CN1065792A - Contain elaeagnus gum hair care hair caring mouse compositions and compound method thereof - Google Patents
Contain elaeagnus gum hair care hair caring mouse compositions and compound method thereof Download PDFInfo
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- CN1065792A CN1065792A CN 92108424 CN92108424A CN1065792A CN 1065792 A CN1065792 A CN 1065792A CN 92108424 CN92108424 CN 92108424 CN 92108424 A CN92108424 A CN 92108424A CN 1065792 A CN1065792 A CN 1065792A
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Abstract
A kind of hair care hair caring mouse compositions is to be substrate with natural Elaeag-naceae plant elaeagnus gum, and it is formulated to add various surfactants, functional additive, spice or essence, distilled water and organic solvent again.The a series of mousses that are mixed with are that to have with the elaeagnus gum be hair conditioning style substrate, and have the natural hair care hair caring mousse of the out of the ordinary or comprehensive good ilities of additional ingredient.After smearing mousse of the present invention, the hair fluffy softness that seems, high resilience, gloss is easy to combing and moulding naturally, and ventilative and poisture-penetrability are arranged.
Description
The invention belongs to cosmetics hair care hair caring mouse compositions and compound method thereof.
The mousse of hair caring of being used to take care of hair mainly is made up of film forming matter and foaming agent, normally used film forming matter mostly is synthetic macromolecular compound, as contain the polymer and the copolymer thereof of vinylpyrrolidone [U.S. Pat 4012501(1977)], vinylacetate, acrylate or siloxanes [U.S. Pat 4744978(1988)], though synthetic macromolecular compound has filming performance and persistent constancy preferably, but because of breathability and poisture-penetrability relatively poor, when running into perspiration and dampness, the easy adhesion of hair is felt under the weather the people.
Elaeag-naceae plant Fructus Elaeagni Angustifoliae (Elaeagnus angustifolia L) natural gum has good filming performance and foam performance, utilizing it is base starting material one-tenth one class natural hair care hair caring mousse capable of being combined, and it can overcome shortcoming such as breathability and poisture-penetrability difference after the synthetic high polymer class mousse film forming.
For this reason, the present invention seeks to prepare a class to contain the hair care hair caring mouse compositions that Elaeag-naceae plant elaeagnus gum is a base starting material.
The hair care hair caring mouse compositions that the present invention relates to, its prescription is composed as follows:
Composition weight %
Elaeagnus gum 0.5-4.0
Surfactant 0.0-3.0
Functional additive 0.0-15.0
Spice or essence 0.02-0.50
Water 80.0-99.4
Organic solvent 0.0-10.0
Gaseous propellant 10.0-30.0 gram/100 gram mousse colloids
The elaeagnus gum that the present invention adopts is the extraction separation thing of natural Elaeag-naceae plant elaeagnus gum virgin rubber or elaeagnus gum, elaeagnus gum is a compound of polysaccharide, the virgin rubber glycosyl mainly comprises the L-rhamnose, L-arabinose, the D-xylose, D-mannose, D-galactose and alduronic acid etc., the extraction separation thing of elaeagnus gum are with the extraction separation thing behind dimethyl sulfoxine or the water logging bubble.
The present invention adopts the surfactant purpose to be being that the mousse of substrate plays some modification with the elaeagnus gum; for example the foam performance that has of surfactant can make the foam of mousse fine and smooth more and stable; antistatic behaviour makes hair be difficult for ash; the effect that protection hair cleaning and minimizing dandruff are arranged; cationic surfactant also has bactericidal action etc. usually; the surfactant that the present invention uses can be an anionic; cationic; amphoteric; nonionic and high molecular type surfactant; they can reasonably select one or more for use in prescription, preferential the having of adopting of the present invention:
1. carboxylate, sulfuric acid, sulfonate or phosphate ester salt type anion surfactant, available following general formula:
R=C in the formula
10-C
20Saturated or unsaturated aliphatic substituent group
M＝Na
+，K
+，NH
+ 4，（HOCH
2CH
2）
3N
+H
Potassium oleate for example, chilli oil, oleyl alcohol sulfuric ester sodium salt, dodecylbenzene sodium sulfonate, lauryl phosphate sodium salt, close-cut fraction lauryl sulfate triethanolamine salt salt (Perlankrol ATL40) etc.
2. amine salt or quaternary ammonium salt cationic surfactant, their general formula is as follows:
R=C in the formula
10-C
20Alkyl
R ', R "=C
1-C
3Alkyl
R ' "=C
1-C
10Alkyl or alcohol radical or aryl
X＝Cl
-，Br
-，SO
2- 4，PO
3- 4
Cetalkonium chloride for example, Dodecyl trimethyl ammonium chloride, dodecyl chlorination ammonium, A Keweier (Aheovel) A type cationic surfactant etc.
3. aminoacid or betaine type amphoteric surfac-tant, available following general formula:
R=C in the formula
10-C
20Alkyl
R ', R "=C
1-C
5Alkyl or acyl group or sulfo group
M＝H
+，Na
+，K
+
Sodium dodecyl aminopropionitrile for example, dodecyldimethylammonium hydroxide inner salt, Cortex cocois radicis sulfobetaines etc.
4. polyethylene glycol type or polyol-based non-ionic surfactant, available following general formula:
R=C in the formula
9-C
20The straight or branched alkyl
R '=C
3-C
20The straight or branched alkyl
M=3-30, best 9-20
N=2-60, best 8-30
p+q＝5-25
x+y+z＝3-30
a+b+c＝20-100
Polyoxyethylene hexadecanol for example, octyl phenol polyoxy ethyl hexanol (Triton X-102 or Triton X-100), isobutyl phenol and polyethylene oxide condensation compound JFC, sorbitan palmitate, this dish (span) type or tween (Tween) type non-ionic surface active agent, the ethylene oxide adduct of polypropylene glycol (Pluronic F), ethylenediamine and expoxy propane addition compound product be access ring oxidative ethane (Tetronic 304) again, ethylene oxide condensate (Intravon JF or Intravon JU) etc.
5. polyvinyl alcohol, carboxymethyl cellulose (CMC), high molecular surfactants such as protein water Jie product.
The present invention is on the basis that keeps natural Elaeag-naceae plant elaeagnus gum hair conditioning style effect, add functional additive again, its objective is in order to make mousse of the present invention have more superior more perfect serviceability, certain requirement with serviceability, can add one or more of following difference in functionality additive in prescription, functional additive comprises:
1. sterilization antiseptic, as benzyl alcohol, the P-hydroxybenzoic acid first (or second, the third, fourth) ester, imidazolidinyl urea, sodium benzoate, sodium acetate, sodium sorbate, fumaric acid, boric acid, sodium borate, Borax etc.
The b.PH regulator, as citric acid, sodium citrate, succinic acid, salicylic acid, malic acid, lactic acid, Tartaric acid, sodium phosphate, sodium hydroxide, sodium carbonate etc.
C. sequestering agent, as disodiumedetate, sodium hexameta phosphate etc.
D. antistatic additive is as cation or amphoteric surfactant etc.
E. viscosity modifier, as lauroyl diethanolamine, Oleum Cocois single ethanol amide dimethicone copolyol, guar gum, methylcellulose, hydroxypropyl emthylcellulose, starch and derivant thereof, hydroxyethyl-cellulose etc.
F. freezing point regulator, as ethanol, propanol, ethylene glycol, glycol dimethyl ether etc.
G. anti-dandruff and itching-relieving agent, as hexachlorophene, salicyloyl para-bromoaniline, sodium tripolyphosphate etc.
H. hair conditioner, as lanoline, high fatty alcohol and derivant thereof, glucitol derivative, the two stearyl alkyl dimethyl ammonium chlorides of hydroxypropyl, sodium tungstate, Herba Menthae acid, acetic acid wool grease, vitamin B
6, cholesterol, lecithin, hydrolyzed animal protein, sodium lauroyl sarcosine, ossein hydrolyzate etc.
I. coloring agent is as FD﹠amp; C or D﹠amp; C coating etc.
J. stain, as the indoles dyestuff, iron salt type hair dye or other natural dye and synthetic dyestuffs etc.
K. oxidant, as two chlorine waters, perborate and persulfate etc.
L. Reducing agent is as thioglycolate salt etc.
M. pearling agent is as ethylene glycol bisthioglycolate stearate, glitter etc.
N. plasticizer, as glycerol, propylene glycol etc.
And other typical additives,
Used spice of the present invention or essence comprise Flos micheliae Albae oil, Australian Oleum Santali albi, Oleum Menthae Rotundifoliae (rectification), ylang ylang oil, Oleum Pelargonii Graveolentis, Folium Lauri nobilis wet goods natural perfume material and Flos Jasmini Sambac, Flos Lilii viriduli, jasmine orchid, Syringa oblata Lindl., Magnolia denudata Desr., violet, orange blossom oil, Dianthus carryophyllus, white orchid, daily essences such as the nine rare and rabbit ear.
Organic solvent such as acetone and alcohols example: ethanol, propanol, butanols, isopropyl alcohol and isobutanol etc.
Gaseous propellant comprises iso-butane, propane/butane (40/60 or 25/75) fluorine Lyons F-12, F-22 and F-13 etc.
It is distilled water or deionized water that the present invention prepares the water that mousse uses.
Mousse of the present invention adopts the compound method of elaeagnus gum virgin rubber to be:
1. apparent impurity in the elaeagnus gum is removed.
2. then elaeagnus gum is ground into 10-50 purpose powder.
3. after above-mentioned powder slowly being dropped in the room temperature water in the stirring or soaking gum powder about diel earlier, be warming up to 60-100 ℃ gradually, stir and became uniform colloid in 1-10 hour, pass through again (or without) activated carbon decolorizing and filtration treatment, making concentration is the elaeagnus gum colloid of 0.5-5.0%.
4. mix by the proportioning of each component in the prescription and stirred 0.5-3 hour, be heated to 25-60 ℃, filtered while hot promptly obtains product mousse colloid.
With the mousse colloid with canned the sealing of moss tank installation, and charge into gaseous propellant.
Mousse of the present invention adopts the compound method of the extraction separation thing of elaeagnus gum to be:
1. get a certain amount of elaeagnus gum, consumption soaks diel for natural gum amount 10-50 dimethyl sulfoxine or water doubly under room temperature, filter, heavily cover 4-5 time, to not having or till seldom polysaccharide can be extracted, can detecting by conventional polysaccharide method for qualitative analysis, again with the 2/3(weight that is about extracting solution) 95% ethanol segregation, separate out floccule, filter.With an amount of 95% washing with alcohol and filtration, heavily cover 3-4 time after, use an amount of absolute ethanol washing and filtration instead, heavily cover 2-3 time gained solid P
2O
5At room temperature to 50 ℃ left and right sides vacuum drying 1-6 hour, get the white powder polyoses extract, divide the point that is situated between to be 171-180 ℃, yield is 85-95%.
2. the white powder polyoses extract is slowly dropped in the room temperature water in the stirring and be warmed up to gradually about 60-100 ℃, stirred 1-10 hour, making uniform concentration is the elaeagnus gum colloid of 0.5-5.0%.
3. mix by the proportioning of each component in the prescription, stirred 0.5-3 hour, promptly get product mousse colloid.
With the mousse colloid with canned the sealing of moss tank installation, and charge into gaseous propellant.
Elaeagnus gum itself has unique filming performance and foam performance, so the present invention can make a class by the 100% All Pure Nature hair conditioning style mousse of elaeagnus gum while as film forming matter and foaming agent.On this basis by more additional surfactants and various functional additive, make it to have concurrently some better additional properties, thereby can produce a series of is hair conditioning style substrate with the elaeagnus gum, and has the natural hair care hair caring mousse of the out of the ordinary or comprehensive good ilities of additional ingredient.This class mousse does not have toxicity and any pair of effect, and contained elaeagnus gum is the natural polysaccharide macromolecular compound among the Yin Mosi, therefore mousse of the present invention contains common unexistent natural nutrient of synthetic macromolecular compound class mousse and trace element, life-time service, nourishing and conditioning hair there are its unique advantages, play significant hair care effect.
Mousse uniform in foaming of the present invention is stable, and film forming is fast, and it is effective finalize the design, and hair style is lasting, smear mousse of the present invention after, the hair fluffy softness that seems, high resilience, the gloss nature is easy to combing, and has and breathe freely and poisture-penetrability.
The elaeagnus gum mousse that contains of the present invention's preparation is not only hair care hair caring good merchantable brand, and because of the elaeagnus gum aboundresources, low price has very strong marketing competitiveness.
For better geographical Jie the present invention, with following embodiment it is described, but the invention is not restricted to these examples.
Embodiment 1:
This example is 100% All Pure Nature mousse, has unique hair conditioning style effect.
Composition weight %
Elaeagnus gum 2.5
Flos micheliae Albae oil 0.5
Distilled water 97.0
Fluorine Lyons F-12 20 grams/100 gram mousse colloids
Compound method is as follows: be ground into 30-40 purpose powder after elaeagnus gum is removed apparent impurity, it is slowly poured in the room temperature water in the stirring, be warmed up to 80 ℃ gradually, stirred 8 hours, make it into the elaeagnus gum colloid of uniform gummy about 3%, calculate the required distilled water of adding by containing 2.5% elaeagnus gum, continue under the room temperature to stir 1.5 hours, add other component in the above-mentioned prescription then, 0.5 hour post-heating to 60 of restir ℃, filtered while hot makes purified mousse colloid, take by weighing 100 and restrain in the air pressure tank of packing into, and charge into 20 gram fluorine Lyons F-12.
Embodiment 2
This example mousse colloid exquisiteness, the odor type gracefulness can make the fluffy softness of hair after smearing, high resilience, the gloss nature is easy to combing, and after the hair dryer moulding, typing effect spy is good, and can make hair style lasting.
Composition weight %
Elaeagnus gum 2.00
Polyethylene glycol type surfactant TX-100 0.87
Polyethylene glycol type surfactant JFC 0.21
Sodium benzoate 0.03
Michelia essence 0.07
Deionized water 96.82
Fluorine Lyons F-22 20 grams/100 gram mousse colloids
Compound method is as follows: be ground into 20-30 purpose powder after elaeagnus gum is removed apparent impurity, it is slowly poured in the room temperature water in the stirring, be warmed up to 70 ℃ gradually, stirred 6 hours, make it into uniform gummy and be 2% elaeagnus gum colloid, the cooling back adds other component by above-mentioned prescription, 1 hour post-heating to 60 of restir ℃, filtered while hot makes purified mousse colloid, take by weighing 100 and restrain in the air pressure tank of packing into, and charge into 20 gram fluorine Lyons F-22.
Embodiment 3
This example mousse has the function of moistening with nourishing hair, and often use can prevent alopecia.
Composition weight %
Elaeagnus gum 1.20
Sodium hexameta phosphate 0.40
Lauryl phosphate sodium salt 0.50
Acetic acid lanoline 0.50
Vitamin B
60.10
Lecithin 0.20
Ethanol 13.00
Jasmine orchid 0.20
Distilled water 83.90
Fluorine Lyons F-12 20 grams/100 gram mousse colloids
Compound method similar embodiment 2, difference is: (1) should fully stir about 0.5 hour after adding sodium hexameta phosphate, adds the lauryl phosphate sodium salt again.(2) with acetic acid lanoline, vitamin B
6Be dissolved in earlier in the ethanol with lecithin, stir then down its solution is slowly poured in the above-mentioned colloidal sol, added the essence stir about at last 0.5 hour, room temperature is filtered.
Embodiment 4
Therefore this example mousse except normal hair conditioning style effect is arranged, also has certain removing scurf and relieving itching and sterilizing function owing to contain salicyloyl para-bromoaniline additive, and often use can make hair bright and clean, comfortable softness.
Composition weight %
Elaeagnus gum 2.80
Lanoline 0.80
Salicyloyl para-bromoaniline 0.05
Orange blossom oil essence 0.10
Distilled water 96.25
Iso-butane 20 grams/100 gram mousse colloids
Compound method is as follows: elaeagnus gum is removed the powder that is ground into behind the apparent impurity about 40 orders, it is slowly poured in the room temperature water in the stirring, be warming up to 100 ℃ gradually, stirred 10 hours, make it into the elaeagnus gum colloid of uniform gummy about 5%, calculate the required distilled water of adding by containing 2.80% elaeagnus gum, continue under the room temperature to stir 1.5 hours, add other component in the above-mentioned prescription then, 0.5 hour post-heating to 50 of restir ℃, filtered while hot makes purified mousse colloid, take by weighing 100 and restrain in the air pressure tank of packing into, and charge into 20 gram iso-butanes.
Embodiment 5
This example mousse also has the auxiliaring effect of hair dyeing except having the hair conditioning style function.
Composition weight %
Relate to jujube tree glue 3.20
Polyoxyethylene hexadecanol 0.10
Ferrous chloride 0.20
3.4-dihydroxyphenyl ethanol 0.40
Borax 0.30
Oleum Menthae Rotundifoliae (rectification) 0.30
Distilled water 95.50
Fluorine Lyons F-12 25 grams/100 gram mousse colloids
Compound method is as follows: be ground into 40～50 purpose powder after elaeagnus gum is removed apparent impurity, soak about diel, be warmed up to 95 ℃ gradually, stirred 3～4 hours, make it into uniform gummy and be 3.2% elaeagnus gum colloid, after the cooling, add other component, 2.5 hours post-heating to 50 of restir ℃ by above-mentioned prescription, filtered while hot, make purified mousse colloid, take by weighing 100 and restrain in the air pressure tank of packing into, and charge into 25 gram fluorine Lyons F12.
Embodiment 6
This example mousse is suitable for men women and children, has haircuting and moisturizing effect of appropriateness.
Composition weight %
Elaeagnus gum 0.67
Cetalkonium chloride 0.1
Lauroyl diethanolamine 0.08
Sorbitan stearate 0.40
Hydroxyethyl-cellulose 0.30
Rabbit ear essence 0.20
Distilled water 98.25
Propane/butane (40/60) 10 gram/100 gram mousse colloids
Compound method is as follows: natural elaeagnus gum is soaked diel with the hydroecium relaxing the bowels with purgatives of warm nature of 30 times of amounts, filter, heavily cover 4 times, with the 2/3(weight of extracting solution) 95% ethanol segregation, separate out floccule, filter.With an amount of 95% washing with alcohol and filtration, heavily cover 4 times, use absolute ethanol washing and filtration instead, heavily cover gained solid P 2 times
2O
5Room temperature vacuum drying 5 hours gets the white powder polyoses extract.Polyoses extract is slowly added in the room temperature water in the stirring, be warming up to 80 ℃ gradually and stirred 4 hours, make uniform concentration and be 0.67% elaeagnus gum colloid.Add other component in the above-mentioned prescription then, restir gets purified mousse colloid after 0.5 hour.Take by weighing 100 and restrain in the air pressure tank of packing into, and charge into 10 gram propane/butane (40/60).
Claims (9)
1, a kind of hair care hair caring mouse compositions is characterized in that its composition is
Composition weight %
Elaeagnus gum 0.5-4.0
Surfactant 0.0-3.0
Functional additive 0.0-15.0
Spice or essence 0.02-0.50
Distilled water or deionized water 80.0-99.4
Organic solvent 0.0-10.0
Gaseous propellant 10.0-30.0 gram/100 gram mousse colloids
2, hair care hair caring mouse compositions as claimed in claim 1 is characterized in that elaeagnus gum is the extraction separation thing after Elaeag-naceae plant elaeagnus gum virgin rubber or elaeagnus gum steep with dimethyl sulfoxine or water logging.
3, hair care hair caring mouse compositions as claimed in claim 1 is characterized in that surfactant can be anionic, and is cationic, amphoteric, and nonionic and high molecular type surfactant can be selected one or more for use in prescription.
4, hair care hair caring mouse compositions as claimed in claim 1 is characterized in that functional additive is a sterilization antiseptic, the PH regulator, sequestering agent, antistatic additive, viscosity modifier, the freezing point regulator, anti-dandruff and itching-relieving agent, hair conditioner, coloring agent, stain, oxidant, Reducing agent, pearling agent and plasticizer.
5, hair care hair caring mouse compositions as claimed in claim 1 is characterized in that spice or essence comprise Flos micheliae Albae oil, Australian Oleum Santali albi, Oleum Menthae Rotundifoliae (rectification), ylang ylang oil, Oleum Pelargonii Graveolentis, laurel natural perfume material and Flos Jasmini Sambac, Flos Lilii viriduli, jasmine orchid, Syringa oblata Lindl., Magnolia denudata Desr., violet, orange blossom oil, Dianthus carryophyllus, white orchid, nine rare and rabbit ear daily essence.
6, hair care hair caring mouse compositions as claimed in claim 1 is characterized in that organic solvent is acetone and alcohols such as ethanol, propanol, butanols, isopropyl alcohol and isobutanol.
7, hair care hair caring mouse compositions as claimed in claim 1 is characterized in that gaseous propellant is an iso-butane, propane/butane (40/60 or 25/75) fluorine Lyons F-12, F-22 and F-13.
8, the compound method of hair care hair caring mouse compositions as claimed in claim 1 is characterized in that mousse adopts the compound method of elaeagnus gum virgin rubber to be:
A. apparent impurity in the elaeagnus gum is removed,
B. elaeagnus gum is ground into 10-50 purpose powder,
C. in the room temperature water in above-mentioned powder input being stirred or after soaking about diel earlier, be warming up to 60-100 ℃, stir and became uniform colloid in 1-10 hour, pass through again (or without) activated carbon decolorizing and filtration treatment, making concentration is the elaeagnus gum colloid of 0.5-5.0%
D. stirred 0.5-3 hour than mixing by each set of dispense in the prescription, be heated to 25-60 ℃ of filtered while hot, promptly get the mousse colloid.
9, the compound method of hair care hair caring mouse compositions as claimed in claim 1 is characterized in that mousse adopts the compound method of the extraction separation thing of elaeagnus gum to be:
A. the amount of taking is that the 10-50 dimethyl sulfoxine or the water doubly of elaeagnus gum amount soaks natural gum under room temperature, filter, to nothing or till seldom polysaccharide can be extracted again, 2/3(weight with extracting solution) the 95% ethanol floccule of emanating out filters, and uses earlier 95% ethanol, reuse absolute ethanol washing and filtration, gained solid vacuum drying gets the white powder polyoses extract
B. in the room temperature water in the extract input being stirred, be warmed up to 60～100 ℃ and stirred 1-10 hour, making concentration is the elaeagnus gum colloid of 0.5-5%,
C. mix by the proportioning of each component in the prescription, stirred 0.5-3 hour, promptly get the mousse colloid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 92108424 CN1065792A (en) | 1992-05-16 | 1992-05-16 | Contain elaeagnus gum hair care hair caring mouse compositions and compound method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 92108424 CN1065792A (en) | 1992-05-16 | 1992-05-16 | Contain elaeagnus gum hair care hair caring mouse compositions and compound method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1065792A true CN1065792A (en) | 1992-11-04 |
Family
ID=4943531
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 92108424 Pending CN1065792A (en) | 1992-05-16 | 1992-05-16 | Contain elaeagnus gum hair care hair caring mouse compositions and compound method thereof |
Country Status (1)
| Country | Link |
|---|---|
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1072011C (en) * | 1994-10-22 | 2001-10-03 | 中国科学院新疆化学所 | Natural gums hair-caring styling mousse |
| CN100528129C (en) * | 2007-07-23 | 2009-08-19 | 艾斯卡尔·艾海提 | Hair care cream containing elaeagnus angustifolia and producing method thereof |
| CN103356406A (en) * | 2013-07-20 | 2013-10-23 | 上海艳紫化工科技有限公司 | The Lignum Santali Albi shampoo |
-
1992
- 1992-05-16 CN CN 92108424 patent/CN1065792A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1072011C (en) * | 1994-10-22 | 2001-10-03 | 中国科学院新疆化学所 | Natural gums hair-caring styling mousse |
| CN100528129C (en) * | 2007-07-23 | 2009-08-19 | 艾斯卡尔·艾海提 | Hair care cream containing elaeagnus angustifolia and producing method thereof |
| CN103356406A (en) * | 2013-07-20 | 2013-10-23 | 上海艳紫化工科技有限公司 | The Lignum Santali Albi shampoo |
| CN103356406B (en) * | 2013-07-20 | 2015-01-21 | 安徽省林锦记食品工业有限公司 | Sandalwood shampoo |
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