CN106626628A - Fluoro-rubber adhesive tape and manufacturing method thereof - Google Patents
Fluoro-rubber adhesive tape and manufacturing method thereof Download PDFInfo
- Publication number
- CN106626628A CN106626628A CN201611023720.5A CN201611023720A CN106626628A CN 106626628 A CN106626628 A CN 106626628A CN 201611023720 A CN201611023720 A CN 201611023720A CN 106626628 A CN106626628 A CN 106626628A
- Authority
- CN
- China
- Prior art keywords
- fluorubber
- adhesive plaster
- parts
- rubber
- fabric
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B25/00—Layered products comprising a layer of natural or synthetic rubber
- B32B25/04—Layered products comprising a layer of natural or synthetic rubber comprising rubber as the main or only constituent of a layer, which is next to another layer of the same or of a different material
- B32B25/042—Layered products comprising a layer of natural or synthetic rubber comprising rubber as the main or only constituent of a layer, which is next to another layer of the same or of a different material of natural rubber or synthetic rubber
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B37/00—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
- B32B37/06—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the heating method
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B37/00—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
- B32B37/10—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the pressing technique, e.g. using action of vacuum or fluid pressure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/30—Properties of the layers or laminate having particular thermal properties
- B32B2307/306—Resistant to heat
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/30—Properties of the layers or laminate having particular thermal properties
- B32B2307/306—Resistant to heat
- B32B2307/3065—Flame resistant or retardant, fire resistant or retardant
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/70—Other properties
- B32B2307/714—Inert, i.e. inert to chemical degradation, corrosion
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2571/00—Protective equipment
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2206—Oxides; Hydroxides of metals of calcium, strontium or barium
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2217—Oxides; Hydroxides of metals of magnesium
- C08K2003/2224—Magnesium hydroxide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Fluid Mechanics (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses a fluoro-rubber adhesive tape and a manufacturing method thereof. The fluoro-rubber adhesive tape comprises a basic fabric and a rubber layer. The basic fabric is a grid fabric, rubber is arranged on two sides of the grid fabric and are fit through fabric mesh holes. The manufacturing method comprises the steps that the fluoro-rubber is plastified and mixed according to a formula, and mixed rubber having good processing properties is formed by adopting a thin-passing process for aiding; the mixed rubber is prepared into the continuous adhesive tape with the thickness of 0.15-0.20 mm through a calendaring process; the grid fabric is arranged between the two adhesive tapes for sulfur bulging, so that the purpose of fitting and vulcanizing the calendared rubber adhesive tape and the grid fabric is achieved, the vulcanizing temperature is 150-180 DEG C, and the time is 6-15 minutes. The fluoro-rubber adhesive tape produced by adopting the manufacturing method is retardant to flame, high in stripping firmness, resistant to high temperature and corrosion from acid, alkali, a strong oxidant, benzene and other organic solvents.
Description
Technical field
The present invention relates to chemical protection material production technical field, more particularly to a kind of fluorubber adhesive plaster and its making side
Method.
Background technology
Fluorubber material is fire-retardant, corrosion-resistant, heat-resisting quantity is good, is usually used in chemical protection field, but fluorubber is excellent because of its
Chemical stability cause the combination of itself and other materials difficult, the stripping of rubber and base fabric is shown as in adhesive plaster production process
Fastness is low, protective materials delamination, the problem of foaming easily occurs.In order to strengthen the peel strength of fluororubber layer and base fabric, generally
Rubber is carried out and with or base fabric pre-processed, existing complex treatment process and rubberized fabric barrier propterty can be caused big
Width declines or makes its feel be hardened.Therefore, the rubberized fabric that prepared by existing process can not fully meet high-performance protective equipment
Using need.
The content of the invention
To solve above-mentioned technical problem, it is an object of the invention to provide a kind of fluorubber adhesive plaster and preparation method thereof, described
Fluorubber adhesive plaster can fire-retardant, high temperature resistant, resistance to strong acid, highly basic, strong oxidizer corrosion, manufacture craft high with the peel strength of base fabric
Simply.
The purpose of the present invention is realized by following technical scheme:
A kind of fluorubber adhesive plaster, including:Base fabric and rubber layer;The base fabric is net fibric, in the both sides of net fibric
Rubber is set, and the rubber fits through Fabric mesh.
A kind of preparation method of fluorubber adhesive plaster, including:
Fluorubber, magnesium hydroxide, calcium hydroxide, age resistor, vulcanizing agent and titanium dioxide are plasticated, kneaded, makes to be formed
Elastomeric compound;
The elastomeric compound is rolled, continuous adhesive plaster of the thickness between 0.15mm~0.20mm is prepared;
Net fibric is placed between two-layer rubberized fabric, and drum-type sulfuration 6min is carried out in the case where temperature is for 150 DEG C~180 DEG C
~12min, makes calendering adhesive plaster reach sulfuration with the net fibric, fit, and forms fluorubber adhesive plaster.
Compared with prior art, one or more embodiments of the invention can have the advantage that:
The fluorubber adhesive plaster that the present invention is provided, with the contrast of preventing rubber material on the market, protection level is high, and functionality advantage is bright
Aobvious, process is simple, low production cost can be used as the material of main part of high-level chemical protection clothes or product.
Description of the drawings
Fig. 1 is the section structure schematic diagram of fluorubber adhesive plaster.
Specific embodiment
To make the object, technical solutions and advantages of the present invention clearer, below in conjunction with embodiment and accompanying drawing to this
It is bright to be described in further detail.
As shown in figure 1, for the section structure of fluorubber adhesive plaster, including base fabric 2 and rubber layer 1;The base fabric is knitted for grid
Thing, in the both sides of net fibric rubber is arranged, and the rubber fits through Fabric mesh.
Above-mentioned elastomeric material is made up of following mass component:Fluorubber, magnesium hydroxide, calcium hydroxide, age resistor, sulfuration
Agent and titanium dioxide, above-mentioned material mass component is:100 parts of fluorubber, 10~30 parts of magnesium hydroxide, 5~15 parts of calcium hydroxide is prevented
1~5 part of old agent, 5~10 parts of vulcanizing agent, 10~50 parts of titanium dioxide.
The vulcanizing agent be N, N- dicinnamylidene -1,6 hexamethylene diamines.
The present embodiment additionally provides a kind of preparation method of fluorubber adhesive plaster, following examples:
Embodiment 1
By 100 parts of fluorubber, 10 parts of magnesium hydroxide, 15 parts of calcium hydroxide, 3 parts of age resistor, 5 parts of vulcanizing agent, titanium dioxide 30
Part is plasticated, is kneaded, and makes to form elastomeric compound;
The elastomeric compound is rolled, sequential like adhesive plaster of the thickness in 0.15mm is prepared, rolling temperature is 80 DEG C, speed
Spend for 20m/min;
Net fibric is placed between two-layer rubberized fabric, and drum-type sulfuration 10min is carried out in the case where temperature is for 170 DEG C, make pressure
Prolong adhesive plaster to reach sulfuration with the net fibric, fit, form fluorubber adhesive plaster.
Fluorubber adhesive plaster thickness prepared by said method is 0.40mm, weight is 550g/m2.Fastness is peeled off with base fabric
0.81N/m, limited oxygen index is 29, and fracture strength is up to 350N/5cm, resistance to 98% sulfuric acid, 40% NaOH, 61% nitre
Acid, 120min is impermeable, and outward appearance is good.Can be used to make heavy chemical protecting suit.
Embodiment 2
100 parts of fluorubber, 15 parts of calcium hydroxide, 2 parts of age resistor, 6 parts of vulcanizing agent, 20 parts of titanium dioxide are plasticated, mixed
Refining, makes to form elastomeric compound.
Elastomeric compound is rolled into the sequential like adhesive plaster that thickness is 0.18mm by way of calendering, rolling temperature is 80 DEG C,
Speed is 20m/min.
Sulfuration laminating:Aramid fiber net fibric is put between two-layer fluorubber adhesive plaster, enters bulging sulfuration, trilaminate material is slight
Apply tension force, it is ensured that enter smooth when rousing sulphur equipment.Curing temperature is 180 DEG C, it is ensured that cure time is 10min.
The thickness of the fluorubber adhesive plaster that the present embodiment makes is 0.45mm, and limited oxygen index is 36.4, and fracture strength is reachable
500N/5cm, resistance to 98% concentrated sulfuric acid, 40% NaOH, 60% nitric acid, 200min is impermeable, and outward appearance is good.
The fluorubber adhesive plaster that above-described embodiment 2 is made carries out anti-strong oxidizer test, and test method is as follows:
Fluorubber adhesive plaster test surfaces are clamped on chemical agent penetration tester, fluorubber adhesive plaster opposite side places oxygen
Change discoloration and indicate paper, strong oxidizer dinitrogen tetroxide 1mL is added by filling opening, stopper filling opening, observation indicates that paper color becomes
Change to judge whether rubber blanket permeates.
Test result shows:The rubberized fabric is resistant to that strong oxidizer dinitrogen tetroxide solution 1h is not saturating, and rubberized fabric surface is slight
Fade, illustrate that the fluorubber adhesive plaster has powerful oxidation corrosion resistance agent function.
Although disclosed herein embodiment as above, described content is only to facilitate understanding the present invention and adopting
Embodiment, is not limited to the present invention.Technical staff in any the technical field of the invention, without departing from this
On the premise of the disclosed spirit and scope of invention, any modification and change can be made in the formal and details implemented,
But the scope of patent protection of the present invention, still must be defined by the scope of which is defined in the appended claims.
Claims (7)
1. a kind of fluorubber adhesive plaster, it is characterised in that include:Base fabric and rubber layer;The base fabric is net fibric, is knitted in grid
The both sides of thing arrange rubber, and the rubber fits through Fabric mesh.
2. fluorubber adhesive plaster as claimed in claim 1, it is characterised in that the elastomeric material include fluorubber, magnesium hydroxide,
Calcium hydroxide, age resistor, vulcanizing agent and titanium dioxide, above-mentioned material mass component is:100 parts of fluorubber, magnesium hydroxide 10~30
Part, 5~15 parts of calcium hydroxide, 1~5 part of age resistor, 5~10 parts of vulcanizing agent, 10~50 parts of titanium dioxide.
3. fluorubber adhesive plaster as claimed in claim 1, it is characterised in that the vulcanizing agent is N, N- dicinnamylidene -1,6 oneself
Diamines.
4. a kind of preparation method of fluorubber adhesive plaster, it is characterised in that methods described includes:
Fluorubber, magnesium hydroxide, calcium hydroxide, age resistor, vulcanizing agent and titanium dioxide are plasticated, kneaded, makes to form mixing
Glue;
The elastomeric compound is rolled, continuous adhesive plaster of the thickness between 0.15mm~0.20mm is prepared;
Net fibric is placed between two-layer rubberized fabric, and temperature be 150 DEG C~180 DEG C at carry out drum-type sulfuration 6min~
12min, makes calendering adhesive plaster reach sulfuration with the net fibric, fit, and forms fluorubber adhesive plaster.
5. the preparation method of fluorubber adhesive plaster as claimed in claim 4, it is characterised in that the constituent of the elastomeric compound
For:100 parts of fluorubber, 10~30 parts of magnesium hydroxide, 5~15 parts of calcium hydroxide, 1~5 part of age resistor, 5~10 parts of vulcanizing agent, titanium
10~50 parts of white powder.
6. the preparation method of fluorubber adhesive plaster as claimed in claim 4, it is characterised in that the vulcanizing agent is N, bis- meat of N-
Gui Ji -1,6 hexamethylene diamines.
7. the preparation method of fluorubber adhesive plaster as claimed in claim 4, it is characterised in that the fluorubber adhesive plaster thickness is
Between 0.35mm~0.45mm, weight be 400g/m2~850g/m2。
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201611023720.5A CN106626628A (en) | 2016-11-14 | 2016-11-14 | Fluoro-rubber adhesive tape and manufacturing method thereof |
Applications Claiming Priority (1)
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CN201611023720.5A CN106626628A (en) | 2016-11-14 | 2016-11-14 | Fluoro-rubber adhesive tape and manufacturing method thereof |
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ID=58807526
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CN201611023720.5A Pending CN106626628A (en) | 2016-11-14 | 2016-11-14 | Fluoro-rubber adhesive tape and manufacturing method thereof |
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Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109130396A (en) * | 2018-08-01 | 2019-01-04 | 扬中市橡胶塑料厂有限公司 | A kind of fluororubber cloth clamp offset plate and its processing technology |
CN109466085A (en) * | 2017-11-17 | 2019-03-15 | 南漳富元鼎航空器材配件有限公司 | A kind of oil-resistant high-temperature high pressure canvas filler rubber diaphragm |
CN111941968A (en) * | 2020-08-10 | 2020-11-17 | 南京曼可新材料有限公司 | Pressure-resistant and corrosion-resistant rubber air bag cloth composite material and preparation method thereof |
CN112810288A (en) * | 2021-01-15 | 2021-05-18 | 江苏彩阳环保科技有限公司 | Bonding forming preparation process of grid glass fiber silica gel adhesive tape |
CN112895504A (en) * | 2021-01-15 | 2021-06-04 | 江苏彩阳环保科技有限公司 | High-temperature bonding and shaping preparation process based on grid aramid fiber fluororubber cloth |
WO2022109815A1 (en) * | 2020-11-24 | 2022-06-02 | 徐网红 | Two-sided grid aramid fiber silicon rubber cloth |
WO2022109814A1 (en) * | 2020-11-24 | 2022-06-02 | 徐网红 | Double-sided mesh aramid fluororubber cloth |
CN114571744A (en) * | 2022-04-21 | 2022-06-03 | 内蒙古工业大学 | Fiber preform reinforced resin rubber ternary composite material and preparation method and application thereof |
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Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109466085A (en) * | 2017-11-17 | 2019-03-15 | 南漳富元鼎航空器材配件有限公司 | A kind of oil-resistant high-temperature high pressure canvas filler rubber diaphragm |
CN109130396A (en) * | 2018-08-01 | 2019-01-04 | 扬中市橡胶塑料厂有限公司 | A kind of fluororubber cloth clamp offset plate and its processing technology |
CN111941968A (en) * | 2020-08-10 | 2020-11-17 | 南京曼可新材料有限公司 | Pressure-resistant and corrosion-resistant rubber air bag cloth composite material and preparation method thereof |
CN111941968B (en) * | 2020-08-10 | 2024-01-26 | 南京曼可新材料有限公司 | Pressure-resistant corrosion-resistant rubber airbag cloth composite material and preparation method thereof |
WO2022109815A1 (en) * | 2020-11-24 | 2022-06-02 | 徐网红 | Two-sided grid aramid fiber silicon rubber cloth |
WO2022109814A1 (en) * | 2020-11-24 | 2022-06-02 | 徐网红 | Double-sided mesh aramid fluororubber cloth |
CN112810288A (en) * | 2021-01-15 | 2021-05-18 | 江苏彩阳环保科技有限公司 | Bonding forming preparation process of grid glass fiber silica gel adhesive tape |
CN112895504A (en) * | 2021-01-15 | 2021-06-04 | 江苏彩阳环保科技有限公司 | High-temperature bonding and shaping preparation process based on grid aramid fiber fluororubber cloth |
CN114571744A (en) * | 2022-04-21 | 2022-06-03 | 内蒙古工业大学 | Fiber preform reinforced resin rubber ternary composite material and preparation method and application thereof |
CN114571744B (en) * | 2022-04-21 | 2024-04-26 | 内蒙古工业大学 | Fiber preform reinforced resin rubber ternary composite material and preparation method and application thereof |
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TA01 | Transfer of patent application right | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20170921 Address after: 100101 9702 Box 15, Beijing Applicant after: HEALTH AND EPIDEMIC PREVENTION TEAM, GENERAL ARMAMENT DEPARTMENT, PLA Applicant after: Beijing Bangwei High-Tech Special Textile Co., Ltd. Address before: 100101 9702 Box 15, Beijing, Chaoyang District Applicant before: HEALTH AND EPIDEMIC PREVENTION TEAM, GENERAL ARMAMENT DEPARTMENT, PLA |
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Application publication date: 20170510 |