CN106430728A - Sludge drying and sewage treatment method - Google Patents

Sludge drying and sewage treatment method Download PDF

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Publication number
CN106430728A
CN106430728A CN201611003503.XA CN201611003503A CN106430728A CN 106430728 A CN106430728 A CN 106430728A CN 201611003503 A CN201611003503 A CN 201611003503A CN 106430728 A CN106430728 A CN 106430728A
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sewage
mud
sludge
stirring
sludge drying
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CN201611003503.XA
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马从勇
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Mobao Ltd By Share Ltd
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Mobao Ltd By Share Ltd
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F9/00Multistage treatment of water, waste water or sewage
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F11/00Treatment of sludge; Devices therefor
    • C02F11/12Treatment of sludge; Devices therefor by de-watering, drying or thickening
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F11/00Treatment of sludge; Devices therefor
    • C02F11/12Treatment of sludge; Devices therefor by de-watering, drying or thickening
    • C02F11/14Treatment of sludge; Devices therefor by de-watering, drying or thickening with addition of chemical agents
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/001Processes for the treatment of water whereby the filtration technique is of importance
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/28Treatment of water, waste water, or sewage by sorption
    • C02F1/283Treatment of water, waste water, or sewage by sorption using coal, charred products, or inorganic mixtures containing them
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/50Treatment of water, waste water, or sewage by addition or application of a germicide or by oligodynamic treatment
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/52Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/52Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • C02F1/5236Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/52Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • C02F1/54Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using organic material
    • C02F1/56Macromolecular compounds
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/66Treatment of water, waste water, or sewage by neutralisation; pH adjustment
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F3/00Biological treatment of water, waste water, or sewage
    • C02F3/30Aerobic and anaerobic processes
    • C02F3/302Nitrification and denitrification treatment

Abstract

The invention discloses a sludge drying and sewage treatment method. The sludge drying and sewage treatment method comprises the following steps: introducing wastewater into a sedimentation tank and adding a pH (Potential of Hydrogen) regulator, nano active carbon and a flocculating agent; after stirring, standing and filtering; carrying out primary mud-water separation to obtain sludge A and sewage B; adding the sludge A into high-speed stirring equipment and regulating the pH regulator; then heating and stirring; after preserving heat and standing, centrifuging; carrying out secondary mud-water separation to obtain sludge C and sewage D; adding the sludge C into an evaporation boiler; controlling heating and stirring time to obtain dried sludge; adding the sewage B and the sewage D into a sewage treatment tank; after adding zeolite and stirring, standing, filtering and carrying out high-degree sterilization. The sludge drying and sewage treatment method disclosed by the invention is simple to operate, short in treatment period and high in treatment efficiency; the drying degree of the sludge is controllable and the cost is low; secondary pollution to the environment is not caused ,and the treated sludge and sewage have a wide applicable range.

Description

A kind of sludge drying and the method for sewage disposal
Technical field
The present invention relates to sewage disposal environmental technology field, the method for more particularly, to a kind of sludge drying and sewage disposal.
Background technology
Sewage disposal is in order that sewage reaches the water quality requirement entering a certain water body or reusing, and it is purified Process, sewage is by sources broadly divided into production waste and sanitary sewage, is broadly divided into nature sewage and artificial sewage by property, Currently larger to water body harm is artificial pollution.Sludge drying is sludge dewatering, and referring to will be dirty to the primary, concentration of fluidised form or digestion Mud removes moisture, is converted into a kind of method for sludge treatment of semisolid or solid-state clod.Produced by sewage disposal, mud has Higher water content, the characteristic being combined with mud granule due to moisture, certain restriction, mud are had using mechanical means removing In the content of organic matter, the addition of ash content ratio particularly flocculant is for final solid content important.Typically come Say, can obtain 20%~30% solid content using mechanical dehydration, the mud being formed is also referred to as mud cake.Mud cake aqueous Rate is still higher, has fluid properties, its dispose difficulty and cost still higher it is therefore necessary to further decrement.Now, exist Outside natural air drying, only pass through to input heat and formed to evaporate, extensive decrement can be realized.It is dried using heat Process is exactly heat drying.In in recent years, whole nation industry and city domestic sewage total emission volumn are all more than 480.5 hundred million t, and are in year by year Growth trend, at present, the nearly family more than 500 of China's municipal wastewater treatment plant, but wastewater treatment rate only 28% about, most of Sewage Plant Have such problems as that efficiency is low, high cost, complex process equipment.Sewage plant sludge annual production is 100,000,000 more than t, and sludge components are multiple Miscellaneous, how it is dealt carefully with so as to problem innoxious, that resource is always the concern of environment circle.Number of patent application is The 201210253450.2 a kind of methods disclosing sludge drying and sewage disposal, using sludge drying system and sewage disposal system System carries out sludge drying and sewage disposal respectively, and it has high degree of automation, the convenient feature of operational management, using precipitation Method realizes mud-water separation, and efficiency is low, and the moisture percentage in sewage sludge that sub-argument goes out is high, repeatedly carries out mud and turn in sewage disposal system Move, in sludge drying system, the simple high-temperature gas heating conduction oil leaning against the extraction of cement kiln dore furnace carries out mud to be done Flower, inefficient, the cycle is long.Based on above statement, a kind of method that the present invention proposes sludge drying and sewage disposal.
Content of the invention
The invention aims to have present in solution prior art that sewage sludge treatment effeciency is low, cycle length, The problems such as high cost, complex process equipment shortcoming, and propose a kind of sludge drying and sewage disposal method.
A kind of sludge drying and the method for sewage disposal, comprise the following steps:
S1, waste water is passed in sedimentation basin, adds PH conditioning agent to adjust the pH value of waste water to 5~9, add nano active Charcoal and flocculant, stir 15~25min with the rotating speed of 80~180r/min, stand 1~3h after the completion of stirring, then utilize mesh number Filter for 200~500 mesh carries out preliminary mud-water separation, respectively obtains the mud A that moisture content is 80~92% and sewage B;
S2, the mud B of gained in step S1 is put in high-speed mixing equipment, add the PH of PH conditioning agent conditioning of mud It is worth to 3.2~4.8 or 9.2~12, and is heated to 60~100 DEG C, in heating, height is carried out with the rotating speed of 600~1000r/min Speed stirring 15~25min, is then incubated standing 2~3h, is centrifuged 5~10min using centrifugation apparatus, carries out second muddy water and divide From respectively obtaining the mud C that moisture content is 48~72% and sewage D;
S3, the mud C of gained in step S2 is added in evaporation boiler, is heated to 80~120 DEG C using boiler afterheat, side Heating side is stirred with the rotating speed of 250~500r/min, controls the heating stirring time, obtains final product dewatered sludge;
S4, the sewage D of gained in the sewage B of gained in step S1 and step S2 is added in treatment tank, and plus Enter zeolite and 10~20min stirred with the rotating speed of 120~260r/min, after the completion of stirring, stand 1~3h, through mesh number be 1250~ After the accurate filter of 10000 mesh filters, carry out high degree of sterilization, obtain purified water.
Preferably, the polyacrylamide solution that the flocculant in described step S1 is 3~8% for concentration.
Preferably, in described step S1, the addition of active carbon nanoparticles is 0.08~0.22 times of waste water total amount, flocculant Addition be 0.002~0.005 times of waste water total amount.
Preferably, the PH conditioning agent in described step S1 and S2 is the concentrated sulfuric acid or NaOH.
Preferably, the zeolite addition in described step S4 is 0.01~0.04 times of sewage B and sewage D total amount.
Preferably, the high degree of sterilization method in described step S4 refers to the water obtaining filtration separation through nitrification tank, denitrification After the degraded of pond, it is added to ozone sterilization pond and is sterilized.
A kind of sludge drying proposed by the present invention and the method for sewage disposal, the difficulty in water is sunk by the effect using flocculant The particle forming sediment removes after being flocculated, and promotes mud-water separation it is ensured that the degree of purity of water, and the absorption using active carbon nanoparticles is made With removing impurities in water further, the color in water being decoloured and is removed the chlorine in eliminating water, reach the work being further purified water With after completing preliminary mud-water separation, mud being broken up by way of high-speed stirred the flco that diminishes, by heating and adjusting dirty The pH value of sewage sludge makes flocculant discharge wrapped moisture, after carrying out mud-water separation further, by the way of heat energy evaporation Mummification is carried out to mud;After sewage is precipitated by zeolite, through nitrification tank, the degraded of denitrification pond, it is finally added to ozone sterilization Pond carries out high degree of sterilization, so that the water energy after process is met and is subsequently required with water, method proposed by the present invention is simple, process cycle Short, treatment effeciency is high, and sludge drying degree is controlled, low cost, and does not result in the secondary pollution of environment, the sewage after process and Mud is applied widely.
Specific embodiment
With reference to specific embodiment, the present invention is explained further.
Embodiment one
A kind of sludge drying proposed by the present invention and the method for sewage disposal, comprise the following steps:
S1, waste water is passed in sedimentation basin, adds NaOH to adjust the pH value of waste water to 7.8, add waste water total amount The concentration of 0.15 times of active carbon nanoparticles and 0.002 times is 5% polyacrylamide solution, with the rotating speed stirring of 120r/min 20min, stands 2h after the completion of stirring, then carries out preliminary mud-water separation using the filter that mesh number is 300 mesh, respectively obtain Moisture content is 88% mud A and sewage B;
S2, the mud B of gained in step S1 is put in high-speed mixing equipment, add the PH of NaOH conditioning of mud It is worth to 12, and is heated to 80 DEG C, in heating, high-speed stirred 22min is carried out with the rotating speed of 800r/min, then insulation standing 2.5h, is centrifuged 8min using centrifugation apparatus, carries out second mud-water separation, respectively obtain the mud C that moisture content is 66% and dirt Water D;
S3, the mud C of gained in step S2 is added in evaporation boiler, is heated to 100 DEG C using boiler afterheat, side is heated While being stirred with the rotating speed of 400r/min, after heating 4h, obtain final product dewatered sludge;
S4, the sewage D of gained in the sewage B of gained in step S1 and step S2 is added in treatment tank, and plus The zeolite entering 0.03 times of above-mentioned sewage total amount stirs 18min with the rotating speed of 180r/min, after the completion of stirring, stands 1.5h, through mesh Number filters for the accurate filter of 4000 mesh, after then the water that filtration separation obtains being degraded through nitrification tank, denitrification pond, adds Carry out high degree of sterilization to ozone sterilization pond, obtain purified water.
Embodiment two
A kind of sludge drying proposed by the present invention and the method for sewage disposal, comprise the following steps:
S1, waste water is passed in sedimentation basin, adds the concentrated sulfuric acid to adjust the pH value of waste water to 5.2, add waste water total amount 0.2 Times active carbon nanoparticles and polyacrylamide solution that 0.005 times of concentration is 6%, 25min is stirred with the rotating speed of 80r/min, Stand 3h after the completion of stirring, then carry out preliminary mud-water separation using the filter that mesh number is 500 mesh, respectively obtain moisture content Mud A for 80% and sewage B;
S2, the mud B of gained in step S1 is put in high-speed mixing equipment, add the pH value of concentrated sulfuric acid conditioning of mud To 4.5 or 9.2~12, and it is heated to 100 DEG C, in heating, high-speed stirred 18min is carried out with the rotating speed of 1000r/min, then Insulation standing 2.2h, is centrifuged 5min using centrifugation apparatus, carries out second mud-water separation, respectively obtain the dirt that moisture content is 55% Mud C and sewage D;
S3, the mud C of gained in step S2 is added in evaporation boiler, is heated to 80 DEG C using boiler afterheat, side is heated While being stirred with the rotating speed of 250r/min, after heating 8h, obtain final product dewatered sludge;
S4, the sewage D of gained in the sewage B of gained in step S1 and step S2 is added in treatment tank, and plus The zeolite entering 0.01 times of above-mentioned sewage total amount stirs 10min with the rotating speed of 250r/min, after the completion of stirring, stands 2h, through mesh number Accurate filter for 8000 mesh filters, and after then the water that filtration separation obtains being degraded through nitrification tank, denitrification pond, is added to Ozone sterilization pond carries out high degree of sterilization, obtains purified water.
Embodiment three
A kind of sludge drying proposed by the present invention and the method for sewage disposal, comprise the following steps:
S1, waste water is passed in sedimentation basin, adds NaOH to adjust the pH value of waste water to 8.8, add waste water total amount The concentration of 0.08 times of active carbon nanoparticles and 0.004 times is 3% polyacrylamide solution, with the rotating speed stirring of 150r/min 18min, stands 1.5h after the completion of stirring, then carries out preliminary mud-water separation using the filter that mesh number is 200 mesh, respectively To moisture content be 92% mud A and sewage B;
S2, the mud B of gained in step S1 is put in high-speed mixing equipment, add the PH of NaOH conditioning of mud It is worth to 11.5, and is heated to 70 DEG C, in heating, high-speed stirred 15min is carried out with the rotating speed of 700r/min, then insulation standing 3h, is centrifuged 10min using centrifugation apparatus, carries out second mud-water separation, respectively obtain the mud C that moisture content is 70% and sewage D;
S3, the mud C of gained in step S2 is added in evaporation boiler, is heated to 110 DEG C using boiler afterheat, side is heated While being stirred with the rotating speed of 300r/min, after heating 7h, obtain final product dewatered sludge;
S4, the sewage D of gained in the sewage B of gained in step S1 and step S2 is added in treatment tank, and plus The zeolite entering 0.02 times of above-mentioned sewage total amount stirs 15min with the rotating speed of 120r/min, after the completion of stirring, stands 3h, through mesh number Accurate filter for 1250 mesh filters, and after then the water that filtration separation obtains being degraded through nitrification tank, denitrification pond, is added to Ozone sterilization pond carries out high degree of sterilization, obtains purified water.
Example IV
A kind of sludge drying proposed by the present invention and the method for sewage disposal, comprise the following steps:
S1, waste water is passed in sedimentation basin, adds NaOH to adjust the pH value of waste water to 7.5, add waste water total amount The concentration of 0.12 times of active carbon nanoparticles and 0.002 times is 4% polyacrylamide solution, with the rotating speed stirring of 100r/min 22min, stands 2.5h after the completion of stirring, then carries out preliminary mud-water separation using the filter that mesh number is 400 mesh, respectively To moisture content be 85% mud A and sewage B;
S2, the mud B of gained in step S1 is put in high-speed mixing equipment, add the PH of NaOH conditioning of mud It is worth to 10.2, and is heated to 90 DEG C, in heating, high-speed stirred 25min is carried out with the rotating speed of 900r/min, then insulation standing 2h, is centrifuged 6min using centrifugation apparatus, carries out second mud-water separation, respectively obtain the mud C that moisture content is 50% and sewage D;
S3, the mud C of gained in step S2 is added in evaporation boiler, is heated to 90 DEG C using boiler afterheat, side is heated While being stirred with the rotating speed of 500r/min, after heating 6h, obtain final product dewatered sludge;
S4, the sewage D of gained in the sewage B of gained in step S1 and step S2 is added in treatment tank, and plus The zeolite entering 0.04 times of above-mentioned sewage total amount stirs 20min with the rotating speed of 200r/min, after the completion of stirring, stands 1h, through mesh number Accurate filter for 10000 mesh filters, and after then the water that filtration separation obtains being degraded through nitrification tank, denitrification pond, adds Carry out high degree of sterilization to ozone sterilization pond, obtain purified water.
Embodiment five
A kind of sludge drying proposed by the present invention and the method for sewage disposal, comprise the following steps:
S1, waste water is passed in sedimentation basin, adds the concentrated sulfuric acid to adjust the pH value of waste water to 6.5, add waste water total amount The concentration of 0.22 times of active carbon nanoparticles and 0.003 times is 8% polyacrylamide solution, with the rotating speed stirring of 180r/min 15min, stands 1h after the completion of stirring, then carries out preliminary mud-water separation using the filter that mesh number is 300 mesh, respectively obtain Moisture content is 82% mud A and sewage B;
S2, the mud B of gained in step S1 is put in high-speed mixing equipment, add the pH value of concentrated sulfuric acid conditioning of mud To 3.5, and it is heated to 60 DEG C, in heating, high-speed stirred 20min is carried out with the rotating speed of 600r/min, then insulation standing 2.8h, is centrifuged 9min using centrifugation apparatus, carries out second mud-water separation, respectively obtain the mud C that moisture content is 48% and dirt Water D;
S3, the mud C of gained in step S2 is added in evaporation boiler, is heated to 120 DEG C using boiler afterheat, side is heated While being stirred with the rotating speed of 350r/min, after heating 5h, obtain final product dewatered sludge;
S4, the sewage D of gained in the sewage B of gained in step S1 and step S2 is added in treatment tank, and plus The zeolite entering 0.03 times of above-mentioned sewage total amount stirs 12min with the rotating speed of 150r/min, after the completion of stirring, stands 2.5h, through mesh Number filters for the accurate filter of 5000 mesh, after then the water that filtration separation obtains being degraded through nitrification tank, denitrification pond, adds Carry out high degree of sterilization to ozone sterilization pond, obtain purified water.
Mummification after respectively the method for the sludge drying proposing through above-described embodiment one~five and sewage disposal being processed is dirty Mud and purified water, carry out detection and draw following result:
The above, the only present invention preferably specific embodiment, but protection scope of the present invention is not limited thereto, Any those familiar with the art the invention discloses technical scope in, technology according to the present invention scheme and its Inventive concept equivalent or change in addition, all should be included within the scope of the present invention.

Claims (6)

1. a kind of method of sludge drying and sewage disposal is it is characterised in that comprise the following steps:
S1, waste water is passed in sedimentation basin, adds PH conditioning agent to adjust the pH value of waste water to 5~9, add active carbon nanoparticles and Flocculant, stirs 15~25min with the rotating speed of 80~180r/min, stands 1~3h, then using mesh number be after the completion of stirring The filter of 200~500 mesh carries out preliminary mud-water separation, respectively obtains the mud A that moisture content is 80~92% and sewage B;
S2, the mud B of gained in step S1 is put in high-speed mixing equipment, add the pH value of PH conditioning agent conditioning of mud extremely 3.2~4.8 or 9.2~12, and it is heated to 60~100 DEG C, in heating, high-speed stirring is carried out with the rotating speed of 600~1000r/min Mix 15~25min, be then incubated standing 2~3h, be centrifuged 5~10min using centrifugation apparatus, carry out second mud-water separation, point Do not obtain mud C and sewage D that moisture content is 48~72%;
S3, the mud C of gained in step S2 is added in evaporation boiler, is heated to 80~120 DEG C using boiler afterheat, side is heated While being stirred with the rotating speed of 250~500r/min, controlling the heating stirring time, obtaining final product dewatered sludge;
S4, the sewage D of gained in the sewage B of gained in step S1 and step S2 is added in treatment tank, and adds boiling Stone stirs 10~20min with the rotating speed of 120~260r/min, after the completion of stirring, stands 1~3h, is 1250~10000 through mesh number After purpose accurate filter filters, carry out high degree of sterilization, obtain purified water.
2. the method for a kind of sludge drying according to claim 1 and sewage disposal is it is characterised in that in described step S1 Flocculant be 3~8% for concentration polyacrylamide solution.
3. the method for a kind of sludge drying according to claim 1 and sewage disposal is it is characterised in that in described step S1 The addition of active carbon nanoparticles is 0.08~0.22 times of waste water total amount, the addition of flocculant be waste water total amount 0.002~ 0.005 times.
4. a kind of sludge drying according to claim 1 and sewage disposal method it is characterised in that described step S1 and PH conditioning agent in S2 is the concentrated sulfuric acid or NaOH.
5. the method for a kind of sludge drying according to claim 1 and sewage disposal is it is characterised in that in described step S4 Zeolite addition be 0.01~0.04 times of sewage B and sewage D total amount.
6. the method for a kind of sludge drying according to claim 1 and sewage disposal is it is characterised in that in described step S4 High degree of sterilization method the water that referring to, filtration separation is obtained degrade through nitrification tank, denitrification pond after, be added to ozone sterilization pond and enter Row sterilizing.
CN201611003503.XA 2016-11-15 2016-11-15 Sludge drying and sewage treatment method Pending CN106430728A (en)

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Publication number Priority date Publication date Assignee Title
CN108298731A (en) * 2018-03-22 2018-07-20 沈阳建筑大学 A kind of deeply removing arsenic system and device and its dearsenicating method
CN109626795A (en) * 2019-01-18 2019-04-16 宝钢湛江钢铁有限公司 A kind of mud dewatering method containing powdered carbon of sintering device flue gas purification Wastewater from Acid Preparation
CN110921912A (en) * 2019-12-13 2020-03-27 西安润川环保科技有限公司 Method for removing impurities in wastewater
CN111606549A (en) * 2020-05-12 2020-09-01 广东中林建筑园林工程有限公司 Municipal sludge drying method

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