CN106398338A - Special high temperature self-dry insulating enamel and preparation method thereof - Google Patents
Special high temperature self-dry insulating enamel and preparation method thereof Download PDFInfo
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- CN106398338A CN106398338A CN201611138667.3A CN201611138667A CN106398338A CN 106398338 A CN106398338 A CN 106398338A CN 201611138667 A CN201611138667 A CN 201611138667A CN 106398338 A CN106398338 A CN 106398338A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
- C08G59/44—Amides
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/54—Silicon-containing compounds
- C08K5/544—Silicon-containing compounds containing nitrogen
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B3/00—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
- H01B3/02—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of inorganic substances
- H01B3/12—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of inorganic substances ceramics
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B3/00—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
- H01B3/18—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances
- H01B3/30—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes
- H01B3/40—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes epoxy resins
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2265—Oxides; Hydroxides of metals of iron
- C08K2003/2272—Ferric oxide (Fe2O3)
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Inorganic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Ceramic Engineering (AREA)
- Paints Or Removers (AREA)
Abstract
The invention relates to the field of coatings, and especially relates to a special high temperature self-dry insulating enamel and a preparation method thereof. The enamel comprises an E06-4 paint component and a curing agent component, and the paint component comprises, by weight, 10-25 parts of titanium dioxide, 3-8 parts of iron oxide red, 8-15 parts of white glaze, 15-70 parts of HG-43 modified organosilicone resin, 3-7 parts of epoxy resin and 0.5-5 parts of a KH-550 assistant; the KH-550 assistant contains 20-45 parts of a KH-550 coupling agent and 55-80 parts of xylene; and the E06-4 curing agent comprises, by weight, 40-65 parts of 650 polyamide resin, 20-40 parts of xylene and 15-20 parts of butanol. The enamel has the advantages of no flashover, pull or breakdown at a high temperature of 400 DEG C, guaranteeing of good insulating property of the surface of a large device, and guaranteeing of the running reliability of the device and the safety of personnel.
Description
Technical field
The present invention relates to paint field, more particularly, to Special high-temperature are from the dry enamel paint and preparation method thereof that insulate.
Background technology
Insulated paint is made up of paint base, solvent or diluent and auxiliary material, has electrical insulating property, heat resistance and chemically-resistant
Property, and there is dicoration.
Electromechanical equipment, steelmaking equipment, Large Electric Furnace, petrochemical equipment, had both been required using paint high temperature resistant, had required resistance to again
High voltage, occurs without flashover under high voltages, pulls out electricity, do not puncture, also have from dryness simultaneously, corrosion-resistant, antirust characteristic, this
Plant paint needs to meet multiple use simultaneously.
Paint base refers to the film forming matter painting, and paint heat resistance depends on the temperature classification of paint base, and high temperature resistant paint needs
Select the high film forming matter of temperature classification, carry out chemical reaction at high temperature, rely on the chemical group crosslinking of itself, generate reticulate body
Structure, such as organic siliconresin, but this kind of resin cannot be from dry, main equipment cannot carry out drying molten heating admittedly in baker again
Change, therefore this kind of high temperature of the uncomfortable cooperation of this resin is from dry insulation enamel paint.
Main equipment can only select to carry out chemical reaction under atmospheric environment, generates netted result, have excellent physics,
Chemistry and electric property.
Content of the invention
The purpose of invention：In order to provide a kind of more preferable Special high-temperature of effect from the dry enamel paint and preparation method thereof that insulate, tool
Body purpose is shown in the multiple substantial technological effects being embodied as part.
In order to reach as above purpose, the present invention adopts the following technical scheme that：
Scheme one：
Special high-temperature does insulation enamel paint certainly it is characterised in that comprising paint component and curing agent component,
Paint component：Comprise the material of following weight portion, rutile titanium white powder 10-25 part, iron oxide 3-8 part, white glaze 8-15 part,
Epoxy resin 3-7 part, KH-550 auxiliary agent 0.5-5 part；Comprise in KH-550 auxiliary agent therein 20-45 part KH-550 coupling agent and
The dimethylbenzene of 55-80 part；
Curing agent component：Comprise the material that following weight is divided, 650 polyamide 40-65 parts, dimethylbenzene 20-40 part, butanol
15-20 part.
The further technical scheme of the present invention is, also comprises acid organic siliconresin in described paint component, its weight portion
For 15-70 part.
Scheme two：
Special high-temperature is from the preparation method of dry insulation enamel paint it is characterised in that using filling a prescription as above, preparation method is such as
Under, add acid organic siliconresin, titanium dioxide, iron oxide red, white glaze according to this toward inside tank of sizing mixing, then start mixer slow
Stirring, properly increases mixing speed after stirring, material is tuned into mill base, enters horizontal skin grinder and is ground, and reaches thin
Degree below 30um；
Mill base through grinding enters sizes mixing in tank, starts stirring and adds remaining epoxy resin, KH-550 coupling agent, uses diformazan
Benzene：Butanol compares 6 according to weight:The viscosity of paint is adjusted to 25-35 second/painting -4, more than 23 degrees Celsius, filter and package by 4.
Using the present invention of as above technical scheme, have the advantages that with respect to prior art：This product is at 400 DEG C
Not flashover under high temperature, does not pull out electricity, do not puncture it is ensured that main equipment surface there is good insulating properties it is ensured that equipment run can
Personal safety by property and personnel.
Specific embodiment
Below embodiments of the invention are illustrated, embodiment is not construed as limiting the invention：
Comprise paint component：It comprises the material of following weight portion, titanium dioxide 10-25 part, iron oxide red 3-8 part, white glaze 8-15
Part, epoxy resin 3-7 part, KH-550 auxiliary agent 0.5-5 part；The KH-550 comprising 20-45 part in KH-550 auxiliary agent therein is coupled
Agent and the dimethylbenzene of 55-80 part；Also comprise curing agent component：It comprises the material of following weight fraction, 650 polyamides
40-65 part, dimethylbenzene 20-40 part, butanol 15-20 part.Acid organic siliconresin is also comprised, its weight portion in described paint component
For 15-70 part.Special high-temperature is filled a prescription from the preparation method of dry insulation enamel paint as above it is characterised in that adopting, preparation side
Method is as follows, adds acid organic siliconresin, titanium dioxide, iron oxide red, white glaze according to this, then start mixer toward inside tank of sizing mixing
It is slowly stirred, after stirring, properly increases mixing speed, material is tuned into mill base, enter skin grinder and be ground, reach thin
Degree below 30um；Mill base through grinding enters in paint mixing tank, starts stirring and adds remaining epoxy resin, KH-550 to be coupled
Agent, uses dimethylbenzene：Butanol compares 6 according to weight:The viscosity of paint is adjusted to 25-35 second/painting -4 by 4, more than 23 degrees Celsius, bag filter
Dress.
Special high-temperature should meet following index from dry insulation enamel paint：
Under atmospheric environment, cannot realize carrying out crosslinking under normal temperature condition from one pack system, generate network structure it is necessary to introduce
Another component, the chemical group of bi-component reacts to each other under atmospheric environment, generates network structure.
1053 organic siliconresins are the best thermosetting resins of heat resistance in insulating materials, because it is hot setting tree
Fat, is not suitable for doing the paint of normal temperature cure.
From modified organic siliconresin, group can be solidified at normal temperatures using curing agent, makes self-drying paint, this patent
From polyamide as curing agent, amide group and epoxy reaction are crosslinked, and modified organic silicone resin heat resistance is than organic
Silicones is lower slightly, but still belongs to H level heat proof material, and modified organic siliconresin increased adhesive force, improves intensity.
Auxiliary material includes coloring pigment and extender pigment and auxiliary agent composition, and the principle of selection must have heat resistance, this product
Product can be made into pink, white paint, because selecting coloring pigment titanium dioxide, its heat resistance and insulating properties all relatively good, titanium
White powder is divided into rutile and two kinds of anatase titanium dioxide again, and the chemical stability of rutile, heat resistance are all good than sharp titanium, the fusing point of rutile
Up to 1850 degrees Celsius, dielectric constant 114, and sharp titanium, at 1200-1300 degree Celsius, converts to rutile, the dielectric of anatase titanium dioxide
Constant is 48, lower than rutile.
Iron oxide red is inert pigment, and optical characteristics and chemical characteristic are stable, and tinting strength, tinting power is only second to carbon black, heat-resist,
Up to 1200 degrees Celsius, ferrite red impurity is few, and purity is high, so using ferrite red as coloring pigment.Carbon black impact is absolutely
Edge, therefore reduces as far as possible and uses.
In order to increase the viscosity of paint, increase the electrical strength of paint film, prevent paint precipitation, increase the mechanicalness of paint
Can, select multiplex extender pigment such as silica flour, powdered whiting, wollastonite in powder etc., all undesirable, introduced electromagnetism material later
White glaze（1130-1200 degree Celsius of fusing point）, heat-resist, there is good insulating properties, sponginess again, be difficult to precipitate, in formula
In also comprise coupling agent KH-550, to increase the adhesive force of paint film.
This product not flashover under 400 degrees Celsius of high temperature, does not pull out electricity, do not puncture it is ensured that main equipment surface have good
Good insulating properties is it is ensured that the safety of equipment and personnel.
In a creative way, each effect above is individually present moreover it is possible to complete the combination of the above results with a nested structure.
It should be noted that multiple schemes that this patent provides comprise the basic scheme of itself, separate, not mutually
Restriction, but it can also be mutually combined in the case of not conflicting, and reach multiple effects and jointly realize.
General principle, principal character and the advantages of the present invention of the present invention have been shown and described above.The technology of this area
Personnel, it should be recognized that the present invention is not restricted to the described embodiments, simply illustrate this described in above-described embodiment and specification
Bright principle, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, these changes
Both fall within claimed scope with improving.
Claims (3)
1. Special high-temperature is from dry insulation enamel paint it is characterised in that comprising E06-4 paint component and curing agent component.
Paint component, comprises the material of following weight portion, titanium dioxide 10-25 part, iron oxide 3-8 part, white glaze 8-15 part, asphalt mixtures modified by epoxy resin
Fat 3-7 part, KH-550 auxiliary agent 0.5-5 part；Wherein KH-550 auxiliary agent comprises KH-550 coupling agent and 55-80 part two of 20-45 part
Toluene；
Curing agent component, comprises the material of following weight fraction：650 polyamide 40-65 parts, dimethylbenzene 20-40 part, butanol
15-20 part.
2. Special high-temperature as claimed in claim 1 is from dry insulation enamel paint it is characterised in that also comprising acid in described paint component
Property organic siliconresin, its weight portion be 15-70 part.
3. Special high-temperature is from the preparation method of dry insulation enamel paint it is characterised in that using joining as described in claim 1 or 2
Side, preparation method is as follows, adds acid organic siliconresin, titanium dioxide, iron oxide red, white glaze according to this, then toward inside tank of sizing mixing
Start mixer to be slowly stirred, after stirring, properly increase mixing speed, material is tuned into mill base, enter skin grinder and ground
Mill, reaches below fineness 30um；
Mill base through grinding enters in paint mixing tank, starts stirring and adds remaining epoxy resin, KH-550 coupling agent, uses diformazan
Benzene：Butanol is according to volume ratio 6:The viscosity of paint is adjusted to 25-35 second/painting -4, more than 23 degrees Celsius, filter and package by 4.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611138667.3A CN106398338B (en) | 2016-12-12 | 2016-12-12 | Special high-temperature self-drying insulating enamel and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201611138667.3A CN106398338B (en) | 2016-12-12 | 2016-12-12 | Special high-temperature self-drying insulating enamel and preparation method thereof |
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| CN106398338A true CN106398338A (en) | 2017-02-15 |
| CN106398338B CN106398338B (en) | 2020-01-21 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108753128A (en) * | 2018-06-21 | 2018-11-06 | 天津市津海特种涂料装饰有限公司 | A kind of superhigh temperature resistant is from dry high temperature lacquer |
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| CN102443339A (en) * | 2010-10-13 | 2012-05-09 | 中国科学院金属研究所 | Ultrahigh-hardness organic protection coating and preparation method thereof |
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2016
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| CN105419409A (en) * | 2015-11-23 | 2016-03-23 | 沈阳黎明航空发动机(集团)有限责任公司 | High-temperature-fuel-gas-washing-resistant coating and preparation method and application thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108753128A (en) * | 2018-06-21 | 2018-11-06 | 天津市津海特种涂料装饰有限公司 | A kind of superhigh temperature resistant is from dry high temperature lacquer |
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