CN106524191A - Fluorine-contained alkane waste gas incineration treatment process and device - Google Patents
Fluorine-contained alkane waste gas incineration treatment process and device Download PDFInfo
- Publication number
- CN106524191A CN106524191A CN201610929562.3A CN201610929562A CN106524191A CN 106524191 A CN106524191 A CN 106524191A CN 201610929562 A CN201610929562 A CN 201610929562A CN 106524191 A CN106524191 A CN 106524191A
- Authority
- CN
- China
- Prior art keywords
- fluorine
- waste gas
- incinerator
- containing alkane
- air
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
- F23G—CREMATION FURNACES; CONSUMING WASTE PRODUCTS BY COMBUSTION
- F23G7/00—Incinerators or other apparatus for consuming industrial waste, e.g. chemicals
- F23G7/06—Incinerators or other apparatus for consuming industrial waste, e.g. chemicals of waste gases or noxious gases, e.g. exhaust gases
- F23G7/061—Incinerators or other apparatus for consuming industrial waste, e.g. chemicals of waste gases or noxious gases, e.g. exhaust gases with supplementary heating
- F23G7/065—Incinerators or other apparatus for consuming industrial waste, e.g. chemicals of waste gases or noxious gases, e.g. exhaust gases with supplementary heating using gaseous or liquid fuel
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
- F23J—REMOVAL OR TREATMENT OF COMBUSTION PRODUCTS OR COMBUSTION RESIDUES; FLUES
- F23J15/00—Arrangements of devices for treating smoke or fumes
- F23J15/02—Arrangements of devices for treating smoke or fumes of purifiers, e.g. for removing noxious material
- F23J15/04—Arrangements of devices for treating smoke or fumes of purifiers, e.g. for removing noxious material using washing fluids
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
- F23L—SUPPLYING AIR OR NON-COMBUSTIBLE LIQUIDS OR GASES TO COMBUSTION APPARATUS IN GENERAL ; VALVES OR DAMPERS SPECIALLY ADAPTED FOR CONTROLLING AIR SUPPLY OR DRAUGHT IN COMBUSTION APPARATUS; INDUCING DRAUGHT IN COMBUSTION APPARATUS; TOPS FOR CHIMNEYS OR VENTILATING SHAFTS; TERMINALS FOR FLUES
- F23L7/00—Supplying non-combustible liquids or gases, other than air, to the fire, e.g. oxygen, steam
- F23L7/002—Supplying water
- F23L7/005—Evaporated water; Steam
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
- F23G—CREMATION FURNACES; CONSUMING WASTE PRODUCTS BY COMBUSTION
- F23G2204/00—Supplementary heating arrangements
- F23G2204/10—Supplementary heating arrangements using auxiliary fuel
- F23G2204/103—Supplementary heating arrangements using auxiliary fuel gaseous or liquid fuel
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
- F23J—REMOVAL OR TREATMENT OF COMBUSTION PRODUCTS OR COMBUSTION RESIDUES; FLUES
- F23J2217/00—Intercepting solids
- F23J2217/50—Intercepting solids by cleaning fluids (washers or scrubbers)
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
- F23L—SUPPLYING AIR OR NON-COMBUSTIBLE LIQUIDS OR GASES TO COMBUSTION APPARATUS IN GENERAL ; VALVES OR DAMPERS SPECIALLY ADAPTED FOR CONTROLLING AIR SUPPLY OR DRAUGHT IN COMBUSTION APPARATUS; INDUCING DRAUGHT IN COMBUSTION APPARATUS; TOPS FOR CHIMNEYS OR VENTILATING SHAFTS; TERMINALS FOR FLUES
- F23L2900/00—Special arrangements for supplying or treating air or oxidant for combustion; Injecting inert gas, water or steam into the combustion chamber
- F23L2900/07009—Injection of steam into the combustion chamber
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- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Combustion & Propulsion (AREA)
- Gasification And Melting Of Waste (AREA)
Abstract
The invention provides a fluorine-contained alkane waste gas incineration treatment process. The process comprises the following steps: (S1) an incineration furnace with a refractory material is preheated; and fluorine-contained alkane waste gas is introduced in the preheated incineration furnace; (S2) water vapor is introduced in the incineration furnace for reaction according to the molecule content of fluorine-contained alkane in the waste gas; (S3) natural gas is introduced in the incineration furnace to control the temperature of the incineration furnace; (S4) the feeding quantity of air is controlled in proportion according to the total quantity of the fluorine-contained alkane waste gas and the natural gas; and (S5) incinerated high-temperature smoke is fed in a graphite sudden cooling tower for water washing and absorption of hydride of halogens in the sudden-cooled smoke. The process can incinerate the fluorine-contained alkane waste gas for decomposition to guarantee full combination of halogen atoms as absorbable molecules. Meanwhile, the incineration automation is realized through effective control to reduce the operation risk. In addition, through methods of selecting refractory materials and graphite materials for high-temperature equipment and controlling the HF concentration through proportional air feeding, the equipment service life is prolonged.
Description
Technical field
The present invention relates to incineration technology field, more particularly to a kind of fluorine-containing alkane burned waste gas handling process and device.
Background technology
In fluorine-containing process of producing product, length occurs some fluorine-containing alkanes incoagulability waste gas and by-product material, most
The by-product of fluorine-containing alkane is recycled in system and continues to participate in reflection or make other materials, but still has the part can not in addition profit
With outer after condensation is reclaimed row need to be entered.However, due to organic efficiency it is limited, it will usually cause a large amount of fluorine-containing alkanes substances straight
Connect and be emitted in air, pollute environment.Additionally, separately have a small amount of enterprise to adopt burning disposal, but as handling process is limited and is set
Standby material type selecting is difficult, causes to process the incomplete, problem that equipment corrosion is serious, service life is extremely low.
Therefore, for the problems referred to above, it is necessary to propose further solution.
The content of the invention
It is an object of the invention to provide a kind of fluorine-containing alkane burned waste gas handling process, is present to overcome in prior art
Deficiency.
For achieving the above object, the present invention provides a kind of fluorine-containing alkane burned waste gas handling process, and which includes:
S1, the incinerator with refractory material is preheated, fluorine-containing alkane waste gas is passed through in the incinerator after preheating;
S2, according to the molecule content of fluorine-containing alkane in waste gas, be passed through vapor in incinerator and reacted;
S3, it is passed through natural gas in incinerator, to control the furnace temperature of incinerator;
S4, the amount of filling into for by fluorine-containing alkane waste and natural gas total amount, controlling air in proportion;
S5, by after burning high-temperature flue gas send into graphite chilling tower, the hydride of halogen in the flue gas after chilling is washed
Absorb.
Used as the improvement of the fluorine-containing alkane burned waste gas handling process of the present invention, the preheating temperature of the incinerator is 1100
More than DEG C.
Used as the improvement of the fluorine-containing alkane burned waste gas handling process of the present invention, the refractory material is chromium oxide and three oxygen
Change two aluminum, the chromium oxide and aluminium sesquioxide content are more than 95wt%, and the chromic oxide content >=10 wt %.
Used as the improvement of the fluorine-containing alkane burned waste gas handling process of the present invention, the amount of filling into of the air is by described fluorine-containing
Ratio value between alkane exhaust gas flow and amount of natural gas determines.
Used as the improvement of the fluorine-containing alkane burned waste gas handling process of the present invention, the amount of filling into of the air is mended as frequency conversion
The setting value of blower fan, when filling into air, according to the setting value, repaiies to the air capacity by mending the actual survey of distinguished and admirable gauge
Order.
Used as the improvement of the fluorine-containing alkane burned waste gas handling process of the present invention, in the high-temperature flue gas after the burning, HF is dense
Degree not higher than 5%.
For achieving the above object, the present invention also provides a kind of fluorine-containing alkane burned waste gas processing meanss, and which includes:It is useless
Blower fan and graphite chilling tower are mended in gas surge tank, incinerator, frequency conversion;
The off-gas buffer tank is connected with the incinerator by waste line, the frequency conversion mend blower fan by air line with
The incinerator is connected, and the graphite chilling tower is connected with the incinerator by high-temperature flue gas pipeline, the incinerator
It is also associated with burning line and vapor pipeline.
As the improvement of the fluorine-containing alkane burned waste gas processing meanss of the present invention, burning at the top of the incinerator, is provided with
Device, the burning line and vapor pipeline are connected with the burner.
As the improvement of the fluorine-containing alkane burned waste gas processing meanss of the present invention, waste gas on the waste line, is also parallel with
Blow-down pipe.
Used as the improvement of the fluorine-containing alkane burned waste gas processing meanss of the present invention, it is two groups, two groups that blower fan is mended in the frequency conversion
Frequency conversion benefit blower fan is parallel with one another, and is connected with the incinerator by respective air line respectively.
Compared with prior art, the invention has the beneficial effects as follows:The fluorine-containing alkane burned waste gas handling process of the present invention can
Fluorine-containing alkane waste gas is decomposed by burning, and guarantee that halogen atom is fully combined into absorbable molecule.Meanwhile, by effective
Control realization burn automatization, reduce operation risk.Additionally, the present invention is by selecting the corundum of high alumina containing chromium resistance to high-temperature service
Fiery material, graphite material and passing ratio mend the means of air control HF concentration, increased the service life of equipment.
Description of the drawings
In order to be illustrated more clearly that the embodiment of the present invention or technical scheme of the prior art, below will be to embodiment or existing
Accompanying drawing to be used needed for having technology description is briefly described, it should be apparent that, drawings in the following description are only this
Some embodiments described in invention, for those of ordinary skill in the art, on the premise of not paying creative work,
Can be with according to these other accompanying drawings of accompanying drawings acquisition.
Fig. 1 is the floor map of fluorine-containing one specific embodiment of alkane burned waste gas processing meanss of the present invention.
Specific embodiment
The present invention is described in detail for shown each embodiment below in conjunction with the accompanying drawings, but it should explanation, these
Embodiment not limitation of the present invention, those of ordinary skill in the art according to these embodiment institute work energy, method,
Or the equivalent transformation or replacement in structure, belong within protection scope of the present invention.
The fluorine-containing alkane burned waste gas handling process of the present invention comprises the steps:
S1, the incinerator with refractory material is preheated, fluorine-containing alkane waste gas is passed through in the incinerator after preheating.
Wherein, during preheating, the incinerator is preheated to into more than 1100 DEG C by fuel, so as to for follow-up halothane hydrocarbon it is useless
Gas carries out pyrolysis and prepares.The refractory material is chromium oxide and aluminium sesquioxide, the chromium oxide and aluminium sesquioxide content
More than 95wt%, and the chromic oxide content >=10 wt %.So as to by using the incinerator with refractory material, Neng Gouke
To prevent high concentration HF etching apparatus, the service life of extension device.
S2, according to the molecule content of fluorine-containing alkane in waste gas, be passed through vapor in incinerator and reacted.
S3, it is passed through natural gas in incinerator, to control the furnace temperature of incinerator.
S4, the amount of filling into for by fluorine-containing alkane waste and natural gas total amount, controlling air in proportion.
Wherein, the purpose for controlling the amount of filling into of air in proportion is that it is same that control air meets burning Minimum requirements oxygen
In time control tobacco curing gas, HF concentration is not higher than 5%, it is ensured that burn stable, to realize that waste gas is fully pyrolyzed and improves service life of equipment
Purpose.Specifically, the amount of filling into of the control air is by being controlled as follows:By exhaust gas flow measured value and
Amount of natural gas measured value is calculated by molecular formula and determines ratio value, is added by both ratios and is determined the air amount of filling into, as benefit
The set-point of air frequency conversion fan, the effusion meter of airduct line as actual air volume measured value, by between measured value and set-point
Bias adjustment frequency conversion fan rotating speed, it is ensured that fill into air quantity infinite approach set-point.
S5, by after burning high-temperature flue gas send into graphite chilling tower, the hydride of halogen in the flue gas after chilling is carried out
Water absorption.
Wherein, the purpose for sending into graphite chilling tower is to prevent the generation of the harmful substances such as two English.
Based on fluorine-containing alkane burned waste gas handling process as above, the fluorine-containing alkane burned waste gas processing meanss bag
Include:Off-gas buffer tank 10, incinerator 20, frequency conversion mend blower fan 30 and graphite chilling tower(It is not shown).
Wherein, the off-gas buffer tank 10 is able to ensure that gas inlet is stable, and system fading margin is steady, without too great fluctuation process.It is no
Then, because system it is all be variable entirely, exhausted air quantity and amount of natural gas determine the air amount of filling into, and such as exhausted air quantity changes greatly, furnace temperature liquid
Position causes change, the also moment change of such amount of natural gas to fill into air capacity and very great fluctuation process also occurs.So as to be unfavorable for system
The stability that automatization is adjusted.
The off-gas buffer tank 10 is connected with the incinerator 20 by waste line 11, and it is logical that blower fan 30 is mended in the frequency conversion
Cross air line 31 to be connected with the incinerator 20, the graphite chilling tower passes through high-temperature flue gas pipeline 41 and the incinerator
20 are connected.Wherein, waste gas blow-down pipe 12 is also parallel with the waste line 11.As needed, the frequency conversion can be mended
Blower fan 30 is set to two groups, and now, two groups of frequency conversion benefit blower fans 30 are parallel with one another, and pass through respective air line 31 and institute respectively
State incinerator 20 to be connected.
Additionally, the incinerator 20 is also associated with burning line 51 and vapor pipeline 61.Specifically, the incinerator 20
Top be provided with burner, the burning line and vapor pipeline are connected with the burner.
In sum, fluorine-containing alkane burned waste gas handling process of the invention can be such that fluorine-containing alkane waste gas divides by burning
Solution, and guarantee that halogen atom is fully combined into absorbable molecule.Meanwhile, automatization, drop are burned by effective control realization
Low operation risk.Additionally, the present invention by high-temperature service select the corundum refractory of high alumina containing chromium, graphite material and by than
Example mends the means of air control HF concentration, increased the service life of equipment.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of spirit or essential attributes without departing substantially from the present invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit is required rather than described above is limited, it is intended that all in the implication and scope of the equivalency of claim by falling
Change is included in the present invention.Any reference in claim should not be considered as and limit involved claim.
Moreover, it will be appreciated that although this specification is been described by according to embodiment, not each embodiment is only wrapped
Containing an independent technical scheme, this narrating mode of description is only that those skilled in the art should for clarity
Using description as an entirety, the technical scheme in each embodiment can also Jing it is appropriately combined, form those skilled in the art
Understandable other embodiment.
Claims (10)
1. a kind of fluorine-containing alkane burned waste gas handling process, it is characterised in that the fluorine-containing alkane burned waste gas handling process bag
Include:
S1, the incinerator with refractory material is preheated, fluorine-containing alkane waste gas is passed through in the incinerator after preheating;
S2, according to the molecule content of fluorine-containing alkane in waste gas, be passed through vapor in incinerator and reacted;
S3, it is passed through natural gas in incinerator, to control the furnace temperature of incinerator;
S4, the amount of filling into for by fluorine-containing alkane waste and natural gas total amount, controlling air in proportion;
S5, by after burning high-temperature flue gas send into graphite chilling tower, the hydride of halogen in the flue gas after chilling is washed
Absorb.
2. fluorine-containing alkane burned waste gas handling process according to claim 1, it is characterised in that the preheating of the incinerator
Temperature is more than 1100 DEG C.
3. fluorine-containing alkane burned waste gas handling process according to claim 1, it is characterised in that the refractory material is oxygen
Change chromium and aluminium sesquioxide, the chromium oxide and aluminium sesquioxide content are more than 95wt%, and chromic oxide content >=10 wt
%。
4. fluorine-containing alkane burned waste gas handling process according to claim 1, it is characterised in that the amount of filling into of the air
Determined by the ratio value between the fluorine-containing alkane exhaust gas flow and amount of natural gas.
5. fluorine-containing alkane burned waste gas handling process according to claim 4, it is characterised in that the amount of filling into of the air
The setting value of blower fan is mended as frequency conversion, when filling into air, according to the setting value, to the air by mending the actual survey of distinguished and admirable gauge
Amount is revised.
6. fluorine-containing alkane burned waste gas handling process according to claim 1, it is characterised in that the high temperature after the burning
In flue gas, HF concentration is not higher than 5%.
7. a kind of fluorine-containing alkane burned waste gas processing meanss, it is characterised in that the fluorine-containing alkane burned waste gas processing meanss bag
Include:Blower fan and graphite chilling tower are mended in off-gas buffer tank, incinerator, frequency conversion;
The off-gas buffer tank is connected with the incinerator by waste line, the frequency conversion mend blower fan by air line with
The incinerator is connected, and the graphite chilling tower is connected with the incinerator by high-temperature flue gas pipeline, the incinerator
It is also associated with burning line and vapor pipeline.
8. fluorine-containing alkane burned waste gas processing meanss according to claim 1, it is characterised in that the top of the incinerator
Burner is provided with, the burning line and vapor pipeline are connected with the burner.
9. fluorine-containing alkane burned waste gas processing meanss according to claim 1, it is characterised in that on the waste line also
It is parallel with waste gas blow-down pipe.
10. fluorine-containing alkane burned waste gas processing meanss according to claim 1, it is characterised in that blower fan is mended in the frequency conversion
For two groups, two groups of frequency conversion benefit blower fans are parallel with one another, and are connected with the incinerator by respective air line respectively.
Priority Applications (1)
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CN201610929562.3A CN106524191A (en) | 2016-10-31 | 2016-10-31 | Fluorine-contained alkane waste gas incineration treatment process and device |
Applications Claiming Priority (1)
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CN201610929562.3A CN106524191A (en) | 2016-10-31 | 2016-10-31 | Fluorine-contained alkane waste gas incineration treatment process and device |
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Publication Number | Publication Date |
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CN106524191A true CN106524191A (en) | 2017-03-22 |
Family
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CN201610929562.3A Pending CN106524191A (en) | 2016-10-31 | 2016-10-31 | Fluorine-contained alkane waste gas incineration treatment process and device |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108815996A (en) * | 2018-07-02 | 2018-11-16 | 江苏三美化工有限公司 | A kind of hydrofluorocarbon exhaust treatment system and its application method |
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CN1924439A (en) * | 2006-09-26 | 2007-03-07 | 昆明理工大学 | Freon treated by premixed combustion and method for producing said resource |
CN102305411A (en) * | 2011-09-02 | 2012-01-04 | 北京航天动力研究所 | Method and system for carrying out incineration treatment on fluorine-containing organic waste liquor/waste gas |
CN102478245A (en) * | 2010-11-29 | 2012-05-30 | 屠国强 | Method for reducing greenhouse effect and treating F23 in difluoro-methane chloride production through environmentally-friendly burning |
CN103292332A (en) * | 2013-05-27 | 2013-09-11 | 北京航天动力研究所 | Negative-pressure incineration disposal system and negative-pressure incineration disposal method for fluorine-containing organic waste liquid and exhaust gas |
CN104501186A (en) * | 2014-12-16 | 2015-04-08 | 江苏百茂源环保科技有限公司 | Treating device and method of waste gas/liquid with high chlorine and fluorine content |
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WO2003047729A1 (en) * | 2001-12-04 | 2003-06-12 | Ebara Corporation | Method and apparatus for treating exhaust gas |
JP2003236337A (en) * | 2002-02-14 | 2003-08-26 | Showa Denko Kk | Method and apparatus for treating exhaust gas |
CN1924439A (en) * | 2006-09-26 | 2007-03-07 | 昆明理工大学 | Freon treated by premixed combustion and method for producing said resource |
CN102478245A (en) * | 2010-11-29 | 2012-05-30 | 屠国强 | Method for reducing greenhouse effect and treating F23 in difluoro-methane chloride production through environmentally-friendly burning |
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CN108815996A (en) * | 2018-07-02 | 2018-11-16 | 江苏三美化工有限公司 | A kind of hydrofluorocarbon exhaust treatment system and its application method |
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Application publication date: 20170322 |