CN106621428A - Distillation device for treating corrosive high-temperature wastewater - Google Patents

Distillation device for treating corrosive high-temperature wastewater Download PDF

Info

Publication number
CN106621428A
CN106621428A CN201710056253.4A CN201710056253A CN106621428A CN 106621428 A CN106621428 A CN 106621428A CN 201710056253 A CN201710056253 A CN 201710056253A CN 106621428 A CN106621428 A CN 106621428A
Authority
CN
China
Prior art keywords
evaporator
pipeline
product water
water tank
condenser
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710056253.4A
Other languages
Chinese (zh)
Inventor
齐春华
刘洪锟
邢玉雷
吕庆春
苗超
张令品
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tianjin Institute of Seawater Desalination and Multipurpose Utilization SOA
Original Assignee
Tianjin Institute of Seawater Desalination and Multipurpose Utilization SOA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tianjin Institute of Seawater Desalination and Multipurpose Utilization SOA filed Critical Tianjin Institute of Seawater Desalination and Multipurpose Utilization SOA
Priority to CN201710056253.4A priority Critical patent/CN106621428A/en
Publication of CN106621428A publication Critical patent/CN106621428A/en
Pending legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/26Multiple-effect evaporating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/30Accessories for evaporators ; Constructional details thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Heat Treatment Of Water, Waste Water Or Sewage (AREA)

Abstract

The invention discloses a distillation device for treating corrosive high-temperature wastewater. The distillation device comprises a shell body, an evaporator, a condenser, a product water tank, a feedstock water pump, a circulating pump, a product water pump, a concentrated water pump, a vacuum pump, a cooling water pump, a steam ejector, a spraying disc and a foam catching mesh. According to the distillation device, the evaporator is arranged above the condenser in a manner of being of a tower type structure from top to bottom, so that an inter-effect pump is omitted; the evaporator and a coil heat exchanger of the condenser are made from polytetrafluoroethylene, so that the caking resistance and corrosion resistance of the device are enhanced; by adopting a spiral coil pipe structure, the effective heat exchange area is increased; and due to the internal structure and arrangement of the device, the reutilization of heat energy and the lowering of pump energy consumption are achieved. The device disclosed by the invention can be used for efficiently treating the corrosive high-temperature wastewater, is compact in structure, large in loading area and high in thermal efficiency and is resistant to caking and corrosion. The problem that wastewater treatment devices are high in energy consumption and poor in caking resistance and corrosion resistance is solved.

Description

A kind of distilling apparatus for processing corrosive high temperatures waste water
Technical field
The invention belongs to hot waste water water-treatment technology field, more particularly to a kind of steaming for processing corrosive high temperatures waste water Distillation unit.
Background technology
With industrial expansion, water pollution accidents are increasingly deepened, and global water resources shortage crisis increasingly increases, waste water Process can not only mitigate water pollution but also can improve water utilization rate, alleviate water resources shortage crisis, therefore various countries are increased to waste water The dynamics of investment of process, and China is used as the country of moderate water shortage, and in the face of resource-type water shortage and the disaster of water quality type water shortage two Topic, thus accelerate water-saving policy and put into effect progress, expedite the emergence of and expand stain disease process recovery market.
Most of in common waste water is corrosive high temperatures waste water, such as Metallurgical Waste Water, paper waste, coke-oven gas waste water Deng, although produce that industry is different, its composition is also different, but can all produce easy fouling during its process, corrosivity is strong, energy consumption is high etc. Problem.Low-temperature multi-effect has realized large-scale application as ripe desalination technology, has an advantage in that the step for realizing energy Utilize, improve energy utilization rate, effective reducing energy consumption.Therefore low temperature multiple-effect distillation technology is applied in the process of hot waste water The shortcoming of high energy consumption can effectively be overcome, and the nucleus equipment of low-temperature multi-effect is heat exchanger, traditional heat exchanger is metallic recuperator, There are many weak points:Common metal heat exchanger has the shortcomings that perishable, energy consumption is higher and heat transfer coefficient changes greatly;With Heat exchanger made by the materials such as graphite, ceramics, with frangible, volume is big and the low shortcoming of efficiency;And use noble dilute metal material system Into heat exchanger it is expensive, it is difficult to popularization and application.
The content of the invention
The purpose of the present invention is to overcome the deficiencies in the prior art, there is provided a kind of distillation dress of process corrosive high temperatures waste water Put.
Technical scheme is summarized as follows:
A kind of distilling apparatus for processing corrosive high temperatures waste water, including housing 11, raw material water pump 22, steam jet ejector 14, Concentrated water pump 15, vavuum pump 16, product water pump 18, cooling water pump 19, circulating pump 20 is provided with tilting dividing plate, institute in housing State tilting dividing plate and space in housing is separated into into from bottom to top condenser 21, sump evaporator 10, central evaporator 24 and top Portion's evaporimeter 5;The position of condenser and each evaporimeter is provided with product water tank in housing outer surface;In housing top wall Lower surface and the lower surface on top of each tilting dividing plate be provided with the vertical hanging deck of perforate;In the following table of housing top wall The lower surface of the middle and lower part of face and each tilting dividing plate is connected by connecting rod with shower tray;It is provided with below shower tray Coil heat exchanger, one end of coil heat exchanger is connected with the upper perforate of vertical hanging deck, the outlet side of steam inlet joint with it is vertical The upper perforate connection of hanging deck;The other end of coil heat exchanger is connected through housing sidewall with the product water tank;In evaporimeter Mist eliminating net is provided between housing sidewall and vertical hanging deck below steam inlet joint;Steam jet ejector 14 is by pipeline and top The inlet end connection of the steam inlet joint 12 of portion's evaporimeter 5;Each product water tank upper is connected respectively by pipeline with vavuum pump 16 Connect;The bottom of roof evaporator product water tank 6 is connected by U-tube with the top of central evaporator product water tank 8;Centre evaporation The bottom of device product water tank is connected by U-tube with the top of sump evaporator product water tank 9;Sump evaporator product water tank Bottom is connected by U-tube with the top of condenser product water tank 17;The bottom of condenser product water tank is by pipeline and product Water pump 18 connects;The entrance point of circulating pump 20 is connected with the bottom of condenser 21, the port of export point two-way of circulating pump 20, leads up to Pipeline is connected with cooling water pump 19, separately leads up to pipeline and is connected with the shower tray 2 of roof evaporator;The bottom of roof evaporator Connected with the shower tray 7 of adjacent central evaporator by U-tube;The bottom of middle part evaporimeter is by U-tube and adjacent bottom The shower tray 27 of portion's evaporimeter connects;The bottom of sump evaporator is connected by pipeline with concentrated water pump 15;Roof evaporator 5 is located at Side wall between steam inlet joint and mist eliminating net by pipeline with from central evaporator product water tank 8 pipeline converge after with The inlet end connection of the steam inlet joint in central evaporator 24;Central evaporator 24 is located at steam inlet joint and mist eliminating net Between side wall by pipeline with from sump evaporator product water tank 9 pipeline converge after and sump evaporator 10 on steam The inlet end connection of inlet suction port;Sump evaporator 10 is located at the side wall between steam inlet joint and mist eliminating net by pipeline point Two-way, all the way pipeline be connected with the ejecting port 26 of steam jet ejector 14, the steam inlet joint of another road pipeline and condenser 21 Inlet end connection;Raw material water pump 22 is connected by pipeline with the shower tray 25 in condenser, and central evaporator is 1-15.
Preferably, the material of coil heat exchanger is polytetrafluoroethylene (PTFE).
The shape of cross section of housing 11 is preferably circular, rectangle or ellipse.
Steam jet ejector 14 is preferably vertical mode and arranges.
Tilting dividing plate is selected from 5-15 ° with the angle of horizontal plane.
Condenser and each evaporimeter are connected between any two by flange.
Advantages of the present invention:
(1) present invention by N (N >=2) imitate evaporimeter from it is upper it is straight under in tower structure be arranged in condenser top, make device whole Body structure is more compact, and equipment filling rate is higher, saves floor space;Save effect between pump, water generation ratio be 1.8-15 in the range of, System power consumption reduces by 18% or so.
(2) present invention by the use of polytetrafluoroethylene (PTFE) as the material of evaporimeter, make evaporimeter corrosion resistant performance more preferably, stain resistance Extremely strong, heat transfer property is more stable, extends the time of equipment normal work, reduces operating cost.
(3) the characteristics of present invention combines polytetrafluoroethylene (PTFE) easy processing, easy-formation, by coil heat exchanger spiral coil is processed as Form, increase heat exchange area in effective space, save space.
(4) connected using flange between evaporimeter of the present invention, be capable of achieving modularization evaporimeter effect body quantity and adjust, met not With wastewater treatment scale.
(5) device of the invention, with corrosion resistance and good, heat exchange area is big, power consumption is little, operating flexibility is big, account for Ground area is little, compact conformation, installs the advantages of safeguarding convenient.
Description of the drawings
Fig. 1 is a kind of structural representation of the distilling apparatus of process corrosive high temperatures waste water.
Specific embodiment
Below by Figure of description, the present invention is further illustrated.
The present invention is further illustrated by taking 1 central evaporator as an example.
A kind of distilling apparatus for processing corrosive high temperatures waste water, is shown in Fig. 1, including housing 11, raw material water pump 22, steam injection Device 14, concentrated water pump 15, vavuum pump 16, product water pump 18, cooling water pump 19, circulating pump 20, be provided with housing tilting every Space in housing is separated into from bottom to top condenser 21, sump evaporator 10, central evaporator 24 by plate, the tilting dividing plate With roof evaporator 5;Tilting dividing plate between condenser 21 and sump evaporator 10 is with shown in 23;It is relative in housing outer surface The position of condenser and each evaporimeter is provided with product water tank;In the lower surface and each tilting dividing plate of housing top wall The lower surface on top is provided with the vertical hanging deck of perforate;Vertical hanging deck in roof evaporator 5 is with shown in 1;In housing top wall Lower surface and the lower surface of middle and lower part of each tilting dividing plate be connected with shower tray by connecting rod;The following table of housing top wall The connecting rod in face is with shown in 3;Coil heat exchanger is provided with below shower tray, the coil heat exchanger in roof evaporator 5 With shown in 4;One end of coil heat exchanger is connected with the upper perforate of vertical hanging deck, the pipe bunchy of coil heat exchanger, bundles of pipe with A variety of spiral forms spiral in evaporimeter, formed high fill-ratio coil pipe, the number of the upper perforate of vertical hanging deck with The number correspondence of pipe in tube bank;The outlet side of steam inlet joint is connected with the upper perforate of vertical hanging deck;Coil heat exchanger it is another One end is connected through housing sidewall with the product water tank;Housing sidewall below the steam inlet joint of evaporimeter and vertical Mist eliminating net is provided between hanging deck;Mist eliminating net in roof evaporator 5 is with shown in 13;Steam jet ejector 14 is by pipeline and top The inlet end connection of the steam inlet joint 12 of portion's evaporimeter 5;Each product water tank upper is connected respectively by pipeline with vavuum pump 16 Connect;The bottom of roof evaporator product water tank 6 is connected by U-tube with the top of central evaporator product water tank 8;Centre evaporation The bottom of device product water tank is connected by U-tube with the top of sump evaporator product water tank 9;Sump evaporator product water tank Bottom is connected by U-tube with the top of condenser product water tank 17;The bottom of condenser product water tank is by pipeline and product Water pump 18 connects;The entrance point of circulating pump 20 is connected with the bottom of condenser 21, the port of export point two-way of circulating pump 20, leads up to Pipeline is connected with cooling water pump 19, separately leads up to pipeline and is connected with the shower tray 2 of roof evaporator;The bottom of roof evaporator Connected with the shower tray 7 of adjacent central evaporator by U-tube;The bottom of middle part evaporimeter is by U-tube and adjacent bottom The shower tray 27 of portion's evaporimeter connects;The bottom of sump evaporator is connected by pipeline with concentrated water pump 15;Roof evaporator 5 is located at Side wall between steam inlet joint and mist eliminating net by pipeline with from central evaporator product water tank 8 pipeline converge after with The inlet end connection of the steam inlet joint in central evaporator 24;Central evaporator 24 is located at steam inlet joint and mist eliminating net Between side wall by pipeline with from sump evaporator product water tank 9 pipeline converge after and sump evaporator 10 on steam The inlet end connection of inlet suction port;Sump evaporator 10 is located at the side wall between steam inlet joint and mist eliminating net by pipeline point Two-way, all the way pipeline be connected with the ejecting port 26 of steam jet ejector 14, the steam inlet joint of another road pipeline and condenser 21 Inlet end connection;Raw material water pump 22 is connected by pipeline with the shower tray 25 in condenser.
Central evaporator is 1-15.
Preferably, the material of coil heat exchanger is polytetrafluoroethylene (PTFE).
The shape of cross section of housing 11 is preferably circular, rectangle or ellipse.
Steam jet ejector 14 is preferably vertical mode and arranges.
Tilting dividing plate is selected from 5 °, 6 °, 7 °, 8 °, 9 °, 10 °, 11 °, 12 °, 13 °, 14 °, 15 ° with the angle of horizontal plane.
Condenser and each evaporimeter are connected between any two by flange.

Claims (6)

1. a kind of distilling apparatus for processing corrosive high temperatures waste water, including housing (11), raw material water pump (22), steam jet ejector (14), concentrated water pump (15), vavuum pump (16), product water pump (18), cooling water pump (19), circulating pump (20) is characterized in that in shell Tilting dividing plate is provided with vivo, and space in housing is separated into from bottom to top condenser (21), bottom by the tilting dividing plate Evaporimeter (10), central evaporator (24) and roof evaporator (5);In housing outer surface relative to condenser and each evaporimeter Position be provided with product water tank;Lower surface on the top of the lower surface and each tilting dividing plate of housing top wall is provided with The vertical hanging deck of perforate;The middle and lower part of the lower surface and each tilting dividing plate of housing top wall lower surface by connecting rod with Shower tray connects;It is provided with coil heat exchanger below shower tray, the upper perforate of one end of coil heat exchanger and vertical hanging deck Connection, the outlet side of steam inlet joint is connected with the upper perforate of vertical hanging deck;The other end of coil heat exchanger runs through housing side Wall is connected with the product water tank;It is provided between housing sidewall and vertical hanging deck below the steam inlet joint of evaporimeter Mist eliminating net;Steam jet ejector (14) is connected by pipeline with the inlet end of the steam inlet joint (12) of roof evaporator (5);Respectively Product water tank upper is connected respectively by pipeline with vavuum pump (16);The bottom of roof evaporator product water tank (6) passes through U-tube It is connected with the top of central evaporator product water tank (8);Evaporated with bottom by U-tube the bottom of central evaporator product water tank The top connection of device product water tank (9);The bottom of sump evaporator product water tank is by U-tube and condenser product water tank (17) Top connection;The bottom of condenser product water tank is connected by pipeline with product water pump (18);Circulating pump (20) entrance point with The bottom connection of condenser (21), the port of export point two-way of circulating pump (20), leads up to pipeline and is connected with cooling water pump (19), Separately lead up to pipeline to be connected with the shower tray (2) of roof evaporator;The bottom of roof evaporator by U-tube with it is adjacent in Between evaporimeter shower tray (7) connection;The bottom of middle part evaporimeter passes through the shower tray of U-tube and adjacent sump evaporator (27) connect;The bottom of sump evaporator is connected by pipeline with concentrated water pump (15);Roof evaporator (5) connects positioned at steam inlet The evaporation of after side wall between head and mist eliminating net is converged by pipeline with the pipeline from central evaporator product water tank (8) and centre The inlet end connection of the steam inlet joint on device (24);Central evaporator (24) is between steam inlet joint and mist eliminating net Side wall by pipeline with from sump evaporator product water tank (9) pipeline converge after and sump evaporator (10) on steam The inlet end connection of inlet suction port;Side wall of the sump evaporator (10) between steam inlet joint and mist eliminating net passes through pipeline Divide two-way, all the way pipeline is connected with the ejecting port (26) of steam jet ejector (14), the steam of another road pipeline and condenser (21) The inlet end connection of inlet suction port;Raw material water pump (22) is connected by pipeline with the shower tray (25) in condenser, centre evaporation Device is 1-15.
2. a kind of distilling apparatus for processing corrosive high temperatures waste water according to claim 1, is characterized in that the coil pipe is changed The material of hot device is polytetrafluoroethylene (PTFE).
3. a kind of distilling apparatus for processing corrosive high temperatures waste water according to claim 1, is characterized in that the housing (11) shape of cross section is circular, rectangle or ellipse.
4. a kind of distilling apparatus for processing corrosive high temperatures waste water according to claim 1, is characterized in that the steam spray Emitter (14) is arranged for vertical mode.
5. a kind of distilling apparatus for processing corrosive high temperatures waste water according to claim 1, is characterized in that described its feature It is tilting dividing plate and the angle of horizontal plane is 5-15 °.
6. a kind of distilling apparatus for processing corrosive high temperatures waste water according to claim 1, is characterized in that condenser and each Evaporimeter is connected between any two by flange.
CN201710056253.4A 2017-01-25 2017-01-25 Distillation device for treating corrosive high-temperature wastewater Pending CN106621428A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710056253.4A CN106621428A (en) 2017-01-25 2017-01-25 Distillation device for treating corrosive high-temperature wastewater

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710056253.4A CN106621428A (en) 2017-01-25 2017-01-25 Distillation device for treating corrosive high-temperature wastewater

Publications (1)

Publication Number Publication Date
CN106621428A true CN106621428A (en) 2017-05-10

Family

ID=58841604

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710056253.4A Pending CN106621428A (en) 2017-01-25 2017-01-25 Distillation device for treating corrosive high-temperature wastewater

Country Status (1)

Country Link
CN (1) CN106621428A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108854125A (en) * 2018-09-11 2018-11-23 首航洁能科技有限公司 A kind of evaporation concentration device of feed liquid

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2154734Y (en) * 1993-03-09 1994-02-02 何晓东 3-effect vacuum concentration evaporator
US5395483A (en) * 1992-07-31 1995-03-07 Al-Hawaj; Osamah M. Rotary apparatus for combined multi flashing and boiling liquids
CN2562830Y (en) * 2002-08-13 2003-07-30 河北工业大学 Dropping film evaporation tower out of horirontal pipe
CN1634834A (en) * 2003-12-29 2005-07-06 淄博万昌科技发展有限公司 Process and device for preparing orthoformate by using byproduct hydrocyanic acid from acrylonitrile production

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5395483A (en) * 1992-07-31 1995-03-07 Al-Hawaj; Osamah M. Rotary apparatus for combined multi flashing and boiling liquids
CN2154734Y (en) * 1993-03-09 1994-02-02 何晓东 3-effect vacuum concentration evaporator
CN2562830Y (en) * 2002-08-13 2003-07-30 河北工业大学 Dropping film evaporation tower out of horirontal pipe
CN1634834A (en) * 2003-12-29 2005-07-06 淄博万昌科技发展有限公司 Process and device for preparing orthoformate by using byproduct hydrocyanic acid from acrylonitrile production

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108854125A (en) * 2018-09-11 2018-11-23 首航洁能科技有限公司 A kind of evaporation concentration device of feed liquid

Similar Documents

Publication Publication Date Title
CN204034294U (en) The board-like forced-circulation evaporator of novel triple effect
CN105403067B (en) One kind utilizes industrial exhaust heat condensed water demisting cooling tower
CN103613155A (en) Heat pipe type low temperature two-effect sea water desalting device
CN202849107U (en) Water ring vacuum negative-pressure evaporation solar-powered seawater desalination device
CN204034287U (en) Board-like thermodynamic steam Compression Evaporation device
CN209500800U (en) A kind of forced circulation MVR evaporator
CN205073697U (en) Falling film evaporator
CN204301555U (en) One utilizes industrial exhaust heat condensed water demist cooling tower
CN203798191U (en) Vapor condensation water recycling device
CN207214849U (en) A kind of mechanical-draft cooling tower group
CN106621428A (en) Distillation device for treating corrosive high-temperature wastewater
CN203123608U (en) Vertical type three-section condensation cooler
CN103185362A (en) Low-position straight heating machine
CN203820474U (en) Flue gas waste heat recovery and utilization device for aluminium hydroxide calcinator
CN206454291U (en) A kind of environmentally friendly falling film evaporator
CN207307226U (en) A kind of methanol rectification recovery system
CN205832659U (en) Ethylene glycol distills multistage energy recovery system
CN206232419U (en) A kind of efficient integrated low temperature multiple-effect distillation sea water desalting device
CN204873907U (en) Hot pressing formula distilled water machine system
CN213060266U (en) Waste water treatment evaporator for alcohol plant
CN210736250U (en) Hot-pressing multi-effect distilled water machine
CN210663442U (en) Waste water direct-feeding lithium bromide absorption heat pump unit
CN106219650A (en) A kind of low-quality bootstrap system of steel plant and using method thereof
CN208265795U (en) A kind of high-salt wastewater evaporation and crystallization system
CN207451656U (en) A kind of continuous removal of ammonia and nitrogen light component organic matter and salt system

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20170510

WD01 Invention patent application deemed withdrawn after publication