CN106619293A - Moisture-preserving and anti-bacterium honeysuckle mask liquid and preparation method thereof - Google Patents

Moisture-preserving and anti-bacterium honeysuckle mask liquid and preparation method thereof Download PDF

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Publication number
CN106619293A
CN106619293A CN201611177578.XA CN201611177578A CN106619293A CN 106619293 A CN106619293 A CN 106619293A CN 201611177578 A CN201611177578 A CN 201611177578A CN 106619293 A CN106619293 A CN 106619293A
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Prior art keywords
honeysuckle
mask liquid
facial mask
peg
solution
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Pending
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CN201611177578.XA
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Chinese (zh)
Inventor
向福
项俊
石长萍
陈瑶
吴龙月
李世升
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Huanggang Normal University
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Huanggang Normal University
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/733—Alginic acid; Salts thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86—Polyethers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005—Antimicrobial preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Engineering & Computer Science (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Biotechnology (AREA)
  • Cosmetics (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)

Abstract

The invention relates to the cosmetic field and discloses moisture-preserving and anti-bacterium honeysuckle mask liquid and a preparation method thereof. The preparation method comprises the following steps: mixing 30%-50% of honeysuckle with a PEG-200 solution, wherein the proportion of the dry weight of the honeysuckle to the volume of the PEG-200 solution is 1g to (20mL-30mL); adding cellulase which is 1%-5% of mass of the honeysuckle to obtain a mixture, regulating the pH value of the mixture to 4-7, maintaining at the temperature of 45-55 DEG C for 1-3 hours, heating to 80-90 DEG C, maintaining the temperature for 10-15 minutes, and carrying out suction filtration on the mixture, so as to obtain the mask liquid. The moisture-preserving and anti-bacterium honeysuckle mask liquid prepared by virtue of the preparation method contains natural anti-bacterium components such as chlorogenic acid and does not need to be added with a preservative; and furthermore, an extracting solution contains moisture-preserving components such as polysaccharides, and the PEG-200 solution has an excellent moisture-preserving effect, so that the honeysuckle mask liquid has an obvious moisture-preserving effect and is natural moisture-preserving and anti-bacterium mask liquid.

Description

A kind of honeysuckle moisture-keeping bacterium-restraining facial mask liquid and preparation method thereof
Technical field
The present invention relates to cosmetic field, more particularly to a kind of moisture-keeping bacterium-restraining facial mask liquid.
Background technology
Honeysuckle contains the pharmacological components such as chlorogenic acid, cyanidenon glycosides, to various pathogens such as Staphylococcus aureus And Causative virus etc. has stronger restraint, also there is in addition clearing heat and detoxicating, wind-heat dissipating medicinal function.Facial mask is used as beauty One of product, has functions that to improve skin.At present the facial mask containing honeysuckle has various, wherein mostly is the honeysuckle for utilizing Aqueous extracts.As the A of patent CN 104887556 discloses a kind of honeysuckle facial mask water, the Flos Lonicerae extractive solution that it is adopted is for by gold Honeysuckle flower concentration is 85～95% ethanol immersion, is soaked at normal temperatures after 20～30h, is filtered, and takes filtrate Rotary Evaporators Ethanol is reclaimed in the evaporation at a temperature of 40～50 DEG C, obtains Flos Lonicerae extractive solution.Complex operation step, the ethanol of extraction needs back The steps such as receipts, extraction time is long, and effect on driving birds is not good.Being applied in facial mask liquid needs to add multiple additives to ensure its effect, Long-Time Service is unfavorable for the health of skin.
The content of the invention
For shortcoming of the prior art, the invention provides a kind of honeysuckle moisture-keeping bacterium-restraining facial mask liquid and its preparation side Method, is extracted using PEG-200 to honeysuckle, using extract as facial mask liquid, is drawn materials natural, no added, with moisturizing, is mended Water, bacteria resistance function are in effect of one.
Specific technical scheme is as follows：
A kind of honeysuckle moisture-keeping bacterium-restraining facial mask liquid, by honeysuckle in PEG-200 solution Jing cellulase degradations, extract system .
Wherein, the ratio of the honeysuckle dry weight and the PEG-200 solution is preferably 1g:20～30mL, the PEG- The mass fraction of 200 solution is preferably 30～50%.
In the present invention, the cellulase quality accounts for the 1～5% of the honeysuckle and the PEG-200 solution gross mass.
Present invention additionally comprises a kind of preparation method of honeysuckle moisture-keeping bacterium-restraining facial mask liquid, comprises the following steps：By honeysuckle Mix with the PEG-200 solution that mass fraction is 30～50%, the ratio of the honeysuckle dry weight and the PEG-200 solution is 1g:20～30mL, adds the cellulase of the quality of Flos Lonicerae 1～5%, and it is 4～7 to adjust mixture ph, and temperature is 45 ～55 DEG C of 1～3h of holding, by temperature 80～90 DEG C of 10～15min of holding are increased to, and suction filtration mixture obtains facial mask liquid.
Preferably, the honeysuckle powder is broken to after the mesh of fineness 60～100, then is mixed with the PEG-200 solution.
In the present invention, also include after the suction filtration：The liquid phase that the suction filtration is obtained is decolourized：With liquid phase matter after the suction filtration Activated carbon decolorizing 6～12h of the amount than 5～10%.
The facial mask liquid prepared in the present invention preferably also includes adaptation step：By the facial mask liquid after the suction filtration or Facial mask liquid after the decolouring dilutes 20～100 times.
Preferably, by dilution after the facial mask liquid addition 0.1～2% described in facial mask liquid quality sodium alginate.
Compared with prior art, it is an advantage of the current invention that：
The present invention draws materials natural with honeysuckle as raw material, and sterilization component is contained in extract；PEG-200 is solvent, to people Body is nontoxic, the characteristics of with good stability and do not destroy organic nutrient therein, and has stronger performance of keeping humidity.This Bright honeysuckle is conducive to the dissolution of effective ingredient of honeysuckle with cellulose hydrolyzation, shortens extraction time.It is with PEG-200 Solvent is extracted, directly by the use of PEG-200 as the moisturizing ingredient of facial mask liquid, it is not necessary to is carried out separation removal again, is simplified Extraction step.The honeysuckle moisture-keeping bacterium-restraining facial mask liquid of the present invention contains the natural bacteriostatic composition such as chlorogenic acid, anti-without the need for addition in addition Rotten agent；And containing moisturizing ingredients such as polysaccharide in extract, PEG-200 also has good moistening effect, moistening effect is a kind of substantially Natural moisture-keeping bacterium-restraining facial mask liquid.
Description of the drawings
Below in conjunction with the accompanying drawings the present invention will be further described.
Fig. 1：Flos Lonicerae extractive solution of the present invention, 50 times of extract, 30% G ＆ W for diluting moisturizing rates in RH43% Rate of descent；
Fig. 2：Flos Lonicerae extractive solution of the present invention, 50 times of extract, 30% G ＆ W for diluting moisturizing rates in RH81% Rate of descent.
Specific embodiment
Below in conjunction with the embodiment in the present invention, the technical scheme in the embodiment of the present invention is carried out clearly and completely Description, it is clear that described embodiment is only a part of embodiment of the invention, rather than the embodiment of whole.Based on this Embodiment in bright, the every other enforcement that those of ordinary skill in the art are obtained under the premise of creative work is not made Example, belongs to the scope of protection of the invention.
A kind of honeysuckle moisture-keeping bacterium-restraining facial mask liquid, by honeysuckle in PEG-200 solution Jing cellulase degradations, extract system .
Honeysuckle used of the invention is preferably dry honeysuckle, the honeysuckle after such as air-drying, dry in the shade or drying.In order to favourable In the extraction that effective ingredient of honeysuckle is faster and better, digested again after preferably honeysuckle is smashed and extracted.The gold Honeysuckle flower smashing fineness is 60～100 mesh, and preferably 70～90 mesh are further 75～85 mesh.
Honeysuckle of the present invention is digested and is extracted in PEG-200 solution.PEG-200 solution both conducts in the present invention Solvent and extractant, for cellulase hydrolysis enzymatic hydrolysis condition is provided, and extracts effective ingredient of honeysuckle, but as facial mask liquid moisturizing into Point, it is no longer necessary to separate and remove.The mass fraction of PEG-200 solution used of the invention is preferably 30～50%, further preferably For 35～45%, specially 40%.
Honeysuckle is mixed with PEG-200 solution first, is obtained mixed liquor.The honeysuckle dry weight and the PEG- The ratio of 200 solution mixing is 1g:20～30mL, preferably 1g:23～28mL, is further 1g:25～27mL.
Cellulase is added to be hydrolyzed in the mixed liquor.The amount that the cellulase is added is that the mixed liquor is total The 1～5% of quality, preferably 2～4%, more preferably 3%.Hydrolysising condition be pH 4～7, preferably pH 5～6, water Solution temperature is 45～55 DEG C, and preferably 48～52 DEG C, hydrolysis time is 1～3h, is further 1.5～2.5h, specially 2h.
After hydrolysis, mixeding liquid temperature is adjusted to 80～90 DEG C and is extracted.It is preferred that Extracting temperature is 83～88 DEG C, enter One step is preferably 85～87 DEG C.Due to honeysuckle Jing cellulose hydrolyzations, the most of dissolution of the active ingredient in honeysuckle, Therefore the very short time is only needed in the extraction stage.The time of extraction step is 10～15min in the present invention, more preferably 11～13min.By extract suction filtration after hydrolyzed, the Flos Lonicerae extractive solution containing chlorogenic acid is obtained, can be used as facial mask liquid.
In order that the Flos Lonicerae extractive solution after extracting has broader use range, Flos Lonicerae extractive solution can be taken off Color.In the present invention Flos Lonicerae extractive solution is decolourized using activated carbon.Preferably, the amount for adding activated carbon is carried for honeysuckle Take the 5～10% of liquid quality, preferably 6～8%；Bleaching time is 6～12h, more preferably 8～10h.
In order that facial mask liquid has more practicality, the extract after extraction or decolouring can be diluted and be used.It is preferred that Extension rate is 20～100 times, is further 40～80 times, further dilutes 50～60 times.Extraction after the dilution Add appropriate sodium alginate in liquid, increase extract viscosity after dilution, it is to avoid dropping liquid.In the present invention, it is preferred to add sea The amount of mosanom is dilute extract quality 0.1～2%, is further 0.5～1.5%, is further 1.0%.Addition Extract after sodium alginate can be used directly as facial mask liquid.
The honeysuckle moisture-keeping bacterium-restraining facial mask liquid of the present invention contains the natural bacteriostatic composition such as chlorogenic acid, without the need for addition anti-corrosion in addition Agent；And containing moisturizing ingredients such as polysaccharide in extract, PEG-200 also has good moistening effect, moistening effect is a kind of day substantially Right moisture-keeping bacterium-restraining facial mask liquid.
Embodiment 1：
A kind of moisture-keeping bacterium-restraining facial mask liquid, its making step includes：
1. prepared by Flos Lonicerae extractive solution：Honeysuckle is dried in the shade naturally, crushes 80 mesh, by solid-liquid ratio 1:27(g:ML) matter is added Amount fraction is 50% PEG-200 solution mixing, under the conditions of 4,55 DEG C of pH, adds the cellulase of 2% mixture quality, Hydrolysis 2h, then at 85 DEG C of extraction 15min, obtains the Flos Lonicerae extractive solution containing chlorogenic acid.
2. decolourize：By extract suction filtration, the activated carbon decolorizing 8h of mass ratio 5% is added in filtrate.
3. dilution allotment：Take the extract 5mL after decolourizing and dilute 50 times, the marine alga of extract quality after the dilution of addition 1% Sour sodium.
Embodiment 2：
A kind of moisture-keeping bacterium-restraining facial mask liquid, its making step includes：
1. prepared by Flos Lonicerae extractive solution：Honeysuckle is dried in the shade naturally, crushes 60 mesh, by solid-liquid ratio 1:21(g:ML) matter is added Amount fraction is 30% PEG-200 solution mixing, under the conditions of 7,50 DEG C of pH, adds the cellulase of 5% mixture quality, Hydrolysis 3h, then at 80 DEG C of extraction 13min, obtains the Flos Lonicerae extractive solution containing chlorogenic acid.
2. decolourize：By extract suction filtration, the activated carbon decolorizing 12h of mass ratio 7% is added in filtrate.
3. dilution allotment：Take the extract 5mL after decolourizing and dilute 30 times, the sea of extract quality after the dilution of addition 0.5% Mosanom.
Embodiment 3：
A kind of moisture-keeping bacterium-restraining facial mask liquid, its making step includes：
1. prepared by Flos Lonicerae extractive solution：Honeysuckle is dried in the shade naturally, crushes 100 mesh, by solid-liquid ratio 1:30(g:ML) add Mass fraction is 40% PEG-200 solution mixing, under the conditions of 5,45 DEG C of pH, adds the cellulose of 3% mixture quality Enzyme, hydrolyzes 1.5h, then at 90 DEG C of extraction 10min, obtains the Flos Lonicerae extractive solution containing chlorogenic acid.
2. decolourize：By extract suction filtration, the activated carbon decolorizing 6h of mass ratio 10% is added in filtrate.
3. dilution allotment：Take the extract 5mL after decolourizing and dilute 100 times, the marine alga of extract quality after the dilution of addition 2% Sour sodium.
Embodiment 4：
Bacteriostatic test：
The preparation of bacteria suspension：By Escherichia coli (Gram-negative bacteria) and aerobacteria (gram-positive bacteria), (Wuhan is big Learn Organism Depositary provide) transposing in beef extract-peptone fluid nutrient medium, in being placed in 37 DEG C of isothermal vibration incubators Culture 12h, 1mL bacterium solutions are drawn in the test tube equipped with 9mL sterilized waters with liquid-transfering gun, and concussion is uniform, bacteria suspension is made, per 10 times Once stepwise dilution is diluted, 10 are taken-5、10-6、10-7The μ L of concentration 100 do coating experiment, each gradient is parallel three groups, completely 3 flat boards of complete blank that any sample is LB culture mediums are not added with, bacteria suspension concentration is adjusted, are surveyed with flat-plate bacterial colony method Fixed its bacterial concentration so as to which mycetome number is 102Cfu/mL, as examination bacteria suspension.
Bacteriostasis preliminary screening：Sterilizing solid medium is heated to into fusing, when being cooled to 50 DEG C, the culture per 20mL Base is poured in sterile petri dish.After flat board dries naturally, 0.1mL testing samples are pipetted respectively, 0.1mL supplies examination bacteria suspension, It is even to coat on sample-adding flat board, it to be inverted after coating 30min, each sample processes 3 repetitions.It is another that control group is set, apply bacterium.Above-mentioned behaviour Work is carried out in superclean bench.By ready-made Bacterial Plate in 37 DEG C of incubated 24h, bacterium colony number is counted.
Table 1：Facial mask liquid of the present invention is to colibacillary antibacterial result
Table 2：Antibacterial result of the facial mask liquid of the present invention to aerobacteria
(x100 times of sample Content of Chlorogenic Acid concentration is 30.778ug/mL；Standard concentration 120ug/mL)
As a result prove：50 times of dilution has obvious fungistatic effect to Gram-negative bacteria and gram-positive bacteria, from Jing Ji angle, from the extract rather than stoste that dilute 50 times.
Embodiment 5：
Moisturizing is tested
Respectively in saturation (NH4)2SO4The aqueous solution (RH 81%) and saturation K2CO3The discoloration silica gel of the aqueous solution (RH 43%) Moistening effect measure is carried out in drier.Flos Lonicerae extractive solution of the present invention, 50 times of extracts for diluting, 30% G ＆ Ws are each 1mL is positioned in the culture dish lid of 10cm, during above-mentioned drier is placed in after precise starting weight, at the 1st, 2,4,8,12 Weigh a weight.
Moisturizing rate rate of descent %=100 (Wn-W0)/W0(W0The amount being respectively with Wn before putting and after putting).
Moisturizing rate rate of descent of each solution in drier is shown in accompanying drawing 1 and accompanying drawing 2.As a result prove：The extraction of 50 times of dilution Liquid has preferable moistening effect under 81% and 43% different relative humidity.
To sum up, Jing tests were demonstrate,proved in 12 hours, and the extract of 50 times of dilution is higher than the hydroscopicity of 30% glycerine 2 percentage points. And the extract of 50 times of dilution has notable fungistatic effect to Escherichia coli and aerobacteria.Prove that the extract has good moisturizing Bacteriostasis efficacy.
It can be that professional and technical personnel in the field realize or use that above-mentioned embodiment is intended to illustrate the present invention, to above-mentioned Embodiment is modified and will be apparent for those skilled in the art, therefore the present invention is included but is not limited to Above-mentioned embodiment, it is any to meet the claims or specification description, meet with principles disclosed herein and novelty, The method of inventive features, technique, product, each fall within protection scope of the present invention.

Claims (10)

1. a kind of honeysuckle moisture-keeping bacterium-restraining facial mask liquid, it is characterised in that by honeysuckle in PEG-200 solution Jing cellulose enzymes Solution, extracts and is obtained.
2. facial mask liquid according to claim 1, it is characterised in that the honeysuckle dry weight and the PEG-200 solution Ratio is 1g:20～30mL.
3. facial mask liquid according to claim 2, it is characterised in that the mass fraction of the PEG-200 solution is 30～ 50%.
4. facial mask liquid according to claim 1, it is characterised in that the cellulase quality account for the honeysuckle with it is described The 1～5% of PEG-200 solution gross masses.
5. a kind of preparation method of honeysuckle moisture-keeping bacterium-restraining facial mask liquid, it is characterised in that comprise the following steps：By honeysuckle and matter It is 1g that amount fraction is the ratio of 30～50% PEG-200 solution mixing, the honeysuckle dry weight and the PEG-200 solution: 20～30mL, adds the cellulase of the quality of Flos Lonicerae 1～5%, and it is 4～7 to adjust mixture ph, and temperature is 45～55 DEG C 1～3h is kept, temperature is increased to into 80～90 DEG C of 10～15min of holding, suction filtration mixture obtains facial mask liquid.
6. preparation method according to claim 5, it is characterised in that the honeysuckle powder is broken to into the mesh of fineness 60～100 Afterwards, then with the PEG-200 solution mix.
7. preparation method according to claim 5, it is characterised in that also include after the suction filtration：The suction filtration is obtained Liquid phase decolourize：With activated carbon decolorizing 6～12h of the liquid phase quality after the suction filtration than 5～10%.
8. preparation method according to claim 5, it is characterised in that the facial mask liquid for preparing also includes allotment step Suddenly：Facial mask liquid after the suction filtration is diluted into 20～100 times.
9. preparation method according to claim 7, it is characterised in that the facial mask liquid for preparing also includes allotment step Suddenly：Facial mask liquid after the decolouring is diluted into 20～100 times.
10. preparation method according to claim 8 or claim 9, it is characterised in that the facial mask liquid addition after by dilution is described The sodium alginate of facial mask liquid 0.1～2wt% of quality.
CN201611177578.XA 2016-12-19 2016-12-19 Moisture-preserving and anti-bacterium honeysuckle mask liquid and preparation method thereof Pending CN106619293A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112501784A (en) * 2020-11-24 2021-03-16 长沙蓝姿生物科技有限公司 Preparation method of antioxidant skin-friendly composite fiber spunlace nonwoven mask cloth

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CN103239372A (en) * 2013-05-13 2013-08-14 南京理工大学 Mild moisturizing mask liquid and preparation method thereof
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Publication number Priority date Publication date Assignee Title
CN101647769A (en) * 2009-08-31 2010-02-17 金粉玉 Facial mask liquid and preparation method thereof
CN103239372A (en) * 2013-05-13 2013-08-14 南京理工大学 Mild moisturizing mask liquid and preparation method thereof
CN105640839A (en) * 2016-02-22 2016-06-08 太仓市荣德生物技术研究所 Moisturizing mask liquid

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112501784A (en) * 2020-11-24 2021-03-16 长沙蓝姿生物科技有限公司 Preparation method of antioxidant skin-friendly composite fiber spunlace nonwoven mask cloth
CN112501784B (en) * 2020-11-24 2021-11-30 清远市伯鑫无纺制品有限公司 Preparation method of antioxidant skin-friendly composite fiber spunlace nonwoven mask cloth

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