CN106562463A - Storage condition-based stable reconstituted tobacco water-soluble sugar content method - Google Patents

Storage condition-based stable reconstituted tobacco water-soluble sugar content method Download PDF

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Publication number
CN106562463A
CN106562463A CN201610974356.4A CN201610974356A CN106562463A CN 106562463 A CN106562463 A CN 106562463A CN 201610974356 A CN201610974356 A CN 201610974356A CN 106562463 A CN106562463 A CN 106562463A
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China
Prior art keywords
storage
condition
reconstituted tobacco
soluble sugar
sugar content
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Pending
Application number
CN201610974356.4A
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Chinese (zh)
Inventor
王晓园
王茜茜
罗岩峰
刘永强
谢晓斌
李宙文
李敏
彭琛
冀浩
雷佳
黄妧婷
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China Tobacco Guangdong Industrial Co Ltd
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China Tobacco Guangdong Industrial Co Ltd
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Priority to CN201610974356.4A priority Critical patent/CN106562463A/en
Publication of CN106562463A publication Critical patent/CN106562463A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B1/00Preparation of tobacco on the plantation
    • A24B1/10Packing or pressing tobacco

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  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Packages (AREA)

Abstract

The invention discloses a storage condition-based stable reconstituted tobacco water-soluble sugar content method. A storage condition comprises a packaging method and storage time. The packaging method is that a lining bag is disposed in a carton or vacuum package is provided for the carton. The storage time is one to three months or seven to nine months. For better stable reconstituted tobacco water-soluble sugar content technical effects, the storage condition further contains a storage region condition. The method solves deficiencies of lack of storage technology reference in the field of reconstituted tobaccos, so deficiencies of standard storage conditions determined in an instructive document Tobacco leaves storage method (GB/T23223-2008) in the field; and powerful technical support is provided for reconstituted tobacco storage quality.

Description

Method based on the stable reconstituted tobacco water-soluble sugar content of condition of storage
Technical field
The present invention relates to reconstituted tobacco storing technology field, more particularly, to a kind of stablizing again based on condition of storage The method for making Nicotiana tabacum L. water-soluble sugar content.
Background technology
Nicotiana tabacum L. has water absorption, and Nicotiana tabacum L. is placed in the air of uniform temperature, humidity, it can absorb from air moisture or Moisture is distributed in air.The storage of raw material (including Nicotiana tabacum L., reconstituted tobacco etc.) is the important ring in production of cigarettes work flow Section, the holding of good storage condition to the stable and cigarette product liquor style of cigarette process raw materials quality has important work With.
Used as Cigarette processing enterprise, it is important in whole production procedure that raw material is stored (including Nicotiana tabacum L., reconstituted tobacco etc.) One ring, is that raw material realizes its management link being worth.The main purpose of Nicotiana tabacum L. storage is to create " the time effect of Nicotiana tabacum L. With ", make Nicotiana tabacum L. be fully used in the effectiveness highest time, the qualitative potential of Nicotiana tabacum L. is given full play to, realize that Nicotiana tabacum L. resource exists Distributing rationally on the time and in quality, reaches protection and improves the purpose of quality of tobacco.
Tobacco leaf warehouse refers to that for the storehouse of stored tobacco leaf commodity the past is mainly open-air storage, at this stage generally reinforcing bar The indoor storage of cement structures, point monolayer and multilamellar storehouse, equipped with functions such as the aeration-cooling dehumidifying of moisture-proof heat-insulation.Tobacco leaf storage Major function be timeliness and the spatiality contradiction for solving tobacco leaf planting and production of cigarettes, production of cigarettes is carried out continuously.
At present, both at home and abroad to Nicotiana tabacum L. storage in terms of research it is more, for example《Nicotiana tabacum L. stores keeping method》(GB/T23220- 2008) be normative document that the current industry preserves Nicotiana tabacum L., it is pointed out that according to different sources, different quality situation piece cigarette it is suitable The preferably phase of refining determines the shelf life, generally 12~36 months.Normative document does not propose to refer to reconstituted tobacco storage aspect Lead, at present to reconstituted tobacco storage in terms of research leaf be rarely reported.Though reconstituted tobacco is similar to Nicotiana tabacum L., but still exists a lot Significant difference.Reconstituted tobacco is the product reconfigured with tobacco materials such as offal, cabo, fragments, and thickness typically exists 0.2mm, is pilotaxitic texture, by table to inner moisture absorption.And blade is herbaceous plant class, thickness, typically in 0.14mm, is with pore Collastromin moisture absorption, directly penetrates into inside.Reconstituted tobacco is different with the organizational structure of Nicotiana tabacum L., and thickness is different, and the property of moisture absorption is just It is different.Meanwhile, stacking states can make to produce sticking effect during papermaking-method reconstituted tobaccos storage, affect mixing for subsequent technique to match somebody with somebody Uniformity etc., these can all cause the decline of papermaking-method reconstituted tobaccos application performance.Therefore, papermaking-method reconstituted tobaccos and Nicotiana tabacum L. phase Than storing mode should have differences.At present, reconstituted tobacco is not different from Nicotiana tabacum L. and is individually stored, from storage feelings before From the point of view of condition, easily there is mildew phenomena during the storage with reference to Nicotiana tabacum L. in portioned product, causes the application performance of reconstituted tobacco Decline, produce economic loss.Furthermore, it is constant-temperature constant-humidity environment that regular warehouse that normative document specifies is required, be embodied as when There is construction of warehouse high cost, wayward and realization a difficult problem in time.
Water-soluble sugar is the sweet taste mouthfeel and mainstream smoke total particulate matter growing amount and tar growing amount with smoking property of cigarette Related important component.It is the contained important component of tobacco material itself, and the important component for also serving as many essence and flavoring agents adds During being added to production of cigarettes, have in terms of local flavor important function sucking for Nicotiana tabacum L. is adjusted.During cigarette burning, water There is a series of chemical change and be converted into other materials in dissolubility sugar, but still have a small amount of sugar to pass through high-temperature heating and distillation etc. and make With the negative pressure produced when sucking filter tip with smoker is entered in the oral cavity of smoker by cigarette and through filter tip.In Medicated cigarette Appropriate water-soluble sugar and nicotine ratio are kept when burning and sucking, can make flue gas alcohol and while keep suitable concentration and strength again Head.Although the water-soluble sugar content into smoker oral cavity is relatively low, regarding the difference of content, the generation to fragrant and sweet and soft and moist mouthfeel Show with different important function research, the sugared content in Nicotiana tabacum L. is too low to make that flue gas is coarse, stimulate and increase;Sugared content is too high Can then make flue gas insipid, affect jealous, unnecessary sugar can also increase tar content, increase harm of the flue gas to human body.Therefore, Improve the interior quality of Medicated cigarette, it should be noted that by water-soluble sugar content control in flue-cured tobacco raw material within the scope of suitably.Generally The water-soluble sugar content of the examination criteria guarantee reconstituted tobacco that manufacturer completes to have strict in reconstituted tobacco production, but In the storage of reconstituted tobacco, whether water-soluble sugar content can change, and how is Changing Pattern, by which condition element Impact, currently without any technical research report and perform standard.Meanwhile, lack be based on by scientific and reasonable factors composition at present Condition of storage, be adjusted and control the technical scheme stable to ensure reconstituted tobacco water-soluble sugar content.
The content of the invention
The technical problem to be solved in the present invention is contained for the existing water-soluble sugar based on the stable reconstituted tobacco of condition of storage A kind of technical deficiency of amount, there is provided method of the regulation reconstituted tobacco water-soluble sugar content based on condition of storage.
The purpose of the present invention is achieved by the following technical programs:
A kind of method of the stable reconstituted tobacco water-soluble sugar content based on condition of storage is provided, the condition of storage includes Manner of packing and storage time;Wherein, the manner of packing is using additional vacuum packet in carton supplemental inner bag packaging or carton Dress;The storage time is 1~3 month or 7~9 months.
The manner of packing preferably adopts carton supplemental inner bag.The material of the inner lining bag is high density polyethylene (HDPE), outward See without visible hole and bag is without gas leak phenomenon.
The storage time is preferably 1~3 month, most preferably stores 1 month.
Preferably, the condition of storage also includes storage location.Preferred storage location needs to meet following condition, constant temperature Constant humidity environment, temperature is 22 ± 1 DEG C, and relative humidity is 60 ± 5%.Meet the storage location condition has regular warehouse.
Or, preferably storage location meets following condition:Its position is between 18 '~116 ° 56 ' of east longitude 115 °, north latitude Between 23 ° 23 '~24 ° 56 ', 20 DEG C of average temperature of the whole year, average relative humidity is 55%, does not require constant temperature and humidity, common coagulation The warehouse of soil structure can meet storage request.Preferably, the warehouse for having a MeiZhou,GuangDong of the storage location condition is met.
The invention has the advantages that:
The present invention interact in condition of storage factor, interfere with each other it is various complexity in the case of summarize science rule Rule, realizes the accurate primary condition for determining storage, there is provided a kind of stable reconstituted tobacco water-soluble sugar based on condition of storage contains The method of amount.Through numerous studies and analysis, present invention determine that the stored key of stable reconstituted tobacco water-soluble sugar content because Element, manner of packing and storage time, accurately determine preferably manner of packing and storage time, ensure that reconstituted tobacco was being stored The stability of water-soluble sugar content in journey, so as to finally ensure the stability of raw materials quality.On this basis, the present invention is further Precisely define preferred storage regional condition, according to present invention determine that regional condition combine manner of packing and storage time Define, it is possible to obtain the technique effect of optimal stable reconstituted tobacco water-soluble sugar content.The present invention changes this area again The deficiency that Nicotiana tabacum L. lacks storing technology reference is made, this area directive document is breached《Nicotiana tabacum L. stores keeping method》(GB/ The deficiency of the normal storage conditions determined in T23220-2008), using the present invention mark of constant temperature and humidity is adopted without considered critical Quasi- warehouse storage reconstituted tobacco can also ensure storage quality.Reconstituted tobacco storage quality being improved for this area, strong technology is provided Support.
Description of the drawings
The reconstituted tobacco sample near infrared spectrum scanning result that tri- kinds of Fig. 1 is randomly selected.
Water-soluble sugar variation tendency under four season of Fig. 2 reconstituted tobaccos each condition of storage.
Wherein, in Fig. 1, I is carton, II is carton+inner lining bag, III is carton+vacuum, IV is carton+nitrogen charging;A is mark Quasi- stock, B are Guangzhou, C is Meizhou, D is Shaoguan;1 for storage 1 season, 2 for storage 2 season, 3 for storage 3 season, 4 To store for 4 season.
Specific embodiment
Further illustrate the present invention with specific embodiment below in conjunction with the accompanying drawings.Following embodiments are only used for verifying that the present invention sets The exemplary illustration of meter thought, it is impossible to be interpreted as limitation of the present invention.Unless stated otherwise, the examination used in following embodiments Agent is the reagent that conventional commercial or commercial sources are obtained, and unless stated otherwise, the method and apparatus used in following embodiments is Method and apparatus commonly used in the art.
Embodiment 1
For convenience of description, the present embodiment randomly selects three kinds again in the reconstituted tobacco of certain tobacco leaf production enterprise large usage quantity Make and illustrated as a example by tobacco leaf product, the product RSGD-126 (species A) and product G DT-3 (species B) of a respectively producer, separately Product G R60ZO1 (species C) of one producer.Fig. 1 is three kinds of reconstituted tobacco sample near infrared spectrum scanning results for randomly selecting, As can be seen that three kinds of product interior qualities have significant difference, the variation tendency one caused because quality is similar can be prevented effectively from Cause, it is ensured that the effectiveness of analysis result.
Randomly select three kinds of reconstituted tobaccos are respectively adopted into four kinds of packaged forms, respectively 1) packed in cases;2) carton Supplemental inner bag packs (inner lining bag);3) carton addition of vacuum packaging (vacuum);4) the additional nitrogen gas packing of carton is packed and (filled Nitrogen).Wherein, the inner lining bag is obtained using high-density polyethylene material, and outward appearance is without visible hole and bag is without gas leak phenomenon.Very Empty package can adopt food grade thin-film material or similar material with the packaging of nitrogen charging, and vacuum and nitrogen charging amount are with reference to existing The routine for having technology packaging to use, does not do considered critical.Such as described nitrogen charging is to be charged to reach purity nitrogen level (instant food using nitrogen Level).
For convenience of description and test operation, the present embodiment is illustrated with four sample warehousing storages, but is not therefore limited Determine the scope of the invention.They are respectively:1) with reference to Nicotiana tabacum L. storage keeping method (GB/T23220-2008) design standard storage bar The regular warehouse of part, is A;2) B warehouse storages condition (Guangdong Shaoguan);3) C warehouse storages condition (Guangzhou Guangdong);4) D warehouses Condition of storage (MeiZhou,GuangDong).
Wherein, warehouse 1 is the regular warehouse that this area normative document specifies, it is constant-temperature constant-humidity environment that regular warehouse is required, Its temperature is 22 ± 1 DEG C, relative humidity is 60 ± 5%.
23 DEG C of the average temperature of the whole year of the their location of warehouse 2, average relative humidity is 60%.Its position is between 112 ° of east longitude 53 '~114 ° 45 ', between 53 '~25 ° 31 ' of north latitude 23 °, middle subtropical zone wet type monsoon climatic region is belonged to residingly, spring is overcast and rainy Unbroken, Autumn Precipitation is on the low side, and winter is cold, summer partial heat, abundant rainfall, 1400~2400 millimeters of average annual rainfall, and 3~August is In rainy season, 9~2 months be dry season.
22 DEG C of the average temperature of the whole year of the their location of warehouse 3, average relative humidity is 68%.Its position is between 23 ° of north latitude 06 ', 113 ° 15 ' of east longitude is located in China's Mainland south, the Guangdong Province middle and south, Delta of the Pearl River the northern fringe.Belong to Southeast Asia heat residingly Band monsoon climate, climatic characteristic is that temperature is high, precipitation is more, frost day is few, sunshine is more, wind speed is little, thunderstorm is frequent, mean annual precipitation 1982.7mm, in more than 1800h, average relative humidity is 68% to annual sunshine time, the annual hydro-thermal same period, abundant rainfall. In whole year, 4~June is rainy season, and 8~September heat, many typhoons, 10~December temperature is moderate.
20 DEG C of the average temperature of the whole year of the their location of warehouse 4, average relative humidity is 55%.Its position is between 115 ° of east longitude 18 '~116 ° 56 ', the low latitudes between 23 '~24 ° 56 ' of north latitude 23 °, local landform based on mountain and hill, weather Belong to subtropical monsoon climate, rainwater enriches, but each Seasonal rainfall is uneven, rainfall is concentrated mainly on 4~September, spring Meizhou City drop The water yield is 567.2mm, accounts for the 37% of annual rainfall;Summer is 552.3mm, accounts for the 36% of annual rainfall;Autumn is 224.7mm, accounts for year The 15% of rainfall;Winter is 184.5mm, accounts for the 12% of annual rainfall.
Warehouse 2, warehouse 3 and warehouse 4 are the warehouse of common xoncrete structure, do not do the strict demand of constant temperature and humidity.
Labelling will be carried out according to the packaged reconstituted tobacco of four kinds of manner of packings respectively, certain batch will be reached in quantity. Packaged reconstituted tobacco is separately stored in into aforementioned four warehousing storage.
Sampling method:Different storage locations storage time different with manner of packing is separately sampled.
Detection method:Samples taken carries out water-soluble sugar index inspection by the corresponding method of detection of Nicotiana tabacum L. and tobacco product respectively Survey.Detection method is with reference to this area routine techniquess.
Data processing method:Data processing adopts spss analysis softwares.
3. result of the test:
On the basis of the testing result 10.23% of initial sample water-soluble sugar.Will be seen that by table 1, paper-making method reconstructed cigarette With I, II, III, IV 4 kind of Different Package mode during 12 months that A, B, C, D storage place is deposited, each index entire change becomes leaf Gesture.The water-soluble sugar index of reconstituted tobacco, it is minimum with carton+inner lining bag manner of packing storage coefficient of variation, it is 1.62%, with prunus mume (sieb.) sieb.et zucc. State storage temperature and humidity condition lower variation coefficient is minimum, and 2.42%, the coefficient of variation minimum of 1~3 month is stored, it is 1.56%;
As shown in Figure 2, from the point of view of storage time situation of change, water-soluble sugar index present continuous decrease the characteristics of.From ground See on point, apparently higher than other three ground, but from manner of packing, I will be less than alternate manner to the annual average of A.I and IV packaging Mode fluctuates larger, and II, III manner of packing is basically identical in different storage areas, different storage time variation tendencies.
As shown in Table 2, it is less with the II and III packing and storing coefficient of variation from the point of view of manner of packing, it is 1.62% He 1.69%, I, IV coefficient of variation is larger, consistent with above-mentioned general morphologictrend, namely II and III manner of packing storage reproduce cigarette Leaf water-soluble sugar content is stablized;From the point of view of area, the various places coefficient of variation is less, wherein it is minimum with the C coefficient of variation, 2.42%, Namely it is most stable in the reconstituted tobacco water-soluble sugar content of C storages;From the point of view of storage time, the coefficient of variation of 1~3 month is stored Minimum, is 1.56%, is secondly 7~9 months, 4~6 months, stores the coefficient of variation maximum of 12 months, that is, store 1 month Reconstituted tobacco water-soluble sugar content is most stable, with standard specimen difference less (≤3).
Reconstituted tobacco water-soluble sugar Indexs measure result under the different conditions of storage of table 1
Reconstituted tobacco water-soluble sugar situation of change under the Different Package mode of table 2, storage place and time conditions
The water-soluble sugar of table 3 changes variance analyses
In table 1, table 2 and table 3, I is carton, II is carton+inner lining bag, III is carton+vacuum, IV is carton+nitrogen charging;A For standard stock, B be Guangzhou, C be Meizhou, D be Shaoguan;1 for storage 1~3 month, 2 for storage 4~6 months, 3 for storage 7~ 9 months, 4 for storage 10~12 months.
To sum up, according to the present invention by determining that accurately condition of storage is to realize the side of stable reconstituted tobacco water-soluble sugar Method, existing single carton is better than by reconstituted tobacco using three kinds of modes such as carton+inner lining bag, carton+nitrogen charging, carton+vacuum Manner of packing, but if enterprise's life can be increased during produce reality using two ways such as carton+nitrogen charging, carton+vacuum Cost is produced, therefore its manner of packing adopts carton+inner lining bag for optimum;Stored in 1 year using the manner of packing of carton+inner lining bag In phase, reconstituted tobacco water-soluble sugar content is relatively stable, is preferred with storing 1~3 month and 7~9 months, to store 1~3 month For optimum.Optimal storage location needs to meet temperature for 22 ± 1 DEG C, and relative humidity is 60 ± 5% constant temperature and humidity standard storehouse Storehouse storage request.If regular warehouse requirement cannot be realized, can by storage location located at its position between 115 ° 18 ' of east longitude~ 116 ° 56 ', the corresponding place between 23 '~24 ° 56 ' of north latitude 23 °, 20 DEG C of average temperature of the whole year, average relative humidity is 55%.It is excellent Select the Meizhou that the storage location is Guangdong.

Claims (9)

1. a kind of method of the stable reconstituted tobacco water-soluble sugar content based on condition of storage, it is characterised in that the storage bar Part includes manner of packing and storage time;Wherein, the manner of packing is packed using carton supplemental inner bag mode or carton is attached Plus vacuum mode packaging;The storage time is 1~3 month or 7~9 months.
2. the method for the stable reconstituted tobacco water-soluble sugar content of condition of storage is based on according to claim 1, and its feature exists In the manner of packing adopts carton supplemental inner bag.
3. the method for the stable reconstituted tobacco water-soluble sugar content based on condition of storage according to claim 1 or claim 2, its feature It is that the material of the inner lining bag is high density polyethylene (HDPE).
4. the method for the stable reconstituted tobacco water-soluble sugar content of condition of storage is based on according to claim 1, and its feature exists In the storage time is 1~3 month.
5. the method for the stable reconstituted tobacco water-soluble sugar content of condition of storage is based on according to claim 4, and its feature exists In the storage time is 1 month.
6. the method for the stable reconstituted tobacco water-soluble sugar content of condition of storage is based on according to claim 1, and its feature exists In the condition of storage also includes storage location.
7. the method for the stable reconstituted tobacco water-soluble sugar content of condition of storage is based on according to claim 6, and its feature exists In the storage location meets following condition:Temperature is 22 ± 1 DEG C, and relative humidity is 60 ± 5%.
8. the method for the stable reconstituted tobacco water-soluble sugar content of condition of storage is based on according to claim 6, and its feature exists In the storage location meets following condition:Its position is between 18 '~116 ° 56 ' of east longitude 115 °, 23 '~24 ° of north latitude 23 ° Between 56 ', 20 DEG C of average temperature of the whole year, average relative humidity is 55%.
9. the method for the stable reconstituted tobacco water-soluble sugar content of condition of storage is based on according to claim 8, and its feature exists In the storage location is the Meizhou in Guangdong.
CN201610974356.4A 2016-10-28 2016-10-28 Storage condition-based stable reconstituted tobacco water-soluble sugar content method Pending CN106562463A (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1721535A1 (en) * 2003-12-04 2006-11-15 Hauni Primary GmbH Container of the tobacco processing industry
CN101416771A (en) * 2008-12-08 2009-04-29 北京科技大学 Disinsection mold-proof method with no effect on tobacco mellowing
CN101632490A (en) * 2009-08-06 2010-01-27 河南省科学院同位素研究所有限责任公司 Tobacco leaf and green mould proof method of products thereof
CN202414334U (en) * 2011-11-30 2012-09-05 许昌市京昌塑料制品有限公司 Air-permeable perforated package lining for tobacco
CN104159824A (en) * 2011-10-20 2014-11-19 联合一国际国际有限公司 Vacuum packing methods and apparatus for tobacco

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1721535A1 (en) * 2003-12-04 2006-11-15 Hauni Primary GmbH Container of the tobacco processing industry
CN101416771A (en) * 2008-12-08 2009-04-29 北京科技大学 Disinsection mold-proof method with no effect on tobacco mellowing
CN101632490A (en) * 2009-08-06 2010-01-27 河南省科学院同位素研究所有限责任公司 Tobacco leaf and green mould proof method of products thereof
CN104159824A (en) * 2011-10-20 2014-11-19 联合一国际国际有限公司 Vacuum packing methods and apparatus for tobacco
CN202414334U (en) * 2011-11-30 2012-09-05 许昌市京昌塑料制品有限公司 Air-permeable perforated package lining for tobacco

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Application publication date: 20170419