CN106430590A - Two-stage AO (Anoxic Oxic) device based treatment method for high-conductivity wastewater - Google Patents
Two-stage AO (Anoxic Oxic) device based treatment method for high-conductivity wastewater Download PDFInfo
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- CN106430590A CN106430590A CN201611166105.XA CN201611166105A CN106430590A CN 106430590 A CN106430590 A CN 106430590A CN 201611166105 A CN201611166105 A CN 201611166105A CN 106430590 A CN106430590 A CN 106430590A
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F3/00—Biological treatment of water, waste water, or sewage
- C02F3/30—Aerobic and anaerobic processes
Abstract
The invention discloses a two-stage AO (Anoxic Oxic) device based treatment method for high-conductivity wastewater, and belongs to the field of treatment of refractory wastewater. The two-stage AO device based treatment method for the high-conductivity wastewater comprises the following steps of carrying out sewage treatment by utilizing an up-flow sediment and hydrolysis pool and a two-stage A/O (Anoxic/Oxic) biochemical treatment device; carrying out pretreatment on the high-conductivity wastewater, then making the high-conductivity wastewater enter the up-flow sediment and hydrolysis pool, and then making the high-conductivity wastewater enter a first-stage A/O pool; feeding combinative filling materials into a first-stage O pool and a second-stage O pool; enabling the combinative filling materials to realize whole-pool fluidization in the pools through aeration action. According to the two-stage AO device based treatment method for the high-conductivity wastewater, the high-conductivity wastewater is treated by combining the up-flow sediment and hydrolysis pool with two-stage AO; the removal effect of an organic matter difficult to degrade and the resistance of a system to a poison impact can be effectively improved; moreover, a carbon source of the sewage is sufficiently utilized; the extra addition of an organic carbon source is not needed. By using the method provided by the invention, the up-to-standard discharge of COD (Chemical Oxygen Demand), ammonia nitrogen and total nitrogen can be realized; relevant requirements of the Chinese new standard GB16171-2012 are met; the COD of outlet water is lower than that of a conventional process; the load of subsequent advanced treatment can be effectively decreased.
Description
Technical field
The present invention relates to a kind of high conductivity method of wastewater treatment based on two-stage AO device, belong to refractory wastewater
Field.
Background technology
Heavy metal leading indicator refers to hydrargyrum (Hg), cadmium (Cd), lead (Pb), chromium (Cr), arsenic (As), copper (Cu), zinc (Zn), cobalt
(Co), nickel (Ni) etc., they are present among environment with different forms, and migration, accumulation in the environment.With China's industry
Fast development, heavy metal wastewater thereby pollution problem is outstanding day by day, and the pollution rate of river,lake and reservior substrate is up to 80.1%.Its source
Extensively, mining, the industry such as metallurgy, chemical industry are main man-made pollution sources in water body.The approach of solution electroplating wastewater pollution is at all
Electroplating wastewater is carried out with advanced treating, and strengthens the recycling of resource.One side formation has up to standard with environment on a fairly large scale
Plating garden;On the other hand, it is easy to implement the effective treating method making electroplating wastewater qualified discharge.An electroplating industry huge sum of money at present
Belong to ion processing and recovery aspect achieved with breakthrough, but in electroplating wastewater after treatment, the content of Organic substance and nitrogen is past
Toward being unable to qualified discharge.The method solving is the electroplating wastewater after factory processes to be collected unified place carry out depth
Process.
Currently for the advanced treating of heavy metal wastewater thereby, mainly there are chemical precipitation method, oxidation-reduction method, absorption method, ion
Exchange process, membrane separation technique, electrochemistry and biological treatment etc..Wherein Biochemical method has low cost, high efficiency, Yi Guan
Reason, the feature of non-secondary pollution, are conducive to the improvement of ecological environment.Additionally, by being answered based on technology such as engineering, molecular biology
With.Biology can be made to have higher absorption, flocculation, regulation repair ability.Single method is often difficult to obtain preferable effect
Really, simultaneously using two kinds or more of methods, play the length of each technology, faster and better realize reaching and administer heavy metal wastewater thereby
Purpose.
Handling process for process commonly used pretreatment --- biochemical treatment --- advanced treating of electroplating wastewater.Its
In, pretreatment is mainly heavy metal ion and the cyanides such as the nickel removing in waste water, copper, cadmium.Biochemical treatment is mainly in waste water
COD, ammonia nitrogen and total nitrogen.Advanced treating is mainly the Organic substance removing bio-refractory in waste water, so that water outlet COD is met up to standard
Emission request.Traditional A/O technique i.e. interior circulation front establishment method, the ammonia nitrogen in waste water is in O pond through nitrosation
Effect is become nitrate nitrogen with Nitrification by oxidation by nitrobacteria, contains substantial amounts of nitrate nitrogen, enter A pond by internal reflux in the water outlet of O pond, is lacking
Under the conditions of oxygen, using the Organic substance in waste water as electron donor, nitrate nitrogen, as electron acceptor, nitrate nitrogen is reduced to nitrogen to denitrifying bacterium
Gas enters air, completes biological denitrification process, simultaneously the Organic substance in degrading waste water.But the total nitrogen concentration of electroplating wastewater exists
50-60mg/L, COD in 300-500mg/L, if adopt one-level A/O, water outlet total nitrogen in 20-30, COD in 80-90mg/L, and
New standard GB16171-2012 can not be met.
Additionally, electroplating wastewater tail electrical conductivity of water is very high, reach 13000us/cm, chloride ion content reaches 3000 and arrives
4000mg/L.Common one-level AO or A2Activated sludge in O technique is affected larger, activity in Aerobic Pond by high conductivity
Mud is difficult to be formed floccule body, easily runs off.Chloride ion can play promotion enzyme anti-as the nutrient of microorganism in low concentration
The effect that, cell membrane equilibrium should be maintained and adjust Premeabilisation of cells pressure;If excessive concentration, also microorganism can be produced with suppression and poison
Evil effect, and these toxic actions show that microbial cell is dehydrated, and cause cellular plasm to separate;Salting out makes dehydrogenase
Activity reduces;High-salt wastewater salinity is high, leads to waste water density to increase, and activated sludge easily floats loss, thus affecting biology
The clean-up effect of processing system.
Content of the invention
In order to solve the above problems, the invention provides a kind of precipitation hydrolysis of up flow type and two-stage A/O (anoxia/aerobic) are raw
Change processing system enhanced biological nitrogen removal technique, this technique is capable of the qualified discharge of ammonia nitrogen and total nitrogen, meet national new standard
The related request of GB16171-2012, water outlet COD is less than traditional handicraft, can effectively reduce the load of successive depths process.This
Bright employing two-stage AO processes the plating tail water of this high conductivity, on the one hand, the impulsive force suffered by activated sludge is Comparatively speaking
Less, on the other hand, be conducive to the qualified discharge of water outlet.
It should be noted that A/O technique of the present invention refers to anoxia/aerobic process, A pond refers to anoxic pond, and O pond refers to
Oxygen pond.
The high conductivity method of wastewater treatment of the present invention, is to precipitate hydrolysis and two-stage A/O (anoxia/aerobic) using up flow type
Biochemical treatment apparatus carry out sewage disposal;Up flow type precipitation hydrolysis will be entered after high conductivity Wastewater Pretreatment, enter back into one-level
A/O, O pond adds combined stuffing, and filling rate is 30%~50%, makes combined stuffing realize full pond in pond by aeration effect
Fluidisation, the hydraulic detention time that up flow type precipitates hydrolytic tank is 12~18h, and the hydraulic detention time of first, second anoxic pond is 4
~6h, the hydraulic detention time of first, second Aerobic Pond is 8~12h.
In one embodiment, described high conductivity waste water is heavy metal wastewater thereby, such as electroplating wastewater.
In one embodiment, described high conductivity waste water quality parameter:COD 200~400mg/L, ammonia nitrogen 19~
20mg/L, total nitrogen 50~100mg/L, pH 7~9, electrical conductivity 12000~15000us/cm.
In one embodiment, the hydraulic detention time that described up flow type precipitates hydrolytic tank is 15h.
In one embodiment, the hydraulic detention time of described first, second anoxic pond is 5h.
In one embodiment, the hydraulic detention time of described first, second Aerobic Pond is 10h.
In one embodiment, in up flow type precipitation hydrolytic tank, dissolved oxygen is less than 0.1mg/L, the close -300mv of ORP;The
The dissolved oxygen of one anoxic pond is less than 5mg/L;The dissolved oxygen of the first Aerobic Pond controls in 2~5mg/L.
In one embodiment, two grades of A/O water outlets enter sedimentation tank, carry out solid-liquid separation by gravitational settling.
In one embodiment, sludge reflux is to one-level A pond, and control of reflux ratio is 50~100%;In second Aerobic Pond
Nitrification liquid one-level anoxic pond is also back to by dosing pump, control of reflux ratio is 100%~400%.
In one embodiment, described combined stuffing is combined porous ring filler.
In one embodiment, described combined porous ring filler is the basis in soft-filler and semi soft packing
Upper development.Aqueous vapor biomembrane can be made fully to be exchanged for it so that the Organic substance in water obtains efficient process.This filler
Buy in Wuxi Siyang Yuan Quan Environmental Protection Technology Co., Ltd.
In one embodiment, described up flow type precipitation hydrolysis and two-stage A/O (anoxia/aerobic) biochemical treatment apparatus,
Including up flow type precipitation hydrolytic tank, the first anoxic pond, the first Aerobic Pond, transition lattice, the second anoxic pond, the second Aerobic Pond, described
Up flow type precipitation hydrolytic tank connects anoxia cell by outlet pipe, described first anoxic pond, the first Aerobic Pond, transition lattice, second scarce
Oxygen pond, the second Aerobic Pond are sequentially arranged, and are separated with partition wall mutually.
In one embodiment, described up flow type precipitates the slope that hydrolytic tank bottom is provided with tendency pond center, is formed
Bucket, slope is 50 °~60 ° with the angle of horizontal plane.
In one embodiment, it is provided with agitator in described first, second anoxic pond;Described first aerobic lattice, second
It is provided with aeration head in aerobic lattice.
In one embodiment, the water inlet pipe of described sedimentation tank enters in central draft tube with horn mouth form, afterwards
To dirty, under central draft tube, mouth is gradually wealthy mouth, and is provided with reflecting plate, and the reflected plate of current reflects, to pond overhead stream, by top
Clear water collected by water leg, then flows out precipitation hydrolytic tank, and bulky grain mud then enters the sludge bucket of reflecting plate bottom, sludge bucket
The gradient is conducive to the sedimentation of mud mixed liquid for 45 °~60 ° it is ensured that heavy mud puts under in bucket.
In one embodiment, up flow type precipitation hydrolytic tank current flow in pond from bottom to top, can be with submerged fermentation
Liquid produces, and VFA is fully contacted, and promotes to release phosphorus.
The beneficial effects of the present invention is:
1st, add combined stuffing in Aerobic Pond, denitrifying bacterium and nitrifier apposition growth show in filler, increase nitrifier
The decline of the denitrification functions that nitrifier loss leads in activated sludge process, reaction tank biomass concentration is avoided while Biomass
1000~3000mg/L can be improved.The biomembrane that floating stuffing shows has the function of simultaneous nitrification and denitrification, and therefore this is
System has higher denitrification functions and capacity of resisting impact load for high conductivity heavy metal wastewater thereby.
2nd, up flow type precipitates the combination of hydrolytic tank and two-stage AO, can effectively improve and be difficult to degradation of organic substances removal effect and be
System opposing toxic impact, and make full use of sewage carbon source, need not additionally add organic carbon source.
3rd, control process condition, final outflow water water quality are passed through:CODcr<50mg/L;TN<10mg/L;Nitrate nitrogen<8mg/L;
Ammonia nitrogen<0.5mg/L.
Brief description
Fig. 1:High conductivity heavy metal waste water treatment system flow chart based on two-stage AO;
Fig. 2:High conductivity heavy metal waste water treatment process operation schematic diagram based on two-stage AO;In figure labelling is as follows:1 detests
Oxygen pond, 2 one-level anoxic pond, 3 one-level Aerobic Ponds, 4 two grades of anoxic pond, 5 two grades of Aerobic Ponds, 6 second ponds;
Fig. 3:Based on ammonia nitrogen Inlet and outlet water variation tendency during the high conductivity heavy metal containing wastewater treatment of two-stage AO;
Fig. 4:Based on total nitrogen Inlet and outlet water variation tendency during the high conductivity heavy metal containing wastewater treatment of two-stage AO;
Fig. 5:Based on COD Inlet and outlet water variation tendency during the high conductivity heavy metal containing wastewater treatment of two-stage AO.
:Specific embodiment
Following examples are used for the present invention is described, but are not limited to the scope of the present invention.
In following embodiments, experimental technique used if no special instructions, is conventional method.
Material used and reagent etc. in following embodiments, if no special instructions.All commercially middle acquisitions.
Embodiment 1:
As shown in figure 1, the present invention provides up flow type precipitation hydrolytic tank to combine to high conductivity electroplating wastewater with two-stage AO
Processing system flow chart.Carry out in Jingjiang City plating garden, after electroplating wastewater pretreatment, water quality is:COD 200~400mg/
L, ammonia nitrogen 19~20mg/L, total nitrogen 50~100mg/L, pH 7~9, electrical conductivity 12000~15000us/cm.Flow of inlet water is
4L/h.
As shown in Fig. 2 being the high conductivity heavy metal waste water treatment process operation schematic diagram based on two-stage AO.Using upstream
Formula precipitation hydrolysis and two-stage A/O (anoxia/aerobic) biochemical treatment apparatus, include up flow type precipitate hydrolytic tank, the first anoxic pond, the
One Aerobic Pond, transition lattice, the second anoxic pond, the second Aerobic Pond, described up flow type precipitation hydrolytic tank connects anoxia by outlet pipe
Lattice, described first anoxic pond, the first Aerobic Pond, transition lattice, the second anoxic pond, the second Aerobic Pond are sequentially arranged, mutually with partition wall
Separate.Described up flow type precipitates the slope that hydrolytic tank bottom is provided with tendency pond center, forms bucket, the folder of slope and horizontal plane
Angle is 50 °~60 °.It is provided with agitator in described first, second anoxic pond;Setting in described first aerobic lattice, the second aerobic lattice
There is aeration head.The water inlet pipe of described sedimentation tank enters in central draft tube with horn mouth form, afterwards to dirty, central draft tube
Lower mouth is gradually wealthy mouth, and is provided with reflecting plate, and the reflected plate of current reflects, and to pond overhead stream, collects clear water by top water leg, then
Flow out precipitation hydrolytic tank, and bulky grain mud then enters the sludge bucket of reflecting plate bottom, the gradient of sludge bucket is 45 °~60 °, can
Ensure that heavy mud puts under in bucket, be conducive to the sedimentation of mud mixed liquid.Up flow type precipitation hydrolytic tank current in pond from bottom to top
Flowing, can be with the generation of submerged fermentation liquid, and VFA is fully contacted, and promotes to release phosphorus.
The water inlet that up flow type precipitates in hydrolytic tank is from lower to upper, adds combined stuffing, filling rate in precipitation hydrolytic tank
For 30%~50%, dissolved oxygen controls in 0.1mg/L and following;
One-level, two grades of anoxic pond add agitator so that mud is mixed homogeneously with sewage, the hydraulic retention of one-level anoxic pond
Time is 5h, and dissolved oxygen controls in 0.5mg/L;
One-level, two grades of Aerobic Ponds adopt micro-hole aerator, add combined stuffing, and filling rate is 30~50%, Aerobic Pond
Hydraulic detention time is 10h, and dissolved oxygen controls in 2~5mg/L.Wherein, described combined stuffing is combined porous ring filler,
Develop on the basis of soft-filler and semi soft packing and form, buy in the limited public affairs of Wuxi Siyang edge spring environmental protection science and technology
Department.
The Organic substance of part difficult degradation in waste water can be converted into degradable Organic substance by up flow type precipitation hydrolytic tank, carry
The biochemical of high waste water, can reduce the additional carbon dosage in two grades of A ponds, can save operating cost;Activity in one-level A pond
The microorganism of mud under anoxic conditions using Denitrification can be carried out by biochemical Organic substance in waste water, by two grades of Aerobic Pond nitre
The nitrate nitrogen changed in liquid is converted into nitrogen discharge, the COD in degrading waste water simultaneously;The biomembrane that in one-level O pond, combined stuffing shows
Passing through Nitrification by the mineralized nitrogen in waste water with the microorganism in activated sludge is the COD in nitrate nitrogen, and degrading waste water;
There is dissolving oxygen gradient inside biomembrane, therefore synchronous nitration and denitrification can occur inside it, can strengthen in removing waste water
Total nitrogen.
Enter up flow type precipitation hydrolysis after high conductivity Wastewater Pretreatment, enter back into one-level A/O, O pond adds combined stuffing,
Filling rate is 30%~50%, makes combined stuffing realize full pond fluidisation, up flow type precipitation hydrolysis in pond by aeration effect
The hydraulic detention time in pond is 15h, and the hydraulic detention time of first, second anoxic pond is 5h, the waterpower of first, second Aerobic Pond
The time of staying is 10h.To one-level A pond, control of reflux ratio is 80% for sludge reflux;Nitrification liquid in second Aerobic Pond passes through metering
Pump is also back to one-level anoxic pond, and control of reflux ratio is 200%.
As seen in figures 3-5, it is two-stage AO to daily during high conductivity heavy metal containing wastewater treatment ammonia nitrogen, total nitrogen, COD
Variation tendency.
As can be seen from Figure 3:At the domestication initial stage, water outlet ammonia nitrogen is higher than influent ammonia nitrogen, and this is mainly due to nitrobacteria
Growth cycle longer.In the reactor stabilization sub stage, the meansigma methodss of water outlet ammonia nitrogen are 0.88mg/L, far below national GB21900-
2008 discharge standards.
As can be seen from Figure 4:The stable water outlet of total nitrogen, in 15mg/L, reaches national GB21900-2008 discharge standard.
Two-stage AO is preferable to the denitrification effect of high conductivity waste water.
As can be seen from Figure 5:Due to industrial characteristic, influent COD fluctuation is larger, and average influent COD is
302mg/L, average COD removal is 73.12%.At the initial stage of reactor domestication, water outlet COD fluctuation is larger, and value is higher, processes
Efficiency is poor.Stablizing with reactor, the clearance of COD gradually rises, and COD water outlet, in 50mg/L, reaches country
GB21900-2008 discharge standard.
Final outflow water water quality:CODcr<50mg/L;TN<10mg/L;Nitrate nitrogen<8mg/L;Ammonia nitrogen<0.5mg/L.
Additionally, inventor also attempts employing suspended biological filler.Table 1 is respectively uses suspended biological filler and combination type many
The indices of orifice ring filler water outlet in reactor the 30th day.The COD water outlet of suspended biological filler is 90mg/L, the row of not reaching
Put standard, and combined stuffing COD water outlet 50mg/L.
The indices of the table 1 suspended biological filler and combined porous ring filler water outlet in reactor the 30th day
Although the present invention is open as above with preferred embodiment, it is not limited to the present invention, any is familiar with this skill
The people of art, without departing from the spirit and scope of the present invention, can do various changes and modification, therefore the protection model of the present invention
Enclosing should be by being defined that claims are defined.
Claims (10)
1. a kind of high conductivity method of wastewater treatment is it is characterised in that methods described is to precipitate hydrolysis and two-stage using up flow type
A/O (anoxia/aerobic) biochemical treatment apparatus carry out sewage disposal;Up flow type precipitation water will be entered after high conductivity Wastewater Pretreatment
Solution, enters back into one-level A/O, O pond adds combined stuffing, and filling rate is 30%~50%, makes combined stuffing by aeration effect
Realize full pond fluidisation in pond, the hydraulic detention time that up flow type precipitates hydrolytic tank is 12~18h, first, second anoxic pond
Hydraulic detention time is 4~6h, and the hydraulic detention time of first, second Aerobic Pond is 8~12h.
2. method according to claim 1 is it is characterised in that described high conductivity waste water is heavy metal wastewater thereby, such as electric
Waste electroplating.
3. method according to claim 1 is less than 0.1mg/L it is characterised in that up flow type precipitates dissolved oxygen in hydrolytic tank,
Close-the 300mv of ORP;The dissolved oxygen of the first anoxic pond is less than 5mg/L;The dissolved oxygen of the first Aerobic Pond controls in 2~5mg/L.
4. method according to claim 1 is it is characterised in that sludge reflux is to one-level A pond, control of reflux ratio 50~
100%;Nitrification liquid in second Aerobic Pond is also back to one-level anoxic pond by dosing pump, control of reflux ratio 100%~
400%.
5. method according to claim 1 is it is characterised in that described high conductivity waste water quality parameter:COD 200~
400mg/L, ammonia nitrogen 19~20mg/L, total nitrogen 50~100mg/L, pH 7~9, electrical conductivity 12000~15000us/cm.
6. method according to claim 1 is it is characterised in that described combined stuffing is combined porous ring filler.
7. method according to claim 1 is it is characterised in that described up flow type precipitation hydrolyzes and two-stage A/O (anoxia/good
Oxygen) biochemical treatment apparatus, including up flow type precipitation hydrolytic tank, the first anoxic pond, the first Aerobic Pond, transition lattice, the second anoxic pond,
Second Aerobic Pond, described up flow type precipitation hydrolytic tank passes through outlet pipe connection anoxia cell, described first anoxic pond, first aerobic
Pond, transition lattice, the second anoxic pond, the second Aerobic Pond are sequentially arranged, and are separated with partition wall mutually.
8. method according to claim 7 is it is characterised in that the water inlet pipe of described sedimentation tank is with the entrance of horn mouth form
In heart guide shell, afterwards to dirty, under central draft tube, mouth is gradually wealthy mouth, and is provided with reflecting plate, and the reflected plate of current reflects, to
Pond overhead stream, collects clear water by top water leg, then flows out precipitation hydrolytic tank, and bulky grain mud then enters reflecting plate bottom
Sludge bucket, the gradient of sludge bucket is 45 °~60 °.
9. method according to claim 1 is it is characterised in that the hydraulic detention time that described up flow type precipitates hydrolytic tank is
15h.
10. method according to claim 1 is it is characterised in that the hydraulic detention time of described first, second anoxic pond is
5h.
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Cited By (3)
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CN109293170A (en) * | 2018-11-22 | 2019-02-01 | 深圳瑞赛环保科技有限公司 | A kind of nickel-contained wastewater treatment device and method |
CN110104893A (en) * | 2019-05-29 | 2019-08-09 | 临邑禹王植物蛋白有限公司 | A kind of sewage water treatment method and system for use in carrying using AO technique drop total nitrogen |
CN114906927A (en) * | 2022-05-27 | 2022-08-16 | 厦门市绿得清新材料科技有限公司 | Method for removing nitrate nitrogen in electroplating wastewater |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN109293170A (en) * | 2018-11-22 | 2019-02-01 | 深圳瑞赛环保科技有限公司 | A kind of nickel-contained wastewater treatment device and method |
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CN110104893A (en) * | 2019-05-29 | 2019-08-09 | 临邑禹王植物蛋白有限公司 | A kind of sewage water treatment method and system for use in carrying using AO technique drop total nitrogen |
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