CN106621873A - Multi-rotor processing device for preparing nano emulsion and application thereof - Google Patents

Multi-rotor processing device for preparing nano emulsion and application thereof Download PDF

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Publication number
CN106621873A
CN106621873A CN201610371496.2A CN201610371496A CN106621873A CN 106621873 A CN106621873 A CN 106621873A CN 201610371496 A CN201610371496 A CN 201610371496A CN 106621873 A CN106621873 A CN 106621873A
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CN
China
Prior art keywords
sleeve
rotary cutter
rotor
emulsion
pinion
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610371496.2A
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Chinese (zh)
Inventor
蔡顺豪
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Individual
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Individual
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Publication date
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Publication of CN106621873A publication Critical patent/CN106621873A/en
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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40Mixing liquids with liquids; Emulsifying
    • B01F23/41Emulsifying
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40Mixing liquids with liquids; Emulsifying
    • B01F23/41Emulsifying
    • B01F23/414Emulsifying characterised by the internal structure of the emulsion
    • B01F23/4143Microemulsions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40Mixing liquids with liquids; Emulsifying
    • B01F23/43Mixing liquids with liquids; Emulsifying using driven stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/90Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms 
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/94Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with rotary cylinders or cones
    • B01F27/941Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with rotary cylinders or cones being hollow, perforated or having special stirring elements thereon
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/30Driving arrangements; Transmissions; Couplings; Brakes
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M177/00Special methods of preparation of lubricating compositions; Chemical modification by after-treatment of components or of the whole of a lubricating composition, not covered by other classes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/39Mixing of ingredients for grease or lubricating compositions

Abstract

The invention discloses a multi-rotor stirring treatment device for preparing nano emulsion, wherein a plurality of rotor systems are arranged in a master pigeon cage type sleeve, and each rotor system comprises a pinion, a slave pigeon cage type sleeve, a rotary cutter head and a cutter head sleeve; each pinion is meshed with the main gear and drives the rotary cutter head to rotate; the main gear is driven by a motor; the main pigeon house type sleeve and the auxiliary pigeon house type sleeve are respectively provided with a top cover and a bottom cover. According to the invention, the stirring of a plurality of rotors simultaneously increases the effective stirring volume, and can also apply strong shearing and high turbulence stirring to the emulsion; the device has simple and compact structure, low manufacturing cost and convenient and flexible use; the emulsion can be supplied in batches or continuously, and the preparation of a large amount of emulsion is convenient.

Description

For preparing many rotor processing meanss and application thereof of nanoemulsions
Technical field
The present invention relates to the preparation of nanoemulsions, specifically, the present invention relates to be used to prepare many rotors of nanoemulsions Processing meanss and application thereof.
Background technology
Nanoemulsions (emulsion) tool has been widely used, and for example, lubricating oil is made into nanoemulsions (nano lubricating oil), The performance and used life of lubricating oil can be effectively improved.
The preparation method of traditional nanoemulsions is by two kinds of immiscible liquid shapes in the presence of surfactant Into emulsion, nano-particle is obtained Jing after nucleation, coalescence, reunion, heat treatment in microvesicle.Above-mentioned these methods are poorly efficient, high costs , so as to limit the extensive application of nanoemulsions.
The present invention produces high speed vortex conditions using many rotor agitators, by physical and chemical reaction by two kinds or two kinds Above immiscible liquid makes nanoemulsions, it is achieved thereby that the preparation of large batch of nanoemulsions.
The content of the invention
The technical problem to be solved in the present invention is the defect for overcoming prior art, there is provided a kind of for preparing nanoemulsions Many rotor processing meanss.
In order to solve above-mentioned technical problem, the invention provides following technical scheme:
The present invention device be:Multiple rotor-support-foundation systems are set in main dove cage sleeve, each rotor-support-foundation system includes secondary tooth Wheel, secondary dove cage sleeve, rotary cutter, bit sleeve;Each pinion is engaged with master gear, and drives rotary cutter to rotate; Master gear is driven by motor;Main dove cage sleeve and secondary dove cage sleeve have respectively top cover and bottom.
Said apparatus constitute the compartment of three types, and the first is surrounded by main dove cage sleeve, its top cover and bottom, its appearance Receive multiple rotor-support-foundation systems, there is hole corresponding with each rotor-support-foundation system on its top cover and bottom;Second by secondary dove cage sleeve, Its top cover and bottom are surrounded, and it accommodates bit sleeve, are had respectively on its top cover and bottom and to be opened with bit sleeve diameter matches Hole;The third is surrounded by bit sleeve, and it accommodates the rotary cutter for stirring, without top cover and bottom.
The sleeve is the cylindrical rotating body of pivoting, hole or the striped that there is hollow out on barrel.Motor rotary speed For 5,000 to 11,000rpm, very strong vortex can be produced when rotating at a high speed.Motor drives master gear, master gear to drive secondary tooth Take turns with the speed rate rotation of about 1.5~3 times of master gear.When pinion rotates, rotary cutter can be with the speed same with pinion Rate is rotated.
Rotary cutter is surround by bit sleeve, have on the wall of the bit sleeve hollow out of different type and size hole or Striped, as shown in Figure 3.The type and size of hole or striped are relevant with the size of emulsion particle.The device of the present invention can be used for Prepare 5 microns to 50 microns of emulsion.
The knife-edge of rotary cutter radially has certain degree of skewness with cutter head, and its angle is the α angles shown in Fig. 4, preferably For 95~105 degree, particularly preferred 100 degree.Described device can be with the manufacture of stainless steel, aluminium alloy, copper and/or titanium, preferably with not Rust steel making.
The using method of many rotor apparatus for kneading apparatus that the present invention is provided is:Pending emulsion is set to enter edge of a knife sleeve, For example edge of a knife sleeve is entered by the opening below edge of a knife sleeve;Motor is started, master gear rotation drives pinion rotation, secondary Gear drives rotary cutter to rotate;Emulsion after process flows out bit sleeve, detects whether to reach quality standards after collection.
The device of the present invention can be used to prepare nano lubricating oil.When nano lubricating oil is prepared, first to lubricating base oil Nanometer additive, such as NanoLub RC-X additives of NIS companies production, then with the present invention's are added in (base oil) Many rotor apparatus for kneading apparatus are processed.
The beneficial effect that reached of the present invention is:
(1) multiple rotors are stirred and not only increase effective stirred volume simultaneously, moreover it is possible to apply Strong shear, high turbulent flow to emulsion Stirring;
(2) apparatus structure is simply compact, low cost of manufacture, easy to use and flexible;
(3) batch of emulsion or continuous supply can be carried out, the preparation of a large amount of emulsions is convenient for.
Description of the drawings
Accompanying drawing is used for providing a further understanding of the present invention, and constitutes a part for specification, the reality with the present invention Applying example is used to explain the present invention together, is not construed as limiting the invention.In the accompanying drawings:
Fig. 1 is the organigram of described device;It is numbered in figure:101- motors;102- master gears;103- pair teeth Wheel;104- rotary cutters;105- pair dove cage sleeves;The main dove cage sleeves of 106-;107- pair dove cage sleeve bottoms; The main pigeon house formula sleeve caps of 108-;109- bit sleeves.
Fig. 2 is the relation schematic diagram of master gear and three pinions, and what wherein mark 2 and 3 referred to is respectively master gear and pair The tooth of gear.
Fig. 3 is the schematic diagram of bit sleeve, and wherein mark 9 refers to hole or the striped of the hollow out of sleeve lateral wall.
Fig. 4 is rotary cutter and bit sleeve schematic diagram.
Specific embodiment
The preferred embodiments of the present invention are illustrated below in conjunction with accompanying drawing, it will be appreciated that preferred reality described herein Apply example and be merely to illustrate and explain the present invention, be not intended to limit the present invention.
Below the invention will be further described as a example by preparing nano lubricating oil with triple-spool apparatus for kneading apparatus.
As shown in figure 1, arranging three rotor-support-foundation systems in main dove cage sleeve 106, each rotor-support-foundation system includes pinion 103rd, secondary dove cage sleeve 105, rotary cutter 104, bit sleeve 109.Each pinion 103 is engaged with master gear 102, and is driven Dynamic rotary cutter 104 is rotated;Master gear 102 is driven by motor 101.Main dove cage sleeve has top cover and bottom, top cover and bottom It is upper to have perforate corresponding with three rotor-support-foundation systems respectively.
The volume ratio of three kinds of compartments mentioned above is:
1 bit sleeve compartment is 15% with the ratio of secondary dove cage sleeve compartment;
2 bit sleeve compartments are 0.45% with the ratio of main dove cage sleeve compartment;
3 secondary dove cage sleeve compartments and the ratio of main dove cage sleeve compartment are 3%.
Secondary dove cage sleeve 105 is the cylindrical rotating body of pivoting, and side wall also has the through hole of hollow out.
As shown in Fig. 2 the pinion 103 in three rotor-support-foundation systems presses equilateral triangle mode around master gear 102.Motor Master gear is driven to drive pinion with the speed rate rotation of master gear twice.
The knife-edge of rotary cutter is 100 degree with the angle [alpha] of the degree of skewness of cutter head radial direction.The height of cutter head is 18mm, The height of bit sleeve is 25.5mm.
When using, according to product description, in lubrication substrate oil NanoLub RC-X nanometer additives are added.Order is added The lubricating base oil of nanometer additive is flowed into from the bottom opening of the compartment of bit sleeve 109, from secondary dove cage sleeve compartment Flow out, then through main dove cage sleeve compartment, finally flow into fluid reservoir.During this period, motor 101 is started, rotating speed is 10, 000rpm。
Motor drives master gear 102 to rotate, and drives pinion 103 to rotate by master gear 102, is connected with pinion 103 Rotary cutter 104 manufactures a large amount of emulsions with identical speed rate rotation, continuous Stirring.
The treated emulsion that detection is collected, it was demonstrated that apparatus of the present invention generate qualified nano lubricating oil.
Fig. 2 is the relation schematic diagram of master gear and three pinions, and what wherein mark 2 and 3 referred to is respectively master gear and pair The tooth of gear.
Fig. 3 is the schematic diagram of bit sleeve, and wherein mark 9 refers to hole or the striped of the hollow out of sleeve lateral wall.
Fig. 4 is rotary cutter and bit sleeve schematic diagram.
Finally it should be noted that:The preferred embodiments of the present invention are the foregoing is only, the present invention is not limited to, Although being described in detail to the present invention with reference to the foregoing embodiments, for a person skilled in the art, it still may be used To modify to the technical scheme described in foregoing embodiments, or equivalent is carried out to which part technical characteristic. All any modification, equivalent substitution and improvements within the spirit and principles in the present invention, made etc., should be included in the present invention's Within protection domain.

Claims (10)

1. a kind of many rotor apparatus for kneading apparatus for preparing nanoemulsions, it is characterised in that:In main dove cage sleeve (106) Interior to arrange multiple rotor-support-foundation systems, each rotor-support-foundation system includes pinion (103), secondary dove cage sleeve (105), rotary cutter (104), bit sleeve (109);Each pinion (103) is engaged with master gear (102), and drives rotary cutter (104) to rotate; Master gear (102) is driven by motor (101).
2. many rotor apparatus for kneading apparatus according to claim 1, it is characterised in that:Rotary cutter (104) is by tool bit casing Cylinder (109) surround, and has hole or the striped of the hollow out of different type and size on the wall of the bit sleeve (109).
3. many rotor apparatus for kneading apparatus according to claim 1, it is characterised in that:The knife-edge and knife of rotary cutter Head radially has certain degree of skewness, and its angle is 95~105 degree.
4. many rotor apparatus for kneading apparatus according to claim 3, it is characterised in that:The angle ranging from 100 degree.
5. many rotor apparatus for kneading apparatus according to claim 1, it is characterised in that:Described device is closed by stainless steel, aluminium The manufacture of gold, copper and/or titanium.
6. many rotor apparatus for kneading apparatus according to claim 5, it is characterised in that:Described device is by stainless steel making.
7. many rotor apparatus for kneading apparatus according to any one of claim 1-6, it is characterised in that:Main dove cage sleeve (106) three rotor-support-foundation systems are set in.
8. the rotary cutter of many rotor apparatus for kneading apparatus being used for described in claim 1, it is characterised in that:The rotary cutter Knife-edge and cutter head radially have certain degree of skewness, its angle is 95~105 degree.
9. rotary cutter according to claim 8, it is characterised in that:The angle ranging from 100 degree.
10. a kind of method that device with described in claim 1 prepares nanoemulsions, it is characterised in that:By under edge of a knife sleeve The opening of side makes pending emulsion enter edge of a knife sleeve;Motor is started, master gear rotation drives pinion rotation, pinion to drive Dynamic rotary cutter is rotated;Emulsion after process flows out bit sleeve, detects after collection.
CN201610371496.2A 2015-10-28 2016-05-30 Multi-rotor processing device for preparing nano emulsion and application thereof Pending CN106621873A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
HK15110672.7 2015-10-28
HK15110672.7A HK1209266A2 (en) 2015-10-28 2015-10-28 A multi-rotator device for producing nano-emulsion and the use thereof

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Publication Number Publication Date
CN106621873A true CN106621873A (en) 2017-05-10

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CN201620508775.4U Expired - Fee Related CN205925472U (en) 2015-10-28 2016-05-30 Multi-rotor processing device for preparing nano emulsion

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Application Number Title Priority Date Filing Date
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HK (1) HK1209266A2 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
HK1209266A2 (en) * 2015-10-28 2016-03-24 蔡順豪 號 A multi-rotator device for producing nano-emulsion and the use thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101836827A (en) * 2010-01-26 2010-09-22 管云天 Reciprocal rotary knife type material processor
CN201807319U (en) * 2010-08-24 2011-04-27 夏超华 Round mixer with multiple rotors rotating synchronously
WO2012038116A1 (en) * 2010-09-23 2012-03-29 Evonik Rohmax Additives Gmbh Process for producing polymer dispersions
TWM454375U (en) * 2012-10-26 2013-06-01 J D Components Co Ltd Central shaft power output mechanism
CN205925472U (en) * 2015-10-28 2017-02-08 蔡顺豪 Multi-rotor processing device for preparing nano emulsion

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101836827A (en) * 2010-01-26 2010-09-22 管云天 Reciprocal rotary knife type material processor
CN201807319U (en) * 2010-08-24 2011-04-27 夏超华 Round mixer with multiple rotors rotating synchronously
WO2012038116A1 (en) * 2010-09-23 2012-03-29 Evonik Rohmax Additives Gmbh Process for producing polymer dispersions
TWM454375U (en) * 2012-10-26 2013-06-01 J D Components Co Ltd Central shaft power output mechanism
CN205925472U (en) * 2015-10-28 2017-02-08 蔡顺豪 Multi-rotor processing device for preparing nano emulsion

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HK1209266A2 (en) 2016-03-24

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