reference examples are the filter screen of certain commercially available brand.
Embodiment 4
Filter screen described in the filter screen 8-2 and reference examples that embodiment 1~3 is prepared carries out using effect contrast.To two
Person's filtering rate, tensile strength, crushing resistance, filter cleaning effect are counted, as a result as shown in table 1.
As seen from Table 1, filter screen 8-2 of the present invention, its filtering rate, tensile strength, crushing resistance, filter cleaning effect
Etc. the product that index is superior to prior art production.
In addition, as shown in figure 4, it is the statistics that filter screen 8-2 material against oxidative rate of the present invention changes with usage time.
Find out in figure, filter screen 8-2 used in embodiment 1~3, its material against oxidative rate is significantly better than existing production with usage time intensity of variation
Product.
Claims (3)
1. hydraulic station device is supplied in a kind of carbon tetrachloride processing, including：Pump oil motor（1）, fan cooler（2）, hydraulic pressure liter
Piston drops（3）, injection pump（4）, pressure detecting table（5）, proportional velocity regulating valve（6）, oil return mechanism（7）, supply reservoir（8）, everything
Wheel（9）, control system（10）；Characterized in that, the supply reservoir（8）For rectangular configuration, it is galvanized steel plain sheet material that it is internal,
PVC material is coated with outside it；The pump oil motor（1）It is fixedly mounted on supply reservoir（8）Top centre position；The injection pump
（4）Positioned at pump oil motor（1）Side, injection pump（4）With pump oil motor（1）Drive connection；The oil return mechanism（7）It is positioned over confession
Fuel tank（8）On front side of top, oil return mechanism（7）Pass through oil pipe and injection pump（4）Through connection；The pressure detecting table（5）Pass through
Lead to and be connected on injection pump（4）On pipeline on；The proportional velocity regulating valve（6）It is arranged at pressure detecting table（5）Side, proportionality velocity modulation
Valve（6）With injection pump（4）On pipeline through connection；The hydraulic lifting piston（3）Positioned at pump oil motor（1）Opposite side, liquid
Press lifting piston（3）With supply reservoir（8）Through connection；The fan cooler（2）It is positioned over supply reservoir（8）Behind top
Side, fan cooler（2）Pass through airduct and injection pump（4）Through connection；The everything wheel（9）Quantity is 4, respectively fixed weldering
It is connected on supply reservoir（8）Bottom surrounding；The control system（10）It is positioned over supply reservoir（8）Side；
The pump oil motor（1）, fan cooler（2）, hydraulic lifting piston（3）, injection pump（4）Pass through wire and control respectively
System（10）Control connection；
The pressure detecting table（5）, proportional velocity regulating valve（6）Pass through wire and control system respectively（10）Control connection；
The oil return mechanism（7）Including：Return filter（7-1）, flow control valve（7-2）, oil return amount detector（7-3）, return
Oil pocket（7-4）, return line（7-5）；Wherein, the oil back chamber（7-4）For rectangle stainless steel structure, oil back chamber（7-4）Pass through
Fixed plate is fixedly welded on supply reservoir（8）Top；The return filter（7-1）It is arranged at oil back chamber（7-4）Top, oil return
Filter（7-1）Bottom and oil back chamber（7-4）Through connection；The flow control valve（7-2）Positioned at oil back chamber（7-4）Upper end,
Flow control valve（7-2）Return filter is inserted in end（7-1）It is internal；The oil return amount detector（7-3）Through connection in return
Oil strainer（7-1）Side；The return line（7-5）For corrosion-proof steel pipe, return line（7-5）Upper end and oil back chamber（7-
4）Insertion；
The flow control valve（7-2）, oil return amount detector（7-3）Pass through wire and control system respectively（10）Control connection；
The supply reservoir（8）Including：Pouring orifice（8-1）, filter screen（8-2）, the viscous viscosity detector of filter screen（8-3）, fluid liquid level
Detector（8-4）, oil liquid temperature detector（8-5）；Wherein, the pouring orifice（8-1）Positioned at supply reservoir（8）Side, oiling
Mouthful（8-1）With supply reservoir（8）Through connection；The filter screen（8-2）It is arranged in oil pipeline one end, filter screen（8-2）Upper setting
There is filter screen to glue viscosity detector（8-3）；The fluid liquid level detector（8-4）It is fixedly mounted on supply reservoir（8）Inwall side,
Fluid liquid level detector（8-4）With supply reservoir（8）The distance of bottom is between 10cm~15cm；The oil liquid temperature detector
（8-5）It is fixedly mounted on supply reservoir（8）Another inwall side, oil liquid temperature detector（8-5）With supply reservoir（8）Bottom
Distance is between 7cm~10cm；
The filter screen glues viscosity detector（8-3）, fluid liquid level detector（8-4）, oil liquid temperature detector（8-5）Pass through respectively
Wire and control system（10）Control connection.
2. supply hydraulic station device in a kind of carbon tetrachloride processing according to claim 1, it is characterised in that the filter screen
（8-2）It is molded by high polymer material pressing mold, filter screen（8-2）Constituent and manufacturing process it is as follows：
First, filter screen（8-2）Constituent：
Count in parts by weight, 2- { [(tert-butoxy) carbonyl] amino } 64~124 parts of -4- methane sulfonyls methyl butyrate, 2- first
Base -2- acrylic acid -4- [methyl (11 fluorine amyl group) sulfuryl amino] 54~154 parts of butyl ester, 2- acrylic acid -2- [[(17 fluorine
For octyl group) sulfonyl] methylamino] 94~214 parts of ethyl ester, acrylic acid-2-ethyl caproite and methyl methacrylate, 2- propylene
14~54 parts of the polymer of acylamino- -2- methyl propane sulfonic acids and methacrylic acid, (chloro- 5, the 6- dihydro-7 H-pyrrolos of 4- are simultaneously by 4-
[2,3-D] pyrimidin-7-yl)-N, 74~134 parts of N- dimethyl benzene sulfonamides, N- (9,10- dihydro -9,10- dioxo -1- anthracenes
Base) 34~74 parts of -7- oxo -7H- benzos [E] pyridine -4- formamides, concentration is that the ppm of 24 ppm~54 (S) -9,10- bis- is fluoro-
2,3- dihydro -3- methyl -7- oxo 54~114 parts of Benzoxazine -6- carboxylic acids of-(3S) -7H- pyridos [1,2,3-DE]-Isosorbide-5-Nitrae -, 5,
34~74 parts of 6- dihydros -6- oxo -11H- pyridos [2,3-B] [Isosorbide-5-Nitrae] benzodiazepine, chloro- 5, the 10- dihydros -11- oxygen of 8-
114~144 parts of -11H- dibenzo [B, E] [Isosorbide-5-Nitrae] diaza of generation, 64~194 parts of crosslinking agent, dibenzo [B, F] [Isosorbide-5-Nitrae] sulphur nitrogen
Miscellaneous 44~114 parts of Zhuo -11- [10H] ketone, 11- piperazines -24~84 parts of dibenzo [B, F] [Isosorbide-5-Nitrae] sulphur azatropylidene hydrochloride, 4- ammonia
44~134 parts of base -2- methyl isophthalic acid 0H- thiophene [2,3-B] [1,5] benzodiazepine hydrochloride, 2- aryl -2,3- dihydro -1,
84~164 parts of 5- benzothiaheptylyins -4 (5H) -one；
The crosslinking agent is 4- isopentyl epoxides phenol, 6- butyl sulfonyl pyridine -3- alcohol, the bromo- 6- of 5- (cyclo propyl methoxy)
Any one in pyridine -3- alcohol；
2nd, filter screen（8-2）Manufacturing process, comprise the steps of：
1st step：1374~1644 parts of the ultra-pure water that electrical conductivity is the μ S/cm of 2.24 μ S/cm~4.24 is added in a kettle, is opened
Agitator in dynamic reactor, rotating speed are the rpm of 64 rpm~124, start heat pump, make reactor temperature rise to 44 DEG C~
74 ℃；Sequentially add 2- { [(tert-butoxy) carbonyl] amino } -4- methane sulfonyls methyl butyrate, 2- methyl -2- acrylic acid -
4- [methyl (11 fluorine amyl group) sulfuryl amino] butyl ester, 2- acrylic acid -2- [[(17 fluoro octyl group) sulfonyl] methyl ammonia
Base] ethyl ester, to being completely dissolved, regulation pH value is 3.4~6.4 for stirring, and agitator speed is adjusted into the rpm of 134 rpm~254, temperature
Spend for 94 DEG C~134 DEG C, esterification 14~24 hours；
2nd step：Take acrylic acid-2-ethyl caproite and methyl methacrylate, 2- acrylamido -2- methyl propane sulfonic acids and first
The polymer of base acrylic acid, 4- (the chloro- 5,6- dihydro-7 H-pyrrolos of 4- simultaneously [2,3-D] pyrimidin-7-yl)-N, N- dimethyl benzene sulphonyl
Amine is crushed, and powder diameter is 524~1354 mesh；Addition N- (9,10- dihydro -9,10- dioxo -1- anthryls) -7- oxos -
7H- benzos [E] pyridine -4- formamides are well mixed, and are laid in pallet, and tiling thickness is the mm of 34 mm~54, use dosage for
The kGy of 3.4 kGy~9.4, energy are that the MeV of 5.4 MeV~14.4 alpha ray irradiates 64~144 minutes, and Isodose
β x ray irradiation xs 54~134 minutes；
3rd step：Through the 2nd step handle mixed-powder be dissolved in fluoro- 2,3- dihydros -3- methyl -7- oxos-(3S) of (S) -9,10- two -
In 7H- pyridos [1,2,3-DE]-Isosorbide-5-Nitrae-Benzoxazine -6- carboxylic acids, reactor is added, agitator speed is 74 rpm~184
Rpm, temperature are 84 DEG C~164 DEG C, and starting vavuum pump makes the vacuum of reactor reach the MPa of 1.34 MPa~1.84, keeps this
State response 14~34 hours；Pressure release is simultaneously passed through radon gas, and making reacting kettle inner pressure, insulation is stood for the MPa of 1.24 MPa~1.64
24~34 hours；Agitator speed is promoted to the rpm of 154 rpm~294, simultaneous reactions kettle pressure release to 0 MPa；Sequentially add 5,
6- dihydros -6- oxo -11H- pyridos [2,3-B] [1,4] benzodiazepine, the chloro- 5,10- dihydros -11- oxos -11H- two of 8-
After benzo [B, E] [Isosorbide-5-Nitrae] diaza is completely dissolved, adds crosslinking agent and be stirred so that the hydrophilic and oleophilic of reactor solution is put down
Weighing apparatus value is 5.4~8.4, and insulation stands 24~44 hours；
4th step：When agitator speed is 144 rpm~224 rpm, sequentially add dibenzo [B, F] [Isosorbide-5-Nitrae] sulphur azatropylidene-
11- [10H] ketone, 11- piperazines-dibenzo [B, F] [1,4] sulphur azatropylidene hydrochloride, 4- amino-2-methyl -10H- thiophene [2,3-
B] [1,5] benzodiazepine hydrochloride and (5H) -one of 2- aryl -2,3- dihydros -1,5- benzothiaheptylyin -4, lift reactor
Pressure, the MPa of 1.94 MPa~2.74 is reached, temperature is 144 DEG C~264 DEG C, polymerisation 14~24 hours；React
Reacting kettle inner pressure is down to 0 MPa after, 24 DEG C~44 DEG C is cooled to, discharging, enters molding press and can be prepared by filter screen（8-
2）.
3. the method for work of hydraulic station device is supplied in a kind of carbon tetrachloride processing, it is characterised in that this method includes following several
Individual step：
1st step：Staff will supply the hydraulic pressure oil inlet and injection pump of hydraulic station（4）Socket connection that oil-out is seamless, simultaneously
Switch on power；
2nd step：Staff presses control system（10）On start button, start pump oil motor（1）, in pump oil motor（1）
Under driving, injection pump（4）By supply reservoir（8）Interior fluid is pumped out by oil pipeline, there is provided is used to supply hydraulic station；
3rd step：In injection pump（4）During pumping out fluid, pressure detecting table（5）Monitoring supply reservoir in real time（8）Interior oil pressure
Situation；When pressure detecting table（5）Detect supply reservoir（8）When interior oil pressure is higher than default value A, control system（10）Control
Hydraulic lifting piston processed（3）Rise, to supply reservoir（8）Carry out row pressure；When pressure detecting table（5）Detect supply reservoir（8）
When interior oil pressure reaches default value A, control system（10）Close hydraulic lifting piston（3）；
4th step：Proportional velocity regulating valve（6）Fluid spray feed speed is monitored in real time；Work as proportional velocity regulating valve（6）Detect fluid spray feed speed
When rate is less than 10cm/ms, control system（10）Scaling up flow speed control valve（6）Aperture；Work as proportional velocity regulating valve（6）Detect that fluid sprays
When transmission rate is higher than 20cm/ms, control system（10）Reduce proportional velocity regulating valve（6）Aperture；
5th step：In injection pump（4）During pumping out fluid, part fluid enters oil return mechanism by oil pipe（7）In；Oil return
Filter（7-1）Purification filtering is carried out to oil return, through oil back chamber（7-4）Pass through return line（7-5）Oil return is to supply reservoir（8）
It is interior；
6th step：Oil return amount detector（7-3）To the real-time monitoring of recirculating oil quantity；When oil return amount detector（7-3）Detect recirculating oil quantity height
When 20ml, oil return amount detector（7-3）Electric signal is sent to control system（10）, control system（10）Interior calculating storage
Unit is by recirculating oil quantity data storage and generates form, while increases flow control valve（7-2）Aperture；
7th step：Positioned at supply reservoir（8）Interior filter screen（8-2）Fluid is filtered, filter screen glues viscosity detector（8-3）It is right
Filter screen（8-2）Viscous viscosity monitors in real time, when filter screen glues viscosity detector（8-3）Detect filter screen（8-2）Viscous viscosity is higher than 75%
When, control system（10）Alarm signal is sent, reminds staff to carry out cleaning process；
8th step：Fluid liquid level detector（8-4）To supply reservoir（8）Interior fluid liquid level monitors in real time, when fluid level sensing
Device（8-4）Detect supply reservoir（8）When interior fluid is less than 50ml, control system（10）Interior warning lamp flicker, reminds work
Make personnel and carry out oiling process；
9th step：Oil liquid temperature detector（8-5）To supply reservoir（8）Interior oil liquid temperature monitors in real time, when oil liquid temperature detects
Device（8-5）Detect supply reservoir（8）When interior oil liquid temperature is higher than 98 DEG C, control system（10）Start fan cooler（2）,
Fan cooler（2）Fluid is cooled by airduct；When oil liquid temperature detector（8-5）Detect supply reservoir（8）It is interior
Oil liquid temperature be less than 25 DEG C when, control system（10）Stop fan cooler（2）.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611176123.6A CN106640793B (en) | 2016-12-19 | 2016-12-19 | Hydraulic station device and its method of work are supplied in a kind of carbon tetrachloride processing |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611176123.6A CN106640793B (en) | 2016-12-19 | 2016-12-19 | Hydraulic station device and its method of work are supplied in a kind of carbon tetrachloride processing |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106640793A CN106640793A (en) | 2017-05-10 |
| CN106640793B true CN106640793B (en) | 2017-12-29 |
Family
ID=58823155
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611176123.6A Active CN106640793B (en) | 2016-12-19 | 2016-12-19 | Hydraulic station device and its method of work are supplied in a kind of carbon tetrachloride processing |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106640793B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108147310A (en) * | 2018-02-08 | 2018-06-12 | 徐州工程学院 | A kind of carbon tetrachloride processing centrifuge movement maintenance unit |
| CN108555770A (en) * | 2018-05-22 | 2018-09-21 | 徐州腾睿智能装备有限公司 | A kind of fuel tank equipment for separating liquid from solid in carbon tetrachloride precipitation block end grinding device |
| CN116399411B (en) * | 2023-06-08 | 2023-08-11 | 寿光诺盟化工有限公司 | Flow monitoring device for mixing reaction kettle |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102966641A (en) * | 2011-09-02 | 2013-03-13 | 上海宝冶集团有限公司 | High/low-pressure composite online circulating flushing and pressure testing device for hydraulic system |
| CN103062161A (en) * | 2013-01-31 | 2013-04-24 | 上海理工大学 | Mobile hydraulic pump station meeting high acceleration performance requirement |
| CN203570710U (en) * | 2013-07-09 | 2014-04-30 | 嘉兴博科精密机械有限公司 | Automatic exhaust oil tank |
| CN203685775U (en) * | 2014-02-19 | 2014-07-02 | 王克文 | Hydraulic pump station with synchronizer |
| CN203962561U (en) * | 2014-07-15 | 2014-11-26 | 烟台中宇航空液压有限公司 | A kind of Mobile hydraulic station |
| CN204851859U (en) * | 2015-07-10 | 2015-12-09 | 重庆市博平液压机械有限公司 | Servo energy -saving hydraulic station |
| CN205331080U (en) * | 2016-01-12 | 2016-06-22 | 湖州优创科技有限公司 | Polyurethane spouts hydraulic pressure station of machine of glue |
| CN205559430U (en) * | 2016-05-09 | 2016-09-07 | 武汉齐达康环保科技有限公司 | Forced air cooler structure is put to hydraulic pressure compressor oil incasement |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3864260B2 (en) * | 2004-05-12 | 2006-12-27 | 株式会社大進商工 | Hydraulic cylinder device with integrated hydraulic unit |
-
2016
- 2016-12-19 CN CN201611176123.6A patent/CN106640793B/en active Active
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102966641A (en) * | 2011-09-02 | 2013-03-13 | 上海宝冶集团有限公司 | High/low-pressure composite online circulating flushing and pressure testing device for hydraulic system |
| CN103062161A (en) * | 2013-01-31 | 2013-04-24 | 上海理工大学 | Mobile hydraulic pump station meeting high acceleration performance requirement |
| CN203570710U (en) * | 2013-07-09 | 2014-04-30 | 嘉兴博科精密机械有限公司 | Automatic exhaust oil tank |
| CN203685775U (en) * | 2014-02-19 | 2014-07-02 | 王克文 | Hydraulic pump station with synchronizer |
| CN203962561U (en) * | 2014-07-15 | 2014-11-26 | 烟台中宇航空液压有限公司 | A kind of Mobile hydraulic station |
| CN204851859U (en) * | 2015-07-10 | 2015-12-09 | 重庆市博平液压机械有限公司 | Servo energy -saving hydraulic station |
| CN205331080U (en) * | 2016-01-12 | 2016-06-22 | 湖州优创科技有限公司 | Polyurethane spouts hydraulic pressure station of machine of glue |
| CN205559430U (en) * | 2016-05-09 | 2016-09-07 | 武汉齐达康环保科技有限公司 | Forced air cooler structure is put to hydraulic pressure compressor oil incasement |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106640793A (en) | 2017-05-10 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106640793B (en) | Hydraulic station device and its method of work are supplied in a kind of carbon tetrachloride processing | |
| CN103130356B (en) | Liquid waste treating apparatus and method for treating waste liquid | |
| CN206045816U (en) | Integrated drug adding apparatus | |
| CN215396803U (en) | Automatic change antiseized even polypropylene plastic granules extruder | |
| CN106698741A (en) | Waste liquid treatment system and waste liquid treatment method | |
| CN204588735U (en) | Dosing reaction tank | |
| CN109012454A (en) | A kind of water treatment agent material high-efficiency mixing arrangement | |
| CN208087349U (en) | A kind of waste water sealing and circulating processing unit | |
| CN208771415U (en) | A kind of liquid reagent production highly effective reaction kettle | |
| CN111573947A (en) | Energy-saving environment-friendly sewage treatment device and treatment method thereof | |
| CN202508893U (en) | Efficient air-float pressure air dissolving tank | |
| CN209652023U (en) | A kind of adaptive sewage disposal system | |
| CN211886799U (en) | Intelligent temperature raising and lowering device of chemical manufacturing equipment | |
| CN107631534A (en) | A kind of recirculated water automatic water-supply cooling system | |
| CN209451779U (en) | A kind of liquid medicine device for formulating | |
| CN209853912U (en) | Release agent recovery plant | |
| CN208378551U (en) | Full-automatic low energy consumption high-efficiency pure oxygen dissolving device | |
| CN109019957B (en) | Industrial waste water rapid oxidation device | |
| CN105621747A (en) | Coagulation and air floatation integrated oil field waste water deep treatment device | |
| CN208183323U (en) | Reforming system and cotton processing equipment | |
| CN113003797A (en) | Electroplating wastewater treatment process and equipment thereof | |
| CN202945177U (en) | Amino acid slow-release compound fertilizer coating device | |
| CN105417692A (en) | Water distribution temperature control and automatic stirring and mixing apparatus used for water treatment anaerobic acidification technology | |
| CN205731878U (en) | A kind of circulation liquid mixing system for high viscosity high solids content masking liquid | |
| CN107058927B (en) | A kind of hot galvanizing washing pool with automatic cycle function |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |