CN106618010A - Degradable milk fiber quilt containing negative ions and preparation method of milk fiber quilt - Google Patents

Degradable milk fiber quilt containing negative ions and preparation method of milk fiber quilt Download PDF

Info

Publication number
CN106618010A
CN106618010A CN201611247925.1A CN201611247925A CN106618010A CN 106618010 A CN106618010 A CN 106618010A CN 201611247925 A CN201611247925 A CN 201611247925A CN 106618010 A CN106618010 A CN 106618010A
Authority
CN
China
Prior art keywords
fiber
quilt
anion
degradable
fibre
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611247925.1A
Other languages
Chinese (zh)
Inventor
王占霞
李民强
李振方
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhengzhou Dehui Textile Technology Co Ltd
Original Assignee
Zhengzhou Dehui Textile Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zhengzhou Dehui Textile Technology Co Ltd filed Critical Zhengzhou Dehui Textile Technology Co Ltd
Priority to CN201611247925.1A priority Critical patent/CN106618010A/en
Publication of CN106618010A publication Critical patent/CN106618010A/en
Pending legal-status Critical Current

Links

Classifications

    • A—HUMAN NECESSITIES
    • A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
    • A47G—HOUSEHOLD OR TABLE EQUIPMENT
    • A47G9/00—Bed-covers; Counterpanes; Travelling rugs; Sleeping rugs; Sleeping bags; Pillows
    • A47G9/02—Bed linen; Blankets; Counterpanes
    • A47G9/0207—Blankets; Duvets
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00—General methods for the manufacture of artificial filaments or the like
    • D01F1/02—Addition of substances to the spinning solution or to the melt
    • D01F1/10—Other agents for modifying properties
    • D01F1/103—Agents inhibiting growth of microorganisms
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
    • D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
    • D01F6/92—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyesters
    • D—TEXTILES; PAPER
    • D02—YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02G—CRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
    • D02G3/00—Yarns or threads, e.g. fancy yarns; Processes or apparatus for the production thereof, not otherwise provided for
    • D02G3/02—Yarns or threads characterised by the material or by the materials from which they are made
    • D02G3/04—Blended or other yarns or threads containing components made from different materials
    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/02—Cotton wool; Wadding
    • D—TEXTILES; PAPER
    • D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
    • D04H1/4382—Stretched reticular film fibres; Composite fibres; Mixed fibres; Ultrafine fibres; Fibres for artificial leather
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/80—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides
    • D06M11/82—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides with boron oxides; with boric, meta- or perboric acids or their salts, e.g. with borax
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/368—Hydroxyalkylamines; Derivatives thereof, e.g. Kritchevsky bases
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02—Natural fibres, other than mineral fibres
    • D06M2101/04—Vegetal fibres
    • D06M2101/06—Vegetal fibres cellulosic
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02—Natural fibres, other than mineral fibres
    • D06M2101/10—Animal fibres
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16—Synthetic fibres, other than mineral fibres
    • D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/32—Polyesters
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
    • D10B2201/01—Natural vegetable fibres
    • D10B2201/02—Cotton
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2211/00—Protein-based fibres, e.g. animal fibres
    • D10B2211/01—Natural animal fibres, e.g. keratin fibres
    • D10B2211/04—Silk
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2211/00—Protein-based fibres, e.g. animal fibres
    • D10B2211/20—Protein-derived artificial fibres
    • D10B2211/24—Casein

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)

Abstract

The invention relates to a degradable milk fiber quilt containing negative ions and a preparation method of the milk fiber quilt. The degradable milk fiber quilt containing the negative ions comprises quilt interior stuffing, wherein the quilt interior stuffing is prepared from the following components in percentage by weight: 40-60% of milk fibers, 10-30% of silk fibers, 10-20% of cotton fibers and 5-20% of nano germanium oxide composite zirconium poly(butylene succinate) fibers. The finished product (the degradable milk fiber quilt) prepared by the method can generate negative oxygen ions and hydroxyl negative ions which can take effects of sterilizing and refreshing air and can also promote cell activation, so that a skin aging speed is reduced.

Description

Containing anion and degradable milk fibre by and preparation method thereof
Technical field
The invention belongs to bedding technical field, and in particular to it is a kind of containing anion and degradable milk fibre by and Its preparation method.
Background technology
In recent years, as people's living standard is improved constantly, operating pressure is increasing, and anion product acceptance is got over Come higher, a series of anion product has wide market.Anion can not only facilitate human body to synthesize and vitamin storage, Reinforcing and the physiological activity of human activin, therefore it is otherwise known as " air vitamin ", it is believed that it as the vitamin of food, There is highly important impact to the vital movement of human body and other biological.
Milk protein fiber is, using cow's milk as base stock, through dehydration, de-oiling, degreasing, separation, purification, to be allowed to into For a kind of MC with linear macromolecule structure；It is blended using high-tech means with polyacrylonitrile again, be crosslinked, is connect Branch, is prepared into spinning solution；Finally by wet spinning into fibre, solidification, drawing-off, drying, curling, setting, chopped fiber cut-out（It is long Silk winding）.Security is taken with fabulous；With natural bacteriostatic function, than wool, cashmere anti-mould and anti-moth, intensity Height, wears well washable, easily storage；Easily do after washing, permanent performance of product etc. can be still kept after washing.
But the Main Function of common quilt is that, for keeping out the cold, feature is single, it is impossible to meet the consumption need of different levels Ask, such as cotton-wadded quilt it is abundant it is warming, be difficult breed bacteria, be a kind of current the most widely used quilt, but cotton-wadded quilt moisture-sensitive, easy plate Knot, great inconvenience can be brought when using in winter, also do not possess health care.
The content of the invention
For defect present in prior art, the invention provides a kind of containing anion and degradable milk fibre quilt And preparation method thereof, product prepared by the method can produce negative oxygen ion and hydroxyl group anion, negative oxygen ion and hydroxyl bear from Son can sterilized and fresh air, cell activation can also be promoted, and then reduce skin senescence speed.
To achieve these goals, the technical solution used in the present invention is as follows：
The invention provides it is a kind of containing anion and degradable milk fibre quilt, including core filler, the core filling Thing is made up of the component of following percentage by weight：Milk fibre 40-60%, silk fiber 10-30%, cotton fiber 10-20% and nanometer The germanium oxide cruel fiber 5-20% of compound poly-succinic acid-butanediol.
According to above-mentioned containing anion and degradable milk fibre quilt, the core filler is by following percentage by weight Component make：Milk fibre 40-50%, silk fiber 20-30%, cotton fiber 10-15% and nano oxidized germanium are combined poly-succinic The cruel fiber 10-20% of butanediol.
According to above-mentioned containing anion and degradable milk fibre quilt, the core filler is by following percentage by weight Component make：The compound poly-succinic acid-butanediol of milk fibre 50%, silk fiber 25%, cotton fiber 10% and nano oxidized germanium is cruel Fiber 15%.
According to it is above-mentioned containing anion and degradable milk fibre quilt preparation method, comprise the following steps：
（1）Above-mentioned various fibers are carried out in proportion blending, blend fibre is obtained；
（2）Blend fibre is added at temperature 50-60 DEG C anion compound finishing agent, and while add hydrophilic softener, Adjustment pH value is warmed up to 80 DEG C to 5-7, is then incubated 30 minutes, you can the finished product of blend fibre is obtained；
（3）The finished product of blend fibre is made into core filler through scutching cotton, carding process, so as to obtain containing anion and can drop The milk fibre quilt of solution.
According to it is above-mentioned containing anion and degradable milk fibre quilt preparation method, step（2）In, the anion Compounding finishing agent is made up of the raw material Jing emulsifications of following percentage by weight with ultrasonically treated；
（1）Raw material：Granularity is the tourmaline Ultramicro-powder 1-3% of 100-200nm, ammonium polyacrylate 0.5-2%, sodium laurate 2-3%, Triethanolamine 1-3% and water 90-95.5%；
（2）Pretreatment：The water of the amount of weighing up is put in container, is then slowly added into ammonium polyacrylate, sodium laurate and triethanolamine And be stirred continuously, then it is slow added into tourmaline micro mist and is stirred continuously；
（3）Emulsification treatment：Pretreated liquid is the emulsified process 30-50min of 4500-5000r/min in emulsification rotating speed；Breast Change adopts high-shear emulsion machine, emulsifying rate to accelerate to 4500-5000r/min with 90-110r/min in processing；
（4）It is ultrasonically treated：Liquid after emulsification treatment ultrasonically treated 8-15min in the case where power is 1000-1200w, you can obtain Anion compounds finishing agent.
Compared with prior art, it is an advantage of the current invention that：
The present invention develops the functional health fiber of more high-tech content on the basis of conventional type milk fibre；The fiber is because having The addition of germanium material, less than in the case of human surface temperature, 32 DEG C can the far infrared ripple that send of high emissivity promote Enter blood circulation；Simultaneously the negative oxygen ion of its generation, hydroxyl group anion reach sterilization and the effect of fresh air, are promoting cell Activation, reduction skin senescence speed；And the micro Ge element in the germanic milk fibre of skin-proximal also can pass through skin and inhale Receive, enter and formed in vivo organic germanium, play anti-cancer, anticancer that generally acknowledged organic germanium rises, the pre- beneficial internal health such as anti-aging Effect.
Specific embodiment
Following examples are that detailed specific description is carried out to present invention, but present disclosure is not limited such as This.
Embodiment 1
The invention provides it is a kind of containing anion and degradable milk fibre quilt, including core filler, the core filling Thing is made up of the component of following percentage by weight：Milk fibre 40-60%, silk fiber 10-30%, cotton fiber 10-20% and nanometer The germanium oxide cruel fiber 5-20% of compound poly-succinic acid-butanediol.
It is above-mentioned containing anion and degradable milk fibre quilt preparation method, comprise the following steps：
（1）Above-mentioned various fibers are carried out in proportion blending, blend fibre is obtained；
（2）Blend fibre is added at temperature 50-60 DEG C anion compound finishing agent, and while add hydrophilic softener, Adjustment pH value is warmed up to 80 DEG C to 5-7, is then incubated 30 minutes, you can the finished product of blend fibre is obtained；
（3）The finished product of blend fibre is made into core filler through scutching cotton, carding process, so as to obtain containing anion and can drop The milk fibre quilt of solution.
Above-mentioned steps（2）In, the anion compounding finishing agent is to be emulsified by the raw material Jing of following percentage by weight and super Sonication is made；
（1）Raw material：Granularity is the tourmaline Ultramicro-powder 1-3% of 100-200nm, ammonium polyacrylate 0.5-2%, sodium laurate 2-3%, Triethanolamine 1-3% and water 90-95.5%；
（2）Pretreatment：The water of the amount of weighing up is put in container, is then slowly added into ammonium polyacrylate, sodium laurate and triethanolamine And be stirred continuously, then it is slow added into tourmaline micro mist and is stirred continuously；
（3）Emulsification treatment：Pretreated liquid is the emulsified process 30-50min of 4500-5000r/min in emulsification rotating speed；Breast Change adopts high-shear emulsion machine, emulsifying rate to accelerate to 4500-5000r/min with 90-110r/min in processing；
（4）It is ultrasonically treated：Liquid after emulsification treatment ultrasonically treated 8-15min in the case where power is 1000-1200w, you can obtain Anion compounds finishing agent.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention It is more than 4200/cubic centimetre.
Embodiment 2
The invention provides it is a kind of containing anion and degradable milk fibre quilt, including core filler, the core filling Thing is made up of the component of following percentage by weight：Milk fibre 50%, silk fiber 25%, cotton fiber 10% and nano oxidized germanium are answered Close the cruel fiber 15% of poly-succinic acid-butanediol.
It is above-mentioned containing anion and degradable milk fibre quilt preparation method, comprise the following steps：
（1）Above-mentioned various fibers are carried out in proportion blending, blend fibre is obtained；
（2）Blend fibre adds at 58 DEG C of temperature anion compounding finishing agent, and while add hydrophilic softener, adjustment PH value is warmed up to 80 DEG C to 5.5, is then incubated 30 minutes, you can the finished product of blend fibre is obtained；
（3）The finished product of blend fibre is made into core filler through scutching cotton, carding process, so as to obtain containing anion and can drop The milk fibre quilt of solution.
Above-mentioned steps（2）In, the anion compounding finishing agent is to be emulsified by the raw material Jing of following percentage by weight and super Sonication is made；
（1）Raw material：Granularity is tourmaline Ultramicro-powder 1%, ammonium polyacrylate 1.5%, sodium laurate 2%, the triethanolamine 2% of 160nm With water 93.5%；
（2）Pretreatment：The water of the amount of weighing up is put in container, is then slowly added into ammonium polyacrylate, sodium laurate and triethanolamine And be stirred continuously, then it is slow added into tourmaline micro mist and is stirred continuously；
（3）Emulsification treatment：Pretreated liquid is the emulsified process 40min of 4800r/min in emulsification rotating speed；In emulsification treatment Using high-shear emulsion machine, emulsifying rate accelerates to 4800r/min with 90r/min；
（4）It is ultrasonically treated：Liquid after emulsification treatment ultrasonically treated 14min in the case where power is 1100w, you can obtain anion Compounding finishing agent.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention 4400/cubic centimetre.
Embodiment 3
The present embodiment part same as Example 1 is no longer repeated, and difference is the core filler by following weight hundred The component for dividing ratio is made：The compound poly-succinic fourth two of milk fibre 40%, silk fiber 30%, cotton fiber 10% and nano oxidized germanium The cruel fiber 20% of alcohol.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention 4380/cubic centimetre.
Embodiment 4
The present embodiment part same as Example 1 is no longer repeated, and difference is the core filler by following weight hundred The component for dividing ratio is made：The compound poly-succinic fourth two of milk fibre 45%, silk fiber 25%, cotton fiber 15% and nano oxidized germanium The cruel fiber 15% of alcohol.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention 4530/cubic centimetre.
Embodiment 5
The present embodiment part same as Example 1 is no longer repeated, and difference is the core filler by following weight hundred The component for dividing ratio is made：The compound poly-succinic fourth two of milk fibre 43%, silk fiber 27%, cotton fiber 12% and nano oxidized germanium The cruel fiber 18% of alcohol.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention 4280/cubic centimetre.
Embodiment 6
The present embodiment part same as Example 1 is no longer repeated, and difference is the core filler by following weight hundred The component for dividing ratio is made：The compound poly-succinic fourth two of milk fibre 42%, silk fiber 28%, cotton fiber 13% and nano oxidized germanium The cruel fiber 17% of alcohol.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention 4360/cubic centimetre.
Embodiment 7
The present embodiment part same as Example 1 is no longer repeated, and difference is the core filler by following weight hundred The component for dividing ratio is made：The compound poly-succinic fourth two of milk fibre 46%, silk fiber 24%, cotton fiber 14% and nano oxidized germanium The cruel fiber 16% of alcohol.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention 4480/cubic centimetre.
Embodiment 8
The present embodiment part same as Example 1 is no longer repeated, and difference is the core filler by following weight hundred The component for dividing ratio is made：The compound poly-succinic fourth two of milk fibre 48%, silk fiber 22%, cotton fiber 16% and nano oxidized germanium The cruel fiber 14% of alcohol.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention 4260/cubic centimetre.
Embodiment 9
The present embodiment part same as Example 1 is no longer repeated, and difference is the core filler by following weight hundred The component for dividing ratio is made：The compound poly-succinic fourth two of milk fibre 52%, silk fiber 20%, cotton fiber 18% and nano oxidized germanium The cruel fiber 10% of alcohol.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention 4380/cubic centimetre.
Embodiment 10
The present embodiment part same as Example 1 is no longer repeated, and difference is the core filler by following weight hundred The component for dividing ratio is made：The compound poly-succinic fourth two of milk fibre 54%, silk fiber 16%, cotton fiber 20% and nano oxidized germanium The cruel fiber 10% of alcohol.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention 4290/cubic centimetre.
Embodiment 11
The present embodiment part same as Example 1 is no longer repeated, and difference is the core filler by following weight hundred The component for dividing ratio is made：The compound poly-succinic fourth two of milk fibre 60%, silk fiber 20%, cotton fiber 15% and nano oxidized germanium The cruel fiber 5% of alcohol.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention 4370/cubic centimetre.
Embodiment 12
The present embodiment part same as Example 1 is no longer repeated, and difference is the core filler by following weight hundred The component for dividing ratio is made：The compound poly-succinic fourth two of milk fibre 59%, silk fiber 12%, cotton fiber 10% and nano oxidized germanium The cruel fiber 19% of alcohol.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention 4420/cubic centimetre.
Embodiment 13
The present embodiment part same as Example 1 is no longer repeated, and difference is the core filler by following weight hundred The component for dividing ratio is made：The compound poly-succinic fourth two of milk fibre 55%, silk fiber 25%, cotton fiber 15% and nano oxidized germanium The cruel fiber 5% of alcohol.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention 4510/cubic centimetre.
Embodiment 14
The present embodiment part same as Example 1 is no longer repeated, and difference is the core filler by following weight hundred The component for dividing ratio is made：The compound poly-succinic fourth two of milk fibre 48%, silk fiber 26%, cotton fiber 13% and nano oxidized germanium The cruel fiber 13% of alcohol.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention 4450/cubic centimetre.
Embodiment 15
The present embodiment part same as Example 1 is no longer repeated, and difference is the core filler by following weight hundred The component for dividing ratio is made：The compound poly-succinic fourth two of milk fibre 47%, silk fiber 18%, cotton fiber 20% and nano oxidized germanium The cruel fiber 15% of alcohol.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention 4370/cubic centimetre.
Embodiment 16
The present embodiment part same as Example 1 is no longer repeated, and it is by such as that difference is the anion compounding finishing agent The raw material Jing emulsifications of lower percentage by weight are made with ultrasonically treated；
（1）Raw material：Granularity is tourmaline Ultramicro-powder 1%, ammonium polyacrylate 2%, sodium laurate 3%, the and of triethanolamine 3% of 120nm Water 91%；
（2）Pretreatment：The water of the amount of weighing up is put in container, is then slowly added into ammonium polyacrylate, sodium laurate and triethanolamine And be stirred continuously, then it is slow added into tourmaline micro mist and is stirred continuously；
（3）Emulsification treatment：Pretreated liquid is the emulsified process 45min of 4600r/min in emulsification rotating speed；In emulsification treatment Using high-shear emulsion machine, emulsifying rate accelerates to 4600r/min with 100r/min；
（4）It is ultrasonically treated：Liquid after emulsification treatment ultrasonically treated 9min in the case where power is 1050w, you can obtain anion and answer With finishing agent.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention 4280/cubic centimetre.
Embodiment 17
The present embodiment part same as Example 1 is no longer repeated, and it is by such as that difference is the anion compounding finishing agent The raw material Jing emulsifications of lower percentage by weight are made with ultrasonically treated；
（1）Raw material：Granularity is tourmaline Ultramicro-powder 3%, ammonium polyacrylate 1%, sodium laurate 3%, the and of triethanolamine 3% of 190nm Water 90%；
（2）Pretreatment：The water of the amount of weighing up is put in container, is then slowly added into ammonium polyacrylate, sodium laurate and triethanolamine And be stirred continuously, then it is slow added into tourmaline micro mist and is stirred continuously；
（3）Emulsification treatment：Pretreated liquid is the emulsified process 30-50min of 4700r/min in emulsification rotating speed；At emulsification High-shear emulsion machine, emulsifying rate is adopted to accelerate to 4700r/min with 110r/min in reason；
（4）It is ultrasonically treated：Liquid after emulsification treatment ultrasonically treated 12min in the case where power is 1150w, you can obtain anion Compounding finishing agent.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention 4280/cubic centimetre.
Embodiment 18
The present embodiment part same as Example 1 is no longer repeated, and it is by such as that difference is the anion compounding finishing agent The raw material Jing emulsifications of lower percentage by weight are made with ultrasonically treated；
（1）Raw material：Granularity is tourmaline Ultramicro-powder 1.5%, ammonium polyacrylate 0.5%, the sodium laurate 2%, triethanolamine of 200nm 2% and water 94%；
（2）Pretreatment：The water of the amount of weighing up is put in container, is then slowly added into ammonium polyacrylate, sodium laurate and triethanolamine And be stirred continuously, then it is slow added into tourmaline micro mist and is stirred continuously；
（3）Emulsification treatment：Pretreated liquid is the emulsified process 45min of 4800r/min in emulsification rotating speed；In emulsification treatment Using high-shear emulsion machine, emulsifying rate accelerates to 4800r/min with 105r/min；
（4）It is ultrasonically treated：Liquid after emulsification treatment ultrasonically treated 8min in the case where power is 1200w, you can obtain anion and answer With finishing agent.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention 4330/cubic centimetre.
Embodiment 19
The present embodiment part same as Example 1 is no longer repeated, and it is by such as that difference is the anion compounding finishing agent The raw material Jing emulsifications of lower percentage by weight are made with ultrasonically treated；
（1）Raw material：Granularity is tourmaline Ultramicro-powder 1%, ammonium polyacrylate 0.5%, sodium laurate 2%, the triethanolamine 1% of 140nm With water 95.5%；
（2）Pretreatment：The water of the amount of weighing up is put in container, is then slowly added into ammonium polyacrylate, sodium laurate and triethanolamine And be stirred continuously, then it is slow added into tourmaline micro mist and is stirred continuously；
（3）Emulsification treatment：Pretreated liquid is the emulsified process 30-50min of 5000r/min in emulsification rotating speed；At emulsification High-shear emulsion machine, emulsifying rate is adopted to accelerate to 5000r/min with 100r/min in reason；
（4）It is ultrasonically treated：Liquid after emulsification treatment ultrasonically treated 15min in the case where power is 1000w, you can obtain anion Compounding finishing agent.
Foundation《SFJJ-QWX25-2006 negative ion concentrations check detailed rules and regulations》Test, negative ion concentration is in product of the present invention 4260/cubic centimetre.
Above-described is only the preferred embodiment of the present invention, it is noted that for a person skilled in the art, Under the premise of without departing from general idea of the present invention, some changes and improvements can also be made, these should also be considered as the present invention's Protection domain.

Claims (5)

1. containing anion and degradable milk fibre quilt, including core filler, it is characterised in that the core filler by The component of following percentage by weight is made：Milk fibre 40-60%, silk fiber 10-30%, cotton fiber 10-20% and nano oxidized The germanium cruel fiber 5-20% of compound poly-succinic acid-butanediol.
2. it is according to claim 1 containing anion and degradable milk fibre quilt, it is characterised in that the core filling Thing is made up of the component of following percentage by weight：Milk fibre 40-50%, silk fiber 20-30%, cotton fiber 10-15% and nanometer The germanium oxide cruel fiber 10-20% of compound poly-succinic acid-butanediol.
3. it is according to claim 1 containing anion and degradable milk fibre quilt, it is characterised in that the core filling Thing is made up of the component of following percentage by weight：Milk fibre 50%, silk fiber 25%, cotton fiber 10% and nano oxidized germanium are answered Close the cruel fiber 15% of poly-succinic acid-butanediol.
4. it is according to claim 1 containing anion and degradable milk fibre quilt preparation method, it is characterised in that bag Include following steps：
（1）Above-mentioned various fibers are carried out in proportion blending, blend fibre is obtained；
（2）Blend fibre is added at temperature 50-60 DEG C anion compound finishing agent, and while add hydrophilic softener, Adjustment pH value is warmed up to 80 DEG C to 5-7, is then incubated 30 minutes, you can the finished product of blend fibre is obtained；
（3）The finished product of blend fibre is made into core filler through scutching cotton, carding process, so as to obtain containing anion and can drop The milk fibre quilt of solution.
5. it is according to claim 4 containing anion and degradable milk fibre quilt preparation method, it is characterised in that：Step Suddenly（2）In, the anion compounding finishing agent is made up of the raw material Jing emulsifications of following percentage by weight with ultrasonically treated；
（1）Raw material：Granularity is the tourmaline Ultramicro-powder 1-3% of 100-200nm, ammonium polyacrylate 0.5-2%, sodium laurate 2-3%, Triethanolamine 1-3% and water 90-95.5%；
（2）Pretreatment：The water of the amount of weighing up is put in container, is then slowly added into ammonium polyacrylate, sodium laurate and triethanolamine And be stirred continuously, then it is slow added into tourmaline micro mist and is stirred continuously；
（3）Emulsification treatment：Pretreated liquid is the emulsified process 30-50min of 4500-5000r/min in emulsification rotating speed；Breast Change adopts high-shear emulsion machine, emulsifying rate to accelerate to 4500-5000r/min with 90-110r/min in processing；
（4）It is ultrasonically treated：Liquid after emulsification treatment ultrasonically treated 8-15min in the case where power is 1000-1200w, you can obtain Anion compounds finishing agent.
CN201611247925.1A 2016-12-29 2016-12-29 Degradable milk fiber quilt containing negative ions and preparation method of milk fiber quilt Pending CN106618010A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611247925.1A CN106618010A (en) 2016-12-29 2016-12-29 Degradable milk fiber quilt containing negative ions and preparation method of milk fiber quilt

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611247925.1A CN106618010A (en) 2016-12-29 2016-12-29 Degradable milk fiber quilt containing negative ions and preparation method of milk fiber quilt

Publications (1)

Publication Number Publication Date
CN106618010A true CN106618010A (en) 2017-05-10

Family

ID=58835913

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611247925.1A Pending CN106618010A (en) 2016-12-29 2016-12-29 Degradable milk fiber quilt containing negative ions and preparation method of milk fiber quilt

Country Status (1)

Country Link
CN (1) CN106618010A (en)

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101671952A (en) * 2009-08-25 2010-03-17 浙江芬雪琳针织服饰有限公司 Anion finishing liquor and preparation method and anion functional seamless underwear
CN102286802A (en) * 2010-06-17 2011-12-21 罗莱家纺股份有限公司 Nanometer germanium health care milk protein composite fiber
CN102327001A (en) * 2010-07-13 2012-01-25 江苏宝缦卧室用品有限公司 Milk silk quilt
CN102995388A (en) * 2012-12-10 2013-03-27 上海水星家用纺织品股份有限公司 Preparation method of water-washable anion wool fiber and application in home textile product
CN203987218U (en) * 2014-08-01 2014-12-10 邱桂琴 There is nano-negative ion germanium titanium oxygen health bed alive quilt
CN105326280A (en) * 2015-10-30 2016-02-17 浙江真爱毯业科技有限公司 Production process of Viloft fiber Raschel blanket

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101671952A (en) * 2009-08-25 2010-03-17 浙江芬雪琳针织服饰有限公司 Anion finishing liquor and preparation method and anion functional seamless underwear
CN102286802A (en) * 2010-06-17 2011-12-21 罗莱家纺股份有限公司 Nanometer germanium health care milk protein composite fiber
CN102327001A (en) * 2010-07-13 2012-01-25 江苏宝缦卧室用品有限公司 Milk silk quilt
CN102995388A (en) * 2012-12-10 2013-03-27 上海水星家用纺织品股份有限公司 Preparation method of water-washable anion wool fiber and application in home textile product
CN203987218U (en) * 2014-08-01 2014-12-10 邱桂琴 There is nano-negative ion germanium titanium oxygen health bed alive quilt
CN105326280A (en) * 2015-10-30 2016-02-17 浙江真爱毯业科技有限公司 Production process of Viloft fiber Raschel blanket

Similar Documents

Publication Publication Date Title
CN103255538B (en) Ultraviolet-preventing antibacterial fabric and preparation technology thereof
CN109652869B (en) Collagen polypeptide regenerated cellulose fiber and preparation method thereof
CN105011391A (en) Natural antibacterial bamboo fiber sock
CN102691132B (en) Microcapsule-type aloe blending regeneration cellulose fiber and its preparation method
CN105821518B (en) A kind of preparation method of pupa albumen/lotus cellulose composite fiber
KR102057673B1 (en) Manufacturing method of functional fabric using natural immersion and multi functional composition and functional fabric by the method
CN108998858A (en) A kind of aquogel type alginate fiber film cloth and preparation method thereof
CN104958023A (en) Preparation method for anti-bacterial acarus-killing medical towel
CN113355761B (en) Pearl traditional Chinese medicine mosquito-proof regenerated cellulose fiber and preparation method thereof
CN109868525A (en) A kind of preparation method of high intensity seaweed and polyvinyl alcohol blending fiber
CN106702572A (en) Anion containing bamboo carbon fiber quilt with antibacterial and deodorizing functions and preparation method of bamboo carbon fiber quilt
CN102146592B (en) Regenerated cellulose fat-burning fiber and production method thereof
CN108903104A (en) Intelligent waistband with microcirculation physical therapy function
CN105105922A (en) Method of preparing medical acarus killing and anti-microbial bandage
CN106618010A (en) Degradable milk fiber quilt containing negative ions and preparation method of milk fiber quilt
CN105133130A (en) Preparation method for bacteria-resistant medical gauze
CN108851260A (en) Intelligent brassiere with microcirculation physical therapy function
CN107227505A (en) A kind of preparation method of soybean fiber towel
CN109487563A (en) A kind of one-way heat conduction cotton fibriia and preparation method thereof
CN109487558A (en) A kind of moisture absorption antibacterial cotton fibriia and preparation method thereof
CN106724474A (en) Containing anion and washable fibre and soya quilt and preparation method thereof
CN105056287A (en) Acarus-killing, antibacterial and medical bandage
CN105520848A (en) Plant essential oil composition with skin-tendering and anti-aging effects
CN109645598A (en) A kind of nano-antibacterial promoting blood circulation johnny
CN109853229A (en) A kind of antibacterial process by and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20170510

RJ01 Rejection of invention patent application after publication