CN106622035A - Overhead tank for dropwise adding thionyl chloride - Google Patents
Overhead tank for dropwise adding thionyl chloride Download PDFInfo
- Publication number
- CN106622035A CN106622035A CN201610874063.9A CN201610874063A CN106622035A CN 106622035 A CN106622035 A CN 106622035A CN 201610874063 A CN201610874063 A CN 201610874063A CN 106622035 A CN106622035 A CN 106622035A
- Authority
- CN
- China
- Prior art keywords
- groove
- thionyl chloride
- cylinder
- charging aperture
- head tank
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C317/00—Sulfones; Sulfoxides
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2204/00—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
- B01J2204/002—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Devices For Medical Bathing And Washing (AREA)
Abstract
The invention discloses an overhead tank for dropwise adding thionyl chloride, belongs to the technical field of overhead tanks and aims to solve the problem that improper handling at feeding ports and discharging ports is prone to causing diffusion of toxic smell, discomfort of human body and damage to physical health of people when overhead tanks are used for dropwise adding thionyl chloride in the prior art. The overhead tank comprises a supporting foot, a barrel arranged on the supporting foot, a feeding port and a discharging port, and the feeding port and the discharging port are arranged on the barrel; at the feeding port, a thionyl chloride smoke treating device is arranged on the barrel and comprises a groove and a groove cover hermetically matched with the groove, a smoke treating liquid tank is arranged in the groove, a pipeline port is arranged on the side wall of the groove, and the feeding port is arranged in the groove. The overhead tank is used for dropwise adding thionyl chloride.
Description
Technical field
One kind is added dropwise thionyl chloride head tank, for the dropwise addition of thionyl chloride, belongs to head tank technical field.
Background technology
Thionyl chloride is faint yellow to red, fuming liquids, there is intense stimulus smell.It is miscible in benzene, chloroform, carbon tetrachloride
Deng organic solvent.Meet water hydrolysis, heat resolve.Mainly for the manufacture of acyl chloride, agricultural chemicals, medicine, dyestuff etc. are additionally operable to
Production.The iodide of some metals can be dissolved, sulfurous acid and hydrochloric acid are decomposed into water.Be heated to about 140 DEG C then resolve into chlorine,
Sulfur dioxide and sulfur monoxide.Sulfonic acid chloride is generated with sulfonic acid reaction, with the grignard reagent reacting corresponding sulfoxide compound of generation.With
The phenol of hydroxyl, the reaction of alcohol organic matter generate corresponding chloride, and its chlorine atom substituted hydroxy sulfydryl ability significantly, may be used also sometimes
Replace sulfur dioxide, hydrogen, oxygen.
It is harmful to body after suction, oral or percutaneous absorbtion.There is strong thorn to eyes, mucous membrane, skin and the upper respiratory tract
Swash effect, can cause and burn.After suction, possible throat, bronchial spasm, inflammation and oedema and it is lethal.Poisoning manifestations can have burning
Burn sense, cough, dizziness, laryngitis, shortness of breath, headache, nausea and vomiting.
When thionyl chloride dropwise addition is carried out using head tank, when charging aperture and discharging opening are dealt with improperly, easily cause
Distributing for poison gas taste, causes personal discomfort, endangers the healthy of people.
The content of the invention
The present invention for above-mentioned weak point provide it is a kind of thionyl chloride head tank is added dropwise, solve in prior art
When carrying out thionyl chloride dropwise addition using head tank, when charging aperture and discharging opening are dealt with improperly, dissipating for toxic odor is easily caused
Send out, cause personal discomfort, endanger the healthy of people.
To achieve these goals, the technical solution used in the present invention is：
One kind is added dropwise thionyl chloride head tank, including leg, the cylinder being arranged on leg, the charging arranged on cylinder
Mouth and discharging opening, it is characterised in that：At charging aperture, the flue gas processing device of a thionyl chloride, the flue gas are provided with cylinder
Processing meanss include a groove, the groove lid being engaged with groove sealing, and fume treatment liquid bath, the side of groove are provided with groove
A pipeline opening is provided with wall, charging aperture is arranged in groove.
Further, the charging aperture is arranged on the bottom of groove.
Further, dividing plate is provided with the groove, fume treatment liquid bath is movably arranged in the groove that dividing plate is separated out.
Further, the tip position in the cylinder is provided with the hollow cone structure of top and bottom opening, open circles
The top of wimble structure is connected with charging aperture, and the bottom of hollow cone structure is connected with cylinder, arranges in hollow cone structure
There is shower, shower is extended to outside cylinder.
Further, in the cylinder, a pipeline is provided with charging aperture, pipeline extends to the bottom of cylinder.
Compared with prior art, it is an advantage of the current invention that：
When the first, thionyl chloride being added into head tank, feed pipe is inserted from the pipeline opening of recess sidewall by feed pipe,
Again pipeline is inserted into charging aperture, if charging aperture coordinates not in place with feed pipe, cause the situation of flue gas, flue gas to reach recessed
During groove, flue gas is processed by the liquid in fume treatment liquid bath, you can reduce the discharge of harmful substance, it is ensured that people's
Identity health；
2nd, the setting of dividing plate, is, in order to fume treatment liquid bath is spaced one from, to be easy to activity to install fume treatment liquid bath and enter
The recovery and replacing of row liquid；
3rd, the setting of the shower in hollow cone structure and hollow cone structure, is in order to be able to more effective spray
Thionyl chloride on the inwall of the cleaning head tank of formula；
4th, pipeline extends to the bottom of cylinder, and when being to prevent from adding liquid very few, liquid need to first be attached to open circles
On wimble structure, the waste of liquid is caused.
Description of the drawings
Fig. 1 is the structural representation of the present invention.
Specific embodiment
With reference to the accompanying drawings and examples the present invention is further illustrated.
Embodiment 1
One kind is added dropwise thionyl chloride head tank, including leg 1, and the cylinder 2 being arranged on leg 1 is arranged on cylinder 2
Charging aperture 3 and discharging opening 4, at charging aperture 3, are provided with the flue gas processing device 5 of a thionyl chloride, at the flue gas on cylinder 2
Reason device 5 includes a groove 6, the groove lid 7 being engaged with the sealing of groove 6, and in groove 6 fume treatment liquid bath 8, groove are provided with
A pipeline opening 9 is provided with 6 side wall, charging aperture 3 is arranged in groove 6.When thionyl chloride is added into head tank, by charging
Pipeline inserts feed pipe from the pipeline opening of recess sidewall, then pipeline is inserted into charging aperture, if charging aperture is matched somebody with somebody with feed pipe
Close not in place, cause the situation of flue gas, when flue gas reaches groove, by the liquid in fume treatment liquid bath to flue gas at
Reason, you can reduce the discharge of harmful substance, it is ensured that the identity health of people.
Embodiment 2
One kind is added dropwise thionyl chloride head tank, including leg 1, and the cylinder 2 being arranged on leg 1 is arranged on cylinder 2
Charging aperture 3 and discharging opening 4, at charging aperture 3, are provided with the flue gas processing device 5 of a thionyl chloride, at the flue gas on cylinder 2
Reason device 5 includes a groove 6, the groove lid 7 being engaged with the sealing of groove 6, and in groove 6 fume treatment liquid bath 8, groove are provided with
A pipeline opening 9 is provided with 6 side wall, charging aperture 3 is arranged in groove 6.When thionyl chloride is added into head tank, by charging
Pipeline inserts feed pipe from the pipeline opening of recess sidewall, then pipeline is inserted into charging aperture, if charging aperture is matched somebody with somebody with feed pipe
Close not in place, cause the situation of flue gas, when flue gas reaches groove, by the liquid in fume treatment liquid bath to flue gas at
Reason, you can reduce the discharge of harmful substance, it is ensured that the identity health of people.Dividing plate 10, fume treatment are provided with the groove 6
Liquid bath 8 is movably arranged in the groove 6 that dividing plate 10 is separated out.
Embodiment 3
One kind is added dropwise thionyl chloride head tank, including leg 1, and the cylinder 2 being arranged on leg 1 is arranged on cylinder 2
Charging aperture 3 and discharging opening 4, at charging aperture 3, are provided with the flue gas processing device 5 of a thionyl chloride, at the flue gas on cylinder 2
Reason device 5 includes a groove 6, the groove lid 7 being engaged with the sealing of groove 6, and in groove 6 fume treatment liquid bath 8, groove are provided with
A pipeline opening 9 is provided with 6 side wall, charging aperture 3 is arranged in groove 6.When thionyl chloride is added into head tank, by charging
Pipeline inserts feed pipe from the pipeline opening of recess sidewall, then pipeline is inserted into charging aperture, if charging aperture is matched somebody with somebody with feed pipe
Close not in place, cause the situation of flue gas, when flue gas reaches groove, by the liquid in fume treatment liquid bath to flue gas at
Reason, you can reduce the discharge of harmful substance, it is ensured that the identity health of people.Dividing plate 10, fume treatment are provided with the groove 6
Liquid bath 8 is movably arranged in the groove 6 that dividing plate 10 is separated out.Tip position in the cylinder 2 is provided with top and bottom opening
Hollow cone structure 11, the top of hollow cone structure 11 is connected with charging aperture 3, the bottom of hollow cone structure 11 and cylinder
Body 2 is connected, and shower 12 is provided with hollow cone structure 11, and shower 12 is extended to outside cylinder 2.
Dividing plate of the present invention is engaged with groove lid, and pipe hole is provided with dividing plate.The charging aperture 3 is arranged on recessed
The bottom of groove 6.In the cylinder 2, a pipeline 13 is provided with charging aperture 3, pipeline 13 extends to the bottom of cylinder 2.Discharging opening 4
On may also set up flue gas processing device 5.
Claims (5)
1. it is a kind of that thionyl chloride head tank, including leg (1), the cylinder (2) being arranged on leg (1), on cylinder (2) is added dropwise
The charging aperture (3) and discharging opening (4) of setting, it is characterised in that：Charging aperture (3) place, cylinder is provided with a thionyl chloride on (2)
Flue gas processing device (5), the flue gas processing device (5) includes a groove (6), the groove lid being engaged with groove (6) sealing
(7), fume treatment liquid bath (8) is provided with groove (6), a pipeline opening (9), charging aperture is provided with the side wall of groove (6)
(3) it is arranged in groove (6).
2. one kind according to claim 1 is added dropwise thionyl chloride head tank, it is characterised in that：The charging aperture (3) sets
Put the bottom in groove (6).
3. one kind according to claim 1 is added dropwise thionyl chloride head tank, it is characterised in that：Set in the groove (6)
Dividing plate (10) is equipped with, fume treatment liquid bath (8) is movably arranged in the groove (6) that dividing plate (10) is separated out.
4. one kind according to claim 1 is added dropwise thionyl chloride head tank, it is characterised in that：In the cylinder (2)
Tip position is provided with the hollow cone structure (11) of top and bottom opening, the top of hollow cone structure (11) and charging aperture
(3) it is connected, the bottom of hollow cone structure (11) is connected with cylinder (2), and hollow cone structure is provided with spray on (11)
Pipe (12), shower (12) extends to cylinder (2) outward.
5. one kind according to claim 1 is added dropwise thionyl chloride head tank, it is characterised in that：In the cylinder (2), enter
A pipeline (13) is provided with material mouth (3), pipeline (13) extends to the bottom of cylinder (2).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610874063.9A CN106622035A (en) | 2016-09-30 | 2016-09-30 | Overhead tank for dropwise adding thionyl chloride |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610874063.9A CN106622035A (en) | 2016-09-30 | 2016-09-30 | Overhead tank for dropwise adding thionyl chloride |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106622035A true CN106622035A (en) | 2017-05-10 |
Family
ID=58854758
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610874063.9A Pending CN106622035A (en) | 2016-09-30 | 2016-09-30 | Overhead tank for dropwise adding thionyl chloride |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106622035A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112897487A (en) * | 2021-04-07 | 2021-06-04 | 浙江三美化工股份有限公司 | Preparation method and feeding device of lithium bis (fluorosulfonyl) imide |
-
2016
- 2016-09-30 CN CN201610874063.9A patent/CN106622035A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112897487A (en) * | 2021-04-07 | 2021-06-04 | 浙江三美化工股份有限公司 | Preparation method and feeding device of lithium bis (fluorosulfonyl) imide |
| CN112897487B (en) * | 2021-04-07 | 2022-06-03 | 浙江三美化工股份有限公司 | Preparation method and feeding device of lithium bis (fluorosulfonyl) imide |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170510 |