CN106621915A - Chromatography filling material automatic homogenizing apparatus - Google Patents
Chromatography filling material automatic homogenizing apparatus Download PDFInfo
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- CN106621915A CN106621915A CN201510724734.9A CN201510724734A CN106621915A CN 106621915 A CN106621915 A CN 106621915A CN 201510724734 A CN201510724734 A CN 201510724734A CN 106621915 A CN106621915 A CN 106621915A
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- manually
- operated gate
- pump
- universal wheel
- paddle
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- Accessories For Mixers (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The invention discloses a homogenizing pot capable of automatically feeding, which is composed of a pipeline, a hand-operated valve A, a control panel assembly, a hand-operated valve B, a pneumatic diaphragm pump, a discharge hatch, a feed inlet, an universal wheel movable support, a hand-operated valve C, a hand-operated valve D, a tank, and a pneumatic stirrer. According to the invention, the valves can be opened/closed by operating the buttons on the control panel assembly, flowing of a material in a pipeline can be controlled, the material can be transported to the homogenizing pot through the pneumatic diaphragm pump, functions of automatic feeding, homogenizing and filling can be realized, a homogenizing process can be automatically carried out, manpower can be saved, pollution of dust on environment is reduced, automation requirement for industrial production can be satisfied, production efficiency is increased, security is enhanced, production cost is reduced, and environment is protected.
Description
Technical field
The present invention relates to a kind of homogenization apparatus, the especially a kind of automatic homogenization apparatus of chromatograph packing material, belong to liquid chromatogram field.
Background technology
With developing rapidly for the industries such as pharmacy, biochemical industry, Preparative Liquid Chromatography obtains more and more extensive development and application, it has also become separates the important method with purifying complex mixture, is particularly suited for the separation of natural products.To be efficiently separated sample, the filling of chromatographic column must is fulfilled for the requirement of continuity, uniformity, stability and the compactness of bed.The filling of chromatographic column, great majority fill post using homogenate method, and an important step for being homogenized method is exactly sufficiently stirred for homogenate and chromatograph packing material, and stationary-phase particle size is suspended in homogenate.For the filling of the major diameter post of commercial production scale, because homogenate amount is more general in more than 100L than larger, there is sizable difficulty in homogenate.
Traditional homogenization apparatus typically have charging aperture on device top, from charging aperture into material are poured chromatograph packing material in homogenate tank by the way of hand feed, after being stirred by motor agitator, discharge material from the discharging opening of tank base.This mode for manually feeding easily sheds overturning during material is poured into, produces substantial amounts of dust polluting environment, brings economic loss, causes potential safety hazard, it is impossible to meet pharmacy corporation GMP authentication requestings.
The content of the invention
It is an object of the invention to provide a kind of automatic homogenization apparatus of chromatograph packing material, can realize the functions such as automatic feed, homogenate, discharging, filling, homogenization process is set to carry out automatically, the problems such as solving traditional homogenization apparatus and need a large amount of manpowers, dust pollution.
Technical scheme is as follows：
This homogenization apparatus is made up of pipeline, manually-operated gate A, Controls Palette, manually-operated gate B, pneumatic diaphragm pump, discharging opening, charging aperture, universal wheel movable supporting frame, manually-operated gate C, manually-operated gate D, tank body, agitator air；Wherein Controls Palette is made up of pump pressure table, stirring pressure gauge, scram button, pump adjusting pressuring knob, stirring adjusting pressuring knob, and agitator air is made up of air motor, paddle；Pneumatic diaphragm pump is connected by screw in the bottom of universal wheel movable supporting frame；Tank body welding is in the bottom of universal wheel movable supporting frame；Controls Palette is welded on the middle part of universal wheel movable supporting frame；Agitator air is connected by screw at the top of tank body；Pipeline, manually-operated gate A, manually-operated gate B, discharging opening, charging aperture, manually-operated gate C, manually-operated gate D are connected to tank base by stainless steel tube and ferrule fitting；Pump pressure table, stirring pressure gauge, scram button, pump adjusting pressuring knob, stirring adjusting pressuring knob are connected by screw on the control panel, and paddle is connected with air motor by bearing pin.Tank body, manually-operated gate A, manually-operated gate B, manually-operated gate C, manually-operated gate D, pipeline, discharging opening, charging aperture and interconnecting tube road are made by Stainless steel 316 L, manufactured, checked and accepted and used by JB/T20074-2005 pharmaceutical machine professional standards, met GMP requirements.Tank inner surface mirror finish, outer surface Asia light is processed.Pneumatic diaphragm pump is used for transported material, adopts compressed air for power source, drives barrier film expansion by gas and shrinks, the change of build-up of pressure, and material is sucked and excluded.For various corrosive liquids, the liquid with particle, high viscosity, volatile, inflammable, hypertoxic liquid, light exhaustion can be taken out.Agitator air is made up of air motor and paddle.Loaded on homogenate tank top, stirring slurry is loaded on tank interior to air motor, and paddle is rectangle paddle.Paddle is driven to complete agitating function by air motor.Pipeline provides closed, pressure, free of contamination carrier for the flowing of logistics.Manually-operated gate A, manually-operated gate B, manually-operated gate C, manually-operated gate D are stainless steel two-way valve, can be ball valve or butterfly valve, for opening and closing pipeline, so as to change the flow direction of material, realize the use function of homogenate tank.Discharging opening, charging aperture are standard sanitary level thimble connector, for the turnover of material.
The present invention is provided the benefit that：
Compared with homogenate tank at present：First, the present invention, disclosure satisfy that industrial automation demand, save manpower, improve production efficiency；Second, material whole process flows in closed pipeline, it is to avoid the dust pollution air of generation, safe；3rd, it is only necessary to which a pneumatic diaphragm pump is capable of achieving charging and discharging function, the low production cost of product；4th, system is met the upper anti-explosion safety of production and is required using pneumatic mode control.
Description of the drawings
Fig. 1 is the structural representation of the present invention
Fig. 2 is structural representation of the agitator air in tank interior
Fig. 3 is the concrete structure schematic diagram of Controls Palette
1st, pipeline
2nd, manually-operated gate A
3rd, Controls Palette
4th, manually-operated gate B
5th, pneumatic diaphragm pump
6th, discharging opening
7th, charging aperture
8th, universal wheel movable supporting frame
9th, manually-operated gate C
10th, manually-operated gate D
11st, tank body
12nd, agitator air
13rd, air motor
14th, paddle
15th, pump pressure table
16th, pressure gauge is stirred
17th, scram button
18th, pump adjusting pressuring knob
19th, adjusting pressuring knob is stirred.
Specific embodiment
The present invention is described in further detail with reference to Fig. 1, Fig. 2, Fig. 3.It is first shut off manually-operated gate B4, manually-operated gate D10, start pneumatic diaphragm pump 5, the mixture of filler and solvent is sucked into tank body 11 from charging aperture 7, being then turned on air motor 13 drives paddle 14 to start stirring, after a period of time, when quantity of solvent is enough, manually-operated gate C9 is turned off, open manually-operated gate D10 and be circulated stirring.It is to be mixed uniform, manually-operated gate A2 is turned off, manually-operated gate B4 is opened, start pneumatic diaphragm pump 5, uniform liquid is discharged from discharging opening 6.
In whipping process, the speed of transported material can be controlled by pump adjusting pressuring knob 18, pressure is observed by pump pressure table 15.The speed for controlling to stir by stirring adjusting pressuring knob 19, pressure is observed by stirring pressure gauge 16.Such as emergency, whole equipment is allowed to stop by pressing scram button 17.
Claims (4)
1. automatic homogenization apparatus of a kind of chromatograph packing material, by pipeline（1）, manually-operated gate A（2）, Controls Palette（3）, manually-operated gate B（4）, pneumatic diaphragm pump（5）, discharging opening（6）, charging aperture（7）, universal wheel movable supporting frame（8）, manually-operated gate C（9）, manually-operated gate D（10）, tank body（11）, agitator air（12）Composition；Wherein Controls Palette（3）By pump pressure table（15）, stirring pressure gauge（16）, scram button（17）, pump adjusting pressuring knob（18）, stirring adjusting pressuring knob（19）Composition；Agitator air（12）By air motor（13）And paddle（14）Composition；Pneumatic diaphragm pump（5）It is connected by screw in universal wheel movable supporting frame（8）Bottom；Tank body（11）It is welded on universal wheel movable supporting frame（8）Bottom；Controls Palette（3）It is welded on universal wheel movable supporting frame（8）Middle part；Agitator air（12）It is connected by screw in tank body（11）Top；Pipeline（1）, manually-operated gate A（2）, manually-operated gate B（4）, discharging opening（6）, charging aperture（7）, manually-operated gate C（9）, manually-operated gate D（10）Tank body is connected to by stainless steel tube and ferrule fitting（11）Bottom；Pump pressure table（15）, stirring pressure gauge（16）, scram button（17）, pump adjusting pressuring knob（18）, stirring adjusting pressuring knob（19）It is connected by screw on the control panel；Paddle（14）With air motor（13）Connected by shaft coupling.
2. a kind of automatic feed according to claim 1 is homogenized tank, it is characterised in that：Described paddle（14）For rectangle paddle.
3. a kind of automatic feed according to claim 1 is homogenized tank, it is characterised in that：Described manually-operated gate A（2）, manually-operated gate B（4）, manually-operated gate C（9）And manually-operated gate D（10）Can be ball valve, butterfly valve.
4. automatic homogenization apparatus of a kind of chromatograph packing material according to claim 1, it is characterised in that：By switching manually-operated gate A（2）, manually-operated gate B（4）, manually-operated gate C（9）And manually-operated gate D（10）Charging, homogenate, discharging, filling process can be automatically performed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510724734.9A CN106621915A (en) | 2015-11-02 | 2015-11-02 | Chromatography filling material automatic homogenizing apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510724734.9A CN106621915A (en) | 2015-11-02 | 2015-11-02 | Chromatography filling material automatic homogenizing apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106621915A true CN106621915A (en) | 2017-05-10 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510724734.9A Pending CN106621915A (en) | 2015-11-02 | 2015-11-02 | Chromatography filling material automatic homogenizing apparatus |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106621915A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117482812A (en) * | 2023-12-27 | 2024-02-02 | 长治市昌路矿山机械设备制造有限公司 | Mining automatic stirring trolley type explosive storage equipment and use method thereof |
-
2015
- 2015-11-02 CN CN201510724734.9A patent/CN106621915A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117482812A (en) * | 2023-12-27 | 2024-02-02 | 长治市昌路矿山机械设备制造有限公司 | Mining automatic stirring trolley type explosive storage equipment and use method thereof |
| CN117482812B (en) * | 2023-12-27 | 2024-03-19 | 长治市昌路矿山机械设备制造有限公司 | Mining automatic stirring trolley type explosive storage equipment and use method thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170510 |
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| WD01 | Invention patent application deemed withdrawn after publication |