CN106395763B - A kind of no pollution dust collector type catalyst draws dress and screening plant and its application method - Google Patents

A kind of no pollution dust collector type catalyst draws dress and screening plant and its application method Download PDF

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Publication number
CN106395763B
CN106395763B CN201610738533.9A CN201610738533A CN106395763B CN 106395763 B CN106395763 B CN 106395763B CN 201610738533 A CN201610738533 A CN 201610738533A CN 106395763 B CN106395763 B CN 106395763B
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China
Prior art keywords
catalyst
scrubbing tower
flexible pipe
groove
screening
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CN201610738533.9A
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CN106395763A (en
Inventor
史万敬
路八智
张曦文
谢成
薛勇
程华花
苏青天
宋�莹
常培珑
陆铮
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Jinchuan Group Co Ltd
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Jinchuan Group Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/69Sulfur trioxide; Sulfuric acid
    • C01B17/74Preparation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B07SEPARATING SOLIDS FROM SOLIDS; SORTING
    • B07BSEPARATING SOLIDS FROM SOLIDS BY SIEVING, SCREENING, SIFTING OR BY USING GAS CURRENTS; SEPARATING BY OTHER DRY METHODS APPLICABLE TO BULK MATERIAL, e.g. LOOSE ARTICLES FIT TO BE HANDLED LIKE BULK MATERIAL
    • B07B7/00Selective separation of solid materials carried by, or dispersed in, gas currents
    • B07B7/06Selective separation of solid materials carried by, or dispersed in, gas currents by impingement against sieves

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Cleaning By Liquid Or Steam (AREA)
  • Treating Waste Gases (AREA)

Abstract

The invention discloses a kind of no pollution dust collector type catalyst to draw dress and screening plant and its application method, including connection flexible pipe, screening chuck, fans entrance flexible pipe, air-introduced machine, scrubbing tower, drawing and pulling type cleaning groove, clear liquid groove, washing pump, power distribution cabinet composition, and the portable pull bar of supporting setting, clip, suction inlet, mounting flange, packed control valve, control valve, atomizer, exhaust outlet plus water nozzle, overfall, upper liquid pipe, return valve, communicating pipe, apocenosis mouth, base;Operating personnel adjust the device, pack position according to live physical location by connection flexible pipe, successively open washing pump, air-introduced machine, catalyst is after suction inlet, connection flexible pipe, screening chuck screening, intact catalyst prepares backfill after pack flange pack, little particle catalyst is after air-introduced machine enters scrubbing tower washing, clear liquid recycles, and dust enters drawing and pulling type cleaning groove with cleaning solution.The present invention is simple to operate, can make to draw dress, the efficiency of screening catalyst greatly improves.

Description

A kind of no pollution dust collector type catalyst draws dress and screening plant and its application method
Technical field
Technical field
The invention belongs to chemical technology field, be related to converter catalyst in a kind of gas washing in SA production draws dress and screening plant, Dress and screening plant and its application method are drawn more particularly to a kind of no pollution dust collector type catalyst.
Background technology
Phenomena such as hardened, poisoning, efflorescence, failure can be produced after sulfate system conversion catalyst long-term use, cause conversion ratio Decline.Therefore, annual annual test, which need to carry out catalyst, draws dress, screening and backfill.At present, catalyst draws dress and uses pure manual work, that is, turns After change device hot blow, cold blowing terminate, open each layer manhole and carry out Temperature fall, temperature is down to 45 DEG C or so after about 24h, draws dress personnel In full rig catalyst is slowly shoveled into woven bag with spade into each layer of converter after protective articles, another bag bag proposes manhole Outside, pour into sieve to be sieved, packed, prepare backfill.Because temperature height, dust content are big in converter, draw dress personnel and often make It must climb out of that manhole is ventilative, cooling after industry half an hour, drawing to reinstall to fill out about needs 20 people continuously to work round the clock 7 days could to complete, work Industry environment is poor, it is low to draw dress efficiency.Draw dress process and want supporting and carry out safeguard measure, prevent that catalyst from drenching with rain failure.
The content of the invention
Present invention aims at draw the problem of dress operating environment is poor, efficiency is low for catalyst, there is provided a kind of no pollution is inhaled Dirt device formula catalyst draws dress and screening plant.
The present invention adopts the following technical scheme that:A kind of no pollution dust collector type catalyst draws dress and screening plant, including base, Base is provided with scrubbing tower, and scrubbing tower top is provided with exhaust outlet, and wash tower bottoms configure one and are used to collect taking out for dust precipitation Pull-type cleaning groove, and overfall is furnished with drawing and pulling type cleaning groove top portion, communicate, wash between drawing and pulling type cleaning groove top and scrubbing tower Wash and communicated between tower top and its other clear liquid groove top set by communicating pipe, clear liquid groove is provided with washing pump, washing pump output End is connected with liquid pipe, the top that upper liquid pipe is passed in scrubbing tower, and the upper liquid pipe passed in scrubbing tower is provided with atomizer, clearly Liquid bath top is communicated with the upper liquid pipe being exposed to outside scrubbing tower by pipeline section, and scrubbing tower bottom is provided with air-introduced machine and exported with air-introduced machine End communicates, and air-introduced machine input is connected with fans entrance flexible pipe, and fans entrance flexible pipe communicates with screening chuck bottom, sieves chuck Top is connected with flexible pipe, and the entrance point of flexible pipe is provided with the catalyst suction inlet that caliber reduces.
Further, flexible pipe is provided with portable pull bar and clip.
Further, the bottom for sieving chuck is connected with packed control valve by mounting flange.
Further, flexible pipe and fans entrance flexible pipe use reinforced plastics flexible pipe.
Further, screening chuck uses closed netted cylinder.
Further, air-introduced machine is provided with the adjustable distribution box of supply frequency.
Further, air-introduced machine output end is provided with control valve.
Further, clear liquid groove top end is communicated with the upper liquid pipe being exposed to outside scrubbing tower by pipeline section, is provided with back in the pipeline section Flow valve.
Further, the bottom of clear liquid groove is provided with the apocenosis mouth for discharging cleaning solution.
Another object of the present invention is to provide a kind of method for drawing dress and screening using said apparatus progress catalyst, specifically Comprise the following steps:
A. after converter cold blowing terminates, carry out catalyst using the device and draw and pretend industry, before operation, operating personnel are first to washing Wash water filling in tower, open washing pump, the alignment of catalyst suction inlet is drawn at dress, closes packed control valve;
B. be then turned on air-introduced machine catalyst through catalyst suction inlet enter flexible pipe in fall into screening chuck sieved, it is intact Catalyst sinks under gravity, after catalyst is sieving accumulation certain thickness in chuck, opens packed control valve, intact Catalyst prepares backfill after pack regulating valve pack;Little particle crushes catalyst and taken out by air-introduced machine entrance negative pressure by mesh screens Enter in scrubbing tower;
C. circulation fluid crushes catalyst to the little particle being pumped into scrubbing tower by atomizer atomisation and washed, small Particle Breakage catalyst, because of broken collision, interception and cohesion between catalyst grit and drop, is broken when by vaporific space Broken catalyst grit settles out into drawing and pulling type with drop and clears up groove, and drawing and pulling type cleaning groove upper clear supernate enters scrubbing tower and carries out one Secondary precipitation, the clear liquid in scrubbing tower enter clear liquid groove after secondary precipitation by communicating pipe;
D. enter the clear liquid in clear liquid groove through upper liquid pipe to enter in scrubbing tower, through atomizer atomisation and broken catalyst Grit contacts, and recycles.
The beneficial effects of the invention are as follows:After converter cold blowing terminates, catalyst can be carried out using the device of the present invention immediately and drawn Pretend industry;Before operation, the first water filling into scrubbing tower of operating personnel, washing pump is opened, standing is outside manhole by suction inlet Alignment is drawn at dress, opens air-introduced machine, catalyst after suction inlet, connection flexible pipe, screening chuck screening, through pack adjust by intact catalyst Prepare backfill after saving valve pack, crush catalyst after air-introduced machine is pumped into scrubbing tower washing, recirculated water is sprayed into mist by atomizer Shape, when by vaporific space, because of the collision between grit and drop, interception and cohesion, grit settles out with drop Groove is cleared up into drawing and pulling type, clear liquid returns to clear liquid groove through secondary precipitation and recycled;The present invention is compact-sized, is readily transported, pacifies Dress, operation, simple to operate, the efficiency for can make to draw dress, sieving catalyst greatly improves, and reduces the cost of overhaul and uses;Package unit is in Confined space is run, and to operating environment, composing environment does not pollute;Operating personnel's quantity is at utmost reduced, it is strong to reduce hand labor Degree, raises labour efficiency.
Brief description of the drawings
Fig. 1 is the device structure schematic diagram of the present invention.
In figure:The portable pull bars of 1-, 2- clips, 3- catalyst suction inlets, 4- flexible pipes, 5- screening chucks, 6- mounting flanges, 7- Packed control valve, 8- fans entrance flexible pipes, 9- air-introduced machines, 10- control valves, 11- scrubbing towers, 12- atomizers, 13- exhausts Mouthful, 14- adds water nozzle, 15- drawing and pulling types cleaning groove, 16- overfalls, the upper liquid pipes of 17-, 18- return valves, 19- communicating pipes, 20- clear liquids Groove, 21- washing pumps, 22- apocenosis mouths, 23- power distribution cabinets, 24- bases.
Embodiment
A kind of no pollution dust collector type catalyst draws dress and screening plant, including base 24, base 24 are provided with scrubbing tower 11, The top of scrubbing tower 11 is provided with exhaust outlet 13, and the bottom of scrubbing tower 11 configures a drawing and pulling type cleaning groove for being used to collect dust precipitation 15, and overfall 16 is furnished with the top of drawing and pulling type cleaning groove 15, communicate, wash between the drawing and pulling type cleaning top of groove 15 and scrubbing tower 11 Wash and communicated between the top of tower 11 and its other top of clear liquid groove 20 set by communicating pipe 19, clear liquid groove 20 is provided with washing pump, washes Wash the output end of pump 21 and be connected with liquid pipe 17, the top that upper liquid pipe 17 is passed in scrubbing tower 11, the upper liquid passed in scrubbing tower 11 Pipe 17 is provided with atomizer 12, and the top of clear liquid groove 20 is communicated with the upper liquid pipe 17 being exposed to outside scrubbing tower 11 by pipeline section, washing The bottom of tower 11 is provided with air-introduced machine and communicated with air-introduced machine output end, and the input of air-introduced machine 9 is connected with fans entrance flexible pipe 8, blower fan Inlet tubes 8 communicate with screening chuck 5 bottom, and screening chuck 5 top is connected with flexible pipe 4, and the entrance point of flexible pipe contracts provided with caliber Small catalyst suction inlet 3.Flexible pipe 4 is provided with portable pull bar 1 and clip 2.The bottom of screening chuck is connected by mounting flange 6 Marsupial cartridge control valve 7.Flexible pipe 4 and fans entrance flexible pipe 8 use reinforced plastics flexible pipe, it is easy to operation during position move, will Whole catalyst are extracted out.The top of clear liquid groove 20 is communicated with the upper liquid pipe 17 being exposed to outside scrubbing tower 11 by pipeline section, is provided with the pipeline section Return valve 18.The bottom of clear liquid groove 20 is provided with the apocenosis mouth 22 for discharging cleaning solution, is easy to the outer row of cleaning solution.Before equipment is driven Packed control valve 7 is closed, after catalyst is sieving accumulation certain thickness in chuck 5, pressure improves at catalyst in chuck, on catalyst Portion's space pressure is constant, and vacuum is internally formed in chuck, ensures that catalyst can be extracted out continuously, now opens packed control valve 7, can Carry out catalyst recovery.Sieve chuck 5 and use closed netted cylinder, little particle catalyst passes through net by the entrance negative pressure of air-introduced machine 9 Shape screen cloth enters follow-up equipment, and intact catalyst is packed by packed control valve 7 under gravity.What scrubbing tower 11 was collected The cleaning solution that dust is sprayed by atomizer 12 carries out dedusting recovery.Plant running, first open washing pump 21, after drive air-introduced machine 9, The output end of air-introduced machine 9 is provided with control valve 10, and air-introduced machine 9 is provided with the adjustable distribution box 23 of supply frequency, using in distribution box 23 Supply frequency tunable characteristic, to motor carry out stepless time adjustment with realize suction pressure adjust, fan outlet can also be passed through Control valve 10, to adjust the change of soakage.The circulation fluid of scrubbing tower 11 is cleared up under groove 15 and scrubbing tower 11 by drawing and pulling type Portion carries out two-stage precipitation to cleaning solution, and clear liquid enters clear liquid groove 20 by communicating pipe 19 in scrubbing tower 11.When washing pump 21 passes through When upper liquid pipe 17 is to the conveying cleaning solution of scrubbing tower 11, return valve 18 can be passed through and control pump discharge.Drawing and pulling type cleaning groove 15 is easy to receive Collect dust precipitation, and overfall 16 is furnished with groove top portion, the clear liquid in groove can be flowed back in scrubbing tower, and the cleaning solution in circulating slot is again By secondary precipitation, clear liquid returns to clear liquid groove 20, then is returned to by washing pump 21 by upper liquid pipe 17 in scrubbing tower 11 and continue to spray.
Embodiment
Before operation, operating personnel need to put the device well according to job site position, and catalyst suction inlet 3 is soft with being connected Pipe 4 is connected by clip 2, and material bag is connected with packed control valve.Screening agent set is determined by fans entrance flexible pipe 8 Position.After being installed in place, external power source is introduced into power distribution cabinet 23 as device general supply nearby.Then by adding water nozzle 14 to washing Water filling in tower 11 is washed, liquid, when liquid level, which reaches washing pump 21, runs height, is closed by communicating pipe 19 and the UNICOM of clear liquid groove 20 Water is added to open pump, cleaning solution by atomizer 12 by upper liquid pipe 17 to tower, being sprayed.After ready, operator Catalyst suction inlet 3 is aligned by member need to draw dress catalyst, close packed control valve 7, open air-introduced machine 9, the negative pressure air quantity of air-introduced machine 9 can Control valve 10 is adjusted according to the length of suction inlet distance means;Entered when catalyst by means of negative pressure quickly through connection flexible pipe 4 After sieving the screening of chuck 5, pack regulating valve 7 is slowly opened, intact catalyst prepares backfill after pack, and broken catalyst is through drawing Blower fan 9 is pumped into scrubbing tower 11 and contacted with the cleaning solution that atomizer 12 sprays, and dust is settled out to enter with cleaning solution and taken out Pull-type cleaning groove 15, one-level washing clear liquid clear up the overfall 16 at the top of groove 15 by drawing and pulling type first, then in scrubbed tower 11 After secondary precipitation, two level washs clear liquid and enters clear liquid groove 20 through communicating pipe 19, is recycled by washing pump 21.Work as equipment During deactivation, cleaning solution is discharged by apocenosis mouth 22.

Claims (10)

1. a kind of no pollution dust collector type catalyst draws dress and screening plant, including base(24), base(24)It is provided with scrubbing tower (11), scrubbing tower(11)Top is provided with exhaust outlet(13), it is characterised in that:Scrubbing tower(11)Bottom configures one and is used to collect powder The drawing and pulling type cleaning groove of dirt precipitation(15), and clear up groove in drawing and pulling type(15)Top is furnished with overfall(16), drawing and pulling type cleaning groove (15)Top and scrubbing tower(11)Between communicate, scrubbing tower(11)Top and its other clear liquid groove set(20)Pass through between top Communicating pipe(19)Communicate, clear liquid groove(20)Provided with washing pump(21), washing pump(21)Output end is connected with liquid pipe(17), upper liquid Pipe(17)Pass to scrubbing tower(11)Interior top, passes to scrubbing tower(11)Interior upper liquid pipe(17)It is provided with atomizer(12), Clear liquid groove(20)Top is with being exposed to scrubbing tower(11)Outer upper liquid pipe(17)Communicated by pipeline section, scrubbing tower(11)Bottom, which is provided with, draws Blower fan(9)And and air-introduced machine(9)Output end communicates, air-introduced machine(9)Input is connected with fans entrance flexible pipe(8), fans entrance Flexible pipe(8)With sieving chuck(5)Bottom communicates, and sieves chuck(5)Top is connected with flexible pipe(4), the entrance point of flexible pipe, which is provided with, manages The catalyst suction inlet that footpath reduces(3).
2. one kind draws dress using a kind of no pollution dust collector type catalyst as claimed in claim 1 and screening plant, its feature exist In:Flexible pipe(4)It is provided with portable pull bar(1)And clip(2).
3. one kind draws dress using a kind of no pollution dust collector type catalyst as claimed in claim 1 and screening plant, its feature exist In:Sieve chuck(5)Bottom pass through mounting flange(6)It is connected with packed control valve(7).
4. one kind draws dress using a kind of no pollution dust collector type catalyst as claimed in claim 1 and screening plant, its feature exist In:Flexible pipe(4)With fans entrance flexible pipe(8)Using reinforced plastics flexible pipe.
5. one kind draws dress using a kind of no pollution dust collector type catalyst as claimed in claim 1 and screening plant, its feature exist In:Sieve chuck(5)Using closed netted cylinder.
6. one kind draws dress using a kind of no pollution dust collector type catalyst as claimed in claim 1 and screening plant, its feature exist In:Air-introduced machine(9)Provided with the adjustable distribution box of supply frequency(23).
7. one kind draws dress using a kind of no pollution dust collector type catalyst as claimed in claim 1 and screening plant, its feature exist In:Air-introduced machine(9)Output end is provided with control valve(10).
8. one kind draws dress using a kind of no pollution dust collector type catalyst as claimed in claim 1 and screening plant, its feature exist In:Clear liquid groove(20)Top is with being exposed to scrubbing tower(11)Outer upper liquid pipe(17)Communicated by pipeline section, backflow is provided with the pipeline section Valve(18).
9. one kind draws dress using a kind of no pollution dust collector type catalyst as claimed in claim 1 and screening plant, its feature exist In:Clear liquid groove(20)Bottom be provided with by cleaning solution discharge apocenosis mouth(22).
A kind of 10. application method that dress and screening are drawn using device as claimed in claim 1 progress catalyst, it is characterised in that:Tool Body comprises the following steps:
A. after converter cold blowing terminates, drawn using device progress catalyst and pretend industry, before operation, operating personnel are first to scrubbing tower (11)Interior water filling, open washing pump(21), by catalyst suction inlet(3)Alignment is drawn at dress, closes packed control valve(7);
B. it is then turned on air-introduced machine(9)Catalyst is through catalyst suction inlet(3)Into flexible pipe(4)In fall into screening chuck(5)Sieved Point, intact catalyst sinks under gravity, when catalyst is in screening chuck(5)After interior accumulation certain thickness, open packed Control valve(7), intact catalyst is through packing regulating valve(7)Prepare backfill after pack;Little particle crushes catalyst and relies on air-introduced machine(9) Entrance negative pressure is pumped into scrubbing tower by mesh screens(11)It is interior;
C. circulation fluid passes through atomizer(12)Atomisation is to being pumped into scrubbing tower(11)Interior little particle crushes catalyst and washed Wash, little particle crushes catalyst when by vaporific space, because broken collision, interception and cohesion between catalyst grit and drop is made With broken catalyst grit is settled out into drawing and pulling type with drop clears up groove(15), drawing and pulling type cleaning groove(15)Upper clear supernate is entered Enter scrubbing tower(11)Carry out primary sedimentation, scrubbing tower(11)In clear liquid pass through communicating pipe after secondary precipitation(19)Into clear liquid Groove(20);
D. clear liquid groove is entered(20)In clear liquid through upper liquid pipe(17)Into scrubbing tower(11)It is middle through atomizer(12)It is sprayed into mist Shape contacts with broken catalyst grit, recycles.
CN201610738533.9A 2016-08-29 2016-08-29 A kind of no pollution dust collector type catalyst draws dress and screening plant and its application method Active CN106395763B (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201711288U (en) * 2010-06-29 2011-01-19 贵阳中化开磷化肥有限公司 Sulfuric acid catalyst sieving machine
CN203599040U (en) * 2013-12-02 2014-05-21 湖北新洋丰肥业股份有限公司 Movable catalytic agent rotary screen with automatic feeding and dust collecting device
CN203621079U (en) * 2013-11-14 2014-06-04 湖北祥云(集团)化工股份有限公司 Catalytic agent recovery device
CN105664717A (en) * 2016-03-09 2016-06-15 南京中电环保科技有限公司 Desulphurization, denitration and dust removal integrated treatment process of exhaust gas

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20040178124A1 (en) * 2003-03-11 2004-09-16 Ke Liu Hydrogen desulfurizer for hydrocarbon feeds with separated adsorption and catalyst material
KR20100082271A (en) * 2009-01-08 2010-07-16 (주)국 제 앤 텍 Heavy water treatment device supporting ozone and cocatalyst composition

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201711288U (en) * 2010-06-29 2011-01-19 贵阳中化开磷化肥有限公司 Sulfuric acid catalyst sieving machine
CN203621079U (en) * 2013-11-14 2014-06-04 湖北祥云(集团)化工股份有限公司 Catalytic agent recovery device
CN203599040U (en) * 2013-12-02 2014-05-21 湖北新洋丰肥业股份有限公司 Movable catalytic agent rotary screen with automatic feeding and dust collecting device
CN105664717A (en) * 2016-03-09 2016-06-15 南京中电环保科技有限公司 Desulphurization, denitration and dust removal integrated treatment process of exhaust gas

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