CN106378069A - Microreactor - Google Patents

Microreactor Download PDF

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Publication number
CN106378069A
CN106378069A CN201610972168.8A CN201610972168A CN106378069A CN 106378069 A CN106378069 A CN 106378069A CN 201610972168 A CN201610972168 A CN 201610972168A CN 106378069 A CN106378069 A CN 106378069A
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China
Prior art keywords
micro fluidic
fluidic plate
plate
microreactor
channels
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Application number
CN201610972168.8A
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Chinese (zh)
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CN106378069B (en
Inventor
张家庚
李处来
李凤
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bold And Generous Chemical Engineering Technology Co Ltd In Shandong
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Bold And Generous Chemical Engineering Technology Co Ltd In Shandong
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Application filed by Bold And Generous Chemical Engineering Technology Co Ltd In Shandong filed Critical Bold And Generous Chemical Engineering Technology Co Ltd In Shandong
Priority to CN201610972168.8A priority Critical patent/CN106378069B/en
Publication of CN106378069A publication Critical patent/CN106378069A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0093Microreactors, e.g. miniaturised or microfabricated reactors
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781Aspects relating to microreactors
    • B01J2219/00889Mixing

Abstract

The invention discloses a microreactor, which comprises at least two microfluid plates connected in a stacking way, wherein each microfluid plate comprises a first surface and a second surface arranged reversely; a heat dissipation channel is arranged on a first surface of each microfluid plate and is communicated with a heat dissipation medium inlet and a heat dissipation medium outlet; a reaction channel is arranged on a second surface of each microfluid plate and is communicated with a reactant inlet and a reactant outlet; each two adjacent microfluid plates are in seal connection; the reaction channel on one microfluid plate and the heat dissipation channel on the other microfluid plate are separated through a clapboard with a heat conduction action. According to the microreactor provided by the invention, the reaction channel and the heat dissipation channel are processed on one microfluid plate, and the reaction channel and the heat dissipation channel between each two adjacent microfluid plates are separated through one clapboard, so that heat in the reaction channel can be directly transmitted to the corresponding heat dissipation channel through the clapboard and the microfluid plates, and the heat exchange efficiency is improved by 30 percent or above.

Description

A kind of microreactor
Technical field
The present invention relates to consersion unit technical field, specifically a kind of application uses in chemical industry, medicine and other fields Microreactor, makes reactant can be sufficiently mixed in the reaction channel of microreactor and carry out physical reactions or chemical reaction.
Background technology
The reaction channel of board-like microreactor being used at present and heat dissipation channel are to be machined in respectively on two substrates, It is fixed together use by certain fastening means again.The reaction channel of this structure and heat dissipation channel are not directly contacted with, instead Answer the heat in passage just can need to reach in heat dissipation channel via two substrates, heat exchange efficiency is low;This structure also needs to increase Extra fastening and sealing, not only increase cost, volume, weight, also bring the risk of heat dissipation channel seal failure.For solution Determine these problems, the present invention proposes a kind of integral type microfluidic structures being made up of reaction channel and heat dissipation channel, and thus Plant structural grouping and form a kind of microreactor.
Content of the invention
For the above-mentioned present situation of prior art, present invention is primarily targeted at providing a kind of microreactor, by jet Realize fluid with the mode that combines of buffering and quickly mix shunting, solve in the chamber of prior art microreactor change in flow not Greatly, the not good problem of mixed effect.
Above-mentioned purpose is achieved through the following technical solutions:
A kind of microreactor, the micro fluidic plate connecting including at least two stackings, described micro fluidic plate includes being disposed opposite to each other First surface and second surface, and the first surface in described micro fluidic plate is provided with heat dissipation channel, described heat dissipation channel with Heat eliminating medium import, heat eliminating medium outlet, the second surface of described micro fluidic plate is set to reaction channel, described reaction channel With reaction-ure inlet, reactant outlet, it is tightly connected between two neighboring described micro fluidic plate, and a described miniflow Between the heat dissipation channel of the reaction channel of body plate and another described micro fluidic plate, the dividing plate by having conductive force separates, excellent Selection of land, described dividing plate is connected on the reaction channel of described micro fluidic plate, or is connected to the heat dissipation channel of described micro fluidic plate On.
Preferably, pass through the first channels in series conducting between the reaction channel of two neighboring described micro fluidic plate, described the One channels in series connects the reactant outlet of upstream micro fluidic plate and the reactant entrance of downstream micro fluidic plate.
Preferably, described first channels in series is located at the outside of described micro fluidic plate, or described first channels in series sets Inside described micro fluidic plate.
Preferably, pass through the second channels in series conducting between the heat dissipation channel of two neighboring described micro fluidic plate, described the The heat eliminating medium outlet of two channels in series connection upstream micro fluidic plate and the heat eliminating medium entrance of downstream micro fluidic plate, described second Channels in series is separate with described first channels in series.
Preferably, described second channels in series is located at the outside of described micro fluidic plate, or described second channels in series sets Inside described micro fluidic plate.
Preferably, the reaction channel of described micro fluidic plate is using being connected in parallel;And/or, the radiating of described micro fluidic plate is led to Road is using being connected in parallel.
Preferably, described dividing plate and the reaction channel of described micro fluidic plate or heat dissipation channel are tightly connected.
Preferably, described reaction channel is provided with turbulence structure.
Preferably, at least one described micro fluidic plate is provided with temperature-detecting device.
Preferably, connecting portion is arranged at the first surface of described micro fluidic plate and/or the edge part of second surface, and adjacent two Individual micro fluidic plate is connected by described connecting portion;
Preferably, connected it is preferable that adopting ultrasonic bond by way of welding between two neighboring described micro fluidic plate Connect.
Preferably, sealed it is preferable that described sealing ring is adopted by sealing ring between two neighboring described micro fluidic plate With O-ring or sealing strip.
The microreactor that the present invention provides, reaction channel and heat dissipation channel are machined in a micro fluidic plate, and phase Reaction channel between two adjacent micro fluidic plate and heat dissipation channel are separated by a dividing plate, make the heat in reaction channel can Directly heat dissipation channel is reached by dividing plate and micro fluidic plate, heat exchange efficiency improves more than 30%;
The microreactor that the present invention provides, be can achieve by the way of welding and connects and seal it is not necessary to increase extra Fastening and sealing, reduce cost, volume and weight, and surface structure be compact;
The microreactor that the present invention provides, heat dissipation channel is tightly connected by reliability patterns such as welding, reduces radiating The risk that medium is revealed.
Brief description
Hereinafter with reference to accompanying drawing, the preferred implementation of the microreactor according to the present invention is described.In figure:
Fig. 1 is the structural representation of microreactor of the present invention;
Fig. 2 is the schematic diagram of micro-reaction plate structure of the present invention;
Fig. 3 is the microreactor schematic diagram of another embodiment of the present invention;
Fig. 4 is the microreactor schematic diagram of another embodiment of the present invention.
In figure:
100th, micro fluidic plate;101st, connecting portion;102nd, heat dissipation channel;103rd, heat eliminating medium import;104th, heat eliminating medium goes out Mouthful;105th, reaction channel;106th, reaction-ure inlet;107th, reactant outlet;108th, the first concatenation passage;109th, the second concatenation is logical Road;
200th, dividing plate;
300th, temperature-detecting device;
400th, sealing ring.
Specific embodiment
For further illustrating that the present invention is to reach technological means and effect that predetermined goal of the invention is taken, below in conjunction with Preferred embodiment, to according to microreactor specific embodiment proposed by the present invention, feature and its effect, describes in detail as follows.
For the aforesaid drawbacks of prior art, the present invention is improved to micro- reaction channel of microreactor first, carries Go out a kind of new microreactor.
Embodiment 1
As Figure 1-4, a kind of microreactor of the embodiment of the present invention, the micro fluidic plate connecting including at least two stackings 100, described micro fluidic plate includes the first surface being disposed opposite to each other and second surface, and first in described micro fluidic plate 100 Surface is provided with heat dissipation channel 102, and described heat dissipation channel 102 is connected with heat eliminating medium import 103, heat eliminating medium outlet 104, described The second surface of micro fluidic plate 100 is provided with reaction channel 105, and described reaction channel 105 and reaction-ure inlet 106, reactant go out Mouth 107 connection, is tightly connected between two neighboring described micro fluidic plate 100, and the reaction channel of a described micro fluidic plate Dividing plate by having conductive force separates it is preferable that described dividing plate and the heat dissipation channel of another described micro fluidic plate between It is connected on the reaction channel of described micro fluidic plate, or be connected on the heat dissipation channel of described micro fluidic plate.
The mounting arrangements of all import and export can be to select using direct punching, welded pipe, to use the modes such as various terminal, can It is adjusted flexibly according to factors such as sizes.
Described micro fluidic plate using stacking connect by the way of, could be arranged to multiple, by between micro fluidic plate 100 every Plate 200, realizes keeping apart reaction channel and heat dissipation channel, and dividing plate has good heat conductivility in itself, consequently facilitating The heat that reaction channel is produced is delivered to the heat eliminating medium of heat dissipation channel by dividing plate 200.
Preferably, turned on by the first channels in series 108 between the reaction channel 105 of two neighboring described micro fluidic plate, Described first channels in series 108 connects the reactant outlet of upstream micro fluidic plate and the reactant entrance of downstream micro fluidic plate.
Preferably, described first channels in series 108 is located at the outside of described micro fluidic plate 100, or described first series connection Passage is located inside described micro fluidic plate 100.By described first channels in series 108 it is only necessary to design phase by the way of peripheral hardware The connecting pipeline answered can achieve connection;By described first channels in series 108 by the way of interior setting, can be in described microfluid The connecting portion at the edge of plate 100 processes corresponding passage.
Preferably, led by the second channels in series 109 between the heat dissipation channel 102 of two neighboring described micro fluidic plate 100 Logical, the radiating of heat eliminating medium outlet and downstream micro fluidic plate 100 that described second channels in series 109 connects upstream micro fluidic plate is situated between Matter entrance, described second channels in series 109 is separate with described first channels in series.
Preferably, described second channels in series 109 is located at the outside of described micro fluidic plate 100, or described second series connection Passage 109 is located inside described micro fluidic plate.The design of described second channels in series 109 and described first channels in series 108 Design is identical, but when in view of design cost, can be by one of the first channels in series 108, the second channels in series 109 Set in being designed as, therein another is designed as peripheral hardware.Can also simultaneously by two passages be designed as in set, or simultaneously will Two passages are designed as peripheral hardware.
Alternatively, the reaction channel of described micro fluidic plate 100 is using being connected in parallel;And/or, described micro fluidic plate 100 Heat dissipation channel using being connected in parallel.
Preferably, described dividing plate 200 and the reaction channel of described micro fluidic plate or heat dissipation channel are tightly connected.The present embodiment In, described dividing plate 200 is tightly connected with the heat dissipation channel of described micro fluidic plate, based on the understanding of those skilled in the art, described Dividing plate 200 can also be tightly connected with the reaction channel of described micro fluidic plate.Common design is, described dividing plate 200 and radiating Upper surface after passage connects is located at same surface, makes described dividing plate 200 after being tightly connected with described heat dissipation channel, on Portion surface keeps smooth, is easy to multiple described micro fluidic plate 100 and carries out stacking connection.
Preferably, described reaction channel 105 is provided with turbulence structure.When fluid-mixing in reaction channel 105 passes through, pass through The flow-disturbing effect of turbulence structure, promotes the mixing of reaction channel fluid more abundant, improves reaction efficiency.
Preferably, at least one described micro fluidic plate 100 is provided with temperature-detecting device 300.Described temperature detection dress Put 300 for detecting the temperature of described micro fluidic plate 100, the particularly temperature in detectable response passage or heat dissipation channel interior temperature Degree.In order to detect reaction medium temperature, it is inserted into internal fluid or SMD, for controlling reaction temperature.
Preferably, connecting portion 101 is arranged at the first surface of described micro fluidic plate and the edge part of second surface, and adjacent two Connected by described connecting portion 101 between individual micro fluidic plate 100.When described first channels in series, the second channels in series are arranged on During described micro fluidic plate 100 inside, described first channels in series, the second channels in series are arranged on the connecting portion of described micro fluidic plate 101.
According to the understanding of those skilled in the art, described connecting portion 101 also can be only arranged at the first of described micro fluidic plate The edge part on one of surface and second surface, so can also make to pass through described connecting portion between two neighboring micro fluidic plate 100 101 connections.
Preferably, connected it is preferable that adopting ultrasonic bond by way of welding between two neighboring described micro fluidic plate Connect.
Preferably, sealed by sealing ring 400 between two neighboring described micro fluidic plate it is preferable that described sealing Circle 400 adopts O-ring or sealing strip.
By the way, the sealing after realizing the stacking of described micro fluidic plate 100 is connected is it is ensured that described microreactor has There is good bearing capacity.When producing microreactor, need the deformation after considering the heat resistance of material and being heated Amplitude is it is ensured that it is ensured that the sealing of microreactor itself and thermostability during microreactor work.
The microreactor that the present invention provides, reaction channel and heat dissipation channel are machined in a micro fluidic plate, and phase Reaction channel between two adjacent micro fluidic plate and heat dissipation channel are separated by a dividing plate, make the heat in reaction channel can Directly heat dissipation channel is reached by dividing plate and micro fluidic plate, heat exchange efficiency improves more than 30%;
The microreactor that the present invention provides, be can achieve by the way of welding and connects and seal it is not necessary to increase extra Fastening and sealing, reduce cost, volume and weight, and surface structure be compact;
The microreactor that the present invention provides, heat dissipation channel is tightly connected by reliability patterns such as welding, reduces radiating The risk that medium is revealed.
Skilled addressee readily understands that, on the premise of not conflicting, above-mentioned each advantageous manner can be freely Combination, superposition.
The above, the only specific embodiment of the present invention, but protection scope of the present invention is not limited thereto, and any Those familiar with the art the invention discloses technical scope in, change or replacement can be readily occurred in, all should contain Cover within protection scope of the present invention.Therefore, protection scope of the present invention should be defined by described scope of the claims.

Claims (10)

1. a kind of microreactor, is laminated the micro fluidic plate connecting it is characterised in that described micro fluidic plate includes including at least two The first surface being disposed opposite to each other and second surface, are provided with heat dissipation channel in the first surface of described micro fluidic plate, and described radiating is led to Road and heat eliminating medium import, heat eliminating medium outlet, the second surface of described micro fluidic plate is provided with reaction channel, described reaction Passage and reaction-ure inlet, reactant outlet, are tightly connected between two neighboring described micro fluidic plate, and described in one Between the heat dissipation channel of the reaction channel of micro fluidic plate and another described micro fluidic plate by have the dividing plate of conductive force every Open it is preferable that described dividing plate is connected on the reaction channel of described micro fluidic plate, or be connected to the radiating of described micro fluidic plate On passage.
2. microreactor as claimed in claim 1 is it is characterised in that between the reaction channel of two neighboring described micro fluidic plate Turned on by the first channels in series, described first channels in series connects reactant outlet and the downstream microfluid of upstream micro fluidic plate The reactant entrance of plate.
3. microreactor as claimed in claim 2 is it is characterised in that described first channels in series is located at described micro fluidic plate Outside, or described first channels in series is located inside described micro fluidic plate.
4. microreactor as claimed in claim 2 is it is characterised in that between the heat dissipation channel of two neighboring described micro fluidic plate Turned on by the second channels in series, described second channels in series connects heat eliminating medium outlet and the downstream miniflow of upstream micro fluidic plate The heat eliminating medium entrance of body plate, described second channels in series is separate with described first channels in series.
5. microreactor as claimed in claim 4 is it is characterised in that described second channels in series is located at described micro fluidic plate Outside, or described second channels in series is located inside described micro fluidic plate.
6. microreactor as claimed in claim 1 is it is characterised in that the reaction channel of described micro fluidic plate is using being connected in parallel;With/ Or, the heat dissipation channel of described micro fluidic plate is using being connected in parallel.
7. the microreactor as described in one of claim 1-6 is it is characterised in that the reaction of described dividing plate and described micro fluidic plate Passage or heat dissipation channel are tightly connected.
8. the microreactor as described in one of claim 1-6 is it is characterised in that described reaction channel is provided with turbulence structure.
9. the microreactor as described in one of claim 1-6 is it is characterised in that micro fluidic plate described at least one is provided with Temperature-detecting device.
10. the microreactor as described in one of claim 1-6 it is characterised in that
Connecting portion is arranged at the first surface of described micro fluidic plate and/or the edge part of second surface, two neighboring micro fluidic plate Connected by described connecting portion;
Preferably, connected it is preferable that adopting ultra-sonic welded by way of welding between two neighboring described micro fluidic plate;
Or, sealed by sealing ring between two neighboring described micro fluidic plate it is preferable that described sealing ring is using O-shaped Circle or sealing strip.
CN201610972168.8A 2016-10-31 2016-10-31 A kind of microreactor Active CN106378069B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108704590A (en) * 2018-08-07 2018-10-26 山东金德新材料有限公司 A kind of silicon carbide microchannel reactor module
CN108704591A (en) * 2018-08-07 2018-10-26 山东金德新材料有限公司 A kind of integrated silicon carbide microchannel reactor of collection heat-exchange system

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20060083675A1 (en) * 2004-10-15 2006-04-20 Daly Francis P Stable, catalyzed, high temperature combustion in microchannel, integrated combustion reactors
CN1907555A (en) * 2006-07-17 2007-02-07 南京工业大学 Composite heat transfer micro reactor
CN103328092A (en) * 2011-01-13 2013-09-25 帝斯曼知识产权资产管理有限公司 Oscillating flow minireactor
CN206343164U (en) * 2016-10-31 2017-07-21 山东豪迈化工技术有限公司 A kind of microreactor

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20060083675A1 (en) * 2004-10-15 2006-04-20 Daly Francis P Stable, catalyzed, high temperature combustion in microchannel, integrated combustion reactors
CN1907555A (en) * 2006-07-17 2007-02-07 南京工业大学 Composite heat transfer micro reactor
CN103328092A (en) * 2011-01-13 2013-09-25 帝斯曼知识产权资产管理有限公司 Oscillating flow minireactor
CN206343164U (en) * 2016-10-31 2017-07-21 山东豪迈化工技术有限公司 A kind of microreactor

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108704590A (en) * 2018-08-07 2018-10-26 山东金德新材料有限公司 A kind of silicon carbide microchannel reactor module
CN108704591A (en) * 2018-08-07 2018-10-26 山东金德新材料有限公司 A kind of integrated silicon carbide microchannel reactor of collection heat-exchange system

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