CN106430376A - Comprehensive sewage treatment agent and preparation method thereof - Google Patents
Comprehensive sewage treatment agent and preparation method thereof Download PDFInfo
- Publication number
- CN106430376A CN106430376A CN201611221913.1A CN201611221913A CN106430376A CN 106430376 A CN106430376 A CN 106430376A CN 201611221913 A CN201611221913 A CN 201611221913A CN 106430376 A CN106430376 A CN 106430376A
- Authority
- CN
- China
- Prior art keywords
- parts
- sewage treatment
- juice
- comprehensive sewage
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention discloses a comprehensive sewage treatment agent. The comprehensive sewage treatment agent is prepared from the following raw materials in parts by weight: 2-6 parts of pulverized coal ash, 12-28 parts of pomelo peels, 20-34 parts of attapulgite, 3-8 parts of sodium chloride, 8-20 parts of modified starch, 0.5-4 parts of zinc oxide, 0.2-1.5 parts of monoethanolamine, 1-3 parts of chitosan, 2-8 parts of zinc sulfate and 2.5-6 parts of birch juice. The invention further discloses a preparation method of the agent. According to the comprehensive sewage treatment agent and the preparation method thereof, the source of the raw materials is wide, the preparation process is simple, and the production cost is low, so that the agent is suitable for being industrially produced on a large scale; all ingredients of the agent are in synergism, the prepared agent is free of pollution during season change, the efficiency of contaminant removal is high, treated water reaches national level-I emission standards, the use effect is good, and the applicable range is wide.
Description
Technical field
The present invention relates to sewage treatment area, specifically a kind of comprehensive sewage treatment drug.
Background technology
In more than 30 years of reform and opening-up, Re-search on Urbanization quickly grows, sewage disposal scale expanding day.City dirt at present
Water treatment capacity reaches more than 100,000,000 cubic metre, and sewage treatment plant reaches more than 3000 seats, and estimating in 5 years to increase Sewage Plant nearly 2000
Seat.Sewage includes sanitary sewage and trade effluent, and with cities and towns quantity and the rapid growth of population, many cities and towns are advised due to environment
Draw and environmental conservation delayed development, sanitary sewage discharged in a large number, the water pollution of surrounding area and body eutrophication phenomenon
Seriously, people need to process sanitary sewage.Sewage-treating agent is the chemical agent that commonly uses in field of sewage, by sewage
The materials such as the impurity in water, Organic substance are separated by inorganic agent, realize the purification of water quality, but existing sewage-treating agent needs to add
Enter substantial amounts of chemical agent, this can bring about the secondary pollution of water quality, this just brings inconvenience for processing water.
Content of the invention
It is an object of the invention to provide a kind of comprehensive sewage treatment drug, to solve proposition in above-mentioned background technology
Problem.
For achieving the above object, the present invention provides following technical scheme：
A kind of comprehensive sewage treatment drug, is made up of according to weight portion following raw material：Flyash 2-6 part, pomelo peel 12-
28 parts, attapulgite 20-34 part, Sodium Chloride 3-8 part, modified starch 8-20 part, zinc oxide 0.5-4 part, monoethanolamine 0.2-1.5
Part, shitosan 1-3 part, zinc sulfate 2-8 part and Betula juice 2.5-6 part, modified starch is starch in the sulphuric acid of 0.2mol/L
15-30 minute is soaked, then deionized water is washed till neutrality and dries and obtains.
As the further scheme of the present invention：Modified starch adopts corn starch, potato starch, tapioca, Semen Tritici aestivi
One or several mixture of starch.
As the further scheme of the present invention：Shitosan adopts water-soluble chitosan, and Betula juice is using Betula platyphylla Suk. juice, red
Birch juice or one or several mixture of black birch juice.
The preparation method of the comprehensive sewage treatment drug, comprises the following steps that：
Step one, pomelo peel is boiled 1-2.5 hour under 60-85 degree Celsius, then gained liquid is separated with solid, liquid
For Fructus Citri grandiss water, solid is dried and is ground into the powder of 20-30 mesh, obtain pomelo peel powder；
Step 2, by pomelo peel powder, monoethanolamine and shitosan add gross weight 5-15 times deionized water in and
Stirring, divides 3-6 equivalent to add Sodium Chloride, zinc oxide and zinc sulfate while stirring, is added completely into 120-210rpm after finishing
Rotating speed stirring 15-45 minute, obtain the first mixed solution；
Step 3, flyash, attapulgite and modified starch pulverizing is 0.05-0.8mm to granularity, obtains the first mixing
Thing；
Step 4, the first mixture and Fructus Citri grandiss water are added in the first mixed solution, with 150- under 35-54 degree Celsius
The rotating speed stirring 18-30 minute of 360rpm, then Betula juice is added thereto to, stir, you can obtain finished product.
As the further scheme of the present invention：The whipping temp of step 2 is 50-75 degree Celsius.
Compared with prior art, the invention has the beneficial effects as follows：The raw material sources of the present invention are extensive, preparation process is simple,
Low production cost, it is adaptable to large-scale industrial production；In the present invention, each component plays synergism, and the medicament of preparation is to season
Do not pollute, the efficiency high of pollutant is removed, the water quality after process reaches national grade one discharge standard, and using effect is good, be suitable for
Scope is wide.
Specific embodiment
With reference to specific embodiment, the technical scheme of this patent is described in more detail.
Embodiment 1
A kind of comprehensive sewage treatment drug, is made up of according to weight portion following raw material：2 parts of flyash, 12 parts of pomelo peel,
20 parts of attapulgite, 3 parts of Sodium Chloride, 8 parts of modified starch, 0.5 part of zinc oxide, 0.2 part of monoethanolamine, 1 part of shitosan, zinc sulfate
2 parts and 2.5 parts of Betula juice, modified starch is soaked 15 minutes in the sulphuric acid of 0.2mol/L for starch, then is washed with deionized water
To neutral and dry and obtain.Modified starch adopts potato starch.
The preparation method of the comprehensive sewage treatment drug, comprises the following steps that：
Step one, pomelo peel is boiled 1.5 hours under 65 degrees Celsius, then gained liquid is separated with solid, and liquid is Fructus Citri grandiss
Sub- water, solid is dried and is ground into the powder of 20 mesh, obtains pomelo peel powder；
Step 2, pomelo peel powder, monoethanolamine and shitosan is added in the deionized water of 7 times of gross weight and stirs
Mix, divide 4 equivalent to add Sodium Chloride, zinc oxide and zinc sulfate while stirring, be added completely into after finishing and stirred with the rotating speed of 140rpm
Mix 18 minutes, obtain the first mixed solution；
Step 3, flyash, attapulgite and modified starch pulverizing is 0.08mm to granularity, obtains the first mixture；
Step 4, the first mixture and Fructus Citri grandiss water are added in the first mixed solution, with 150rpm's under 35 degrees Celsius
Rotating speed is stirred 18 minutes, then is added thereto to Betula juice, is stirred, you can obtain finished product.
Embodiment 2
A kind of comprehensive sewage treatment drug, is made up of according to weight portion following raw material：3 parts of flyash, 15 parts of pomelo peel,
24 parts of attapulgite, 5 parts of Sodium Chloride, 11 parts of modified starch, 1.5 parts of zinc oxide, 0.7 part of monoethanolamine, 1.5 parts of shitosan, sulfur
5 parts of sour zinc and 4 parts of Betula juice, modified starch is soaked 20 minutes in the sulphuric acid of 0.2mol/L for starch, then deionized water
It is washed till neutrality and dries and obtains.Shitosan adopts water-soluble chitosan, and Betula juice is using Betula platyphylla Suk. juice and black birch juice
Mixture.
The preparation method of the comprehensive sewage treatment drug, comprises the following steps that：
Step one, pomelo peel is boiled 2 hours under 68 degrees Celsius, then gained liquid is separated with solid, and liquid is Fructus Citri grandiss
Water, solid is dried and is ground into the powder of 24 mesh, obtains pomelo peel powder；
Step 2, pomelo peel powder, monoethanolamine and shitosan is added in the deionized water of 8 times of gross weight and 56
Stir under degree Celsius, divide 4 equivalent to add Sodium Chloride, zinc oxide and zinc sulfate while stirring, be added completely into after finishing with
The rotating speed of 140rpm is stirred 20 minutes, obtains the first mixed solution；
Step 3, flyash, attapulgite and modified starch pulverizing is 0.15mm to granularity, obtains the first mixture；
Step 4, the first mixture and Fructus Citri grandiss water are added in the first mixed solution, with 180rpm's under 42 degrees Celsius
Rotating speed is stirred 21 minutes, then is added thereto to Betula juice, is stirred, you can obtain finished product.
Embodiment 3
A kind of comprehensive sewage treatment drug, is made up of according to weight portion following raw material：4.5 parts of flyash, pomelo peel 21
Part, 28 parts of attapulgite, 6 parts of Sodium Chloride, 16 parts of modified starch, 2 parts of zinc oxide, 0.9 part of monoethanolamine, 2.5 parts of shitosan, sulfur
7 parts of sour zinc and 5 parts of Betula juice, modified starch is soaked 24 minutes in the sulphuric acid of 0.2mol/L for starch, then deionized water
It is washed till neutrality and dries and obtains.Modified starch is using corn starch and the mixture of wheaten starch.Shitosan adopts water solublity
Shitosan, Betula juice adopts black birch juice.
The preparation method of the comprehensive sewage treatment drug, comprises the following steps that：
Step one, pomelo peel is boiled 2 hours under 74 degrees Celsius, then gained liquid is separated with solid, and liquid is Fructus Citri grandiss
Water, solid is dried and is ground into the powder of 28 mesh, obtains pomelo peel powder；
Step 2, pomelo peel powder, monoethanolamine and shitosan is added in the deionized water of 12 times of gross weight and stirs
Mix, divide 5 equivalent to add Sodium Chloride, zinc oxide and zinc sulfate while stirring, be added completely into after finishing and stirred with the rotating speed of 170rpm
Mix 30 minutes, obtain the first mixed solution；
Step 3, flyash, attapulgite and modified starch pulverizing is 0.4mm to granularity, obtains the first mixture；
Step 4, the first mixture and Fructus Citri grandiss water are added in the first mixed solution, with 280rpm's under 48 degrees Celsius
Rotating speed is stirred 26 minutes, then is added thereto to Betula juice, is stirred, you can obtain finished product.
Embodiment 4
A kind of comprehensive sewage treatment drug, is made up of according to weight portion following raw material：6 parts of flyash, 27 parts of pomelo peel,
32 parts of attapulgite, 8 parts of Sodium Chloride, 20 parts of modified starch, 4 parts of zinc oxide, 1.3 parts of monoethanolamine, 3 parts of shitosan, zinc sulfate 7
Part and 6 parts of Betula juice, modified starch is soaked 28 minutes in the sulphuric acid of 0.2mol/L for starch, then during deionized water is washed till
Property and drying is obtained.Modified starch is using the mixture of corn starch, potato starch, tapioca and wheaten starch.Shell
Polysaccharide adopts water-soluble chitosan, and Betula juice is using the mixture of Betula platyphylla Suk. juice, red birch juice and black birch juice.
The preparation method of the comprehensive sewage treatment drug, comprises the following steps that：
Step one, pomelo peel is boiled 2.5 hours under 82 degrees Celsius, then gained liquid is separated with solid, and liquid is Fructus Citri grandiss
Sub- water, solid is dried and is ground into the powder of 30 mesh, obtains pomelo peel powder；
Step 2, by pomelo peel powder, monoethanolamine and shitosan add 13 times of gross weight deionized water in and
Stir under 66 degrees Celsius, divide 5 equivalent to add Sodium Chloride, zinc oxide and zinc sulfate while stirring, be added completely into after finishing with
The rotating speed of 200rpm is stirred 38 minutes, obtains the first mixed solution；
Step 3, flyash, attapulgite and modified starch pulverizing is 0.5mm to granularity, obtains the first mixture；
Step 4, the first mixture and Fructus Citri grandiss water are added in the first mixed solution, with 320rpm's under 48 degrees Celsius
Rotating speed is stirred 28 minutes, then is added thereto to Betula juice, is stirred, you can obtain finished product.
Comparative example
Except Betula juice is not contained, remaining component of comparative example 1 and preparation method are all same as Example 2.
The product of embodiment 1-4, the product of comparative example 1 and existing product are put in sanitary sewage with the amount of 10mg/L,
Indices in sanitary sewage are determined, test result is shown in Table 1.
Table 1
| COD(10mg/g) | Ammonia-nitrogen content (10mg/L) | Float (10mg/L) | |
| Sanitary sewage | 32567.4 | 12483.5 | 4583.5 |
| Embodiment 1 | 34.8 | 8.4 | 21.3 |
| Embodiment 2 | 41.3 | 12.6 | 12.7 |
| Embodiment 3 | 32.7 | 11.7 | 15.4 |
| Embodiment 4 | 28.4 | 9.5 | 17.8 |
| Comparative example 1 | 687.3 | 348.7 | 187.4 |
| Existing product | 87.6 | 24.8 | 65.9 |
From table 1 it follows that the using effect of embodiment 1-4 product is reached better than product and the existing product of comparative example 1
Primary standard to national sewage discharge.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of spirit or essential attributes without departing substantially from the present invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit is required rather than described above is limited, it is intended that all in the implication and scope of the equivalency of claim by falling
Change is included in the present invention.
Moreover, it will be appreciated that although this specification is been described by according to embodiment, not each embodiment is only wrapped
Containing an independent technical scheme, this narrating mode of description is only that those skilled in the art should for clarity
Using description as an entirety, the technical scheme in each embodiment can also form those skilled in the art through appropriately combined
Understandable other embodiment.
Claims (5)
1. a kind of comprehensive sewage treatment drug, it is characterised in that be made up of according to weight portion following raw material：Flyash 2-6 part,
Pomelo peel 12-28 part, attapulgite 20-34 part, Sodium Chloride 3-8 part, modified starch 8-20 part, zinc oxide 0.5-4 part, monoethanol
Amine 0.2-1.5 part, shitosan 1-3 part, zinc sulfate 2-8 part and Betula juice 2.5-6 part, modified starch is starch in 0.2mol/L
Sulphuric acid in soak 15-30 minute, then deionized water is washed till neutrality and dries and obtain.
2. comprehensive sewage treatment drug according to claim 1, it is characterised in that the modified starch is formed sediment using Semen Maydiss
Powder, potato starch, tapioca, one or several mixture of wheaten starch.
3. comprehensive sewage treatment drug according to claim 1 and 2, it is characterised in that the shitosan is using water-soluble
Property shitosan, Betula juice using Betula platyphylla Suk. juice, red birch juice or black birch juice one or several mixture.
4. a kind of preparation method of the comprehensive sewage treatment drug as described in claim 1-3 is arbitrary, it is characterised in that concrete
Step is as follows：
Step one, pomelo peel is boiled 1-2.5 hour under 60-85 degree Celsius, then gained liquid is separated with solid, and liquid is Fructus Citri grandiss
Sub- water, solid is dried and is ground into the powder of 20-30 mesh, obtains pomelo peel powder；
Step 2, pomelo peel powder, monoethanolamine and shitosan is added in the deionized water of gross weight 5-15 times and stirs,
3-6 equivalent is divided to add Sodium Chloride, zinc oxide and zinc sulfate, the rotating speed being added completely into after finishing with 120-210rpm while stirring
Stirring 15-45 minute, obtain the first mixed solution；
Step 3, flyash, attapulgite and modified starch pulverizing is 0.05-0.8mm to granularity, obtains the first mixture；
Step 4, the first mixture and Fructus Citri grandiss water are added in the first mixed solution, with 150-360rpm under 35-54 degree Celsius
Rotating speed stirring 18-30 minute, then be added thereto to Betula juice, stir, you can obtain finished product.
5. the preparation method of comprehensive sewage treatment drug according to claim 4, it is characterised in that the step 2
Whipping temp is 50-75 degree Celsius.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611221913.1A CN106430376A (en) | 2016-12-27 | 2016-12-27 | Comprehensive sewage treatment agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611221913.1A CN106430376A (en) | 2016-12-27 | 2016-12-27 | Comprehensive sewage treatment agent and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106430376A true CN106430376A (en) | 2017-02-22 |
Family
ID=58215876
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611221913.1A Pending CN106430376A (en) | 2016-12-27 | 2016-12-27 | Comprehensive sewage treatment agent and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106430376A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108892188A (en) * | 2018-07-26 | 2018-11-27 | 赣州市翔义科技有限公司 | A kind of medicament and preparation method thereof for treatment of Organic Wastewater |
| CN112007617A (en) * | 2019-05-29 | 2020-12-01 | 西南科技大学 | Preparation method of shaddock peel/attapulgite composite material |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104445455A (en) * | 2014-11-03 | 2015-03-25 | 芜湖市祥荣食品有限公司 | Activated zinc oxide antibacterial blue-green algae treatment agent and preparation method thereof |
| CN104876312A (en) * | 2015-05-15 | 2015-09-02 | 王英英 | Sewage treatment agent prepared from fruit peels and preparation process thereof |
| CN105016494A (en) * | 2015-07-30 | 2015-11-04 | 陈朝民 | Composite water treatment agent |
-
2016
- 2016-12-27 CN CN201611221913.1A patent/CN106430376A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104445455A (en) * | 2014-11-03 | 2015-03-25 | 芜湖市祥荣食品有限公司 | Activated zinc oxide antibacterial blue-green algae treatment agent and preparation method thereof |
| CN104876312A (en) * | 2015-05-15 | 2015-09-02 | 王英英 | Sewage treatment agent prepared from fruit peels and preparation process thereof |
| CN105016494A (en) * | 2015-07-30 | 2015-11-04 | 陈朝民 | Composite water treatment agent |
Non-Patent Citations (4)
| Title |
|---|
| 刘心恕: "《农产品加工工艺学》", 31 May 1997, 中国农业出版社 * |
| 李文英: "负载Fe/Al/Na的不同吸附剂对焦化废水中有机污染物质吸附实验的研究", 《山西化工》 * |
| 汪多仁: "《绿色降解化学品》", 31 January 2008, 科学技术文献出版社 * |
| 肇启明 等: "柑橘属果皮用于废水除臭的研究", 《贵州师范大学学报(自然科学版)》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108892188A (en) * | 2018-07-26 | 2018-11-27 | 赣州市翔义科技有限公司 | A kind of medicament and preparation method thereof for treatment of Organic Wastewater |
| CN112007617A (en) * | 2019-05-29 | 2020-12-01 | 西南科技大学 | Preparation method of shaddock peel/attapulgite composite material |
| CN112007617B (en) * | 2019-05-29 | 2022-03-04 | 西南科技大学 | Preparation method of shaddock peel/attapulgite composite material |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106430504A (en) | Domestic sewage phosphate removing agent | |
| CN104828883A (en) | Bentonite-containing blue-green alga treating agent and preparation method thereof | |
| CN107117695A (en) | It is a kind of for environmentally friendly medicament of Industrial Waste Water Treatments and preparation method thereof | |
| CN105858736B (en) | A kind of compound sewage inorganic agent and preparation method thereof based on natural crystal and biogas residue | |
| CN104891607A (en) | Shell powder treating agent for cyanobacteria and preparation method of shell powder treating agent | |
| CN107128999A (en) | It is a kind of for medicament of municipal sewage treatment and preparation method thereof | |
| CN106430376A (en) | Comprehensive sewage treatment agent and preparation method thereof | |
| CN106564972A (en) | Domestic sewage purification agent and preparation method thereof | |
| CN106745388A (en) | A kind of dyeing and printing sewage treatment agent and preparation method thereof | |
| CN105948339A (en) | Treatment process of aquaculture waste water | |
| CN105540703A (en) | Composite efficient sewage treatment agent based on natural ore and preparing method thereof | |
| CN107512744A (en) | A kind of inorganic agent for sanitary sewage and preparation method thereof | |
| CN106430370A (en) | High-efficiency sewage treatment agent and preparation method thereof | |
| CN106477653A (en) | A kind of for processing medicament of sanitary sewage and preparation method thereof | |
| CN106745387A (en) | A kind of domestic sewage treating compound and preparation method thereof | |
| CN104604948A (en) | Blue algae treating agent prepared from kelp and preparation method thereof | |
| CN106380059A (en) | High-efficiency sludge treating agent and preparation method thereof | |
| CN106629888A (en) | Efficient sewage treatment agent based on xanthan gum and preparation method of efficient sewage treatment agent | |
| CN103232079B (en) | Formula and preparation method of natural mineral dyeing and printing industry wastewater treatment agent | |
| CN106669616A (en) | Heavy metal adsorption material prepared from corn cob and preparation method thereof | |
| CN108751275A (en) | A kind of environmentally friendly domestic sewage treating compound | |
| CN107585981A (en) | A kind of urban sewer sludge curing agent and preparation method thereof | |
| CN106430360A (en) | Efficient sewage treatment agent based on xanthan gum and preparation method thereof | |
| CN106395942A (en) | Efficient sewage treating agent specially used for sanitary sewage and preparing method thereof | |
| CN106587199A (en) | Cleaning agent used for sewage comprehensive treatment and preparing method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170222 |
|
| WD01 | Invention patent application deemed withdrawn after publication |