CN106621930A - Mixing device for preparing high purity lithium carbonate by lithium Zhifu - Google Patents

Mixing device for preparing high purity lithium carbonate by lithium Zhifu Download PDF

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Publication number
CN106621930A
CN106621930A CN201611146646.6A CN201611146646A CN106621930A CN 106621930 A CN106621930 A CN 106621930A CN 201611146646 A CN201611146646 A CN 201611146646A CN 106621930 A CN106621930 A CN 106621930A
Authority
CN
China
Prior art keywords
agitator
lithium carbonate
lithium
female
gate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201611146646.6A
Other languages
Chinese (zh)
Inventor
邹辉飞
朱强辉
钟亮
黄艳军
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
YICHUN YINLI NEW ENERGY CO Ltd
Original Assignee
YICHUN YINLI NEW ENERGY CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by YICHUN YINLI NEW ENERGY CO Ltd filed Critical YICHUN YINLI NEW ENERGY CO Ltd
Priority to CN201611146646.6A priority Critical patent/CN106621930A/en
Publication of CN106621930A publication Critical patent/CN106621930A/en
Withdrawn legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/90Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms 
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05Stirrers
    • B01F27/07Stirrers characterised by their mounting on the shaft
    • B01F27/074Stirrers characterised by their mounting on the shaft having two or more mixing elements being concentrically mounted on the same shaft
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05Stirrers
    • B01F27/11Stirrers characterised by the configuration of the stirrers
    • B01F27/19Stirrers with two or more mixing elements mounted in sequence on the same axis
    • B01F27/191Stirrers with two or more mixing elements mounted in sequence on the same axis with similar elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/10Maintenance of mixers
    • B01F35/13Maintenance of mixers using one or more of the components of the mixture to wash-out the mixer
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/10Maintenance of mixers
    • B01F35/145Washing or cleaning mixers not provided for in other groups in this subclass; Inhibiting build-up of material on machine parts using other means
    • B01F35/1452Washing or cleaning mixers not provided for in other groups in this subclass; Inhibiting build-up of material on machine parts using other means using fluids
    • B01F35/1453Washing or cleaning mixers not provided for in other groups in this subclass; Inhibiting build-up of material on machine parts using other means using fluids by means of jets of fluid, e.g. air
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/50Mixing receptacles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/71Feed mechanisms
    • B01F35/712Feed mechanisms for feeding fluids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00Lithium compounds
    • C01D15/08Carbonates; Bicarbonates

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)
  • Accessories For Mixers (AREA)

Abstract

The invention discloses a mixing device for preparing high purity lithium carbonate by lithium Zhifu. The mixing device comprises a motor, a stirring barrel, a machine body and a machine door. The lower side of the motor is connected to a rotary shaft, liquid injection ports are formed inside liquid tanks, a rotary rod is mounted in the middle of the machine body, stirring plates are mounted on the rotary rod, pipelines in the stirring plate are connected to the liquid tanks, an unloading valve is mounted in the bottom of the stirring barrel, a filling layer is formed between the machine body and the stirring barrel, a sampling port is formed in the right side of the machine body, a handle is mounted on the machine door, and an observation window is mounted in the lower side of the machine door. According to the mixing device for preparing high purity lithium carbonate by lithium Zhifu disclosed by the invention, pipelines are mounted in the stirring rod and the stirring plate, and the pipelines are connected to the liquid injection ports through the liquid tanks; additives and water can scour a mixture on the stirring plate below from the stirring plate above through a nozzle, so that the mixing device is convenient to clean, and the condition that the materials are in chaos to react is avoided, too.

Description

A kind of lithium is female to prepare high-purity lithium carbonate mixing arrangement
Technical field
The present invention relates to lithium mother prepares high-purity lithium carbonate field, the female high-purity lithium carbonate for preparing of specially a kind of lithium uses mixed Attach together and put.
Background technology
Lithium and salt are strategic materials significant in national economy and national defense construction, are also and people's life breath manner of breathing The energy and material of pass.As the basis of lithium salts --- lithium carbonate, particularly pure Lithium Carbonate, because with excellent performance, it should With more extensive.When pure Lithium Carbonate is manufactured, the first step is to mix lithium carbonate with other solution, at this moment needs mixing dress Put to complete.
Mixing arrangement number of species in the market has had much, and existing mixing arrangement is mostly to fall material Enter in agitator, be stirred for uniformly, but mixture is often stained with blade, on the one hand be inconvenient to clean, on the other hand Easily cause material chaotic, produce reaction, affect the making of high-purity lithium carbonate.
The content of the invention
It is an object of the invention to provide a kind of lithium is female to prepare high-purity lithium carbonate mixing arrangement, to solve existing mixing Mixture is often stained with blading, on the one hand is inconvenient to clean, on the other hand easily cause material confusion, produced anti- Should, affect the problem of the making of high-purity lithium carbonate.
For achieving the above object, the present invention provides following technical scheme:A kind of female high-purity lithium carbonate for preparing of lithium uses mixed Attach together and put, including motor, agitator, body and gate, the motor lower section is connected with rotary shaft, and is provided with rotary shaft Liquid tank, the liquid tank outside is provided with liquid injection port, and swingle, and swingle top are provided with the middle of the internal body Portion is connected with rotary shaft, top in agitating plate, and agitating plate is provided with the swingle and is provided with pipeline, the agitating plate Interior pipeline is connected with liquid tank, and agitating plate lower section is provided with the spout being connected with pipeline, and the stirring bottom of the barrel is installed There is discharge valve, and agitator is arranged on internal body, and packed layer, and agitator lower section peace are provided between the body and agitator Equipped with support, the body right side is provided with sample tap, and handle is provided with the gate, and gate is arranged on body outside, Baffle plate is installed, the gate lower section is provided with observation window on the agitator in the gate, and observation window outside be provided with it is close Seal.
Preferably, the liquid injection port, liquid tank and pipeline are provided with two.
Preferably, the sample tap is provided with three, and installed in differing heights.
Preferably, the stirring bottom of the barrel is set to " u "-shaped structure, and observation window setting height(from bottom) and stirring bottom of the barrel phase Together.
Preferably, the packed layer is set to vacuum layer.
Preferably, the baffle plate setting is slide construction device.
Compared with prior art, the invention has the beneficial effects as follows:The lithium is female to prepare high-purity lithium carbonate mixing arrangement Pipeline is installed in puddler and agitating plate, and pipeline is connected with liquid injection port by liquid tank, additive and water Mixture that can be on the agitating plate from the agitating plate of top by spout to lower section washes away so that convenient cleaning, Avoid and cause material chaotic, aitiogenic situation, in addition, sample tap is provided with into three, and installed in differing heights, one Aspect can take out the mixture of differing heights to be contrasted, and be conducive to pinpointing the problems corresponding measure of take in time, the opposing party When face reaction end is needed separation of solid and liquid, first liquid can be bled off by sample tap, so as to reduce operation, mitigate work The work pressure of personnel.
Description of the drawings
Fig. 1 is schematic structural view of the invention;
Fig. 2 is outboard structure schematic diagram of the present invention.
In figure:1st, liquid injection port, 2, liquid tank, 3, motor, 4, rotary shaft, 5, swingle, 6, pipeline, 7, sample tap, 8th, agitating plate, 9, spout, 10, discharge valve, 11, support, 12, agitator, 13, packed layer, 14, body, 15, gate, 16, Hand, 17, baffle plate, 18, sealing ring, 19, observation window.
Specific embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clearly and completely Description, it is clear that described embodiment is only a part of embodiment of the invention, rather than the embodiment of whole.Based on this Embodiment in bright, the every other enforcement that those of ordinary skill in the art are obtained under the premise of creative work is not made Example, belongs to the scope of protection of the invention.
Fig. 1-2 is referred to, the present invention provides a kind of technical scheme:A kind of lithium is female to prepare high-purity lithium carbonate mixing dress Put, including liquid injection port 1, liquid tank 2, motor 3, rotary shaft 4, swingle 5, pipeline 6, sample tap 7, agitating plate 8, spout 9, Discharge valve 10, support 11, agitator 12, packed layer 13, body 14, gate 15, handle 16, baffle plate 17, sealing ring 18 and observation Window 19, the lower section of motor 3 is connected with rotary shaft 4, and liquid tank 2 is provided with rotary shaft 4, and the outside of liquid tank 2 is provided with liquid Inlet 1, the bosom of body 14 is provided with swingle 5, and the top of swingle 5 is connected with rotary shaft 4, pacifies on swingle 5 Pipeline 6 is installed equipped with top in agitating plate 8, and agitating plate 8, the pipeline 6 in agitating plate 8 is connected with liquid tank 2, and stirs The lower section of plate 8 is provided with the spout 9 being connected with pipeline 6, and liquid injection port 1, liquid tank 2 and pipeline 6 are provided with two, agitator 12 bottoms are provided with discharge valve 10, and agitator 12 is arranged on inside body 14, and filling is provided between body 14 and agitator 12 Layer 13, and the lower section of agitator 12 is provided with support 11, packed layer 13 is set to vacuum layer, reduces ambient temperature to agitator 12 The impact of interior mixture, the right side of body 14 is provided with sample tap 7, and sample tap 7 is provided with three, and installed in differing heights, can Contrasted with taking out the mixture of differing heights, be conducive to pinpointing the problems corresponding measure of take in time, installed on gate 15 There is handle 16, and gate 15 is arranged on the outside of body 14, and baffle plate 17 is provided with the agitator 12 in gate 15, baffle plate 17 is arranged For slide construction device, the lower section of gate 15 is provided with observation window 19, and the outside of observation window 19 is provided with sealing ring 18, agitator 12 Bottom is set to " u "-shaped structure, and the setting height(from bottom) of observation window 19 is identical with the bottom of agitator 12, is conducive to output mixture, " U " The bottom of shape structure is conducive to material turning, improves the uniformity, and the setting height(from bottom) of observation window 19 is identical with the bottom of agitator 12 can be with Staff's mixture directly perceived is made, conveniently observes and be aware of when to carry out further work.
Operation principle:Before using the female preparation high-purity lithium carbonate mixing arrangement of the lithium, need to whole mixing Device carries out simple structure understanding, and the whole process for processing can generally carry out the division of three parts, and handle is held first Hand 16 opens gate 15, pulls open baffle plate 17, and lithium carbonate is poured in agitator 12, then baffle plate 17 and gate 15 are shut, from liquid Body inlet 1 pours additive into, then additive influent groove 2, then from the flow ipe 6 of liquid tank 2, then flows into agitating plate 8 pipeline 6, finally flows out from spout 9, the top of part stream to lower section agitating plate 8, and the material of the top of agitating plate 8 is washed away Fall, meanwhile, motor 3 is rotated axle 4 so that swingle 5 drives agitating plate 8 to be stirred, and another part additive is in stirring Under the rotation of plate 8, it is thrown under the influence of centrifugal force on the inwall of agitator 12, then slides to bottom and the material product of agitator 12 Raw reaction, staff can be contrasted from the mixture of the taking-up differing heights of sample tap 7, it is also possible to by observation window 19 Observed, after hybrid reaction terminates, discharge valve 10 can be opened and take out in mixture.
Although being described in detail to the present invention with reference to the foregoing embodiments, for a person skilled in the art, It still can modify to the technical scheme described in foregoing embodiments, or which part technical characteristic is carried out etc. With replacing, all any modification, equivalent substitution and improvements within the spirit and principles in the present invention, made etc. should be included in this Within the protection domain of invention.

Claims (6)

1. a kind of lithium is female prepares high-purity lithium carbonate mixing arrangement, including motor(3), agitator(12), body(14)With Gate(15), it is characterised in that:The motor(3)Lower section and rotary shaft(4)It is connected, and rotary shaft(4)Inside it is provided with liquid Groove(2), the liquid tank(2)Outside is provided with liquid injection port(1), the body(14)Bosom is provided with swingle (5), and swingle(5)Top and rotary shaft(4)It is connected, the swingle(5)On agitating plate is installed(8), and agitating plate (8)Interior top is provided with pipeline(6), the agitating plate(8)Interior pipeline(6)With liquid tank(2)It is connected, and agitating plate(8) Lower section is provided with and pipeline(6)The spout being connected(9), the agitator(12)Bottom is provided with discharge valve(10), and agitator (12)Installed in body(14)Inside, the body(14)With agitator(12)Between be provided with packed layer(13), and agitator (12)Lower section is provided with support(11), the body(14)Right side is provided with sample tap(7), the gate(15)On handle is installed Hand(16), and gate(15)Installed in body(14)Outside, the gate(15)Interior agitator(12)On baffle plate is installed (17), the gate(15)Lower section is provided with observation window(19), and observation window(19)Outside is provided with sealing ring(18).
2. a kind of lithium according to claim 1 is female prepares high-purity lithium carbonate mixing arrangement, it is characterised in that:It is described Liquid injection port(1), liquid tank(2)And pipeline(6)It is provided with two.
3. a kind of lithium according to claim 1 is female prepares high-purity lithium carbonate mixing arrangement, it is characterised in that:It is described Sample tap(7)Three are provided with, and installed in differing heights.
4. a kind of lithium according to claim 1 is female prepares high-purity lithium carbonate mixing arrangement, it is characterised in that:It is described Agitator(12)Bottom is set to " u "-shaped structure, and observation window(19)Setting height(from bottom) and agitator(12)Bottom is identical.
5. a kind of lithium according to claim 1 is female prepares high-purity lithium carbonate mixing arrangement, it is characterised in that:It is described Packed layer(13)It is set to vacuum layer.
6. a kind of lithium according to claim 1 is female prepares high-purity lithium carbonate mixing arrangement, it is characterised in that:It is described Baffle plate(17)It is set to slide construction device.
CN201611146646.6A 2016-12-13 2016-12-13 Mixing device for preparing high purity lithium carbonate by lithium Zhifu Withdrawn CN106621930A (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
CN201611146646.6A CN106621930A (en) 2016-12-13 2016-12-13 Mixing device for preparing high purity lithium carbonate by lithium Zhifu

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Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2012143712A (en) * 2011-01-13 2012-08-02 Toray Ind Inc Dynamic mixer
CN203725154U (en) * 2014-02-18 2014-07-23 合肥安利聚氨酯新材料有限公司 DMF (dimethylformamide) solvent spraying feeding device
CN204710187U (en) * 2015-06-01 2015-10-21 安徽诚泰环保工程有限公司 A kind of rotary flue dust desulfurization purifier
CN204768369U (en) * 2015-06-29 2015-11-18 惠州市建科实业有限公司 Novel stirred tank
CN204799271U (en) * 2015-07-01 2015-11-25 施婷婷 High quality reation kettle
CN204973653U (en) * 2015-07-07 2016-01-20 新乡东方工业科技有限公司 Technology can washing apparatus
CN105457580A (en) * 2014-08-14 2016-04-06 无锡成博科技发展有限公司 Reaction kettle
CN205157245U (en) * 2015-11-19 2016-04-13 襄阳亚克化学有限公司 Sampling system
CN105536591A (en) * 2016-01-13 2016-05-04 薛成俊 Intelligent fodder stirring device with self-cleaning function
CN205413033U (en) * 2016-03-26 2016-08-03 张嘉汉 Thermostatic reaction kettle
CN106076161A (en) * 2016-04-28 2016-11-09 柳江县科益搪瓷有限公司 Agitating device for culture medium of edible fungus
CN206304636U (en) * 2016-12-13 2017-07-07 宜春银锂新能源有限责任公司 A kind of lepidolite prepares high-purity lithium carbonate mixing arrangement

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2012143712A (en) * 2011-01-13 2012-08-02 Toray Ind Inc Dynamic mixer
CN203725154U (en) * 2014-02-18 2014-07-23 合肥安利聚氨酯新材料有限公司 DMF (dimethylformamide) solvent spraying feeding device
CN105457580A (en) * 2014-08-14 2016-04-06 无锡成博科技发展有限公司 Reaction kettle
CN204710187U (en) * 2015-06-01 2015-10-21 安徽诚泰环保工程有限公司 A kind of rotary flue dust desulfurization purifier
CN204768369U (en) * 2015-06-29 2015-11-18 惠州市建科实业有限公司 Novel stirred tank
CN204799271U (en) * 2015-07-01 2015-11-25 施婷婷 High quality reation kettle
CN204973653U (en) * 2015-07-07 2016-01-20 新乡东方工业科技有限公司 Technology can washing apparatus
CN205157245U (en) * 2015-11-19 2016-04-13 襄阳亚克化学有限公司 Sampling system
CN105536591A (en) * 2016-01-13 2016-05-04 薛成俊 Intelligent fodder stirring device with self-cleaning function
CN205413033U (en) * 2016-03-26 2016-08-03 张嘉汉 Thermostatic reaction kettle
CN106076161A (en) * 2016-04-28 2016-11-09 柳江县科益搪瓷有限公司 Agitating device for culture medium of edible fungus
CN206304636U (en) * 2016-12-13 2017-07-07 宜春银锂新能源有限责任公司 A kind of lepidolite prepares high-purity lithium carbonate mixing arrangement

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