CN106501441A - A kind of test kit for detecting Detection of Magdala in Food Through - Google Patents
A kind of test kit for detecting Detection of Magdala in Food Through Download PDFInfo
- Publication number
- CN106501441A CN106501441A CN201611132481.7A CN201611132481A CN106501441A CN 106501441 A CN106501441 A CN 106501441A CN 201611132481 A CN201611132481 A CN 201611132481A CN 106501441 A CN106501441 A CN 106501441A
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- CN
- China
- Prior art keywords
- test kit
- sealed bottle
- food
- magdala
- box body
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/90—Plate chromatography, e.g. thin layer or paper chromatography
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- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analysing Biological Materials (AREA)
Abstract
The invention discloses a kind of test kit for detecting Detection of Magdala in Food Through, the test kit includes box body and lid, the capillary tube that can be placed in box body and tlc silica gel plate, the sealed bottle also equipped with normal hexane, the sealed bottle equipped with ethyl acetate and the Reagent Tube equipped with tonyred standard sample.The reagent cartridge configuration of the present invention is simple, reasonable in design, is convenient for carrying, preserves, not vulnerable to pollution.When being detected using the present invention, program is simple, reduces the work difficulty of detection.
Description
Technical field
The present invention relates to technical field of food detection, more particularly to a kind of test kit for detecting Detection of Magdala in Food Through.
Background technology
Tonyred is a kind of azo stain of synthetic, is three class carcinogen, and its metabolite belongs to two classes
Carcinogen, it is impossible to add for food, but as which is bright-colored, Color is good, low cost, by some illegal businessmans
It is used as food additive.Detection to Detection of Magdala in Food Through is mainly in the indoor high performance liquid chromatography of experiment, mass spectrum at present
Detected etc. method, but complex operation, time-consuming.
Content of the invention
It is an object of the invention to provide a kind of test kit for detecting Aluminum Content in Food, for achieving the above object,
The concrete scheme of the present invention is as follows：
A kind of test kit for detecting Detection of Magdala in Food Through, the test kit include box body (1) and lid (2), can put
The capillary tube (3) that inserts in box body and tlc silica gel plate (4), are also equipped with the sealed bottle (5) of normal hexane, acetic acid second are housed
The sealed bottle (6) of ester and the Reagent Tube (7) equipped with tonyred standard sample.
Wherein, analytically pure normal hexane is housed in sealed bottle (5).
Wherein, analytically pure ethyl acetate is housed in sealed bottle (6).
Wherein, the quantity of capillary tube (3) is at least 2.
Compared with prior art, the present invention has the advantages that：
The reagent cartridge configuration of the present invention is simple, reasonable in design, is convenient for carrying, preserves, not vulnerable to pollution.Using the present invention
When being detected, program is simple, reduces the work difficulty of detection.
Description of the drawings
Fig. 1 is the structural representation of the present invention.
In figure, the sealed bottle of 1- box bodys, 2- lids, 3- capillary tubies, 4- tlc silica gel plates, 5- equipped with normal hexane, 6-
Reagent Tube of the sealed bottle, 7- equipped with ethyl acetate equipped with tonyred standard sample.
Specific embodiment
Below in conjunction with the accompanying drawings, the specific embodiment of the present invention is described in detail, it is to be understood that the guarantor of the present invention
Shield scope is not limited by specific embodiment.
Experimental technique used in following embodiments if no special instructions, is conventional method.
In following embodiments, material used, reagent etc., if no special instructions, commercially obtain.
As described in Figure 1, the invention provides a kind of test kit for detecting Detection of Magdala in Food Through, the test kit includes
Box body 1 and lid 2, the capillary tube 3 that can be placed in box body and tlc silica gel plate 4, the also sealed bottle equipped with normal hexane
5th, the sealed bottle 6 and the Reagent Tube 7 equipped with tonyred standard sample equipped with ethyl acetate.
Wherein, analytically pure normal hexane is housed in the sealed bottle 5.
Wherein, analytically pure ethyl acetate is housed in the sealed bottle 6.
Wherein, the quantity of the capillary tube 3 is 2.
Detecting step is as follows：
(1) about 1g samples are taken in test tube, adds 3ml normal hexane, fully shaking 5min to stand 10min, obtain sample and carry
Take liquid；
(2) chromatoplate is taken, and one horizontal line is gently being drawn with pencil away from the 1cm of bottom, as reference；
(3) no longer risen to liquid level in capillary tube with capillary tube pipette samples extracting solution, in the same of chromatoplate parallel lines
Site carries out point sample, and each point sample to sample in pipe is put doing completely, in triplicate.During point sample, tonyred standard is also taken
Sample carries out point sample, used as control.
(4) by normal hexane and ethyl acetate according to volume ratio 98:2 are configured to developing solvent, and 10ml developing solvents are added 150ml
In beaker, chromatoplate sample end is inserted in developing solvent down, upper end is leaned against on wall of cup, seal up beaker mouth, sample will be with exhibition
Open agent slowly to launch upwards, to be deployed is observable result to the 2/3 of chromatoplate.
Aforementioned to the present invention specific illustrative embodiment description illustrate that and illustration purpose.These descriptions
It is not wishing to limit the invention to disclosed precise forms, and it will be apparent that according to above-mentioned teaching, much can be changed
And change.The purpose of selecting and describing the exemplary embodiment is that explaining that the certain principles and its reality of the present invention should
With so that those skilled in the art can realize and using the present invention a variety of exemplaries and
A variety of selections and change.The scope of the present invention is intended to be limited by claims and its equivalents.
Claims (4)
1. a kind of test kit for detecting Detection of Magdala in Food Through, it is characterised in that：The test kit includes box body (1) and box
Lid (2), the capillary tube (3) that can be placed in box body and tlc silica gel plate (4), be also equipped with normal hexane sealed bottle (5),
Sealed bottle (6) and the Reagent Tube (7) equipped with tonyred standard sample equipped with ethyl acetate.
2. according to the test kit described in claim 1, it is characterised in that：Analytically pure normal hexane is housed in sealed bottle (5).
3. according to the test kit described in claim 1, it is characterised in that：Analytically pure acetic acid is housed in sealed bottle (6)
Ethyl ester.
4. according to the test kit described in claim 1, it is characterised in that：The quantity of capillary tube (3) is at least 2.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611132481.7A CN106501441A (en) | 2016-12-09 | 2016-12-09 | A kind of test kit for detecting Detection of Magdala in Food Through |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611132481.7A CN106501441A (en) | 2016-12-09 | 2016-12-09 | A kind of test kit for detecting Detection of Magdala in Food Through |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106501441A true CN106501441A (en) | 2017-03-15 |
Family
ID=58329694
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611132481.7A Pending CN106501441A (en) | 2016-12-09 | 2016-12-09 | A kind of test kit for detecting Detection of Magdala in Food Through |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106501441A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101067620A (en) * | 2007-06-08 | 2007-11-07 | 重庆市计量质量检测研究院 | Fast screening reagent kit and method for sudan dye in hot pepper products |
| US20120156794A1 (en) * | 2008-03-19 | 2012-06-21 | Florian Schweigert | Method for the extraction and detection of fat-soluble components from biological materials |
| CN103645177A (en) * | 2013-12-23 | 2014-03-19 | 武汉大学 | Method for improving Sudan red I detection kit |
| CN104101661A (en) * | 2014-07-03 | 2014-10-15 | 广西大学 | Quick detecting method for sudan red in food |
-
2016
- 2016-12-09 CN CN201611132481.7A patent/CN106501441A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101067620A (en) * | 2007-06-08 | 2007-11-07 | 重庆市计量质量检测研究院 | Fast screening reagent kit and method for sudan dye in hot pepper products |
| US20120156794A1 (en) * | 2008-03-19 | 2012-06-21 | Florian Schweigert | Method for the extraction and detection of fat-soluble components from biological materials |
| CN103645177A (en) * | 2013-12-23 | 2014-03-19 | 武汉大学 | Method for improving Sudan red I detection kit |
| CN104101661A (en) * | 2014-07-03 | 2014-10-15 | 广西大学 | Quick detecting method for sudan red in food |
Non-Patent Citations (1)
| Title |
|---|
| 常平平 等: "苏丹红Ⅰ～Ⅳ现场快速检测试剂盒的研制", 《黑龙江畜牧兽医》 * |
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|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170315 |