CN106621873A - Multi-rotor processing device for preparing nano emulsion and application thereof - Google Patents
Multi-rotor processing device for preparing nano emulsion and application thereof Download PDFInfo
- Publication number
- CN106621873A CN106621873A CN201610371496.2A CN201610371496A CN106621873A CN 106621873 A CN106621873 A CN 106621873A CN 201610371496 A CN201610371496 A CN 201610371496A CN 106621873 A CN106621873 A CN 106621873A
- Authority
- CN
- China
- Prior art keywords
- sleeve
- rotary cutter
- rotor
- emulsion
- pinion
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000007908 nanoemulsion Substances 0.000 title claims abstract description 14
- 239000000839 emulsion Substances 0.000 claims abstract description 16
- 238000004519 manufacturing process Methods 0.000 claims abstract description 5
- 238000004898 kneading Methods 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 5
- 239000010935 stainless steel Substances 0.000 claims description 3
- 229910001220 stainless steel Inorganic materials 0.000 claims description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 2
- 229910052802 copper Inorganic materials 0.000 claims description 2
- 239000010949 copper Substances 0.000 claims description 2
- 238000009628 steelmaking Methods 0.000 claims description 2
- 239000010936 titanium Substances 0.000 claims description 2
- 229910052719 titanium Inorganic materials 0.000 claims description 2
- 239000004411 aluminium Substances 0.000 claims 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims 1
- 229910052782 aluminium Inorganic materials 0.000 claims 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims 1
- 229910052737 gold Inorganic materials 0.000 claims 1
- 239000010931 gold Substances 0.000 claims 1
- 238000003756 stirring Methods 0.000 abstract description 7
- 241000272201 Columbiformes Species 0.000 abstract description 5
- 238000002360 preparation method Methods 0.000 abstract description 5
- 238000010008 shearing Methods 0.000 abstract 1
- 239000010687 lubricating oil Substances 0.000 description 7
- 238000010586 diagram Methods 0.000 description 6
- 239000000654 additive Substances 0.000 description 4
- 239000002199 base oil Substances 0.000 description 3
- 230000000996 additive effect Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 230000001050 lubricating effect Effects 0.000 description 2
- 229910000838 Al alloy Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000004581 coalescence Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 238000005461 lubrication Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000002105 nanoparticle Substances 0.000 description 1
- 238000010899 nucleation Methods 0.000 description 1
- 230000006911 nucleation Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/40—Mixing liquids with liquids; Emulsifying
- B01F23/41—Emulsifying
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/40—Mixing liquids with liquids; Emulsifying
- B01F23/41—Emulsifying
- B01F23/414—Emulsifying characterised by the internal structure of the emulsion
- B01F23/4143—Microemulsions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/40—Mixing liquids with liquids; Emulsifying
- B01F23/43—Mixing liquids with liquids; Emulsifying using driven stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/90—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/94—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with rotary cylinders or cones
- B01F27/941—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with rotary cylinders or cones being hollow, perforated or having special stirring elements thereon
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/30—Driving arrangements; Transmissions; Couplings; Brakes
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M177/00—Special methods of preparation of lubricating compositions; Chemical modification by after-treatment of components or of the whole of a lubricating composition, not covered by other classes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
- B01F2101/39—Mixing of ingredients for grease or lubricating compositions
Abstract
The invention discloses a multi-rotor stirring treatment device for preparing nano emulsion, wherein a plurality of rotor systems are arranged in a master pigeon cage type sleeve, and each rotor system comprises a pinion, a slave pigeon cage type sleeve, a rotary cutter head and a cutter head sleeve; each pinion is meshed with the main gear and drives the rotary cutter head to rotate; the main gear is driven by a motor; the main pigeon house type sleeve and the auxiliary pigeon house type sleeve are respectively provided with a top cover and a bottom cover. According to the invention, the stirring of a plurality of rotors simultaneously increases the effective stirring volume, and can also apply strong shearing and high turbulence stirring to the emulsion; the device has simple and compact structure, low manufacturing cost and convenient and flexible use; the emulsion can be supplied in batches or continuously, and the preparation of a large amount of emulsion is convenient.
Description
Technical field
The present invention relates to the preparation of nanoemulsions, specifically, the present invention relates to be used to prepare many rotors of nanoemulsions
Processing meanss and application thereof.
Background technology
Nanoemulsions (emulsion) tool has been widely used, and for example, lubricating oil is made into nanoemulsions (nano lubricating oil),
The performance and used life of lubricating oil can be effectively improved.
The preparation method of traditional nanoemulsions is by two kinds of immiscible liquid shapes in the presence of surfactant
Into emulsion, nano-particle is obtained Jing after nucleation, coalescence, reunion, heat treatment in microvesicle.Above-mentioned these methods are poorly efficient, high costs
, so as to limit the extensive application of nanoemulsions.
The present invention produces high speed vortex conditions using many rotor agitators, by physical and chemical reaction by two kinds or two kinds
Above immiscible liquid makes nanoemulsions, it is achieved thereby that the preparation of large batch of nanoemulsions.
The content of the invention
The technical problem to be solved in the present invention is the defect for overcoming prior art, there is provided a kind of for preparing nanoemulsions
Many rotor processing meanss.
In order to solve above-mentioned technical problem, the invention provides following technical scheme:
The present invention device be:Multiple rotor-support-foundation systems are set in main dove cage sleeve, each rotor-support-foundation system includes secondary tooth
Wheel, secondary dove cage sleeve, rotary cutter, bit sleeve;Each pinion is engaged with master gear, and drives rotary cutter to rotate;
Master gear is driven by motor;Main dove cage sleeve and secondary dove cage sleeve have respectively top cover and bottom.
Said apparatus constitute the compartment of three types, and the first is surrounded by main dove cage sleeve, its top cover and bottom, its appearance
Receive multiple rotor-support-foundation systems, there is hole corresponding with each rotor-support-foundation system on its top cover and bottom;Second by secondary dove cage sleeve,
Its top cover and bottom are surrounded, and it accommodates bit sleeve, are had respectively on its top cover and bottom and to be opened with bit sleeve diameter matches
Hole;The third is surrounded by bit sleeve, and it accommodates the rotary cutter for stirring, without top cover and bottom.
The sleeve is the cylindrical rotating body of pivoting, hole or the striped that there is hollow out on barrel.Motor rotary speed
For 5,000 to 11,000rpm, very strong vortex can be produced when rotating at a high speed.Motor drives master gear, master gear to drive secondary tooth
Take turns with the speed rate rotation of about 1.5~3 times of master gear.When pinion rotates, rotary cutter can be with the speed same with pinion
Rate is rotated.
Rotary cutter is surround by bit sleeve, have on the wall of the bit sleeve hollow out of different type and size hole or
Striped, as shown in Figure 3.The type and size of hole or striped are relevant with the size of emulsion particle.The device of the present invention can be used for
Prepare 5 microns to 50 microns of emulsion.
The knife-edge of rotary cutter radially has certain degree of skewness with cutter head, and its angle is the α angles shown in Fig. 4, preferably
For 95~105 degree, particularly preferred 100 degree.Described device can be with the manufacture of stainless steel, aluminium alloy, copper and/or titanium, preferably with not
Rust steel making.
The using method of many rotor apparatus for kneading apparatus that the present invention is provided is:Pending emulsion is set to enter edge of a knife sleeve,
For example edge of a knife sleeve is entered by the opening below edge of a knife sleeve;Motor is started, master gear rotation drives pinion rotation, secondary
Gear drives rotary cutter to rotate;Emulsion after process flows out bit sleeve, detects whether to reach quality standards after collection.
The device of the present invention can be used to prepare nano lubricating oil.When nano lubricating oil is prepared, first to lubricating base oil
Nanometer additive, such as NanoLub RC-X additives of NIS companies production, then with the present invention's are added in (base oil)
Many rotor apparatus for kneading apparatus are processed.
The beneficial effect that reached of the present invention is:
(1) multiple rotors are stirred and not only increase effective stirred volume simultaneously, moreover it is possible to apply Strong shear, high turbulent flow to emulsion
Stirring;
(2) apparatus structure is simply compact, low cost of manufacture, easy to use and flexible;
(3) batch of emulsion or continuous supply can be carried out, the preparation of a large amount of emulsions is convenient for.
Description of the drawings
Accompanying drawing is used for providing a further understanding of the present invention, and constitutes a part for specification, the reality with the present invention
Applying example is used to explain the present invention together, is not construed as limiting the invention.In the accompanying drawings:
Fig. 1 is the organigram of described device;It is numbered in figure:101- motors;102- master gears;103- pair teeth
Wheel;104- rotary cutters;105- pair dove cage sleeves;The main dove cage sleeves of 106-;107- pair dove cage sleeve bottoms;
The main pigeon house formula sleeve caps of 108-;109- bit sleeves.
Fig. 2 is the relation schematic diagram of master gear and three pinions, and what wherein mark 2 and 3 referred to is respectively master gear and pair
The tooth of gear.
Fig. 3 is the schematic diagram of bit sleeve, and wherein mark 9 refers to hole or the striped of the hollow out of sleeve lateral wall.
Fig. 4 is rotary cutter and bit sleeve schematic diagram.
Specific embodiment
The preferred embodiments of the present invention are illustrated below in conjunction with accompanying drawing, it will be appreciated that preferred reality described herein
Apply example and be merely to illustrate and explain the present invention, be not intended to limit the present invention.
Below the invention will be further described as a example by preparing nano lubricating oil with triple-spool apparatus for kneading apparatus.
As shown in figure 1, arranging three rotor-support-foundation systems in main dove cage sleeve 106, each rotor-support-foundation system includes pinion
103rd, secondary dove cage sleeve 105, rotary cutter 104, bit sleeve 109.Each pinion 103 is engaged with master gear 102, and is driven
Dynamic rotary cutter 104 is rotated;Master gear 102 is driven by motor 101.Main dove cage sleeve has top cover and bottom, top cover and bottom
It is upper to have perforate corresponding with three rotor-support-foundation systems respectively.
The volume ratio of three kinds of compartments mentioned above is:
1 bit sleeve compartment is 15% with the ratio of secondary dove cage sleeve compartment;
2 bit sleeve compartments are 0.45% with the ratio of main dove cage sleeve compartment;
3 secondary dove cage sleeve compartments and the ratio of main dove cage sleeve compartment are 3%.
Secondary dove cage sleeve 105 is the cylindrical rotating body of pivoting, and side wall also has the through hole of hollow out.
As shown in Fig. 2 the pinion 103 in three rotor-support-foundation systems presses equilateral triangle mode around master gear 102.Motor
Master gear is driven to drive pinion with the speed rate rotation of master gear twice.
The knife-edge of rotary cutter is 100 degree with the angle [alpha] of the degree of skewness of cutter head radial direction.The height of cutter head is 18mm,
The height of bit sleeve is 25.5mm.
When using, according to product description, in lubrication substrate oil NanoLub RC-X nanometer additives are added.Order is added
The lubricating base oil of nanometer additive is flowed into from the bottom opening of the compartment of bit sleeve 109, from secondary dove cage sleeve compartment
Flow out, then through main dove cage sleeve compartment, finally flow into fluid reservoir.During this period, motor 101 is started, rotating speed is 10,
000rpm。
Motor drives master gear 102 to rotate, and drives pinion 103 to rotate by master gear 102, is connected with pinion 103
Rotary cutter 104 manufactures a large amount of emulsions with identical speed rate rotation, continuous Stirring.
The treated emulsion that detection is collected, it was demonstrated that apparatus of the present invention generate qualified nano lubricating oil.
Fig. 2 is the relation schematic diagram of master gear and three pinions, and what wherein mark 2 and 3 referred to is respectively master gear and pair
The tooth of gear.
Fig. 3 is the schematic diagram of bit sleeve, and wherein mark 9 refers to hole or the striped of the hollow out of sleeve lateral wall.
Fig. 4 is rotary cutter and bit sleeve schematic diagram.
Finally it should be noted that:The preferred embodiments of the present invention are the foregoing is only, the present invention is not limited to,
Although being described in detail to the present invention with reference to the foregoing embodiments, for a person skilled in the art, it still may be used
To modify to the technical scheme described in foregoing embodiments, or equivalent is carried out to which part technical characteristic.
All any modification, equivalent substitution and improvements within the spirit and principles in the present invention, made etc., should be included in the present invention's
Within protection domain.
Claims (10)
1. a kind of many rotor apparatus for kneading apparatus for preparing nanoemulsions, it is characterised in that:In main dove cage sleeve (106)
Interior to arrange multiple rotor-support-foundation systems, each rotor-support-foundation system includes pinion (103), secondary dove cage sleeve (105), rotary cutter
(104), bit sleeve (109);Each pinion (103) is engaged with master gear (102), and drives rotary cutter (104) to rotate;
Master gear (102) is driven by motor (101).
2. many rotor apparatus for kneading apparatus according to claim 1, it is characterised in that:Rotary cutter (104) is by tool bit casing
Cylinder (109) surround, and has hole or the striped of the hollow out of different type and size on the wall of the bit sleeve (109).
3. many rotor apparatus for kneading apparatus according to claim 1, it is characterised in that:The knife-edge and knife of rotary cutter
Head radially has certain degree of skewness, and its angle is 95~105 degree.
4. many rotor apparatus for kneading apparatus according to claim 3, it is characterised in that:The angle ranging from 100 degree.
5. many rotor apparatus for kneading apparatus according to claim 1, it is characterised in that:Described device is closed by stainless steel, aluminium
The manufacture of gold, copper and/or titanium.
6. many rotor apparatus for kneading apparatus according to claim 5, it is characterised in that:Described device is by stainless steel making.
7. many rotor apparatus for kneading apparatus according to any one of claim 1-6, it is characterised in that:Main dove cage sleeve
(106) three rotor-support-foundation systems are set in.
8. the rotary cutter of many rotor apparatus for kneading apparatus being used for described in claim 1, it is characterised in that:The rotary cutter
Knife-edge and cutter head radially have certain degree of skewness, its angle is 95~105 degree.
9. rotary cutter according to claim 8, it is characterised in that:The angle ranging from 100 degree.
10. a kind of method that device with described in claim 1 prepares nanoemulsions, it is characterised in that:By under edge of a knife sleeve
The opening of side makes pending emulsion enter edge of a knife sleeve;Motor is started, master gear rotation drives pinion rotation, pinion to drive
Dynamic rotary cutter is rotated;Emulsion after process flows out bit sleeve, detects after collection.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
HK15110672.7 | 2015-10-28 | ||
HK15110672.7A HK1209266A2 (en) | 2015-10-28 | 2015-10-28 | A multi-rotator device for producing nano-emulsion and the use thereof |
Publications (1)
Publication Number | Publication Date |
---|---|
CN106621873A true CN106621873A (en) | 2017-05-10 |
Family
ID=55530823
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201610371496.2A Pending CN106621873A (en) | 2015-10-28 | 2016-05-30 | Multi-rotor processing device for preparing nano emulsion and application thereof |
CN201620508775.4U Expired - Fee Related CN205925472U (en) | 2015-10-28 | 2016-05-30 | Multi-rotor processing device for preparing nano emulsion |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201620508775.4U Expired - Fee Related CN205925472U (en) | 2015-10-28 | 2016-05-30 | Multi-rotor processing device for preparing nano emulsion |
Country Status (2)
Country | Link |
---|---|
CN (2) | CN106621873A (en) |
HK (1) | HK1209266A2 (en) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
HK1209266A2 (en) * | 2015-10-28 | 2016-03-24 | 蔡順豪 號 | A multi-rotator device for producing nano-emulsion and the use thereof |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101836827A (en) * | 2010-01-26 | 2010-09-22 | 管云天 | Reciprocal rotary knife type material processor |
CN201807319U (en) * | 2010-08-24 | 2011-04-27 | 夏超华 | Round mixer with multiple rotors rotating synchronously |
WO2012038116A1 (en) * | 2010-09-23 | 2012-03-29 | Evonik Rohmax Additives Gmbh | Process for producing polymer dispersions |
TWM454375U (en) * | 2012-10-26 | 2013-06-01 | J D Components Co Ltd | Central shaft power output mechanism |
CN205925472U (en) * | 2015-10-28 | 2017-02-08 | 蔡顺豪 | Multi-rotor processing device for preparing nano emulsion |
-
2015
- 2015-10-28 HK HK15110672.7A patent/HK1209266A2/en not_active IP Right Cessation
-
2016
- 2016-05-30 CN CN201610371496.2A patent/CN106621873A/en active Pending
- 2016-05-30 CN CN201620508775.4U patent/CN205925472U/en not_active Expired - Fee Related
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101836827A (en) * | 2010-01-26 | 2010-09-22 | 管云天 | Reciprocal rotary knife type material processor |
CN201807319U (en) * | 2010-08-24 | 2011-04-27 | 夏超华 | Round mixer with multiple rotors rotating synchronously |
WO2012038116A1 (en) * | 2010-09-23 | 2012-03-29 | Evonik Rohmax Additives Gmbh | Process for producing polymer dispersions |
TWM454375U (en) * | 2012-10-26 | 2013-06-01 | J D Components Co Ltd | Central shaft power output mechanism |
CN205925472U (en) * | 2015-10-28 | 2017-02-08 | 蔡顺豪 | Multi-rotor processing device for preparing nano emulsion |
Also Published As
Publication number | Publication date |
---|---|
CN205925472U (en) | 2017-02-08 |
HK1209266A2 (en) | 2016-03-24 |
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SE01 | Entry into force of request for substantive examination | ||
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AD01 | Patent right deemed abandoned |
Effective date of abandoning: 20200508 |
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