CN106586570A - System and method for discharging dust in hydrogen-containing medium state environment - Google Patents

System and method for discharging dust in hydrogen-containing medium state environment Download PDF

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Publication number
CN106586570A
CN106586570A CN201510661815.9A CN201510661815A CN106586570A CN 106586570 A CN106586570 A CN 106586570A CN 201510661815 A CN201510661815 A CN 201510661815A CN 106586570 A CN106586570 A CN 106586570A
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China
Prior art keywords
dust
surge tank
gas
nitrogen
pressure
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CN201510661815.9A
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CN106586570B (en
Inventor
周通
何阳
徐成裕
鹿志勇
刘飞
柳亮亮
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China Petroleum and Chemical Corp
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China Petroleum and Chemical Corp
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Abstract

The invention relates to the field of oil refining production, and discloses a system for discharging dust in the hydrogen-containing medium state environment. The system comprises a dust collector (1). The system further comprises a nitrogen feeding device (2), a dust buffer tank (3) and a controller. The dust buffer tank (3) is connected with the dust collector (1) and the nitrogen feeding device (2). The controller is used for controlling the nitrogen feeding device (2) to supply nitrogen to the dust buffer tank (3), controlling the dust buffer tank (3) to exhaust gas as so to replace the gas in the dust buffer tank (3) and further controlling the dust collector (1) to discharge dust to the dust buffer tank (3). By means of the system for discharging the dust in the hydrogen-containing medium state environment, the dust can be discharged without stopping the dust collector, field operation risks are lowered, elutriation gas flow fluctuation is reduced, stable control over the pressure of a catalyst regeneration system is enhanced, and labor intensity is relieved.

Description

Face the system and method that dust is unloaded under hydrogen environment
Technical field
The present invention relates to production is refined oil, in particular it relates to a kind of face the system and that dust is unloaded under hydrogen environment Plant and face the method that dust is unloaded under hydrogen environment.
Background technology
Continuous reformer is modern refineries agent set, mainly for the production of high grade clean gasoline and Industrial chemicals, continuous reformer as modern aromatics production faucet device, each main oil plant at home There is construction;Continuous reforming process is uninterruptedly lifted, circulated, being burnt by catalyst, reducing/regenerating, Make reforming catalyst activity be maintained at a preferable level, reach the purpose for improving reaction depth.Reform Catalyst has a small amount of dust and broken granule to produce during circular regeneration, needs continual collection, And periodically produce.In reforming process catalyst dust collection system be high-temperature hydrogen environment, normal operating Temperature is 170 DEG C, pressure 0.40MPa, and hydrogen and dust are all inflammable and explosive media.
Original design have two large-scale dust collections, normal one come into operation one it is standby, during daily production, Switching is needed weekly once, and dust collection must first stop transport and cut out, and dust be drawn off after nitrogen displacement, so Afterwards again with just coming into operation after nitrogen displacement air.
Because dust collection is very high to filtering accuracy requirement, dust collection is equipped with blowback system, pine Dynamic system etc., turnover pipeline is various, switches come into operation operation process complexity, workload huge;Turnover in addition Valve is various, and when isolation is cut out, Jing is commonly present valves leakage, and hydrogen exchange is not thorough, and operation Temperature is high, causes operating risk to rise, unload dust it is serious when may cause hydrogen and catalyst dust burning. Furthermore original design all operations need hand switch valve, operation difficulty and operating risk are increased, worked Inefficiency.
The content of the invention
It is an object of the invention to provide a kind of face the system and method that dust is unloaded under hydrogen environment, the system and side Method can unload dust in the case where dust collection is not stopped transport, and reduce field operation risk, reduce and wash in a pan Gassing flowed fluctuation, strengthens catalyst regeneration system pressure and steadily controls, and reduces labor intensity.
To achieve these goals, present invention offer is a kind of faces the system that dust is unloaded under hydrogen environment, including powder Dirt catcher, the system also includes:Nitrogen feedway;Dust surge tank, with the dust collection With nitrogen feedway connection;Controller, nitrogen is provided extremely for controlling the nitrogen feedway During the dust surge tank and the control dust surge tank discharge gas to replace the dust surge tank Gas, and control the dust collection and unload dust to dust surge tank.
The present invention also provide it is a kind of face the method for dust unloaded under hydrogen environment include:Buffered with nitrogen displacement dust Gas in tank;And from dust collection dust is unloaded to the dust surge tank.
By above-mentioned technical proposal, dust is unloaded at facing of providing using present invention system and side under hydrogen environment Method, is provided with dust surge tank, using dust is discharged into into powder after the gas in nitrogen displacement dust surge tank The gas in dust surge tank is replaced in dirt surge tank and again, then the dust in dust surge tank is discharged into Dust bucket.Below can be automatically controlled by control valve and be completed, can not stopped transport in dust collection In the case of unload dust, and reduce field operation risk, reduce the fluctuation of elutriation throughput, strengthen catalyst Regenerative system pressure is steadily controlled, and reduces labor intensity.
Other features and advantages of the present invention will be described in detail in subsequent specific embodiment part.
Description of the drawings
Accompanying drawing is, for providing a further understanding of the present invention, and to constitute the part of description, with Detailed description below is used to explain the present invention together, but is not construed as limiting the invention. In accompanying drawing:
Fig. 1 is the structural representation for facing the system that dust is unloaded under hydrogen environment that the present invention is provided;
Fig. 2 is the structural representation for facing the system that dust is unloaded under hydrogen environment of the embodiment that the present invention is provided Figure;
Fig. 3 is the flow chart for facing the method that dust is unloaded under hydrogen environment that the present invention is provided;
Fig. 4 is the flow process for facing under hydrogen environment the gas used in nitrogen displacement dust surge tank that the present invention is provided Figure.
Description of reference numerals
The nitrogen feedway of 1 dust collection 2
3 dust surge tank 51 first controls valve
The 52 second control control valves of valve 53 the 3rd
The pressure detector of 6 filter 7
8 temperature detectors
Specific embodiment
The specific embodiment of the present invention is described in detail below in conjunction with accompanying drawing.It should be appreciated that Specific embodiment described herein is merely to illustrate and explains the present invention, is not limited to this It is bright.
Fig. 1 is the structural representation for facing the system that dust is unloaded under hydrogen environment that the present invention is provided.Such as Fig. 1 institutes Show, a kind of to face the system that dust is unloaded under hydrogen environment, including dust collection 1, the system also includes:Nitrogen Air feed system 2;Dust surge tank 3, with the dust collection 1 and the nitrogen feedway 2 Connection;Controller, nitrogen is provided to the dust surge tank 3 for controlling the nitrogen feedway 2 Gas in discharging gas to replace the dust surge tank 3 with the control dust surge tank 3, and Control the dust collection 1 and unload dust to dust surge tank 3.
Because hydrogen and dust are all inflammable and explosive media, thus in view of need nitrogen ensure unload dust Shi Jinhang effects prevent danger, and in the present invention, controller can adopt PLC, make Nitrogen is provided with to control nitrogen feedway 2, and controls dust surge tank 3 and discharge gas, with as far as possible The gas being sufficiently displaced from dust surge tank 3, then controls dust collection 1 and starts to unload dust to dust Surge tank 3, after dust is unsnatched, again repeatedly substitution gas step ensures safety, finally controls dust Surge tank 3 unloads dust to dust bucket.
The device connected due to dust collection 1 and the periphery of dust collection 1 and connected mode etc. are existing Technology, therefore will not be described here.The present invention can arrange the temperature detection being connected with dust collection 1 Device and pressure-detecting device, the temperature and pressure of convenient monitoring dust collection 1.
Below by by introduce a kind of more detailed embodiment be better described the present invention offer face hydrogen The system that dust is unloaded under environment.
Fig. 2 is the structural representation for facing the system that dust is unloaded under hydrogen environment of the embodiment that the present invention is provided Figure.As shown in Fig. 2 the system also includes:First control valve 51, positioned at the nitrogen feedway 2 And the dust surge tank 3 between, for opening when needing to provide nitrogen to the dust surge tank 3; Second control valve 52, on the discharge duct of dust surge tank 3, needs to discharge the powder for working as Open during gas in dirt surge tank 3;3rd control valve 53, positioned at the dust collection 1 and described Between dust surge tank 3, for opening when the dust collection 1 unloads dust to dust surge tank 3.
When the system is provided with valve, control device can transfer control valve, and such as control first is controlled The opening and closing of valve processed 51 controls the opening and closing of the second control valve 52 to control dust to control the supplement of nitrogen Gas in surge tank 3 is discharged, and controls start and stop of the opening and closing of the 3rd valve 53 to control to unload dust.It is logical Valve controlling is crossed, whole control process can be caused simpler and reasonable.
Gas in more accurately to replace dust surge tank 3, the present invention can also be to supplementing nitrogen and row The opportunity for going out gas is defined, therefore the system can also include pressure detector 7, with the dust Surge tank 3 connects, for detecting dust surge tank 3 in gas pressure.Pressure detector 7 can divide For site pressure detector and remote pressure detector.As its name suggests, site pressure detector can be for existing The gas pressure that field personnel are checked in dust surge tank 3, and remote pressure detector can be for non-at-scene people Member understands the pressure in dust surge tank 3 from other channels.
When the offer of nitrogen feedway 2 nitrogen is controlled, when the pressure in dust surge tank 3 rises to During first pressure threshold value, stop supplementing nitrogen.In the present invention, first pressure threshold value is 0.2-0.4MPa, Preferably 0.3MPa.
When controlling the dust surge tank 3 and discharging gas, when the pressure in dust surge tank 3 is down to the During two pressure thresholds, stop discharging gas.In the present invention, second pressure threshold value is 0.02-0.04MPa, Preferably 0.03MPa.
The system also includes temperature detector 8, is connected with the dust surge tank 3, for detecting dust Temperature in surge tank 3.It act as, although having completed substitution gas step, when dust surge tank When 3 temperature is still too high, the step of carrying out substitution gas again is still needed to, until dust surge tank 3 Temperature is normal, just can start to unload dust.Thus, just can be properly completed from High Temperature High Pressure hydrogen environment to Low-temp low-pressure nitrogen environment is changed.
Further, since the dust for unloading may be carried when dust surge tank 3 discharges gas, therefore should System also includes filter 6, on the discharge duct of dust surge tank 3, for blocking with gas The dust of discharge.In the case where there is filter 6, filter 6 often has because use time is long The situation of blocking occurs, therefore can set on the right (i.e. outgassing direction) of filter as depicted 6 Putting another nitrogen feedway (not drawing) carries out blowback, and the dust of blocking filter 6 is blown back into powder Dirt surge tank 3.Because the gas for blowback is still nitrogen, therefore will not be in dust surge tank 6 Gas impact.
The step of controller performs the gas in the use nitrogen displacement dust surge tank is once or more It is secondary, when the temperature and pressure in dust surge tank 3 is normal till.
The controller is additionally operable to:Hold to the dust surge tank from dust collection unloading dust described After the continuous scheduled time, the gas in the control discharge dust surge tank is until the dust surge tank Pressure is down to second pressure threshold value, again with the gas in dust surge tank described in nitrogen displacement.
Fig. 3 is the flow chart for facing the method that dust is unloaded under hydrogen environment that the present invention is provided.As shown in figure 3, It is a kind of face the method for dust unloaded under hydrogen environment include:With the gas in nitrogen displacement dust surge tank;And From dust collection dust is unloaded to the dust surge tank.
Fig. 4 is the flow process for facing under hydrogen environment the gas used in nitrogen displacement dust surge tank that the present invention is provided Figure.As shown in figure 4, in facing the method that dust is unloaded under hydrogen environment, with nitrogen displacement dust surge tank The step of gas, includes:Nitrogen is supplemented to the dust surge tank, the pressure in the dust surge tank When rising to first pressure threshold value, stop supplementing nitrogen;The gas in the dust surge tank is discharged, works as institute When stating the pressure in dust surge tank and being down to second pressure threshold value, stop discharging gas;Execution is described to use nitrogen The step of gas replaces the gas in dust surge tank one or many.
In addition, in order to ensure to replace thorough and more preferably safety, therefore described from dust collection Unloading dust discharges the gas in the dust surge tank to the dust surge tank predetermined hold-time Body is down to second pressure threshold value until the pressure of the dust surge tank, again with dust described in nitrogen displacement Gas in surge tank.
Face unload under hydrogen environment dust method entirety detailed step be:
Start to supplement nitrogen to the dust surge tank;When the pressure in the dust surge tank rises to first During pressure threshold, stop supplementing nitrogen, otherwise continue to supplement;Discharge the gas in the dust surge tank; When the pressure in the dust surge tank is down to second pressure threshold value, stop discharging gas, otherwise continue Discharge;Repeat above gas displacement step repeatedly (present invention is preferably 4 times);Dust is unloaded to the powder Dirt surge tank predetermined hold-time;The gas in the dust surge tank is discharged until the dust surge tank Pressure when being down to second pressure threshold value, stop discharging gas, otherwise continue to discharge;Start to supplement nitrogen To the dust surge tank;When the pressure in the dust surge tank rises to first pressure threshold value, stop Nitrogen is supplemented, otherwise continues to supplement;Discharge the gas in the dust surge tank;When dust buffering When pressure in tank is down to second pressure threshold value, stop discharging gas, otherwise continue to discharge;More than repeating Gas displacement step is repeatedly (present invention is preferably 4 times);Dust is unloaded to dust bucket.
If be controlled using control valve in above-mentioned steps, then nitrogen is supplemented each time, is discharged each time Gas in dust surge tank and unload dust to closing control valve during dust surge tank, for the sake of insurance Need to check whether control valve closes in place, due to being obvious common knowledge, here is just repeated no more.
By above-mentioned technical proposal, dust is unloaded at facing of providing using present invention system and side under hydrogen environment Method, is provided with dust surge tank, using dust is discharged into into powder after the gas in nitrogen displacement dust surge tank The gas in dust surge tank is replaced in dirt surge tank and again, then the dust in dust surge tank is discharged into Dust bucket.Below can be automatically controlled by control valve and be completed, can not stopped transport in dust collection In the case of unload dust, and reduce field operation risk, reduce the fluctuation of elutriation throughput, strengthen catalyst Regenerative system pressure is steadily controlled, and reduces labor intensity.
The preferred embodiment of the present invention is described in detail above in association with accompanying drawing, but, the present invention is not limited Detail in above-mentioned embodiment, in the range of the technology design of the present invention, can be to the present invention Technical scheme carry out various simple variants, these simple variants belong to protection scope of the present invention.
It is further to note that each particular technique described in above-mentioned specific embodiment is special Levy, in the case of reconcilable, can be combined by any suitable means, in order to avoid need not The repetition wanted, the present invention is no longer separately illustrated to various possible compound modes.
Additionally, combination in any can also be carried out between a variety of embodiments of the present invention, as long as its Without prejudice to the thought of the present invention, it should equally be considered as content disclosed in this invention.

Claims (12)

  1. It is 1. a kind of to face the system that dust is unloaded under hydrogen environment, including dust collection (1), it is characterised in that The system also includes:
    Nitrogen feedway (2);
    Dust surge tank (3), with the dust collection (1) and the nitrogen feedway (2) even Connect;
    Controller, nitrogen is provided to the dust surge tank for controlling the nitrogen feedway (2) (3) and control during the dust surge tank (3) discharges gas to replace the dust surge tank (3) Gas, and control the dust collection (1) and unload dust to dust surge tank (3).
  2. 2. it is according to claim 1 to face the system that dust is unloaded under hydrogen environment, it is characterised in that should System also includes:
    First control valve (51), positioned at the nitrogen feedway (2) and the dust surge tank (3) Between, for opening when needing to provide nitrogen to dust surge tank (3);
    Second control valve (52), on dust surge tank (3) discharge duct, for when needs Open when discharging the gas in the dust surge tank (3);
    3rd control valve (53), positioned at the dust collection (1) and the dust surge tank (3) Between, for opening when the dust collection (1) unloads dust to dust surge tank (3).
  3. 3. it is according to claim 1 to face the system that dust is unloaded under hydrogen environment, it is characterised in that should System also includes filter (6), on dust surge tank (3) discharge duct, for blocking With the dust that gas is discharged.
  4. 4. it is according to claim 1 to face the system that dust is unloaded under hydrogen environment, it is characterised in that should System also includes pressure detector (7), is connected with the dust surge tank (3), for detecting dust Gas pressure in surge tank (3).
  5. 5. it is according to claim 4 to face the system that dust is unloaded under hydrogen environment, it is characterised in that control Make the nitrogen feedway (2) nitrogen is provided and dust surge tank (3) the discharge gas is controlled Including:
    When the pressure in dust surge tank (3) rises to first pressure threshold value, stop supplementing nitrogen;With And
    When the pressure in dust surge tank (3) is down to second pressure threshold value, stop discharging gas.
  6. 6. it is according to claim 4 to face the method that dust is unloaded under hydrogen environment, it is characterised in that institute State one or many step of controller performs the gas in the use nitrogen displacement dust surge tank.
  7. 7. it is according to claim 4 to face the method that dust is unloaded under hydrogen environment, it is characterised in that institute State controller to be additionally operable to:
    Dust is unloaded to the dust surge tank predetermined hold-time, control described from dust collection Gas in the system discharge dust surge tank is down to second pressure until the pressure of the dust surge tank Threshold value, again with the gas in dust surge tank described in nitrogen displacement.
  8. 8. it is according to claim 1 to face the system that dust is unloaded under hydrogen environment, it is characterised in that should System also includes temperature detector (8), is connected with the dust surge tank (3), for detecting dust Temperature in surge tank (3).
  9. 9. it is a kind of to face the method that dust is unloaded under hydrogen environment, it is characterised in that the method includes:
    With the gas in nitrogen displacement dust surge tank;And
    From dust collection dust is unloaded to the dust surge tank.
  10. 10. it is according to claim 9 to face the method that dust is unloaded under hydrogen environment, it is characterised in that to use The step of gas in nitrogen displacement dust surge tank, includes:
    Nitrogen is supplemented to the dust surge tank, when the pressure in the dust surge tank rises to first pressure During threshold value, stop supplementing nitrogen;And
    The gas in the dust surge tank is discharged, when the pressure in the dust surge tank is down to the second pressure During force threshold, stop discharging gas.
  11. 11. according to claim 9 face the method that dust is unloaded under hydrogen environment, it is characterised in that hold The step of gas in the row use nitrogen displacement dust surge tank one or many.
  12. 12. according to claim 9 face the method that dust is unloaded under hydrogen environment, it is characterised in that
    Dust is unloaded to the dust surge tank predetermined hold-time, arrange described from dust collection The gas gone out in the dust surge tank is down to second pressure threshold value until the pressure of the dust surge tank, Again with the gas in dust surge tank described in nitrogen displacement.
CN201510661815.9A 2015-10-14 2015-10-14 Face the system and method that dust is unloaded under hydrogen environment Active CN106586570B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108946176A (en) * 2017-05-19 2018-12-07 中国石化工程建设有限公司 A kind of devices and methods therefor of catalyst safe transport between mutual exclusion environment
CN111170822A (en) * 2019-08-26 2020-05-19 浙江卫星能源有限公司 Process for preparing propylene by propane dehydrogenation in superimposed on-line switchable fluid bed

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US5372653A (en) * 1993-05-28 1994-12-13 Courtaulds Fibres (Holdings) Limited Cleaning of filters
CN102698541A (en) * 2012-06-29 2012-10-03 邹岳明 Phosphorus steam dust cleaning device and working method thereof
CN102886182A (en) * 2012-10-17 2013-01-23 宿玉华 Protection device and protection method for filter bag of bag-type dust remover
CN103332458A (en) * 2013-06-28 2013-10-02 中冶南方工程技术有限公司 Pneumatic conveying system for removing dust and fine ash in dry process of converter gas
CN103736339A (en) * 2014-01-21 2014-04-23 内蒙古大唐国际锡林浩特褐煤综合开发有限责任公司 Bulk material drying and dust collection system and coal powder collection method
CN203737016U (en) * 2013-12-12 2014-07-30 中国石油化工股份有限公司 Coal gas blowback device for PSA analytical gas
CN203998911U (en) * 2014-07-24 2014-12-10 湖北博凯医药科技有限公司 The special-purpose filling apparatus of a kind of acyl chloride compound
CN104623990A (en) * 2015-02-15 2015-05-20 北京烨晶科技有限公司 High-temperature gas-solid filtering separation device

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5372653A (en) * 1993-05-28 1994-12-13 Courtaulds Fibres (Holdings) Limited Cleaning of filters
CN102698541A (en) * 2012-06-29 2012-10-03 邹岳明 Phosphorus steam dust cleaning device and working method thereof
CN102886182A (en) * 2012-10-17 2013-01-23 宿玉华 Protection device and protection method for filter bag of bag-type dust remover
CN103332458A (en) * 2013-06-28 2013-10-02 中冶南方工程技术有限公司 Pneumatic conveying system for removing dust and fine ash in dry process of converter gas
CN203737016U (en) * 2013-12-12 2014-07-30 中国石油化工股份有限公司 Coal gas blowback device for PSA analytical gas
CN103736339A (en) * 2014-01-21 2014-04-23 内蒙古大唐国际锡林浩特褐煤综合开发有限责任公司 Bulk material drying and dust collection system and coal powder collection method
CN203998911U (en) * 2014-07-24 2014-12-10 湖北博凯医药科技有限公司 The special-purpose filling apparatus of a kind of acyl chloride compound
CN104623990A (en) * 2015-02-15 2015-05-20 北京烨晶科技有限公司 High-temperature gas-solid filtering separation device

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108946176A (en) * 2017-05-19 2018-12-07 中国石化工程建设有限公司 A kind of devices and methods therefor of catalyst safe transport between mutual exclusion environment
CN111170822A (en) * 2019-08-26 2020-05-19 浙江卫星能源有限公司 Process for preparing propylene by propane dehydrogenation in superimposed on-line switchable fluid bed

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