CN106389286A - 一种具有美容和抗菌作用的超临界蜂胶酊剂配方及工艺 - Google Patents
一种具有美容和抗菌作用的超临界蜂胶酊剂配方及工艺 Download PDFInfo
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Abstract
本发明涉及一种利用超临界流体萃取技术,提取高纯度、高浓度和无有机溶剂残留的天然蜂胶,能够有效的脱出蜂胶中的致敏成分,减少过敏效应,并按蜂胶酊剂的配方为:浓度为2%的超临界蜂胶液5~30%,芦荟浸泡油0.1~0.5%,金盏花精油0.1~0.5%,玫瑰精油0.1~0.5%,薰衣草精油0.1~0.5%,乙醇溶液定容至100%,单位为体积百分比(v/v)。科学配置成具有治疗皮肤过敏、促进伤口愈合、延缓皮肤衰老、抗菌杀菌、促进细胞再生的化妆品或者药物喷剂等的外用酊剂。制成蜂胶酊剂具有良好的可溶性,不含重金属和杂质。
Description
技术领域
本发明涉及一种利用超临界流体萃取技术,提取高纯度、高浓度有机溶剂残留的天然物质蜂胶,作为主原料与芦荟浸泡油、金盏花精油、玫瑰精油和薰衣草精油,科学配制成具有美白活血作用的外用酊剂。
发明背景
蜂胶使天然的美容物质,即可以内服,也可以外敷,经常食用蜂胶能够全面调节器官功能,促进血液循环,防止皮肤病变,分解色斑、减少皱纹、防冻防裂、止痒止痛和看感染等作用。
芦荟浸泡油是保持皮肤水润、抗菌消炎作用的精油,具有保湿、防皱纹、延缓皮肤衰老、抗菌消炎,长期使用还能防止皮肤过敏、促进伤口愈合,用于各种皮肤外伤的治疗和晒后修复。
金盏花精油是滋养皮肤、抗炎、促进细胞再生作用的精油,具有治疗各种皮肤病和问题皮肤,对于痘痘肌肤有良好的治疗效果,治理发言,消除暗疮,防止疤痕产生与毛孔粗大,对敏感肌肤具有镇定舒缓效果,改善敏感性肤质,滋润特别干燥的皮肤。
玫瑰精油是抗菌杀菌、作用的精油,具有预防传染病、治疗皮肤、调节内分泌、促进人体生理和心理活动,长期使用玫瑰精油,能使人精神舒适、愉悦、惬意、缓解焦虑、抑郁、压力,帮助睡眠,促进新陈代谢、细胞再生、血液循环,使人健康、美丽,对老化皮肤有极佳的回春效果。
薰衣草精油是止血生肤、美容养颜作用的精油,具有消除面上的痤疮留下的痕迹,长期使用可以使肌肤上的痤疮消除,使肌肤润滑。
传统的蜂胶提取方法为乙醇提取法,也就是将蜂胶原胶冷冻粉碎后,使用高浓度的乙醇惊跑一段时间后,经过过滤、除杂达至使用标准,超临界蜂胶是使用超临界工艺制作而成,能有效的清除蜂胶中的额致敏成分,减少过敏效应。
发明内容
本发明提出一种具有美容和抗菌作用的超临界蜂胶酊剂配方,超临界蜂胶本身就具有良好的美容养颜的作用,又加入了芦荟精华、金盏花精油和薰衣草精油制成了具有美容和抗菌作用的蜂胶外用产品蜂胶酊剂,这种蜂胶酊剂具有良好的可溶性,不含重金属和其他杂质,颜色鲜亮纯净透明,
该蜂胶酊剂的配方为:浓度为2%的超临界蜂胶液5~30%,芦荟浸泡油0.1~0.5%,金盏花精油0.1~0.5%,玫瑰精油0.1~0.5%,薰衣草精油0.1~0.5%,乙醇溶液定容至100%,单位为体积百分比(v/v)。
该蜂胶酊剂的生产方法如下:
制备超临界蜂胶提取物:将蜂胶原料冷冻粉碎至40目放置萃取釜内,将CO2气体通入放有蜂胶原料的萃取釜中,调节萃取釜的温度至40~60℃,压力至35~40MPa,溶有蜂胶的超临界CO2气体由萃取釜流入分离釜Ⅰ与分离釜Ⅱ中,调节分离釜Ⅰ的温度至50~60℃,压力至10~11MPa,分离釜Ⅱ的温度至30~40℃,压力至5~6MPa,通过分步降低压力并且改变温度,使蜂胶可安其性质分布从CO2中析出并从分离釜底部排出,CO2气体从分离釜顶部排出,进行下一个循环;
制备芦荟浸泡油:将芦荟洗干净,去皮削成芦荟块,之后将芦荟块晒干放入干净干燥的广口瓶中压实,再将浸泡油倒入放有芦荟干的广口瓶中,放置一段时间就能得芦荟浸泡油;
制备金盏花精油:将金盏花冷冻粉碎置50目放置萃取釜内,将CO2气体通入放有金盏花的萃取釜中,调节萃取釜温度至40~60℃,压力至30~35MPa,溶有金盏花的超临界CO2气体由萃取釜流入分离釜中,调节分离釜的温度至45~60℃,压力至10~11MPa,金盏花精油从分离釜底部排出,CO2气体分离釜顶部排出,进行下一个循环;
制备玫瑰精油:将玫瑰花冷冻粉碎至50目放置萃取釜内,将CO2气体通入放有玫瑰花的萃取釜中,调节萃取釜温度至40~60℃,压力至30~35MPa,溶有玫瑰花的超临界CO2气体由萃取釜流入分离釜中,调节分离釜的温度至45~60℃,压力至10~11MPa,玫瑰精油从分离釜底部排出,CO2气体分离釜顶部排出,进行下一个循环;
制备薰衣草精油:薰衣草精油可以利用传统的蒸馏法从薰衣草中提取;
制备浓度为2%的超临界蜂胶液:取超临界蜂胶提取物,并与乙醇溶液充分混合,得到浓度为2%的超临界蜂胶液;
按体积比称取浓度为2%的超临界蜂胶液、芦荟浸泡油、金盏花精油、玫瑰精油和薰衣草精油,取出2%超临界蜂胶液与芦荟浸泡油、金盏花精油、玫瑰精油、薰衣草精油充分混合,最后加入乙醇溶液,利用超声混合均匀,从而得到纯净均匀的超临界蜂胶酊剂。
所述的乙醇溶液为浓度为75%的乙醇溶液。
本发明的配方是以五种容易得到的纯天然的材料,并显示出杰出的保养皮肤、延缓衰老和和杀菌作用。
本发明的蜂胶酊剂可以用于治疗皮肤过敏、促进伤口愈合、延缓皮肤衰老和杀菌的化妆品或者药物喷剂。
附图说明
图1本发明的工艺流程图。
具体实施方式
实施案例1,按体积比称取浓度为2%的超临界蜂胶液、芦荟浸泡油、金盏花精油、玫瑰精油和薰衣草精油,取出2%超临界蜂胶液25%与芦荟浸泡油0.1%、金盏花精油0.1%、玫瑰精油0.1%、薰衣草精油0.1%充分混合,最后加入73.6%乙醇,利用超声混合均匀,从而得到纯净均匀的超临界蜂胶酊剂。
实施案例2,按体积比称取浓度为2%的超临界蜂胶液、芦荟浸泡油、金盏花精油、玫瑰精油和薰衣草精油,取出2%超临界蜂胶液22%与芦荟浸泡油0.2%、金盏花精油0.2%、玫瑰精油0.2%、薰衣草精油0.2%充分混合,最后加入77.2%乙醇,利用超声混合均匀,从而得到纯净均匀的超临界蜂胶酊剂。
实施案例3,按体积比称取浓度为2%的超临界蜂胶液、芦荟浸泡油、金盏花精油、玫瑰精油和薰衣草精油,取出2%超临界蜂胶液20%与芦荟浸泡油0.3%、金盏花精油0.3%、玫瑰精油0.3%、薰衣草精油0.3%充分混合,最后加入78.8%乙醇,利用超声混合均匀,从而得到纯净均匀的超临界蜂胶酊剂。
实施案例4,按体积比称取浓度为2%的超临界蜂胶液、芦荟浸泡油、金盏花精油、玫瑰精油和薰衣草精油,取出2%超临界蜂胶液18%与芦荟浸泡油0.4%、金盏花精油0.4%、玫瑰精油0.4%、薰衣草精油0.4%充分混合,最后加入80.4%乙醇,利用超声混合均匀,从而得到纯净均匀的超临界蜂胶酊剂。
实施案例5,按体积比称取浓度为2%的超临界蜂胶液、芦荟浸泡油、金盏花精油、玫瑰精油和薰衣草精油,取出2%超临界蜂胶液15%与芦荟浸泡油0.5%、金盏花精油0.5%、玫瑰精油0.5%、薰衣草精油0.5%充分混合,最后加入83%乙醇,利用超声混合均匀,从而得到纯净均匀的超临界蜂胶酊剂。
以上所述,仅为本发明较佳的具体实施方式,但本发明的保护范围并不局限于此,任何熟悉本技术领域的技术人员在本发明揭露的技术范围内,可轻易想至的变化或替换,都应涵盖在本发明的保护范围内。因此,本发明的保护范围应该以权利要求书的保护范围为准。
Claims (4)
1.该蜂胶酊剂的配方为:浓度为2%的超临界蜂胶液5~30%,芦荟浸泡油0.1~0.5%,金盏花精油0.1~0.5%,玫瑰精油0.1~0.5%,薰衣草精油0.1~0.5%,乙醇溶液定容至100%,单位为体积百分比(v/v)。
2.如权利要求1所述,本发明提出一种具有美容和抗菌作用的超临界蜂胶酊剂配方,其特征在于,蜂胶、金盏花和玫瑰精油的加工均可采用超临界CO2流体萃取方式萃取,芦荟浸泡油可通过将芦荟晒干之后加入浸泡油放置一段时间后获得,薰衣草精油可采用传统的蒸馏法提取。
3.如权利要求1所述,本发明提出一种具有美容和抗菌作用的超临界蜂胶酊剂配方,其特征在于,乙醇溶液为浓度为75%的乙醇溶液。
4.如权利要求1所述,本发明提出一种具有美容和抗菌作用的超临界蜂胶酊剂配方,其特征在于,本发明的配方是以五种容易得到的纯天然的材料,并显示出杰出的保养皮肤、延缓衰老和和杀菌作用。
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