CN106544686A - A kind of corrosion sample acid dip pickle and method - Google Patents
A kind of corrosion sample acid dip pickle and method Download PDFInfo
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- CN106544686A CN106544686A CN201510589755.4A CN201510589755A CN106544686A CN 106544686 A CN106544686 A CN 106544686A CN 201510589755 A CN201510589755 A CN 201510589755A CN 106544686 A CN106544686 A CN 106544686A
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- inner core
- outer tube
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- pickle
- lid
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- Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
Abstract
A kind of corrosion sample acid dip pickle and method, device includes outer tube, inner core, bracing frame, rotating shaft, rocking handle, outer tube is fixed on bracing frame, inner core is placed within outer tube, one end of inner core is by rotating shaft and outer tube and bracing frame axial restraint, the other end of inner core is fixedly connected with rocking handle, and rocking handle is erected on bracing frame through outer tube, and shake rocking handle can drive inner core to rotate.Compared with prior art, the invention has the beneficial effects as follows：The batch pickling of achievable corrosion sample, compared to existing common method and device, can improve corrosion sample pickling efficiency；Acid cleaning process carried out under sealing condition, it is to avoid acid solution is splashed and acid mist is diffused, safety and environmental protection；Apparatus structure is simple, it is easy to safeguard.
Description
Technical field
The present invention relates to a kind of corrosion sample acid dip pickle and method, specifically refer to one kind and remove for specimen surface after corrosion test
The acid dip pickle and its using method of rust.
Background technology
Decay resistance is an important performance of metal material.In metal material decay resistance evaluation method, lose
Weight method is a kind of classical and reliable method.It is related to the removal of specimen surface corrosion product in weight-loss method implementation process, at present,
It is pickling to remove the most widely used method of corrosion product.The common acid washing method of corrosion sample is to use hook or suspension wire by sample
Hang in pickle and soaked, this method treatment effeciency is low and sample easily drops and causes acid solution to be splashed.Exploitation is a kind of
The method and device for carrying out corrosion sample pickling that can efficiently, safe has its necessity and practical value.
The patent document of 202974818 U of Patent No. CN discloses a kind of rust cleaning specimen mounting, and the specimen mounting includes two
Gate frame and crossbeam therebetween is placed in, on the inside of gate frame, is provided with sample basket, it is parallel on two side frames of sample basket to be provided with many
Individual upper draw-in groove, sample basket bottom are provided with and the one-to-one lower bayonet slot of upper draw-in groove, and draw-in groove can realize fixing and making to sample
Do not contact between sample.Can conveniently realize that sample is put into and takes out the process of descaling bath using the specimen mounting and be capable of achieving criticizing for sample
Amount pickling.But as the size of specimen mounting and its draw-in groove is fixed, thus the specimen mounting cannot realize for sizes sample and
The batch pickling of special-shaped sample, meanwhile, being difficult of sample and draw-in groove contact position reaches satisfied pickling effect.Patent No. CN
The patent document of 202808948 U discloses a kind of stainless-steel environment-friendly type totally enclosed type pickler, and equipment box is molten by pickling
Pond and cleaning bath are constituted, and two parts have independent case lid, and pickling tube lid is provided with the solution inlet for bringing lid into for noting
Enter the chemical reagent such as acid, alkali, horizontal sample mount is provided with pickling tube for sample of placing and take.The device structure letter
Single, easy to operate, acid cleaning process is carried out under conditions of relative closure, can effectively prevent acid solution from splashing.The deficiency of the equipment
Part is that sample is hung on specimen mounting, and pickling is inefficient and pickle and cleaning fluid injection rate can not be according to samples
Amount is adjusted, additionally, inconvenience is picked up when sample falls into bottom once coming off.
The content of the invention
It is an object of the invention to provide a kind of corrosion sample acid dip pickle and method, in being different from existing common method, sample is static
The processing mode of bubble, is fully contacted with pickle and cleaning fluid with the dynamical fashion that sample is rolled, can efficiently, safely
Pickling is carried out to corrosion test sample.
For achieving the above object, the present invention employs the following technical solutions realization：
A kind of corrosion sample acid dip pickle, including outer tube, inner core, bracing frame, rotating shaft, rocking handle, outer tube are fixed on bracing frame
On, inner core is placed within outer tube, one end of inner core by rotating shaft and outer tube and bracing frame axial restraint, the other end of inner core with
Rocking handle is fixedly connected, and rocking handle is erected on bracing frame through outer tube, and shake rocking handle can drive inner core to rotate.
The outer tube include on outer tube main body, outer tube covering on lid, outer tube cover tightly on page, outer tube solid lock buckle, steam vent, row
The one end covered on liquid valve, outer tube main body and outer tube is by lid gemel connection on outer tube, the other end covered in outer tube main body and outer tube
Tight by solid lock padlock is covered tightly on outer tube, the top covered on outer tube is provided with steam vent, is provided with the bottom of outer tube main body
Tapping valve.
The inner core includes on inner core main body, inner core covering on lid, inner core solid lock button, pod apertures is covered tightly on page, inner core, interior
The one end covered in cylinder main body and inner core passes through inner core by lid gemel connection on inner core, the other end covered in inner core main body and inner core
On to cover tightly solid lock padlock tight, pod apertures are provided with inner tube wall.
A kind of method that employing corrosion sample acid dip pickle carries out pickling to corrosion sample, sample is with the dynamical fashion that rolls and acid
Washing lotion and cleaning fluid are fully contacted, so as to reach the purpose that batch, efficient pickling are carried out to corrosion sample, specific side
Method step is as follows：
1) sample is placed in into inner core bottom when cleaning, is closed and is locked；
2) sample injected in appropriate pickle submergence inner core into outer tube, closes and locks；
3) slow rotation crank rolls inner core, sample rolls with the rolling of inner core in pickle, and pickle it is abundant
Contact, completes acid cleaning process；
4) tapping valve is opened after pickling is finished and discharges pickle, opened, then slow rotation crank rolls inner core
While the sample that rinsed in inner core with clear water, tapping valve is opened during flushing discharging waste water；
5) as further cleaned to sample using organic solvents such as ethanol, tapping valve is closed, is injected with outer tube
Machine solvent, sample rolls inner core and is cleaned in submergence inner core；
6) waste liquid is discharged after cleaning, inner core sample is dried up or opened lid taking-up sample on inner core with hair-dryer and is dried.
Compared with prior art, the invention has the beneficial effects as follows：
A kind of corrosion sample acid dip pickle and method, are capable of achieving the batch pickling of corrosion sample, compared to existing common method and
Device, can improve corrosion sample pickling efficiency；Acid cleaning process carried out under sealing condition, it is to avoid acid solution is splashed and acid mist is put
Dissipate, safety and environmental protection；Apparatus structure is simple, it is easy to safeguard.
Description of the drawings
Fig. 1 is a kind of structural representation of corrosion sample acid dip pickle of the invention；
Fig. 2 is a kind of left view of corrosion sample acid dip pickle of the invention
In figure：1- outer tube, covers on 2- outer tube, and 3- bracing frames cover tightly solid lock on 4- outer tube and buckle, and page, 6- rows are covered on 5- outer tube
Liquid valve, 7- steam vents, 8- inner cores cover on 9- inner cores, cover tightly solid lock button, cover page on 11- inner cores on 10- inner cores；12- leads
Discharge orifice, 13- rotating shafts, 14- rocking handles.
Specific embodiment
A kind of corrosion sample acid dip pickle of the present invention is described in detail with reference to Figure of description.
As Figure 1-Figure 2, a kind of corrosion sample acid dip pickle, including outer tube 1, inner core 8, bracing frame 3, rotating shaft 13,
Rocking handle 14, outer tube 1 are fixed on bracing frame 3, and inner core 8 is placed within outer tube 1, and one end of inner core 8 passes through rotating shaft 13
With 3 axial restraint of outer tube 1 and bracing frame, the other end of inner core 8 is fixedly connected with rocking handle 14, and rocking handle 14 passes through outer tube 1
It is erected on bracing frame 3, shake rocking handle 14 can drive inner core 8 to rotate.
Outer tube 1, inner core 8, rotating shaft 13 and rocking handle 14 are coaxially disposed.One end of outer tube 1 be fixed on bracing frame 3
Rotating shaft 13 is fixedly connected, and the other end is connected with rocking handle 14 by bearing.One end of inner core 8 is connected with rotating shaft 13 by bearing
Connect, the other end is fixedly connected with rocking handle 14, bearing is installed between rocking handle 14 and bracing frame 3, by shaking rocking handle 14
Inner core 8 can be made to roll in outer tube 1.
This device outer tube 1, the material of inner core 8 are acidproof engineering plastics and have certain thickness, to meet splendid attire cleaning fluid
And sample rolls the requirement to device rigidity and intensity；Bracing frame 3 and rotating shaft 13 adopt ferrous materials.
The outer tube 1 include covering on lid 2, outer tube on outer tube main body, outer tube cover tightly on page 5, outer tube solid lock buckle 4, exhaust
Hole 7, tapping valve 6, one end of outer tube main body and lid on outer tube 2 are connected by covering page 5 on outer tube, outer tube main body with it is outer
On cylinder, the other end of lid 2 is locked by covering tightly solid lock on outer tube and buckleing 4, and on outer tube, the top of lid 2 is provided with steam vent 7,
The bottom of outer tube main body is provided with tapping valve 6.
Outer tube 1 is cylinder, and level is fixed on bracing frame 3.On outer tube, lid 2 can be opened for sample of placing and take.
Outer tube main body is used to contain pickle and cleaning fluid.The steam vent 7 arranged at the top of outer tube 1 is used to discharging produce during pickling useless
Gas.Tapping valve 6 immediately below outer tube 1 can be connected with waste liquid tank or sewer by flexible pipe, for discharging waste liquid.
The inner core includes covering on lid 9, inner core on inner core main body, inner core solid lock button 10, water conservancy diversion is covered tightly on page 11, inner core
Hole 12, inner core main body are connected by covering page 11 on inner core with one end of lid on inner core 9, lid 9 in inner core main body and inner core
The other end locked by covering tightly solid lock button 10 on inner core, pod apertures 12 are provided with inner tube wall.
The cage construction of generally eight prismatics of inner core 8, surface are uniformly distributed pod apertures 12, accommodate examination during cleaning in inner core 8
The part of sample is dipped in the cleaning fluid of outer tube 1, and cleaning fluid can be freed in and out in inner core 8 by pod apertures 12, so as to reach
To submergence and wash away the purpose of sample.Inner core 8 can make sample roll in bucket, fall in eight prismatics, so as to pickle
And cleaning fluid is fully contacted.On inner core, lid 9 can be equally opened for sample of placing and take.
When place and take sample when lid 9 on lid on outer tube 2 and inner core is opened, during sample pickling close outer tube on lid 2 and
Lid 9 locked with cylinder by solid lock is covered tightly on outer tube buckleing solid lock is covered tightly on 4 and inner core to buckle 10 respectively on inner core.
Below by a kind of method of the embodiment to carrying out pickling to corrosion sample using corrosion sample acid dip pickle in the present invention
It is further described.
Embodiment 1, carries out pickling to the sample of surface corrosion product easy-clear using a kind of corrosion sample acid dip pickle.
1) when cleaning, sample is placed in 8 bottom of inner core, closes and lock lid 9 on inner core.
2) sample injected in appropriate pickle submergence inner core 8 into outer tube 1, closes and locks lid 2 on outer tube.
3) slow rotation crank 14, rolls inner core 8, now sample roll in pickle with the rolling of inner core 8,
It is fully contacted with pickle, completes acid cleaning process.
4) tapping valve 6 is opened after pickling is finished and discharges pickle, open lid 2 on outer tube, then in slowly rotation crank 14 makes
The sample that cylinder 8 is rinsed in inner core 8 with clear water while rolling, during flushing, tapping valve 6 is opened to discharge waste water.
5) sample in inner core 8 is dried up or opened lid 9 on inner core with hair-dryer take out sample and dry.
Embodiment 2, carries out pickling to the difficult sample removed of surface corrosion product using a kind of corrosion sample acid dip pickle.
The plastic cement grinding stone of commercially available different size can be added when the more difficult removal of specimen surface corrosion product in inner core 8 optionally
So that corrosion product is thoroughly removed.Other steps are same as Example 1.
Embodiment 3, carries out pickling and organic solvent cleaning using a kind of corrosion sample acid dip pickle to sample.
The acid cleaning process of sample is same as Example 1.When further being cleaned to sample using organic solvents such as ethanol,
Tapping valve 6 is closed, organic solvent is injected in outer tube 1, sample rolled inner core 8 and cleaned in submergence inner core 8.Clearly
Waste liquid is discharged after washing, sample in inner core 8 is dried up or opened lid 9 on inner core with hair-dryer is taken out sample and dry.
Although being described above in conjunction with enforcement of the accompanying drawing to the present invention, above-mentioned being embodied as is the invention is not limited in
Mode, above-mentioned embodiment are not restricted, and one of ordinary skill in the art is not being taken off under the enlightenment of the present invention
In the case of present inventive concept and scope of the claimed protection, the concrete conversion of various ways can be also made, and these are not
Should exclude outside protection scope of the present invention.
Claims (4)
1. a kind of corrosion sample acid dip pickle, it is characterised in that including outer tube, inner core, bracing frame, rotating shaft, rocking handle,
Outer tube is fixed on bracing frame, and inner core is placed within outer tube, and one end of inner core passes through rotating shaft and outer tube and bracing frame axial restraint,
The other end of inner core is fixedly connected with rocking handle, and rocking handle is erected on bracing frame through outer tube, and shake rocking handle can drive inner core to rotate.
2. a kind of corrosion sample acid dip pickle according to claim 1, it is characterised in that：The outer tube includes outer tube
Lid on main body, outer tube, cover on outer tube cover tightly on page, outer tube solid lock buckle, steam vent, tapping valve, outer tube main body and outer tube
Buckled by covering tightly solid lock on outer tube by lid gemel connection on outer tube, the other end covered in outer tube main body and outer tube one end of upper lid
Locking, the top covered on outer tube is provided with steam vent, the bottom of outer tube main body is provided with tapping valve.
3. a kind of corrosion sample acid dip pickle according to claim 1, it is characterised in that：The inner core includes inner core
Cover on lid, inner core on main body, inner core and on page, inner core, cover tightly solid lock button, pod apertures, covered in inner core main body and inner core
By lid gemel connection on inner core, the other end covered in inner core main body and inner core is tight by solid lock padlock is covered tightly on inner core at end,
Pod apertures are provided with inner tube wall.
4. the method that the corrosion sample acid dip pickle described in a kind of employing claim 1 carries out pickling to corrosion sample, which is special
Levy and be, sample is fully contacted with pickle and cleaning fluid with the dynamical fashion for rolling, and corrosion sample is entered so as to reach
Row batch, the purpose of efficient pickling, specific method and step are as follows：
1) sample is placed in into inner core bottom when cleaning, is closed and is locked；
2) sample injected in appropriate pickle submergence inner core into outer tube, closes and locks；
3) slow rotation crank rolls inner core, sample rolls with the rolling of inner core in pickle, and pickle it is abundant
Contact, completes acid cleaning process；
4) tapping valve is opened after pickling is finished and discharges pickle, opened, then slow rotation crank rolls inner core
While the sample that rinsed in inner core with clear water, tapping valve is opened during flushing discharging waste water；
5) as further cleaned to sample using organic solvents such as ethanol, tapping valve is closed, is injected with outer tube
Machine solvent, sample rolls inner core and is cleaned in submergence inner core；
6) waste liquid is discharged after cleaning, inner core sample is dried up or opened lid taking-up sample on inner core with hair-dryer and is dried.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510589755.4A CN106544686A (en) | 2015-09-17 | 2015-09-17 | A kind of corrosion sample acid dip pickle and method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510589755.4A CN106544686A (en) | 2015-09-17 | 2015-09-17 | A kind of corrosion sample acid dip pickle and method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106544686A true CN106544686A (en) | 2017-03-29 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510589755.4A Pending CN106544686A (en) | 2015-09-17 | 2015-09-17 | A kind of corrosion sample acid dip pickle and method |
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| Country | Link |
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| CN (1) | CN106544686A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116334607A (en) * | 2023-03-31 | 2023-06-27 | 江苏领创新材料有限公司 | Passivation treatment device for aluminum veneer production and processing |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5906215A (en) * | 1997-11-20 | 1999-05-25 | Reel Clean Corporation | Fishing reel cleaning solution |
| CN201538817U (en) * | 2009-08-14 | 2010-08-04 | 张崇伦 | Wire surface treatment machine |
| CN203419989U (en) * | 2013-07-11 | 2014-02-05 | 杭州华光焊接新材料股份有限公司 | Stainless steel cylinder used for cleaning annular brazing filler metal |
| CN203917243U (en) * | 2014-06-17 | 2014-11-05 | 重庆金山通用机械制造有限公司 | Stainless steel waste material greasy dirt cleaning machine |
| CN204466846U (en) * | 2015-01-28 | 2015-07-15 | 罗石 | Foot-operated peanut cleaning machine |
| CN205067194U (en) * | 2015-09-17 | 2016-03-02 | 鞍钢股份有限公司 | Corrode sample acid dip pickle |
-
2015
- 2015-09-17 CN CN201510589755.4A patent/CN106544686A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5906215A (en) * | 1997-11-20 | 1999-05-25 | Reel Clean Corporation | Fishing reel cleaning solution |
| CN201538817U (en) * | 2009-08-14 | 2010-08-04 | 张崇伦 | Wire surface treatment machine |
| CN203419989U (en) * | 2013-07-11 | 2014-02-05 | 杭州华光焊接新材料股份有限公司 | Stainless steel cylinder used for cleaning annular brazing filler metal |
| CN203917243U (en) * | 2014-06-17 | 2014-11-05 | 重庆金山通用机械制造有限公司 | Stainless steel waste material greasy dirt cleaning machine |
| CN204466846U (en) * | 2015-01-28 | 2015-07-15 | 罗石 | Foot-operated peanut cleaning machine |
| CN205067194U (en) * | 2015-09-17 | 2016-03-02 | 鞍钢股份有限公司 | Corrode sample acid dip pickle |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116334607A (en) * | 2023-03-31 | 2023-06-27 | 江苏领创新材料有限公司 | Passivation treatment device for aluminum veneer production and processing |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
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| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170329 |