CN106489989A - 一种纳米乳杀虫剂及其制备方法 - Google Patents

一种纳米乳杀虫剂及其制备方法 Download PDF

Info

Publication number
CN106489989A
CN106489989A CN201610818846.5A CN201610818846A CN106489989A CN 106489989 A CN106489989 A CN 106489989A CN 201610818846 A CN201610818846 A CN 201610818846A CN 106489989 A CN106489989 A CN 106489989A
Authority
CN
China
Prior art keywords
parts
nano
oil
pleocidin
matrine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610818846.5A
Other languages
English (en)
Inventor
蒋承建
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guangxi University
Original Assignee
Guangxi University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Guangxi University filed Critical Guangxi University
Priority to CN201610818846.5A priority Critical patent/CN106489989A/zh
Publication of CN106489989A publication Critical patent/CN106489989A/zh
Pending legal-status Critical Current

Links

Classifications

    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
    • A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
    • A01N31/02—Acyclic compounds
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/06—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings
    • A01N43/12—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings condensed with a carbocyclic ring
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/22—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom rings with more than six members
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N53/00—Biocides, pest repellants or attractants, or plant growth regulators containing cyclopropane carboxylic acids or derivatives thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/10—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
    • A01N57/12—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds containing acyclic or cycloaliphatic radicals

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Plant Pathology (AREA)
  • Environmental Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Agronomy & Crop Science (AREA)
  • Zoology (AREA)
  • Pest Control & Pesticides (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Toxicology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Medicinal Preparation (AREA)

Abstract

本发明提供了一种纳米乳杀虫剂，原材料按照如下份数比组成：氯氟氰菊酯1‑2份、多杀菌素0.1‑0.6份、苦参碱0.2‑0.9份、纳米二氧化钛11‑21份、大豆油200‑310份、蛋黄卵磷脂52‑71份、正丁醇11‑17份、吐温0.2‑0.6份、阿维菌素10‑11份、灰黄霉素5‑15份。相对于现有技术，本发明所得的纳米乳杀虫剂，成本低，工艺简单，很低的药量就可以达到较强的杀虫效果，且持效期长，对生态系统破坏性低。

Description

一种纳米乳杀虫剂及其制备方法
技术领域
本发明涉及农药领域，尤其涉及一种纳米乳杀虫剂及其制备方法。
背景技术
杀虫剂(英文：Pesticide.Insecticide)，主要用于防治农业害虫和城市卫生害虫的药品.使用历史长远、用量大、品种多。在二十世纪，农业的迅速发展，杀虫剂令农业产量大升。但是，几乎所有杀虫剂都会严重地改变生态系统，大部分对人体有害，其它的会被集中在食物链中。我们必须在农业发展与环境及健康中取得平衡。
农用抗生素是在20世纪40年代医用抗生素发展的基础上研究开发的，70年代以来，一些具有防治昆虫、螨、动物寄生原虫和蠕虫、除草和调节动植物生长功能的农用抗生素，不断研究开发出来，扩大了农用抗生素的应用领域。一些抗生素药物为难溶性药物，进入害虫体内时难以吸收，并且杀灭持续时间短，这就需要应用现代药剂学的原理来设计新的剂型。目前，现有的杀虫剂不仅杀虫效果不强，药效持久力差，而且还存在严重破坏生态系统的问题。
发明内容
针对上述现有技术中存在的问题，本发明的目的在于提供一种纳米乳杀虫剂及其制备方法。
一种纳米乳杀虫剂，原材料按照如下份数比组成：
氯氟氰菊酯1-2份、多杀菌素0.1-0.6份、苦参碱0.2-0.9份、纳米二氧化钛11-21份、大豆油200-310份、蛋黄卵磷脂52-71份、正丁醇11-17份、吐温0.2-0.6份、阿维菌素10-11份、灰黄霉素5-15份。
进一步说明，所述的一种纳米乳杀虫剂，原材料按照如下份数比组成：
氯氟氰菊酯1.5份、多杀菌素0.2份、苦参碱0.7份、纳米二氧化钛13份、大豆油230份、蛋黄卵磷脂58份、正丁醇15份、吐温0.5份、阿维菌素11份、灰黄霉素9份。
进一步说明，所述的一种纳米乳杀虫剂，包括如下步骤：
(1)将阿维菌素、灰黄霉素、氯氟氰菊酯、多杀菌素、蛋黄卵磷脂和吐温，加入到大豆油中，混匀，得油相溶液；
(2)在搅拌条件下，将上述油相溶液加入到水中，得油水混合液；
(3)将正丁醇、苦参碱和纳米二氧化钛加入水中溶解，缓慢滴加入上述油水混合液中，控制油水混合液温度为30-40℃；
(4)滴加结束后，将溶液超声至透明，超声功率为200-400W，超声时间为5-15分钟即得。
本发明的有益效果如下：
相对于现有技术，本发明所得的纳米乳杀虫剂，成本低，工艺简单，很低的药量就可以达到较强的杀虫效果，且持效期长，对生态系统破坏性低。
具体实施方式
下面将结合本发明实施例，对本发明实施例中的技术方案进行清楚、完整地描述，显然，所描述的实施例仅是本发明一部分实施例，而不是全部的实施例。基于本发明中的实施例，领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例，都属于本发明保护的范围。
实施例1
一种纳米乳杀虫剂，原材料按照如下份数比组成：
氯氟氰菊酯1份、多杀菌素0.1份、苦参碱0.2份、纳米二氧化钛11份、大豆油200份、蛋黄卵磷脂52份、正丁醇11份、吐温0.2份、阿维菌素10份、灰黄霉素5份。
所述的一种纳米乳杀虫剂，包括如下步骤：
(1)将阿维菌素、灰黄霉素、氯氟氰菊酯、多杀菌素、蛋黄卵磷脂和吐温，加入到大豆油中，混匀，得油相溶液；
(2)在搅拌条件下，将上述油相溶液加入到水中，得油水混合液；
(3)将正丁醇、苦参碱和纳米二氧化钛加入水中溶解，缓慢滴加入上述油水混合液中，控制油水混合液温度为30℃；
(4)滴加结束后，将溶液超声至透明，超声功率为200W，超声时间为5分钟即得。
实施2
一种纳米乳杀虫剂，原材料按照如下份数比组成：
氯氟氰菊酯2份、多杀菌素0.6份、苦参碱0.9份、纳米二氧化钛21份、大豆油310份、蛋黄卵磷脂71份、正丁醇17份、吐温0.6份、阿维菌素11份、灰黄霉素15份。
所述的一种纳米乳杀虫剂，包括如下步骤：
(1)将阿维菌素、灰黄霉素、氯氟氰菊酯、多杀菌素、蛋黄卵磷脂和吐温，加入到大豆油中，混匀，得油相溶液；
(2)在搅拌条件下，将上述油相溶液加入到水中，得油水混合液；
(3)将正丁醇、苦参碱和纳米二氧化钛加入水中溶解，缓慢滴加入上述油水混合液中，控制油水混合液温度为40℃；
(4)滴加结束后，将溶液超声至透明，超声功率为400W，超声时间为15分钟即得。
实施例3
一种纳米乳杀虫剂，原材料按照如下份数比组成：
氯氟氰菊酯1.5份、多杀菌素0.2份、苦参碱0.7份、纳米二氧化钛13份、大豆油230份、蛋黄卵磷脂58份、正丁醇15份、吐温0.5份、阿维菌素11份、灰黄霉素9份。
所述的一种纳米乳杀虫剂，包括如下步骤：
(1)将阿维菌素、灰黄霉素、氯氟氰菊酯、多杀菌素、蛋黄卵磷脂和吐温，加入到大豆油中，混匀，得油相溶液；
(2)在搅拌条件下，将上述油相溶液加入到水中，得油水混合液；
(3)将正丁醇、苦参碱和纳米二氧化钛加入水中溶解，缓慢滴加入上述油水混合液中，控制油水混合液温度为35℃；
(4)滴加结束后，将溶液超声至透明，超声功率为280W，超声时间为8分钟即得。
上述实施例为本发明较佳的实施方式，但本发明的实施方式并不受上述实施例的限制，其他的任何未背离本发明的精神实质与原理下所作的改变、修饰、替代、组合、简化，均应为等效的置换方式，都包含在本发明的保护范围之内。

Claims (3)

1.一种纳米乳杀虫剂，其特征在于，原材料按照如下份数比组成：
氯氟氰菊酯1-2份、多杀菌素0.1-0.6份、苦参碱0.2-0.9份、纳米二氧化钛11-21份、大豆油200-310份、蛋黄卵磷脂52-71份、正丁醇11-17份、吐温0.2-0.6份、阿维菌素10-11份、灰黄霉素5-15份。
2.根据权利要求1所述的一种纳米乳杀虫剂，其特征在于，原材料按照如下份数比组成：
氯氟氰菊酯1.5份、多杀菌素0.2份、苦参碱0.7份、纳米二氧化钛13份、大豆油230份、蛋黄卵磷脂58份、正丁醇15份、吐温0.5份、阿维菌素11份、灰黄霉素9份。
3.根据权利要求1所述的一种纳米乳杀虫剂，其特征在于，包括如下步骤：
(1)将阿维菌素、灰黄霉素、氯氟氰菊酯、多杀菌素、蛋黄卵磷脂和吐温，加入到大豆油中，混匀，得油相溶液；
(2)在搅拌条件下，将上述油相溶液加入到水中，得油水混合液；
(3)将正丁醇、苦参碱和纳米二氧化钛加入水中溶解，缓慢滴加入上述油水混合液中，控制油水混合液温度为30-40℃；
(4)滴加结束后，将溶液超声至透明，超声功率为200-400W，超声时间为5-15分钟即得。
CN201610818846.5A 2016-09-13 2016-09-13 一种纳米乳杀虫剂及其制备方法 Pending CN106489989A (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610818846.5A CN106489989A (zh) 2016-09-13 2016-09-13 一种纳米乳杀虫剂及其制备方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610818846.5A CN106489989A (zh) 2016-09-13 2016-09-13 一种纳米乳杀虫剂及其制备方法

Publications (1)

Publication Number Publication Date
CN106489989A true CN106489989A (zh) 2017-03-15

Family

ID=58289990

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610818846.5A Pending CN106489989A (zh) 2016-09-13 2016-09-13 一种纳米乳杀虫剂及其制备方法

Country Status (1)

Country Link
CN (1) CN106489989A (zh)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107372632A (zh) * 2017-07-28 2017-11-24 镇江绿健农业科技开发有限公司 一种茅苍术用高效农药及其制备方法
CN114016289A (zh) * 2021-10-27 2022-02-08 常熟市华瑞针纺织有限公司 一种防蚊面料及其制备方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1526406A (zh) * 2003-09-25 2004-09-08 浙江省农业科学院 防治动物皮癣菌病和螨虫病联合缓释剂的制备方法
CN103478144A (zh) * 2013-09-26 2014-01-01 卞佳林 一种阿维菌素和灰黄霉素复合纳米乳杀虫剂
CN104206406A (zh) * 2014-09-17 2014-12-17 句容亿格纳米材料厂 一种纳米乳杀虫剂及其制备方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1526406A (zh) * 2003-09-25 2004-09-08 浙江省农业科学院 防治动物皮癣菌病和螨虫病联合缓释剂的制备方法
CN103478144A (zh) * 2013-09-26 2014-01-01 卞佳林 一种阿维菌素和灰黄霉素复合纳米乳杀虫剂
CN104206406A (zh) * 2014-09-17 2014-12-17 句容亿格纳米材料厂 一种纳米乳杀虫剂及其制备方法

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107372632A (zh) * 2017-07-28 2017-11-24 镇江绿健农业科技开发有限公司 一种茅苍术用高效农药及其制备方法
CN114016289A (zh) * 2021-10-27 2022-02-08 常熟市华瑞针纺织有限公司 一种防蚊面料及其制备方法
CN114016289B (zh) * 2021-10-27 2023-09-29 常熟市华瑞针纺织有限公司 一种防蚊面料及其制备方法

Similar Documents

Publication Publication Date Title
CN103689017B (zh) 一种复合植物源农药及其制备方法
CN105147561B (zh) 一种宠物香波及其制备方法
CN107047638A (zh) 一种纯中药成分的农药
CN106165705A (zh) 一种绿色植物杀虫剂及其制备方法
CN106489989A (zh) 一种纳米乳杀虫剂及其制备方法
CN102823616A (zh) 一种防治天牛的植物性杀虫剂及其使用方法
CN104892146B (zh) 一种适用于橙树壮果期施用的肥料及其制备方法
CN106479694A (zh) 一种农药清洁剂及其制备方法
CN105165920A (zh) 一种土鸡鸡场杀菌消毒液及其制备方法
CN107439897A (zh) 一种植物源抑菌剂
CN105272538A (zh) 一种改善土质营养丰富的驱虫杀菌掺混肥辅料制备方法
CN108440087A (zh) 一种具有土壤灭菌杀虫作用的肥料
CN107494905A (zh) 一种植物源抑菌剂的制备方法
CN107788229A (zh) 一种植物源抑菌剂的用途
CN107372660A (zh) 一种用于金银花的植物源杀蚜虫剂及其制备方法
CN106234466A (zh) 一种含有微生物杀虫剂及其制备方法
CN106135314A (zh) 一种防治蚧壳虫的杀虫剂配方及生产方法
CN104206406B (zh) 一种纳米乳杀虫剂及其制备方法
CN110476982A (zh) 一种含生物凝集素的生物农药杀虫剂及其制备方法
CN105165491A (zh) 一种综合防治木瓜炭疽病的方法
CN105941423B (zh) 一种含有虫螨腈和灭蝇胺的杀虫组合物
CN104382935B (zh) 一种用于水产养殖的杀虫灭菌组合物及其制备方法和应用
CN102863299B (zh) 一种50g/l高效氯氟氰菊酯乳油及其制备方法
CN103783097A (zh) 一种驱虫灭菌药物
CN104304332A (zh) 一种用于食用菌栽培料的杀虫剂

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20170315

WD01 Invention patent application deemed withdrawn after publication