CN106519808A - Environment-friendly thermal-sublimation coating material - Google Patents
Environment-friendly thermal-sublimation coating material Download PDFInfo
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- CN106519808A CN106519808A CN201610854458.2A CN201610854458A CN106519808A CN 106519808 A CN106519808 A CN 106519808A CN 201610854458 A CN201610854458 A CN 201610854458A CN 106519808 A CN106519808 A CN 106519808A
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D101/00—Coating compositions based on cellulose, modified cellulose, or cellulose derivatives
- C09D101/08—Cellulose derivatives
- C09D101/26—Cellulose ethers
- C09D101/28—Alkyl ethers
- C09D101/286—Alkyl ethers substituted with acid radicals
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses an environment-friendly thermal-sublimation coating material. The environment-friendly thermal-sublimation coating material comprises the following components in parts by weight: 20-40 parts of carboxymethylcellulose, 5-15 parts of starch, 10-18 parts of polyacrylamide, 10-20 parts of polysaccharides and polysaccharide derivatives, 15-25 parts of polycitric acid and polyethylene glycol-citric acid copolymer, 8-15 parts of silicon dioxide, 5-10 parts of barium sulphate, 5-10 parts of alumina, 4-12 parts of titanium dioxide, 5-12 parts of kaolin, 8-17 parts of calcium carbonate, 3-10 parts of bentonite powder and 1-4 parts of nano-silver ion powder. The environment-friendly thermal-sublimation coating material disclosed by the invention is simple in production process, and environment-friendly and pollution-free in preparation process; and the prepared coating material enables the various indexes of finished paper to meet the requirements of high-fidelity sublimation transfer printing, is bright in colour, excellent in colour fixation and high in transfer rate, and ensures the high definition and reality of the original colour pattern.
Description
Technical field
The present invention relates to coating material preparing technical field, specially a kind of environment-friendly type heat sublimation coating material.
Background technology
Thermal transfer is new method of the impressing pattern on various material commodity, is particularly suitable for making a small amount of various personalization
And the pattern of customization class commodity and printing comprising full color image or photo.Its principle be by numerical digit pattern transfers printer with
Special transfer ink watermark is on transfer dedicated paper, then with special transfer interpreter, pattern is accurately transferred to commodity HTHP
Surface, completes commodity printing；Can be in leather, textile cloth, lucite, metal, plastics, crystal, woodwork, copperplate paper
Deng in Arbitrary Relative plane material, disposable polychrome, arbitrarily complicated color, the digital printer of intermediate color printing is carried out, it is not required to
Make a plate, the hanger plate program of chromatography and complexity, will not to material cause damage, since launch, obtained every profession and trade people
The high evaluation of scholar, the factory client for carrying out secondary increasing purchase are increasing；Thermal-printing Technology it is also possible to use a variety of transfers
Material, reaches different printing effects, topmost to have glued membrane transfer and sublimation transfer.Existing thermal transfer heat sublimation coating
Material preparation process is complicated, and after thermal transfer, clear color degree is poor, transfers the visual effect of pattern, color on later stock gorgeous
Beautiful degree, the fidelity effect of image are all affected by types of coatings, performance.
The content of the invention
It is an object of the invention to provide a kind of environment-friendly type heat sublimation coating material, to solve to propose in above-mentioned background technology
Problem.
For achieving the above object, the present invention provides following technical scheme：A kind of environment-friendly type heat sublimation coating material, its component
It is derivative including carboxymethylcellulose calcium 20-40 parts, starch 5-15 parts, polyacrylamide 10-18 parts, polysaccharide and polysaccharide by weight
Thing 10-20 parts, poly- citric acid and polyethylene glycol-citric acid copolymer 1 5-25 parts, silica 8-15 parts, barium sulfate 5-10 parts,
Aluminum oxide 5-10 parts, titanium dioxide 4-12 parts, kaolin 5-12 parts, calcium carbonate 8-17 parts, bentonite powder 3-10 parts and receive
Nano silver ion powder 1-4 parts.
Preferably, the polysaccharide and polysaccharide derivates include polydextrose, glucan, Arabic gum, agar, glycogen, thoroughly
Bright matter acid, methylcellulose, sodium alginate, trehalose.
Preferably, preferred composition proportion is：30 parts of carboxymethylcellulose calcium, 10 parts of starch, 14 parts of polyacrylamide, polysaccharide
With 15 parts of polysaccharide derivates, poly- citric acid and polyethylene glycol -20 parts of lemon acid copolymer, 2 parts of silica 1,8 parts of barium sulfate,
3 parts of 8 parts of aluminum oxide, 8 parts of titanium dioxide, 9 parts of kaolin, 12 parts of calcium carbonate, 7 parts of bentonite powder and nano-silver ionic powder.
Preferably, its preparation method is comprised the following steps：
A, by carboxymethylcellulose calcium, starch, polyacrylamide, polysaccharide and polysaccharide derivates, poly- citric acid and polyethylene glycol-
Knead during kneading machine is added after lemon acid copolymer, silica mixing, kneading machine temperature is 75 DEG C -90 DEG C, mixing time is
30min-50min, obtains mixture A；
B, by mixture A be cooled to after normal temperature add mixer in, sequentially add barium sulfate, aluminum oxide, titanium dioxide afterwards
Titanium, kaolin, calcium carbonate, bentonite powder, carry out height speed stirring, first carry out stirring at low speed, carry out afterwards at a high speed after mixing
Stirring, obtains mixture B；
C, the last addition nano-silver ionic powder in mixture B, stand 3h at normal temperatures after stirring mixing, that is, obtain coating
Material.
Preferably, in step B, low speed speed is 300-500 rev/min, and mixing time is 10min-20min；Height hastens
Rate is 3000-4000 rev/min, and mixing time is 5min-15min.
Compared with prior art, the invention has the beneficial effects as follows：Manufacture craft of the present invention is simple, and preparation process environmental protection is without dirt
Dye, obtained coating material cause into the requirement that the indices of paper meet high-fidelity distillation bat printing, and bright in luster, fixation is excellent
The good, rate of transform is high, it is ensured that the fine definition and authenticity of original color pattern；In addition, being added with nano-silver ionic in the present invention
Powder, can extend the storage time of coating material.
Specific embodiment
Below the technical scheme in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment
Only a part of embodiment of the invention, rather than the embodiment of whole.Based on the embodiment in the present invention, the common skill in this area
The every other embodiment obtained under the premise of creative work is not made by art personnel, belongs to the model of present invention protection
Enclose.
The present invention provides a kind of technical scheme：A kind of environment-friendly type heat sublimation coating material, its component include by weight
Carboxymethylcellulose calcium 20-40 parts, starch 5-15 parts, polyacrylamide 10-18 parts, polysaccharide and polysaccharide derivates 10-20 parts, poly- lemon
Lemon acid and polyethylene glycol-citric acid copolymer 1 5-25 parts, silica 8-15 parts, barium sulfate 5-10 parts, aluminum oxide 5-10 parts,
Titanium dioxide 4-12 parts, kaolin 5-12 parts, calcium carbonate 8-17 parts, bentonite powder 3-10 parts and nano-silver ionic powder 1-4
Part；Wherein carboxymethylcellulose calcium rises and stops ink, absorption ink, makes ink form fine pattern, there is provided the heat sublimation rate of transform is made
With；Polysaccharide and polysaccharide derivates include polydextrose, glucan, Arabic gum, agar, glycogen, hyaluronic acid, Methyl cellulose
Element, sodium alginate, trehalose.
Embodiment one：
The composition proportion for adopting for：20 parts of carboxymethylcellulose calcium, 5 parts of starch, 10 parts of polyacrylamide, polysaccharide and polysaccharide spread out
Biological 10 parts, poly- citric acid and polyethylene glycol -5 parts of citric acid copolymer 1,8 parts of silica, 5 parts of barium sulfate, 5 parts of aluminum oxide,
1 part of 4 parts of titanium dioxide, 5 parts of kaolin, 8 parts of calcium carbonate, 3 parts of bentonite powder and nano-silver ionic powder.
The preparation method of the present embodiment is comprised the following steps：
A, by carboxymethylcellulose calcium, starch, polyacrylamide, polysaccharide and polysaccharide derivates, poly- citric acid and polyethylene glycol-
Knead during kneading machine is added after lemon acid copolymer, silica mixing, kneading machine temperature is 75 DEG C, and mixing time is 30min,
Obtain mixture A；
B, by mixture A be cooled to after normal temperature add mixer in, sequentially add barium sulfate, aluminum oxide, titanium dioxide afterwards
Titanium, kaolin, calcium carbonate, bentonite powder, carry out height speed stirring, first carry out stirring at low speed, carry out afterwards at a high speed after mixing
Stirring, obtains mixture B；
C, the last addition nano-silver ionic powder in mixture B, stand 3h at normal temperatures after stirring mixing, that is, obtain coating
Material.
In the present embodiment, in step B, low speed speed is 300 revs/min, and mixing time is 10min；High speed is 3000
Rev/min, mixing time is 5min.
Embodiment two：
The composition proportion for adopting for：40 parts of carboxymethylcellulose calcium, 15 parts of starch, 18 parts of polyacrylamide, polysaccharide and polysaccharide
20 parts of derivative, poly- citric acid and polyethylene glycol -25 parts of lemon acid copolymer, 5 parts of silica 1,10 parts of barium sulfate, aluminum oxide
4 parts of 10 parts, 12 parts of titanium dioxide, 12 parts of kaolin, 17 parts of calcium carbonate, 10 parts of bentonite powder and nano-silver ionic powder.
The preparation method of the present embodiment is comprised the following steps：
A, by carboxymethylcellulose calcium, starch, polyacrylamide, polysaccharide and polysaccharide derivates, poly- citric acid and polyethylene glycol-
Knead during kneading machine is added after lemon acid copolymer, silica mixing, kneading machine temperature is 90 DEG C, and mixing time is 50min,
Obtain mixture A；
B, by mixture A be cooled to after normal temperature add mixer in, sequentially add barium sulfate, aluminum oxide, titanium dioxide afterwards
Titanium, kaolin, calcium carbonate, bentonite powder, carry out height speed stirring, first carry out stirring at low speed, carry out afterwards at a high speed after mixing
Stirring, obtains mixture B；
C, the last addition nano-silver ionic powder in mixture B, stand 3h at normal temperatures after stirring mixing, that is, obtain coating
Material.
In the present embodiment, in step B, low speed speed is 500 revs/min, and mixing time is 20min；High speed is 4000
Rev/min, mixing time is 15min.
Embodiment three：
The composition proportion for adopting for：25 parts of carboxymethylcellulose calcium, 8 parts of starch, 11 parts of polyacrylamide, polysaccharide and polysaccharide spread out
Biological 12 parts, poly- citric acid and polyethylene glycol -7 parts of citric acid copolymer 1,9 parts of silica, 6 parts of barium sulfate, 6 parts of aluminum oxide,
2 parts of 6 parts of titanium dioxide, 6 parts of kaolin, 9 parts of calcium carbonate, 4 parts of bentonite powder and nano-silver ionic powder.
The preparation method of the present embodiment is comprised the following steps：
A, by carboxymethylcellulose calcium, starch, polyacrylamide, polysaccharide and polysaccharide derivates, poly- citric acid and polyethylene glycol-
Knead during kneading machine is added after lemon acid copolymer, silica mixing, kneading machine temperature is 80 DEG C, and mixing time is 35min,
Obtain mixture A；
B, by mixture A be cooled to after normal temperature add mixer in, sequentially add barium sulfate, aluminum oxide, titanium dioxide afterwards
Titanium, kaolin, calcium carbonate, bentonite powder, carry out height speed stirring, first carry out stirring at low speed, carry out afterwards at a high speed after mixing
Stirring, obtains mixture B；
C, the last addition nano-silver ionic powder in mixture B, stand 3h at normal temperatures after stirring mixing, that is, obtain coating
Material.
In the present embodiment, in step B, low speed speed is 350 revs/min, and mixing time is 12min；High speed is 3200
Rev/min, mixing time is 7min.
Example IV：
The composition proportion for adopting for：35 parts of carboxymethylcellulose calcium, 12 parts of starch, 15 parts of polyacrylamide, polysaccharide and polysaccharide
18 parts of derivative, poly- citric acid and polyethylene glycol -22 parts of lemon acid copolymer, 4 parts of silica 1,8 parts of barium sulfate, aluminum oxide 7
Part, 11 parts of titanium dioxide, 10 parts of kaolin, 15 parts of calcium carbonate, 8 parts of bentonite powder and 3 parts of nano-silver ionic powder.
The preparation method of the present embodiment is comprised the following steps：
A, by carboxymethylcellulose calcium, starch, polyacrylamide, polysaccharide and polysaccharide derivates, poly- citric acid and polyethylene glycol-
Knead during kneading machine is added after lemon acid copolymer, silica mixing, kneading machine temperature is 85 DEG C, and mixing time is 45min,
Obtain mixture A；
B, by mixture A be cooled to after normal temperature add mixer in, sequentially add barium sulfate, aluminum oxide, titanium dioxide afterwards
Titanium, kaolin, calcium carbonate, bentonite powder, carry out height speed stirring, first carry out stirring at low speed, carry out afterwards at a high speed after mixing
Stirring, obtains mixture B；
C, the last addition nano-silver ionic powder in mixture B, stand 3h at normal temperatures after stirring mixing, that is, obtain coating
Material.
In the present embodiment, in step B, low speed speed is 450 revs/min, and mixing time is 18min；High speed is 3800
Rev/min, mixing time is 13min.
Embodiment five：
The composition proportion for adopting for：30 parts of carboxymethylcellulose calcium, 10 parts of starch, 14 parts of polyacrylamide, polysaccharide and polysaccharide
15 parts of derivative, poly- citric acid and polyethylene glycol -20 parts of lemon acid copolymer, 2 parts of silica 1,8 parts of barium sulfate, aluminum oxide 8
Part, 8 parts of titanium dioxide, 9 parts of kaolin, 12 parts of calcium carbonate, 7 parts of bentonite powder and 3 parts of nano-silver ionic powder.
The preparation method of the present embodiment is comprised the following steps：
A, by carboxymethylcellulose calcium, starch, polyacrylamide, polysaccharide and polysaccharide derivates, poly- citric acid and polyethylene glycol-
Knead during kneading machine is added after lemon acid copolymer, silica mixing, kneading machine temperature is 80 DEG C, and mixing time is 40min,
Obtain mixture A；
B, by mixture A be cooled to after normal temperature add mixer in, sequentially add barium sulfate, aluminum oxide, titanium dioxide afterwards
Titanium, kaolin, calcium carbonate, bentonite powder, carry out height speed stirring, first carry out stirring at low speed, carry out afterwards at a high speed after mixing
Stirring, obtains mixture B；
C, the last addition nano-silver ionic powder in mixture B, stand 3h at normal temperatures after stirring mixing, that is, obtain coating
Material.
In the present embodiment, in step B, low speed speed is 400 revs/min, and mixing time is 15min；High speed is 3500
Rev/min, mixing time is 10min.
Experimental example：
Common coating material and various embodiments of the present invention are obtained after coating material is coated transfer on photo to be carried out
Adhesion property and senile experiment, obtain data such as following table：
Manufacture craft of the present invention is simple, and preparation process is environment friendly and pollution-free, and obtained coating material causes into the items of paper and refers to
Mark meets the requirement of high-fidelity distillation bat printing, and bright in luster, fixation is excellent, the rate of transform is high, it is ensured that the high definition of original color pattern
Clear degree and authenticity；In addition, being added with nano-silver ionic powder in the present invention, the storage time of coating material can be extended.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding can carry out various changes, modification, replacement to these embodiments without departing from the principles and spirit of the present invention
And modification, the scope of the present invention be defined by the appended.
Claims (5)
1. a kind of environment-friendly type heat sublimation coating material, it is characterised in that：Its component includes carboxymethylcellulose calcium 20- by weight
40 parts, starch 5-15 parts, polyacrylamide 10-18 parts, polysaccharide and polysaccharide derivates 10-20 parts, poly- citric acid and polyethylene glycol-
Citric acid copolymer 1 5-25 parts, silica 8-15 parts, barium sulfate 5-10 parts, aluminum oxide 5-10 parts, titanium dioxide 4-12 parts,
Kaolin 5-12 parts, calcium carbonate 8-17 parts, bentonite powder 3-10 parts and nano-silver ionic powder 1-4 parts.
2. a kind of environment-friendly type heat sublimation coating material according to claim 1, it is characterised in that：The polysaccharide and polysaccharide spread out
It is biological to include polydextrose, glucan, Arabic gum, agar, glycogen, hyaluronic acid, methylcellulose, sodium alginate, marine alga
Sugar.
3. a kind of environment-friendly type heat sublimation coating material according to claim 1, it is characterised in that：Preferred composition proportion
For：15 parts of 30 parts of carboxymethylcellulose calcium, 10 parts of starch, 14 parts of polyacrylamide, polysaccharide and polysaccharide derivates, poly- citric acid and poly-
Ethylene glycol -20 parts of lemon acid copolymer, 2 parts of silica 1,8 parts of barium sulfate, 8 parts of aluminum oxide, 8 parts of titanium dioxide, kaolin 9
Part, 12 parts of calcium carbonate, 7 parts of bentonite powder and 3 parts of nano-silver ionic powder.
4. a kind of preparation method of the environment-friendly type heat sublimation coating material described in claim 1 is realized, it is characterised in that：Its preparation
Method is comprised the following steps：
A, by carboxymethylcellulose calcium, starch, polyacrylamide, polysaccharide and polysaccharide derivates, poly- citric acid and polyethylene glycol-lemon
Knead during kneading machine is added after acid copolymer, silica mixing, kneading machine temperature is 75 DEG C -90 DEG C, mixing time is
30min-50min, obtains mixture A；
B, by mixture A be cooled to after normal temperature add mixer in, sequentially add barium sulfate, aluminum oxide, titanium dioxide, height afterwards
Ridge soil, calcium carbonate, bentonite powder, carry out height speed stirring, first carry out stirring at low speed, carry out high-speed stirred afterwards after mixing,
Obtain mixture B；
C, the last addition nano-silver ionic powder in mixture B, stand 3h at normal temperatures after stirring mixing, that is, obtain coating material
Material.
5. the preparation method of a kind of environment-friendly type heat sublimation coating material according to claim 4, it is characterised in that：The step
In rapid B, low speed speed is 300-500 rev/min, and mixing time is 10min-20min；High speed is 3000-4000 rev/min, is stirred
The time is mixed for 5min-15min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610854458.2A CN106519808A (en) | 2016-09-27 | 2016-09-27 | Environment-friendly thermal-sublimation coating material |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610854458.2A CN106519808A (en) | 2016-09-27 | 2016-09-27 | Environment-friendly thermal-sublimation coating material |
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| CN106519808A true CN106519808A (en) | 2017-03-22 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610854458.2A Pending CN106519808A (en) | 2016-09-27 | 2016-09-27 | Environment-friendly thermal-sublimation coating material |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108978342A (en) * | 2018-08-09 | 2018-12-11 | 中国制浆造纸研究院衢州分院 | A kind of preparation method for thermal dye sublimation transfer printing paper surface coating |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108978342A (en) * | 2018-08-09 | 2018-12-11 | 中国制浆造纸研究院衢州分院 | A kind of preparation method for thermal dye sublimation transfer printing paper surface coating |
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