CN106515055A - Preparation method of inflation pool with permanent antibacterial function - Google Patents
Preparation method of inflation pool with permanent antibacterial function Download PDFInfo
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- CN106515055A CN106515055A CN201610941580.3A CN201610941580A CN106515055A CN 106515055 A CN106515055 A CN 106515055A CN 201610941580 A CN201610941580 A CN 201610941580A CN 106515055 A CN106515055 A CN 106515055A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29D—PRODUCING PARTICULAR ARTICLES FROM PLASTICS OR FROM SUBSTANCES IN A PLASTIC STATE
- B29D22/00—Producing hollow articles
- B29D22/02—Inflatable articles
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29D—PRODUCING PARTICULAR ARTICLES FROM PLASTICS OR FROM SUBSTANCES IN A PLASTIC STATE
- B29D24/00—Producing articles with hollow walls
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K13/00—Use of mixtures of ingredients not covered by one single of the preceding main groups, each of these compounds being essential
- C08K13/04—Ingredients characterised by their shape and organic or inorganic ingredients
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/08—Metals
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K7/00—Use of ingredients characterised by shape
- C08K7/22—Expanded, porous or hollow particles
- C08K7/24—Expanded, porous or hollow particles inorganic
- C08K7/26—Silicon- containing compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/08—Metals
- C08K2003/0806—Silver
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2203/00—Applications
- C08L2203/16—Applications used for films
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Greenhouses (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
Abstract
The invention provides a preparation method of an inflation pool with a permanent antibacterial function. A process of bonding a double-layer PVC material on warp-knitted and weft-inserted cloth is adopted; the inner layer of PVC material mainly achieves the waterproof effect; the outer layer of PVC material mainly achieves the antibacterial effect; the warp-knitted and weft-inserted cloth achieves the support effect; marbles are added; a natural replacement mode is used for using all antibacterial agent in the whole outer layer of PVC material to not only achieve the surface antibacterial effect; expanded vermiculite powder is added to achieve the following main effects: (1) a certain absorbing effect is achieved on a nanosilver antibacterial agent to prevent quicker loss of nanosilver under acid conditions; and (2) a certain absorbing and treating effect is achieved on other impurities in water, in particular heavy metals. The preparation method of the inflation pool with the permanent antibacterial function achieves natural and permanent antibacterial effect of the antibacterial agent through adding nanosilver, marble leftovers and expanded vermiculite powder in traditional PVC films.
Description
Technical field
The present invention relates to stationery sports goods Material Field, more particularly to a kind of Inflation water pond with long-term antibacterial function
Preparation method.
Background technology
There are 400 insufficient waters, 110 serious water shortages in 669 cities in the whole nation at present;More than 32 a population of one million
In megalopolis, there are 30 to be perplexed by hydropenia for a long time.In 46 key cities, 45.6% water quality is poor, 14 coastal opening cities
There are 9 serious water shortages in city.Solve the problems, such as that the amusement and leisure of citizen's summer just highlight the cities such as Beijing, Tianjin, Qingdao, Dalian
City's hydropenia is the most serious.As global warming, the extreme weather that summer breaks through 40 DEG C are more and more, various places issue height again and again
Warm early warning, developing rapidly now with urban construction, land price are grown to even greater heights, and are available for the place that citizen's rest is played increasingly
It is few.It is higher for seasonal recreation ground requirement condition, routinely build a natatorium and must invest more than millions of, build a trip
Theme park based on swimming is made an investment in more than up to ten million, and faces season operation in a hurry, the embarrassment that three seasons safeguarded.
The appearance in mobile aeration pond, solves the problems referred to above, and an Inflation water pond only needs to thousand of yuan and can just solve
The demand that certainly people play with water summer, is particularly these Inflation water ponds, can add cartoon elements, with the shape in animation water world paradise
Formula occurs.
After long-term preservation, Inflation water pond it may happen that bacteria breed, it is mouldy situations such as.Therefore it is necessary that research one kind can
To reach the Inflation water pond of long-term antibacterial effect, so as to ensure the health of user.
The content of the invention
In view of this, it is an object of the invention to provide a kind of preparation method of the Inflation water pond with long-term antibacterial function.
A kind of preparation method of the Inflation water pond with long-term antibacterial function, is carried out as steps described below:
Step one:The preparation of internal layer PVC film
A, material is weighed according to formula, be gradually added the thing for weighing in high-speed mixer in the case of low-speed running
Material, then operate under high speed 300-350s, and low speed is 60-100rpm, is 1000-1400rpm at a high speed, and temperature rises to 150-160
DEG C, cold mixing 3-5min in cold mixing machine is discharged to automatically, natural temperature cooling then passes to middle bucket mix homogeneously;
B, by the material for mixing incoming planetary extruder, setting is extruded as 130-140 DEG C, then flows into and rolls in turbine
Filter filtration is delivered to after gel;
C, by the colloidal objects for having filtered using six roll calendar of inverted L shape roll;
Step 2:The preparation of outer layer PVC film
A, material is weighed according to formula, be gradually added the thing for weighing in high-speed mixer in the case of low-speed running
Material, then operate under high speed 300-350s, and low speed is 60-100rpm, is 1000-1400rpm at a high speed, and temperature rises to 100-130
DEG C, cold mixing 12-15min in cold mixing machine is discharged to automatically, natural temperature cooling then passes to middle bucket mix homogeneously;
B, by the material for mixing incoming planetary extruder, setting is extruded as 130-140 DEG C, then flows into and rolls in turbine
Filter filtration is delivered to after gel;
C, by the colloidal objects for having filtered using six roll calendar of inverted L shape roll;
Step 3:The preparation of Inflation water pond
A, the internal layer after warp knit inlaid thread cloth both sides fit calendering respectively and outer layer PVC film, obtain composite;
B, composite is cooled down and oil removing through tank;
C, composite is made by Inflation water pond using conventional method.
Preferably, described internal layer PVC film, including the main component of following percentage by weight:
Polyvinyl chloride resin 65-75%
Heat stabilizer 2-5%
Anti- precipitation agent 1-2%
Colorant 2-5%
Plasticizer surplus.
Preferably, described outer layer PVC film, including the main component of following percentage by weight:
Polyvinyl chloride resin 60-70%
Heat stabilizer 2-5%
Anti- precipitation agent 1-2%
Colorant 2-5%
Dispersant 0.3-0.5%
Marble leftover pieces 1-2%
Nano silver antimicrobials 0.02-0.05%
Expanded vermiculite powder 2-4%
Plasticizer surplus.
Preferably, in described outer layer PVC film preparation process, nano silver antimicrobials are added into marble leftover pieces first, altogether
After grinding, add expanded vermiculite powder and dispersant is ground altogether, other raw material stirring are added after being uniformly dispersed uniform.
A kind of preparation method of Inflation water pond with long-term antibacterial function provided by the present invention, has the advantage that:
1st, using the technique of double-deck PVC material laminating warp knit inlaid thread cloth, internal layer PVC material primarily serves waterproof action, and
Outer layer PVC material primarily serves antibacterial action, and warp knit inlaid thread cloth is played a supporting role.
2nd, after being ground nanometer silver and marble leftover pieces altogether, then ground with expanded vermiculite powder and dispersant altogether, it is ensured that receive
The dispersion effect of meter Yin, and marmorean main component is Calcium Carbonate, stably can be preserved in the water of neutral and alkalescence, but
Can be reacted generation carbon dioxide and water in acid condition, so as to the nanometer silver stream for causing to be attached on marble material
Lose;After adding marble mainly to prevent the antibacterial long-time on top layer in the present invention, antibacterial effect is significantly reduced, with it is this from
Antibacterial in whole PVC cladding materials all can be used by the mode for so substituting, and be merely not only that antibacterial surface is made
With;Expanded vermiculite powder Main Function is added to have:One is have certain adsorption to nano silver antimicrobials, is prevented in acid condition
Under, nanometer silver loss is too fast, and two is have certain adsorption treatment effect to other impurity in water, especially heavy metal.
3rd, the preparation method of the Inflation water pond with long-term antibacterial function of the invention, by adding in traditional PVC film
Enter nanometer silver, marble leftover pieces and expanded vermiculite powder, reach the effect of antibacterial nature long-term antibacterial.
Specific embodiment
Embodiment 1
A kind of preparation method of the Inflation water pond with long-term antibacterial function, is carried out as steps described below:
Step one:The preparation of internal layer PVC film
A, material is weighed according to formula, be gradually added the thing for weighing in high-speed mixer in the case of low-speed running
Material, then operate under high speed 320s, and low speed is 85rpm, is 1200rpm at a high speed, and temperature rises to 155 DEG C, is discharged to automatically cold mixing machine
Middle cold mixing 4min, natural temperature cooling, then passes to middle bucket mix homogeneously;
B, by the material for mixing incoming planetary extruder, setting is extruded as 135 DEG C, then flows into and rolls gel in turbine
After deliver to filter filtration;
C, by the colloidal objects for having filtered using six roll calendar of inverted L shape roll;
Step 2:The preparation of outer layer PVC film
A, material is weighed according to formula, be gradually added the thing for weighing in high-speed mixer in the case of low-speed running
Material, then operate under high speed 320s, and low speed is 80rpm, is 1150rpm at a high speed, and temperature rises to 120 DEG C, is discharged to automatically cold mixing machine
Middle cold mixing 12min, natural temperature cooling, then passes to middle bucket mix homogeneously;
B, by the material for mixing incoming planetary extruder, setting is extruded as 135 DEG C, then flows into and rolls gel in turbine
After deliver to filter filtration;
C, by the colloidal objects for having filtered using six roll calendar of inverted L shape roll;
Step 3:The preparation of Inflation water pond
A, the internal layer after warp knit inlaid thread cloth both sides fit calendering respectively and outer layer PVC film, obtain composite;
B, composite is cooled down and oil removing through tank;
C, composite is made by Inflation water pond using conventional method.
Described internal layer PVC film, including the main component of following percentage by weight:
Polyvinyl chloride resin 70%
Heat stabilizer 3%
Anti- precipitation agent 1.5%
Colorant 2.5%
Plasticizer surplus.
Described outer layer PVC film, including the main component of following percentage by weight:
Polyvinyl chloride resin 65%
Heat stabilizer 2.5%
Anti- precipitation agent 1.5%
Colorant 3%
Dispersant 0.4%
Marble leftover pieces 1.5%
Nano silver antimicrobials 0.03%
Expanded vermiculite powder 3%
Plasticizer surplus.
In described outer layer PVC film preparation process, nano silver antimicrobials are added into marble leftover pieces, co-ground first
Afterwards, add expanded vermiculite powder and dispersant is ground altogether, other raw material stirring are added after being uniformly dispersed uniform.
Embodiment 2
A kind of preparation method of the Inflation water pond with long-term antibacterial function, is carried out as steps described below:
Step one:The preparation of internal layer PVC film
A, material is weighed according to formula, be gradually added the thing for weighing in high-speed mixer in the case of low-speed running
Material, then operate under high speed 300s, and low speed is 100rpm, is 1000rpm at a high speed, and temperature rises to 160 DEG C, is discharged to automatically cold mixing machine
Middle cold mixing 3min, natural temperature cooling, then passes to middle bucket mix homogeneously;
B, by the material for mixing incoming planetary extruder, setting is extruded as 140 DEG C, then flows into and rolls gel in turbine
After deliver to filter filtration;
C, by the colloidal objects for having filtered using six roll calendar of inverted L shape roll;
Step 2:The preparation of outer layer PVC film
A, material is weighed according to formula, be gradually added the thing for weighing in high-speed mixer in the case of low-speed running
Material, then operate under high speed 300s, and low speed is 100rpm, is 1000rpm at a high speed, and temperature rises to 130 DEG C, is discharged to automatically cold mixing machine
Middle cold mixing 12min, natural temperature cooling, then passes to middle bucket mix homogeneously;
B, by the material for mixing incoming planetary extruder, setting is extruded as 140 DEG C, then flows into and rolls gel in turbine
After deliver to filter filtration;
C, by the colloidal objects for having filtered using six roll calendar of inverted L shape roll;
Step 3:The preparation of Inflation water pond
A, the internal layer after warp knit inlaid thread cloth both sides fit calendering respectively and outer layer PVC film, obtain composite;
B, composite is cooled down and oil removing through tank;
C, composite is made by Inflation water pond using conventional method.
Described internal layer PVC film, including the main component of following percentage by weight:
Polyvinyl chloride resin 65%
Heat stabilizer 5%
Anti- precipitation agent 1%
Colorant 5%
Plasticizer surplus.
Described outer layer PVC film, including the main component of following percentage by weight:
Polyvinyl chloride resin 60%
Heat stabilizer 5%
Anti- precipitation agent 1%
Colorant 5%
Dispersant 0.3%
Marble leftover pieces 2%
Nano silver antimicrobials 0.02%
Expanded vermiculite powder 4%
Plasticizer surplus.
In described outer layer PVC film preparation process, nano silver antimicrobials are added into marble leftover pieces, co-ground first
Afterwards, add expanded vermiculite powder and dispersant is ground altogether, other raw material stirring are added after being uniformly dispersed uniform.
Embodiment 3
A kind of preparation method of the Inflation water pond with long-term antibacterial function, is carried out as steps described below:
Step one:The preparation of internal layer PVC film
A, material is weighed according to formula, be gradually added the thing for weighing in high-speed mixer in the case of low-speed running
Material, then operate under high speed 350s, and low speed is 60rpm, is 1400rpm at a high speed, and temperature rises to 150 DEG C, is discharged to automatically cold mixing machine
Middle cold mixing 5min, natural temperature cooling, then passes to middle bucket mix homogeneously;
B, by the material for mixing incoming planetary extruder, setting is extruded as 130-140 DEG C, then flows into and rolls in turbine
Filter filtration is delivered to after gel;
C, by the colloidal objects for having filtered using six roll calendar of inverted L shape roll;
Step 2:The preparation of outer layer PVC film
A, material is weighed according to formula, be gradually added the thing for weighing in high-speed mixer in the case of low-speed running
Material, then operate under high speed 350s, and low speed is 60rpm, is 1400rpm at a high speed, and temperature rises to 100 DEG C, is discharged to automatically cold mixing machine
Middle cold mixing 15min, natural temperature cooling, then passes to middle bucket mix homogeneously;
B, by the material for mixing incoming planetary extruder, setting is extruded as 130 DEG C, then flows into and rolls gel in turbine
After deliver to filter filtration;
C, by the colloidal objects for having filtered using six roll calendar of inverted L shape roll;
Step 3:The preparation of Inflation water pond
A, the internal layer after warp knit inlaid thread cloth both sides fit calendering respectively and outer layer PVC film, obtain composite;
B, composite is cooled down and oil removing through tank;
C, composite is made by Inflation water pond using conventional method.
Described internal layer PVC film, including the main component of following percentage by weight:
Polyvinyl chloride resin 75%
Heat stabilizer 2%
Anti- precipitation agent 2%
Colorant 2%
Plasticizer surplus.
Described outer layer PVC film, including the main component of following percentage by weight:
Polyvinyl chloride resin 70%
Heat stabilizer 2%
Anti- precipitation agent 2%
Colorant 2%
Dispersant 0.5%
Marble leftover pieces 1%
Nano silver antimicrobials 0.05%
Expanded vermiculite powder 2%
Plasticizer surplus.
In described outer layer PVC film preparation process, nano silver antimicrobials are added into marble leftover pieces, co-ground first
Afterwards, add expanded vermiculite powder and dispersant is ground altogether, other raw material stirring are added after being uniformly dispersed uniform.
Comparative example 1
Marble leftover pieces in outer layer PVC film in embodiment 1 are removed, remaining preparation condition is constant.
Comparative example 2
Expanded vermiculite powder in outer layer PVC film in embodiment 1 is removed, remaining preparation condition is constant.
Inflation water pond prepared by embodiment of the present invention 1-3 and comparative example 1 and 2 is resisted after using 3 years
Bacterium, bacteriostasis property detection, obtain following data:
Bacteriostasis rate % | Staphylococcus aureuses | Candida albicans | Escherichia coli |
Embodiment 1 | 97 | 98 | 98 |
Embodiment 2 | 98 | 97 | 97 |
Embodiment 3 | 97 | 98 | 98 |
Comparative example 1 | 0 | 0 | 0 |
Comparative example 2 | 0 | 0 | 0 |
The above, the only present invention preferably specific embodiment, but protection scope of the present invention is not limited thereto,
Any those familiar with the art the invention discloses technical scope in, technology according to the present invention scheme and its
Inventive concept equivalent or change in addition, should all be included within the scope of the present invention.
Claims (4)
1. a kind of preparation method of the Inflation water pond with long-term antibacterial function, it is characterised in that carry out as steps described below:
Step one:The preparation of internal layer PVC film
A, material is weighed according to formula, be gradually added the material for weighing, so in high-speed mixer in the case of low-speed running
Operate under high speed 300-350s afterwards, and low speed is 60-100rpm, is 1000-1400rpm at a high speed, and temperature rises to 150-160 DEG C, from
Dynamic to be discharged to cold mixing 3-5min in cold mixing machine, natural temperature cooling then passes to middle bucket mix homogeneously;
B, by the material for mixing incoming planetary extruder, setting is extruded as 130-140 DEG C, then flows into and rolls gel in turbine
After deliver to filter filtration;
C, by the colloidal objects for having filtered using six roll calendar of inverted L shape roll;
Step 2:The preparation of outer layer PVC film
A, material is weighed according to formula, be gradually added the material for weighing, so in high-speed mixer in the case of low-speed running
Operate under high speed 300-350s afterwards, and low speed is 60-100rpm, is 1000-1400rpm at a high speed, and temperature rises to 100-130 DEG C, from
Dynamic to be discharged to cold mixing 12-15min in cold mixing machine, natural temperature cooling then passes to middle bucket mix homogeneously;
B, by the material for mixing incoming planetary extruder, setting is extruded as 130-140 DEG C, then flows into and rolls gel in turbine
After deliver to filter filtration;
C, by the colloidal objects for having filtered using six roll calendar of inverted L shape roll;
Step 3:The preparation of Inflation water pond
A, the internal layer after warp knit inlaid thread cloth both sides fit calendering respectively and outer layer PVC film, obtain composite;
B, composite is cooled down and oil removing through tank;
C, composite is made by Inflation water pond using conventional method.
2. there is the preparation method of the Inflation water pond of long-term antibacterial function as claimed in claim 1, it is characterised in that described
Internal layer PVC film, including the main component of following percentage by weight:
Polyvinyl chloride resin 65-75%
Heat stabilizer 2-5%
Anti- precipitation agent 1-2%
Colorant 2-5%
Plasticizer surplus.
3. there is the preparation method of the Inflation water pond of long-term antibacterial function as claimed in claim 1, it is characterised in that described
Outer layer PVC film, including the main component of following percentage by weight:
Polyvinyl chloride resin 60-70%
Heat stabilizer 2-5%
Anti- precipitation agent 1-2%
Colorant 2-5%
Dispersant 0.3-0.5%
Marble leftover pieces 1-2%
Nano silver antimicrobials 0.02-0.05%
Expanded vermiculite powder 2-4%
Plasticizer surplus.
4. there is the preparation method of the Inflation water pond of long-term antibacterial function as claimed in claim 1, it is characterised in that described
In outer layer PVC film preparation process, nano silver antimicrobials are added into marble leftover pieces first, after co-ground, add expansion trematodiasiss
Stone powder and dispersant are ground altogether, add other raw material stirring uniform after being uniformly dispersed.
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Cited By (3)
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CN106905613A (en) * | 2017-04-01 | 2017-06-30 | 浙江亚德复合材料有限公司 | A kind of ageing-resistant antibacterial drinking water tubing and preparation method thereof |
CN106928549A (en) * | 2017-04-01 | 2017-07-07 | 浙江亚德复合材料有限公司 | A kind of ageing-resistant drinking water tubing and preparation method thereof |
CN107011578A (en) * | 2017-04-01 | 2017-08-04 | 浙江亚德复合材料有限公司 | It is a kind of that there is ageing-resistant drinking water tubing of dechlorination effect and preparation method thereof |
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CN106905613A (en) * | 2017-04-01 | 2017-06-30 | 浙江亚德复合材料有限公司 | A kind of ageing-resistant antibacterial drinking water tubing and preparation method thereof |
CN106928549A (en) * | 2017-04-01 | 2017-07-07 | 浙江亚德复合材料有限公司 | A kind of ageing-resistant drinking water tubing and preparation method thereof |
CN107011578A (en) * | 2017-04-01 | 2017-08-04 | 浙江亚德复合材料有限公司 | It is a kind of that there is ageing-resistant drinking water tubing of dechlorination effect and preparation method thereof |
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