CN106497379A - A kind of aqueous one-component fireproof coating and preparation method thereof - Google Patents

A kind of aqueous one-component fireproof coating and preparation method thereof Download PDF

Info

Publication number
CN106497379A
CN106497379A CN201611049279.8A CN201611049279A CN106497379A CN 106497379 A CN106497379 A CN 106497379A CN 201611049279 A CN201611049279 A CN 201611049279A CN 106497379 A CN106497379 A CN 106497379A
Authority
CN
China
Prior art keywords
parts
epoxy resin
standby
raw material
aqueous
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611049279.8A
Other languages
Chinese (zh)
Inventor
王顺峰
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiangsu Huanyu Textile Technology Co Ltd
Original Assignee
Jiangsu Huanyu Textile Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jiangsu Huanyu Textile Technology Co Ltd filed Critical Jiangsu Huanyu Textile Technology Co Ltd
Priority to CN201611049279.8A priority Critical patent/CN106497379A/en
Publication of CN106497379A publication Critical patent/CN106497379A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D175/00Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
    • C09D175/04Polyurethanes
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/18Fireproof paints including high temperature resistant paints
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/61Additives non-macromolecular inorganic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/63Additives non-macromolecular organic
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00Properties
    • C08L2201/02Flame or fire retardant/resistant
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/02Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/02Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C08L2205/025Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
  • Paints Or Removers (AREA)

Abstract

The present invention discloses a kind of aqueous one-component fireproof coating and preparation method thereof, it is characterised in that:It is made up of following raw material:Epoxy resin, methyl trichlorosilane, polyaminoester emulsion, ATO dispersion liquids, acrylic modified epoxy resin, amino resins, glycol ether, two methylene level diisocyanate of durol, triethylamine, sodium bicarbonate, non-ionic associative type polyurethane, benzimidazole methyl carbamate, polydimethylsiloxane, deionized water, water;The aqueous one-component fireproof coating and preparation method thereof water resistance is high, effect of heat insulation and light transmission are high.

Description

A kind of aqueous one-component fireproof coating and preparation method thereof
Technical field
The present invention relates to a kind of aqueous one-component fireproof coating and preparation method thereof.
Background technology
Glass and glass, because of attractive in appearance and performance needs, need to coat coating thereon, but existing glass coating There is a problem that as follows:1st, existing glass coating is dual-component coating, needs to allocate on the spot, after deployed, it is necessary to Just use in very short time(In several hours), will otherwise fail, not only using inconvenience, and easily cause the wave of material Take;2nd, the glass coating that sells currently on the market mostly is oil paint, and its film forming matter is essentially from petroleum chemicals, and its solvent Also adopt organic solvent more, usually contain the noxious substances such as formaldehyde, free TDI and dimethylbenzene, these materials are given birth in glass coating Constantly come out during product process and use, not only cause environmental pollution, and damage health;3rd, to water, ethanol Poor performance is tolerated Deng common liquid, wearability is poor.
Content of the invention
The technical problem to be solved in the present invention is to provide that a kind of water resistance is high, the water that good heat-insulation effect and light transmission are high Property one-component glass coating.
For solving the above problems, the present invention is adopted the following technical scheme that:
A kind of aqueous one-component fireproof coating and preparation method thereof, is made up of following raw material:Epoxy resin, methyl trichlorosilane, Polyaminoester emulsion, ATO dispersion liquids, acrylic modified epoxy resin, amino resins, glycol ether, two methylene level two of durol Isocyanates, triethylamine, sodium bicarbonate, non-ionic associative type polyurethane, benzimidazole methyl carbamate, polydimethylsiloxanes Alkane, deionized water, water;The raw material is made up of following parts by weight proportioning:Epoxy resin 10-18 parts, methyl trichlorosilane 12- 20 parts, polyaminoester emulsion 14-20 parts, ATO dispersion liquid 8-16 parts, acrylic modified epoxy resin 8-14 parts, amino resins 14-18 Part, glycol ether 14-18 parts, two methylene level diisocyanate 10-16 parts of durol, triethylamine 6-10 parts, sodium bicarbonate 10- 16 parts, non-ionic associative type polyurethane 5-10 parts, benzimidazole methyl carbamate 4-8 parts, polydimethylsiloxane 12-16 Part, deionized water 10-20 parts, water 12-20 parts.
Further, the raw material is made up of following optimum parts by weight proportioning:14 parts of epoxy resin, methyl trichlorosilane 16 parts, 17 parts of polyaminoester emulsion, 12 parts of ATO dispersion liquids, 11 parts of acrylic modified epoxy resin, 16 parts of amino resins, dihydroxylic alcohols 16 parts of ether, two 13 parts of methylene level diisocyanate of durol, 8 parts of triethylamine, 13 parts of sodium bicarbonate, the poly- ammonia of non-ionic associative type 7.5 parts of ester, 6 parts of benzimidazole methyl carbamate, 14 parts of polydimethylsiloxane, 15 parts of deionized water, 16 parts of water.
The invention solves the problems that another technical problem be to provide a kind of aqueous one-component fireproof coating and its preparation side Method, comprises the following steps:
1)By epoxy resin 10-18 parts, methyl trichlorosilane 12-20 parts, the mixing of deionized water 10-20 parts, it is put into sand milling, divides Dissipate, stir in multiple purpose aeroplane, under the conditions of rotating speed is 2800rmp, disperses 15min at a high speed, standby;
2) polyaminoester emulsion 14-20 parts are added on the magnetic force heating stirrer with magneton, are 500r/min bars in rotating speed It is stirred continuously under part, continues 5min, standby;
3)To step 2)In again plus ATO dispersion liquid 8-16 parts, add water 12-20 parts, mixing speed to be adjusted to 1200r/min, continue 40min, standby;
4)Glycol ether 14-18 parts and the dehydration of two methylene level diisocyanate 10-16 parts of durol are added in four-hole boiling flask, Nitrogen protection is passed through, after 20min, triethylamine 6-10 parts is added, temperature is down to 30 DEG C, standby;
5)Sodium bicarbonate 10-16 parts are added to step 4)Raw material in, adjust pH value, stir, standby;
6)Will acrylic modified epoxy resin 8-14 parts add high-speed dispersing kettle in, add polydimethylsiloxane 12-16 parts, Non-ionic associative type polyurethane 5-10 parts, benzimidazole methyl carbamate 4-8 parts, stir, standby;
7)By step 6)Middle raw material sends into grinding machine for grinding to fineness≤12 μm, adds amino resins 14-18 parts, and stirring is Even, standby;
8)By step 1), step 3)With step 5)In raw material be added to step 7)In, stir, be cooled to room temperature, you can Obtain a kind of aqueous one-component glass coating.
Beneficial effects of the present invention are:Need not allocate on the spot during the aqueous one-component glass coating use, and possess Longer working life, it is to avoid the problems such as what conventional two-component coating easily occurred cause wastes, working life is short;This glass coating fills After dividing solidification, adhesive force is strong, intensity is big, tolerate excellent performance to common liquids such as water, ethanol, and exterior water moistens smooth, fire line Can be stable, light transmittance is high and effect of heat insulation is obvious.
Specific embodiment
Embodiment 1
A kind of aqueous one-component fireproof coating and preparation method thereof, is made up of following raw material:Epoxy resin, methyl trichlorosilane, Polyaminoester emulsion, ATO dispersion liquids, acrylic modified epoxy resin, amino resins, glycol ether, two methylene level two of durol Isocyanates, triethylamine, sodium bicarbonate, non-ionic associative type polyurethane, benzimidazole methyl carbamate, polydimethylsiloxanes Alkane, deionized water, water;The raw material is made up of following parts by weight proportioning:Epoxy resin 10-18 parts, methyl trichlorosilane 12- 20 parts, polyaminoester emulsion 14-20 parts, ATO dispersion liquid 8-16 parts, acrylic modified epoxy resin 8-14 parts, amino resins 14-18 Part, glycol ether 14-18 parts, two methylene level diisocyanate 10-16 parts of durol, triethylamine 6-10 parts, sodium bicarbonate 10- 16 parts, non-ionic associative type polyurethane 5-10 parts, benzimidazole methyl carbamate 4-8 parts, polydimethylsiloxane 12-16 Part, deionized water 10-20 parts, water 12-20 parts.
A kind of aqueous one-component fireproof coating and preparation method thereof, comprises the following steps:
1)By 10 parts of epoxy resin, 12 parts of methyl trichlorosilane, the mixing of 10 parts of deionized water, be put into sand milling, disperse, stir multiplex In machine, under the conditions of rotating speed is 2800rmp, disperse 15min at a high speed, standby;
2) by 14 parts of magnetic force heating stirrers being added to magneton of polyaminoester emulsion, under the conditions of rotating speed is 500r/min It is stirred continuously, continues 5min, standby;
3)To step 2)In again plus 8 parts of ATO dispersion liquids, add 12 parts of water, mixing speed is adjusted to 1200r/min, continues 40min, Standby;
4)The 10 parts of dehydrations of 14 parts of glycol ether and two methylene level diisocyanate of durol are added in four-hole boiling flask, nitrogen is passed through Gas shielded, adds 6 parts of triethylamine after 20min, and temperature is down to 30 DEG C, standby;
5)By sodium bicarbonate, 10 parts are added to step 4)Raw material in, adjust pH value, stir, standby;
6)By acrylic modified epoxy resin, 8 parts add in high-speed dispersing kettle, add 12 parts of polydimethylsiloxane, nonionic 5 parts of association type polyurethane, 4 parts of benzimidazole methyl carbamate, stir, standby;
7)By step 6)Middle raw material sends into grinding machine for grinding to fineness≤12 μm, adds 14 parts of amino resins, stirs, Standby;
8)By step 1), step 3)With step 5)In raw material be added to step 7)In, stir, be cooled to room temperature, you can Obtain a kind of aqueous one-component glass coating.
Embodiment 2
A kind of aqueous one-component fireproof coating and preparation method thereof, is made up of following raw material:Epoxy resin, methyl trichlorosilane, Polyaminoester emulsion, ATO dispersion liquids, acrylic modified epoxy resin, amino resins, glycol ether, two methylene level two of durol Isocyanates, triethylamine, sodium bicarbonate, non-ionic associative type polyurethane, benzimidazole methyl carbamate, polydimethylsiloxanes Alkane, deionized water, water;The raw material is made up of following parts by weight proportioning:Epoxy resin 10-18 parts, methyl trichlorosilane 12- 20 parts, polyaminoester emulsion 14-20 parts, ATO dispersion liquid 8-16 parts, acrylic modified epoxy resin 8-14 parts, amino resins 14-18 Part, glycol ether 14-18 parts, two methylene level diisocyanate 10-16 parts of durol, triethylamine 6-10 parts, sodium bicarbonate 10- 16 parts, non-ionic associative type polyurethane 5-10 parts, benzimidazole methyl carbamate 4-8 parts, polydimethylsiloxane 12-16 Part, deionized water 10-20 parts, water 12-20 parts.
A kind of aqueous one-component fireproof coating and preparation method thereof, comprises the following steps:
1)By 14 parts of epoxy resin, 16 parts of methyl trichlorosilane, the mixing of 15 parts of deionized water, be put into sand milling, disperse, stir multiplex In machine, under the conditions of rotating speed is 2800rmp, disperse 15min at a high speed, standby;
2) by 17 parts of magnetic force heating stirrers being added to magneton of polyaminoester emulsion, under the conditions of rotating speed is 500r/min It is stirred continuously, continues 5min, standby;
3)To step 2)In again plus 12 parts of ATO dispersion liquids, add 16 parts of water, mixing speed is adjusted to 1200r/min, continues 40min, Standby;
4)The 13 parts of dehydrations of 16 parts of glycol ether and two methylene level diisocyanate of durol are added in four-hole boiling flask, nitrogen is passed through Gas shielded, adds 8 parts of triethylamine after 20min, and temperature is down to 30 DEG C, standby;
5)By sodium bicarbonate, 13 parts are added to step 4)Raw material in, adjust pH value, stir, standby;
6)11 parts of acrylic modified epoxy resin is added in high-speed dispersing kettles, add 14 parts of polydimethylsiloxane, non-from 7.5 parts of sub- association type polyurethane, 6 parts of benzimidazole methyl carbamate, stir, standby;
7)By step 6)Middle raw material sends into grinding machine for grinding to fineness≤12 μm, adds 16 parts of amino resins, stirs, Standby;
8)By step 1), step 3)With step 5)In raw material be added to step 7)In, stir, be cooled to room temperature, you can Obtain a kind of aqueous one-component glass coating.
Embodiment 3
A kind of aqueous one-component fireproof coating and preparation method thereof, is made up of following raw material:Epoxy resin, methyl trichlorosilane, Polyaminoester emulsion, ATO dispersion liquids, acrylic modified epoxy resin, amino resins, glycol ether, two methylene level two of durol Isocyanates, triethylamine, sodium bicarbonate, non-ionic associative type polyurethane, benzimidazole methyl carbamate, polydimethylsiloxanes Alkane, deionized water, water;The raw material is made up of following parts by weight proportioning:Epoxy resin 10-18 parts, methyl trichlorosilane 12- 20 parts, polyaminoester emulsion 14-20 parts, ATO dispersion liquid 8-16 parts, acrylic modified epoxy resin 8-14 parts, amino resins 14-18 Part, glycol ether 14-18 parts, two methylene level diisocyanate 10-16 parts of durol, triethylamine 6-10 parts, sodium bicarbonate 10- 16 parts, non-ionic associative type polyurethane 5-10 parts, benzimidazole methyl carbamate 4-8 parts, polydimethylsiloxane 12-16 Part, deionized water 10-20 parts, water 12-20 parts.
A kind of aqueous one-component fireproof coating and preparation method thereof, comprises the following steps:
1)By 18 parts of epoxy resin, 20 parts of methyl trichlorosilane, the mixing of 20 parts of deionized water, be put into sand milling, disperse, stir multiplex In machine, under the conditions of rotating speed is 2800rmp, disperse 15min at a high speed, standby;
2) by 20 parts of magnetic force heating stirrers being added to magneton of polyaminoester emulsion, under the conditions of rotating speed is 500r/min It is stirred continuously, continues 5min, standby;
3)To step 2)In again plus ATO dispersion liquid 8-16 parts, add 20 parts of water, mixing speed is adjusted to 1200r/min, continues 40min, standby;
4)The 16 parts of dehydrations of 18 parts of glycol ether and two methylene level diisocyanate of durol are added in four-hole boiling flask, nitrogen is passed through Gas shielded, adds 10 parts of triethylamine after 20min, and temperature is down to 30 DEG C, standby;
5)By sodium bicarbonate, 16 parts are added to step 4)Raw material in, adjust pH value, stir, standby;
6)14 parts of acrylic modified epoxy resin is added in high-speed dispersing kettles, add 16 parts of polydimethylsiloxane, non-from 10 parts of sub- association type polyurethane, 8 parts of benzimidazole methyl carbamate, stir, standby;
7)By step 6)Middle raw material sends into grinding machine for grinding to fineness≤12 μm, adds 18 parts of amino resins, stirs, Standby;
8)By step 1), step 3)With step 5)In raw material be added to step 7)In, stir, be cooled to room temperature, you can Obtain a kind of aqueous one-component glass coating.
Experimental example
Choose embodiment 1), embodiment 2)With embodiment 3)In sample and simple glass coating, be divided into four groups, observe each group glass Impact of the glass coating to glass.
Comparing result see the table below:
Project group Light transmittance Adhesive force Hardness Water-fast natural law
Simple glass coating 79.8% 2 grades HB 3 days
Embodiment 1 90.2% 1 grade H 10 days
Embodiment 2 92.6% 1 grade 2H 13 days
Embodiment 3 91.4% 1 grade H 10 days
As can be seen here, embodiment 2)In aqueous one-component glass coating effect preferably, optimal implementation result can be reached.
Beneficial effects of the present invention are:Need not allocate on the spot during the aqueous one-component glass coating use, and possess Longer working life, it is to avoid the problems such as what conventional two-component coating easily occurred cause wastes, working life is short;This glass coating fills After dividing solidification, adhesive force is strong, intensity is big, tolerate excellent performance to common liquids such as water, ethanol, and exterior water moistens smooth, fire line Can be stable, light transmittance is high and effect of heat insulation is obvious.
The above, the only specific embodiment of the present invention, but protection scope of the present invention is not limited thereto, any The change or replacement that expects without creative work, should all cover within the scope of the present invention.

Claims (3)

1. a kind of aqueous one-component fireproof coating and preparation method thereof, it is characterised in that:It is made up of following raw material:Epoxy resin, Methyl trichlorosilane, polyaminoester emulsion, ATO dispersion liquids, acrylic modified epoxy resin, amino resins, glycol ether, tetramethyl Two methylene level diisocyanate of benzene, triethylamine, sodium bicarbonate, non-ionic associative type polyurethane, benzimidazole methyl carbamate, Polydimethylsiloxane, deionized water, water;The raw material is made up of following parts by weight proportioning:Epoxy resin 10-18 parts, first Base trichlorosilane 12-20 part, polyaminoester emulsion 14-20 parts, ATO dispersion liquid 8-16 parts, acrylic modified epoxy resin 8-14 parts, Amino resins 14-18 parts, glycol ether 14-18 parts, two methylene level diisocyanate 10-16 parts of durol, triethylamine 6-10 Part, sodium bicarbonate 10-16 parts, non-ionic associative type polyurethane 5-10 parts, benzimidazole methyl carbamate 4-8 parts, poly- diformazan Radical siloxane 12-16 parts, deionized water 10-20 parts, water 12-20 parts.
2. aqueous one-component fireproof coating as claimed in claim 1 and preparation method thereof, it is characterised in that:The raw material by with Lower optimum parts by weight proportioning composition:14 parts of epoxy resin, 16 parts of methyl trichlorosilane, 17 parts of polyaminoester emulsion, ATO dispersion liquids 12 parts, 11 parts of acrylic modified epoxy resin, 16 parts of amino resins, 16 parts of glycol ether, two methylene level of durol, two isocyanide 13 parts of acid esters, 8 parts of triethylamine, 13 parts of sodium bicarbonate, 7.5 parts of non-ionic associative type polyurethane, benzimidazole methyl carbamate 6 Part, 14 parts of polydimethylsiloxane, 15 parts of deionized water, 16 parts of water.
3. a kind of aqueous one-component fireproof coating as claimed in claim 1 and preparation method thereof, it is characterised in that:Including following Step:
1)By epoxy resin 10-18 parts, methyl trichlorosilane 12-20 parts, the mixing of deionized water 10-20 parts, it is put into sand milling, divides Dissipate, stir in multiple purpose aeroplane, under the conditions of rotating speed is 2800rmp, disperses 15min at a high speed, standby;
2) polyaminoester emulsion 14-20 parts are added on the magnetic force heating stirrer with magneton, are 500r/min bars in rotating speed It is stirred continuously under part, continues 5min, standby;
3)To step 2)In again plus ATO dispersion liquid 8-16 parts, add water 12-20 parts, mixing speed to be adjusted to 1200r/min, continue 40min, standby;
4)Glycol ether 14-18 parts and the dehydration of two methylene level diisocyanate 10-16 parts of durol are added in four-hole boiling flask, Nitrogen protection is passed through, after 20min, triethylamine 6-10 parts is added, temperature is down to 30 DEG C, standby;
5)Sodium bicarbonate 10-16 parts are added to step 4)Raw material in, adjust pH value, stir, standby;
6)Will acrylic modified epoxy resin 8-14 parts add high-speed dispersing kettle in, add polydimethylsiloxane 12-16 parts, Non-ionic associative type polyurethane 5-10 parts, benzimidazole methyl carbamate 4-8 parts, stir, standby;
7)By step 6)Middle raw material sends into grinding machine for grinding to fineness≤12 μm, adds amino resins 14-18 parts, and stirring is Even, standby;
8)By step 1), step 3)With step 5)In raw material be added to step 7)In, stir, be cooled to room temperature, you can Obtain a kind of aqueous one-component glass coating.
CN201611049279.8A 2016-11-25 2016-11-25 A kind of aqueous one-component fireproof coating and preparation method thereof Pending CN106497379A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611049279.8A CN106497379A (en) 2016-11-25 2016-11-25 A kind of aqueous one-component fireproof coating and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611049279.8A CN106497379A (en) 2016-11-25 2016-11-25 A kind of aqueous one-component fireproof coating and preparation method thereof

Publications (1)

Publication Number Publication Date
CN106497379A true CN106497379A (en) 2017-03-15

Family

ID=58328195

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611049279.8A Pending CN106497379A (en) 2016-11-25 2016-11-25 A kind of aqueous one-component fireproof coating and preparation method thereof

Country Status (1)

Country Link
CN (1) CN106497379A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11332637B2 (en) * 2018-05-11 2022-05-17 Zhenglin Chen Single-component coating for automobile seal trip

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101974274A (en) * 2010-10-27 2011-02-16 常州光辉化工有限公司 Water-based acrylic heat insulation coating and preparation method thereof
CN103333600A (en) * 2013-05-30 2013-10-02 中国科学院合肥物质科学研究院 Preparation method for one-component waterborne polyurethane transparent heat-insulating coating
CN105219138A (en) * 2015-11-17 2016-01-06 杨洋 A kind of protection against corrosion environment protection architecture water-borne coatings and preparation method thereof
CN105273593A (en) * 2015-10-09 2016-01-27 浙江新迪在龙涂料科技有限公司 Waterborne one-component glass coating and preparation method thereof
CN105505060A (en) * 2015-12-31 2016-04-20 长沙民德消防工程涂料有限公司 Water-based nano reflection and heat insulation transparent coating and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101974274A (en) * 2010-10-27 2011-02-16 常州光辉化工有限公司 Water-based acrylic heat insulation coating and preparation method thereof
CN103333600A (en) * 2013-05-30 2013-10-02 中国科学院合肥物质科学研究院 Preparation method for one-component waterborne polyurethane transparent heat-insulating coating
CN105273593A (en) * 2015-10-09 2016-01-27 浙江新迪在龙涂料科技有限公司 Waterborne one-component glass coating and preparation method thereof
CN105219138A (en) * 2015-11-17 2016-01-06 杨洋 A kind of protection against corrosion environment protection architecture water-borne coatings and preparation method thereof
CN105505060A (en) * 2015-12-31 2016-04-20 长沙民德消防工程涂料有限公司 Water-based nano reflection and heat insulation transparent coating and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11332637B2 (en) * 2018-05-11 2022-05-17 Zhenglin Chen Single-component coating for automobile seal trip

Similar Documents

Publication Publication Date Title
CN105273593B (en) A kind of aqueous one-component glass coating and preparation method thereof
CN106432684B (en) A kind of self-catalysis type anacardol/lignin-base polyurethane foam and preparation method thereof
CN102863889B (en) Double-component polyurethane white high-gloss woodware paint, and preparation method and application thereof
CN102174292B (en) Resin paint surface nursing emulsion and preparation method thereof
CN101831102B (en) Aqueous environmentally-friendly leather finishing and delustering handfeel wax assistant and preparation process thereof
CN102409552A (en) Preparation method of environment-friendly foamed artificial leather
CN105001773B (en) A kind of matte varnish and preparation method thereof
CN103740205A (en) Water-based spray lacquer and preparation method thereof
CN107189084A (en) The aqueous epoxy emulsion prepared by the emulsifying agent of the functional group of bis-epoxy containing isocyanates
CN102220698A (en) Aqueous PU mechanically foamed resin for synthetic leather
CN108641573A (en) A kind of sealer and preparation method thereof with the efficiently anti-muscle energy that rises
CN106497379A (en) A kind of aqueous one-component fireproof coating and preparation method thereof
CN103589233A (en) Gravure alcohol ester plastic in-print environment-friendly ink
CN106669237A (en) Organic silicon defoamer containing sodium tripolyphosphate
CN102363704A (en) Aqueous blocking agent and its preparation method
CN102363684A (en) Aqueous two-component white priming paint and preparation method thereof
CN102363703B (en) Waterborne single-component white primer and preparation method thereof
CN105802463A (en) Waterborne polyurethane high-gloss 2K coating and preparation method thereof
CN107033753A (en) A kind of safety cap protection paint vehicle and preparation method thereof
CN102732129A (en) Environment-friendly photo-cured electrostatic spray finish
CN106621480A (en) Industrial organic silicon defoamer
CN102363693B (en) Aqueous dual component matting white top finish and its preparation method
CN105400390A (en) Self-repairing polyurethane matt finishing coat
CN102367347B (en) Waterborne double-component full-glossy white finish and preparation method thereof
CN102363707B (en) Aqueous monocomponent matting white finish and preparation method thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20170315