CN106362715B - Adsorption microspheres former with netted liquid pearl separator - Google Patents
Adsorption microspheres former with netted liquid pearl separator Download PDFInfo
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- CN106362715B CN106362715B CN201610906788.1A CN201610906788A CN106362715B CN 106362715 B CN106362715 B CN 106362715B CN 201610906788 A CN201610906788 A CN 201610906788A CN 106362715 B CN106362715 B CN 106362715B
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/3028—Granulating, agglomerating or aggregating
Abstract
The present invention provides a kind of adsorption microspheres formers of the netted liquid pearl separator of band, belong to production equipment technology.It solves and can not prepare diameter in the prior art between 0.1-1mm the problems such as adsorption microspheres.This adsorption microspheres former with netted liquid pearl separator, including pedestal, storage barrel and molding bucket are provided on pedestal, it is characterized in that, being provided with magnetic stirring apparatus on the pedestal, molding bucket is arranged on magnetic stirring apparatus, being molded bucket top has opening, upper opening portion is provided with mounting plate, and mounting plate is set on the base by an elevation positioning structure, and mounting plate is equipped with the selecting mechanism that can select needle aperture size;Netted liquid pearl separator is additionally provided in mounting plate and between being molded the opening of bucket, netted liquid pearl separator includes a silk screen, and silk screen is detachably arranged between left column and right column.The present invention has the advantages that adsorption microspheres of the diameter between 0.1-1mm can be prepared.
Description
Technical field
The invention belongs to production equipment technologies, are related to a kind of former, especially a kind of netted liquid pearl separation of band
The adsorption microspheres former of device.
Background technology
With the progress of human society, scientific and technological development, people exploitation, using water resource when, also do not break all the time
Water resource is gone bad, nowadays water pollution has become more serious.So in order to adapt to the theory of today's society sustainable development,
The big theme that water pollution this problem is current ecological environment is administered.
Water pollution is to cause the use value of water to reduce or lose by harmful chemical, the water of environment is polluted, in sewage
Acid, alkali, oxidant, the compounds such as Yi Jitong, cadmium, mercury, arsenic, the organic poisons such as benzene, dichloroethanes, ethylene glycol can poison water with poison
Biology, influences drinking water source, scenic spot landscape.The oxygen in water is consumed when organic matter in sewage is decomposed by the microorganisms, and is influenced
The life of aquatile, after oxygen in water exhausts, organic matter carries out anaerobic digestion, generates the offensive gases such as hydrogen sulfide, mercaptan,
Water quality is set further to deteriorate.
Currently, people have researched and developed administers water pollution using various methods, such as using ion-exchange, membrane filter method, height
Grade oxidizing process and bioanalysis carry out improvement water pollution.But there is the shortcomings that being not easy regeneration in ion-exchange;Membrane filter method
Have the shortcomings that processing cost is high;Advanced oxidation processes are also easy to produce secondary pollution;The processing time of bioanalysis is longer.
Meanwhile people have developed a kind of absorption method and are used for administering water pollution again, with easy to operate, raw material is wide, system
Make simple advantage.The raw material of absorption method is more, there is carbon-based sorbing material, synthetic resin sorbing material and biomass absorbent material
Material.But carbon-based sorbing material is of high cost, service life is short, and operating cost is high;Synthetic resin sorbing material it is of high cost,
Non-degradable can cause secondary pollution;And the material of biomass absorbent material is cheap, easy to operate, non-secondary pollution, as this
Green, economic, efficient, multi-functional sorbent material is the leading of current sorbing material.
And in the real processing procedure of sewage, porous microsphere also is made in biomass absorbent material, and then to water
Matter is administered.
In the prior art, the production equipment of porous microsphere lacks, even if producing porous microsphere, is relatively large in diameter, and
And mostly in 1mm or more, it is difficult to make the porous microsphere less than 1mm.So for those skilled in the art, it need
A kind of equipment that can produce porous microsphere is developed, while the porous microsphere that diameter is less than 1mm can be produced, so that porous
Microballoon meets the application under various Water condition environment.
Invention content
The purpose of the present invention is there is the above problem in view of the prior art, it is proposed that a kind of netted liquid pearl separator of band
Adsorption microspheres former, the technical problem to be solved by the present invention is to the liquid pearl diameters for how making to overflow from syringe needle to become more
It is small, to produce smaller diameter and uniform adsorption microspheres.
Object of the invention can be realized by the following technical scheme:Adsorption microspheres molding with netted liquid pearl separator is set
It is standby, including pedestal, the storage barrel for storing stoste and the molding bucket for balling-up are provided on pedestal, which is characterized in that
Solidification liquid is housed in molding bucket, stoste is housed in storage barrel;Be provided with magnetic stirring apparatus on the pedestal, it is above-mentioned at
Type bucket is arranged on magnetic stirring apparatus, and there is opening, the upper opening portion to be provided with mounting plate on molding bucket top, and mounting plate is logical
It crosses an elevation positioning structure to be set on the base, the elevation positioning structure includes left column and right column, left column and the right side
Column is vertically fixed on pedestal, and above-mentioned magnetic stirring apparatus is between left column and right column, the left column court
It is plane to the one side of right column, is provided with graduation mark in the plane, graduation mark is from top to bottom arranged, scale from top to bottom
Line is arranged using the alternate mode of the white three kinds of colors of red indigo plant, is fixed with top plate at left column top and right column top, is pushing up
Plate lower part is fixed with motor, is fixed with lead screw by shaft coupling on the output shaft of motor, spiral shell is threaded on the lead screw
The outer wall of mother, nut are equipped with bearing, and inner ring and the nut of bearing are fixed, and the outer ring of bearing is mutually fixed with mounting plate, described
Several guide cylinders and guide post are additionally provided between mounting plate and top plate, guide post is slidably arranged in guide cylinder, and the one of guide post
End is fixed on a mounting board, and one end of guide cylinder is fixed on top plate, is fixed with pointer on mounting plate, and the pointer is towards above-mentioned
Graduation mark;The mounting plate is equipped with the selecting mechanism that can select needle aperture size, and selecting mechanism includes several opens
If through-hole on a mounting board, several magnet rings are fixed in the through-hole, the internal diameter of the magnet ring is all different, one wherein
Be provided with syringe needle in magnet ring, described syringe needle one end is liquid feeding end, and the other end is outlet end, the liquid feeding end of syringe needle by inlet tube with
Storage barrel is connected, and delivery pump is provided in inlet tube, flow control valve is additionally provided in the inlet tube;In mounting plate and
Netted liquid pearl separator is additionally provided between the opening of molding bucket, the netted liquid pearl separator includes a silk screen, described
Silk screen is detachably arranged between left column and right column, a diameter of 0.1-1mm of mesh on silk screen;It is arranged on the pedestal
There are controller, the motor to be connected with the controller by circuit.
This adsorption microspheres former with netted liquid pearl separator, operation principle is such:
1, first, stoste is loaded onto in storage barrel, solidification liquid is loaded onto in being molded bucket, and adjusts turning for magnetic stirring apparatus
Speed and temperature are stirred molding bucket using magnetic stirring apparatus;
2, then, using selecting mechanism, suitable magnet ring and syringe needle are selected, and magnet ring is installed to and is specified on mounting plate
In through-hole, syringe needle is installed in specified magnet ring;
3, then, using elevation positioning structure, suitable height is adjusted to mounting plate, specifically, under the action of motor,
Make output shaft drive lead screw rotate forward, to make mounting plate push downwards by nut and bearing, until mounting plate on pointer refer to
Specified graduation mark;
4, last, it extracts the stoste in storage barrel using delivery pump and flow to syringe needle through flow control valve and inlet tube, and wear
It crosses silk screen to instill into molding bucket, forms it into adsorption microspheres, complete the making of adsorption microspheres.
Fluid infusion bucket is additionally provided on the pedestal, fluid infusion bucket upper end has outlet, and fluid infusion bucket one end is hinged on storage
At the upper end for depositing barrel side, the lower part of the fluid infusion bucket other end is provided with the second cylinder, and the cylinder body of the second cylinder is fixed on the base,
Straight up, the piston rod upper end of the second cylinder is connected with the fluid infusion bucket other end, the second gas for the piston rod upper end of second cylinder
Cylinder is connected by circuit with above-mentioned controller;It is logical that liquid is further opened with out at the lower part of the side of storage barrel in fluid infusion bucket
Hole, is provided with solenoid valve in going out fluid through-hole, and the solenoid valve is connected by circuit with above-mentioned controller.
In the case of filling with liquid in fluid infusion bucket, stretched out upwards using the piston rod of the second cylinder, so that it may so that fluid infusion
Bucket tilts, and liquid flows out from the outlet of fluid infusion bucket, so that liquid is entered in storage barrel, supplement liquid is carried out to storage barrel;?
In the case that liquid is less than half in fluid infusion bucket, is stretched out upwards using the piston rod of the second cylinder, make the inclined degree of fluid infusion bucket
It is larger, open solenoid valve, liquid flows out from going out in fluid through-hole for fluid infusion bucket, and liquid is made to enter in storage barrel, to storage barrel into
Row supplement liquid.
Under the action of controller, the second cylinder and solenoid valve can be made to realize and automatically controlled, without artificially controlling, carried
The degree of automation of high equipment.
Discharging net bucket is provided in the molding bucket, discharging net bucket lower part and side offer several micropores, discharge
Left connection ring is fixed on the left of net bucket top, discharging net bucket is fixed with right connection ring on the right side of top, is provided on pedestal
Storage box for storing adsorption microspheres, storage upper box part have feed inlet, are fixed with close to the side of molding bucket in storage box
Placement plate, placement plate and molding bucket flush with each other, are provided with third cylinder in placement plate, and the piston rod of third cylinder is separate to be deposited
Case setting is put, sealing plate is fixed on the piston rod of third cylinder, guide rail, guide rail direction molding are additionally provided with above storage box
The top of bucket extends, and guide rail is in below top plate, and guide rail both ends are fixed on the base by several holders, and cunning is provided on guide rail
Block one and sliding block two, spring is fixed between sliding block one and sliding block two, and connecting rope one, connecting rope one are fixed in one lower part of sliding block
Lower end be fixed with hook one, hook one can hanging support in the left connection ring, be fixed with connecting rope two in two lower part of sliding block,
The lower end of connecting rope two is fixed with hook two, hook two can hanging supports in the right connection ring, the sliding block two passes through the
Four cylinders drive, and the cylinder body of the 4th cylinder is fixed on holder, and the piston rod of the 4th cylinder is connected with sliding block two;Described
Three cylinders and the 4th cylinder are connected by circuit with above-mentioned controller.
After being molded the making for completing adsorption microspheres in bucket, adsorption microspheres all accumulate in discharging net bucket:First, the 4th
Under the action of cylinder, the piston rod of the 4th cylinder is protruding, is moved along the position of guide rail towards storage box with movable slider two,
Under the action of the spring, while with movable slider one along the position of guide rail towards storage box it moves, sliding block one is led to by connecting rope one
Hook is crossed one to connect with left connection ring, thus sliding block one can drive the other end for the net bucket that discharges to slide, sliding block two by
Connecting rope two is connect by hook two with right connection ring, and thus sliding block two can drive one end of discharging net bucket to slide;
Then, when the net bucket that discharges slides into the top of storage box, overturning discharging net bucket can pour into the adsorbing sphere in the net bucket that discharges
It has been suffered to storage box;Secondly, under the action of third cylinder, the piston rod of third cylinder is protruding, and sealing plate can incite somebody to action
The feed inlet of storage box is closed;Finally, the piston rod of third cylinder and the 4th cylinder is retracted, and sliding block one, spring and sliding block two are multiple
Position.
The delivery pump is peristaltic pump.Peristaltic pump can carry out fluid alternately extruding and release, to fluid into
Row intermittent delivery realizes that adsorption microspheres are slowly molded.
The solidification liquid is water, ethyl alcohol, acid solution or alkaline solution.
The stoste is cellulose, chitin or Glucomannan lysate.
Temperature sensor one, liquid level sensor one, a high position for the liquid level sensor one are equipped in the storage barrel
The distance between probe and storage barrel the top are 1-2cm, between the low level probe of liquid level sensor one and storage barrel bottom
Distance be 3-5cm, liquid level sensor one is connected by circuit with above-mentioned controller.Temperature sensor one can be to storage
The temperature of solution monitors in real time in bucket, and liquid level sensor one can monitor the liquid level of solution in storage barrel in real time.Work as liquid
When level sensor one monitors that liquid level declines in storage barrel, controller can be passed information to, controller orders the second cylinder again
Piston rod stretch out, to storage barrel carry out fluid infusion.
Temperature sensor two, PH sensor, liquid level sensor two, the liquid level sensor are equipped in the molding bucket
The distance between two high-order probe and molding bucket the top are 5-8cm, and the low level probe and molding bucket of liquid level sensor two are most
The distance between lower end is 1-3cm, and liquid level sensor two is connected by circuit with above-mentioned controller.Two energy of temperature sensor
The temperature of solution monitors in real time in enough buckets to molding, and PH sensor can monitor the pH value of solution in molding bucket in real time, liquid level
Sensor two can monitor the liquid level of solution in molding bucket in real time.When liquid level sensor two monitors liquid level in molding bucket
When rising or declining, controller can be passed information to, the output shaft of controller order motor again, which corresponds to, to be rotated forward or reversion,
When the liquid level of molding bucket being made to increase, when the liquid level that mounting plate with rising, can also be molded bucket declines, mounting plate also can be under
Drop makes the distance between mounting plate and molding bucket liquid level remain certain.
Compared with prior art, the present invention has the following advantages:
1, the present invention can select suitable syringe needle as the forming diameter of adsorption microspheres by selecting mechanism, to basis
The different-diameter of syringe needle produces the adsorption microspheres of different-diameter.
2, the present invention can reasonably adjust the height of mounting plate by lift locating device, so as to adjust the height of syringe needle
Degree keeps the height that stoste instills molding bucket suitable.
3, the stoste that the present invention is extracted from storage barrel flow to syringe needle through flow control valve and inlet tube, then in silk screen
Under effect, liquid pearl is split, so as to generate the smaller adsorption microspheres of diameter.
4, the present invention can carry out stoste alternately extruding and release by peristaltic pump, intermittent defeated to be carried out to fluid
It send, realizes the orderly stable molding of adsorption microspheres.
5, the present invention can control the temperature of solidification liquid by magnetic stirring apparatus, you can be heated to solidification liquid,
Solidification liquid can be cooled down, temperature is allow to be adjusted between 0-100 degree;Solidification can also be controlled by magnetic stirring apparatus
The mixing speed of liquid avoids the adsorption microspheres stick to each other not solidified.
6, the present invention can carry out automatic liquid supply, in the second cylinder and controller under the action of fluid infusion bucket to storage barrel
Under the action of, realize automatically controlling for the second cylinder.
7, the adsorption microspheres that formation is solidified in being molded bucket can be transferred to and deposit under the action of discharging net bucket by the present invention
It puts in case, under the action of the 4th cylinder and controller, realizes automatically controlling for the 4th cylinder.
8, the present invention can monitor molding bucket in pH value come supplement and discharge be molded bucket in solidification liquid, make the PH of solidification liquid
Value meets the coagulation forming requirement of adsorption microspheres.
Description of the drawings
Fig. 1 is the structural schematic diagram of the present invention;
Fig. 2 is the structural schematic diagram of elevation positioning structure in the present invention;
Fig. 3 is the structural schematic diagram of selecting mechanism in the present invention;
Fig. 4 is the partial structural diagram of the present invention.
In figure, 1, pedestal;2, storage barrel;3, it is molded bucket;4, magnetic stirring apparatus;5, mounting plate;6, magnet ring;7, syringe needle;8,
Inlet tube;9, delivery pump;10, flow control valve;11, left column;12, right column;13, top plate;14, motor;15, lead screw;16,
Nut;17, bearing;18, guide cylinder;19, guide post;20, silk screen;21, clip one;22, clip two;23, pointer;24, fluid infusion
Bucket;25, the second cylinder;26, controller;27, solenoid valve;28, discharge net bucket;29, left connection ring;30, right connection ring;31, it deposits
Put case;32, placement plate;33, third cylinder;34, sealing plate;35, guide rail;36, holder;37, sliding block one;38, sliding block two;39,
Spring;40, connecting rope one;41, one is linked up with;42, connecting rope two;43, two are linked up with;44, the 4th cylinder.
Specific implementation mode
Following is a specific embodiment of the present invention in conjunction with the accompanying drawings, technical scheme of the present invention will be further described,
However, the present invention is not limited to these examples.
As shown in Figure 1, a kind of adsorption microspheres former of the netted liquid pearl separator of band, including pedestal 1, on pedestal 1
It is provided with the storage barrel 2 for storing stoste and the molding bucket 3 for balling-up, solidification liquid is housed in molding bucket 3, in storage barrel
Stoste is housed in 2.Specifically, stoste is the lysates such as cellulose, chitin or Glucomannan, the forming material as adsorption microspheres
Material as the solidification liquid of adsorption microspheres is formed is the solution such as water, ethyl alcohol according to different stoste, or sulfuric acid, hydrochloric acid, nitre
The acid solutions such as acid, or the alkaline solutions such as sodium hydroxide, sodium carbonate, sodium bicarbonate.
As illustrated in fig. 1 and 2, magnetic stirring apparatus 4 is additionally provided on pedestal 1, molding bucket 3 is arranged on magnetic stirring apparatus 4.
There is opening, the top of opening to be provided with mounting plate 5 on the top for being molded bucket 3, and mounting plate 5 is arranged by an elevation positioning structure
On pedestal 1.Specifically, elevation positioning structure includes left column 11 and right column 12, left column 11 and right column 12 are vertical solid
It is scheduled on pedestal 1, above-mentioned magnetic stirring apparatus 4 is between left column 11 and right column 12, and the left column 11 is towards the right side
The one side of column 12 is plane, is provided with graduation mark in the plane, graduation mark is from top to bottom arranged, graduation mark from top to bottom
It is arranged using the alternate mode of the white three kinds of colors of red indigo plant, is further fixed on pointer 23 on mounting plate 5, pointer 23 is towards on left column 11
Graduation mark.It is fixed with top plate 13 at 12 top of 11 top of left column and right column, motor 14 is fixed in 13 lower part of top plate,
Lead screw 15 is fixed with by shaft coupling on the output shaft of motor 14, nut 16, nut 16 are threaded on the lead screw 15
Outer wall be equipped with bearing 17, the inner ring of bearing 17 is fixed with nut 16, and outer ring and 5 phase of mounting plate of bearing 17 are fixed, described
Mounting plate 5 and top plate 13 between be additionally provided with several guide cylinders 18 and guide post 19, guide post 19 is slidably arranged in guide cylinder 18
Interior, one end of guide post 19 is fixed on mounting plate 5, and one end of guide cylinder 18 is fixed on top plate 13, is fixed on mounting plate 5
Pointer 23, the pointer 23 is towards above-mentioned graduation mark.
As shown in Fig. 2, being additionally provided with netted liquid pearl separator, the net in mounting plate 5 and between being molded the opening of bucket 3
Shape liquid pearl separator includes a silk screen 20, and the silk screen 20 is detachably arranged between left column 11 and right column 12, specifically
, which includes several clips 1 being fixed on left column 11 and several clips being fixed on right column 12
2 22, silk screen 20 is clamped in by clip 1 and clip 2 22 between left column 11 and right column 12.Mesh is straight on silk screen 20
Diameter is 0.6mm, specifically, the diameter of mesh can be determined according to the diameter of required adsorption microspheres on silk screen 20, it generally can be in 0.1-
It is selected between 1mm.
As shown in figs. 1 and 3, the selecting mechanism of 7 pore size of syringe needle can be selected by being additionally provided on mounting plate 5.Specifically,
The selecting mechanism includes several through-holes being opened on mounting plate 5, and several magnet rings 6 are fixed in through-hole, and the internal diameter of magnet ring 6 is homogeneous
Together, the internal diameter of magnet ring 6 is all different, and syringe needle 7 is provided in a wherein magnet ring 6, and 7 one end of the syringe needle is liquid feeding end, separately
One end is outlet end, and the liquid feeding end of syringe needle 7 is connected by inlet tube 8 with storage barrel 2, and the outlet end of syringe needle 7 is vertically arranged, and
Towards molding bucket 3, the stoste fallen from syringe needle 7 is enable to instill into molding bucket 3.
It is additionally provided with delivery pump 9 in inlet tube 8, the stream that can control fluid flow size is additionally provided in inlet tube 8
Adjustable valve 10.In the present embodiment, delivery pump 9 is the peristaltic pump that can be bought on existing market, and structure is not done retouches in detail
It states.Peristaltic pump can carry out fluid alternately extruding and release, to carry out intermittent delivery to fluid, realize that adsorption microspheres are slow
Slow molding.
Fluid infusion bucket 24 is additionally provided on pedestal 1, the upper end of fluid infusion bucket 24 has outlet, and 24 side of fluid infusion bucket passes through hinge
One and free bearing one be hinged at the upper end of 2 side of storage barrel, wherein hinge one is fixed on fluid infusion bucket 24, and free bearing one is fixed on storage
It deposits on bucket 2;The lower part of 24 other side of fluid infusion bucket is provided with the second cylinder 25, and the cylinder body of the second cylinder 25 passes through hinge two and free bearing
Two are hinged on pedestal 1, and wherein free bearing two is fixed on pedestal 1, and hinge two is fixed on the cylinder body of the second cylinder 25;Second gas
Straight up, piston rod end and 24 other end of fluid infusion bucket of the second cylinder 25 pass through hinge three and free bearing three to the piston rod of cylinder 25
It is connected, wherein free bearing three is fixed on fluid infusion bucket 24, and hinge three is fixed on the piston rod end of the second cylinder 25.Specifically
, between storage barrel 2 and fluid infusion bucket 24, between fluid infusion bucket 24 and the piston rod of the second cylinder 25, the cylinder body of the second cylinder 25 with
It is relatively hinged between pedestal 1.It is further opened with out fluid through-hole at the lower part of 2 side of storage barrel in fluid infusion bucket 24, is going out liquid
It is provided with solenoid valve 27 in through-hole, solenoid valve 27 and going out between fluid through-hole is realized by rubber ring to be sealed.Go out fluid through-hole from fluid infusion
Vertical distance between 24 bottoms of bucket is 3-5cm, specifically, in the present embodiment, which is 4cm, but can also root
It is suitably adjusted according to the actual size of fluid infusion bucket 24.
In the case of filling with liquid in fluid infusion bucket 24, stretched out upwards using the piston rod of the second cylinder 25, so that it may so that
Fluid infusion bucket 24 tilts, and liquid flows out from the outlet of fluid infusion bucket 24, so that liquid is entered in storage barrel 2, mended to storage barrel 2
Filling liquid body;In the case that liquid is less than half in fluid infusion bucket 24, is stretched out upwards using the piston rod of the second cylinder 25, make fluid infusion
The inclined degree of bucket 24 is larger, opens solenoid valve 27, and liquid is flowed out from going out in fluid through-hole for fluid infusion bucket 24, and liquid is made to enter storage
It deposits in bucket 2, supplement liquid is carried out to storage barrel 2.
As shown in figs. 1 and 4, discharging net bucket 28 is provided in molding bucket 3,28 lower part of discharging net bucket and side offer
Several micropores, discharging net bucket are fixed with left connection ring 29 on the left of 28 top, and right company is fixed on the right side of 28 top of net bucket that discharges
Ring 30 is connect, the storage box 31 for storing adsorption microspheres is provided on pedestal 1,31 top of storage box has feed inlet, depositing
It puts case 31 and is fixed with placement plate 32, placement plate 32 and molding 3 flush with each other of bucket close to the side of molding bucket 3, in placement plate 32
It is provided with third cylinder 33, the piston rod of third cylinder 33 is arranged far from storage box 31, fixed on the piston rod of third cylinder 33
There is sealing plate 34, guide rail 35 is additionally provided with above storage box 31, the top of guide rail 35 towards molding bucket 3 extends, at guide rail 35
In 13 lower section of top plate, 35 both ends of guide rail are fixed on by several holders 36 on pedestal 1, and sliding block 1 is provided on guide rail 35 and is slided
Block 2 38 is fixed with spring 39 between sliding block 1 and sliding block 2 38, connecting rope 1 is fixed in one 37 lower part of sliding block, connection
Restrict 1 lower end be fixed with hook 1, hook 1 can hanging supports in the left connection ring 29, in 2 38 lower part of sliding block
It is fixed with connecting rope 2 42, the lower end of connecting rope 2 42 is fixed with hook 2 43, and 2 43 energy hanging support of hook is in the right connection
On ring 30, the sliding block 2 38 is driven by the 4th cylinder 44, and the cylinder body of the 4th cylinder 44 is fixed on holder 36, the 4th gas
The piston rod of cylinder 44 is connected with sliding block 2 38.
After being molded the making for completing adsorption microspheres in bucket 3, adsorption microspheres all accumulate in discharging net bucket 28:First, exist
Under the action of 4th cylinder 44, the piston rod of the 4th cylinder 44 is protruding, and band movable slider 2 38 is along guide rail 35 towards storage
The position of case 31 is moved, under the action of spring 39, while with movable slider 1 along guide rail 35 towards the position of storage box 31
Mobile, sliding block 1 is connect by hook 1 with left connection ring 29 by connecting rope 1, and thus sliding block 1 can drive
What the other end of discharging net bucket 28 had slided, sliding block 2 38 is connect by hook 2 43 with right connection ring 30 by connecting rope 2 42,
Thus sliding block 2 38 can drive one end of discharging net bucket 28 to slide;Then, when discharging net bucket 28 slides into storage box
When 31 top, the adsorbing sphere in the net bucket 28 that discharges can be poured into what storage box 31 had suffered by overturning discharging net bucket 28;Its
Secondary, under the action of third cylinder 33, the piston rod of third cylinder 33 is protruding, sealing plate 34 can by storage box 31 into
Material mouth is closed;Finally, the piston rod of third cylinder 33 and the 4th cylinder 44 is retracted, and sliding block 1, spring 39 and sliding block 2 38 are multiple
Position.
In the present embodiment, controller 26 is additionally provided on pedestal 1, controller 26 is that can be bought on existing market
PLC programmable controller 26, the motor 14, the second cylinder 25, solenoid valve 27, third cylinder 33 and the 4th cylinder 44 pass through
Circuit is connected with the controller 26.Under the action of controller 26, can make motor 14, the second cylinder 25, solenoid valve 27,
Third cylinder 33 and the realization of the 4th cylinder 44 automatically control, and without artificially controlling, improve the degree of automation of equipment.
Temperature sensor one, liquid level sensor one are equipped in storage barrel 2, temperature sensor one, liquid level sensor one are logical
Circuit is crossed with above-mentioned controller 26 to be connected.Temperature sensor one can monitor the temperature of solution in storage barrel 2 in real time, liquid level
Sensor one can monitor the liquid level of solution in storage barrel 2 in real time.High-order probe and the storage barrel 2 of liquid level sensor one
Be the distance between topmost 1-2cm, specifically, the distance is 1.5cm, also can according to the actual size of storage barrel 2 to its into
Row adjustment appropriate, the distance between the low level probe of liquid level sensor one and 2 bottom of storage barrel are 3-5cm, specifically, should
Distance is 4cm, also can carry out adjustment appropriate to it according to the actual size of storage barrel 2.When liquid level sensor one monitors to store up
When depositing the liquid level decline in bucket 2, controller 26 can be passed information to, controller 26 orders the piston rod of the second cylinder 25 to be stretched again
Go out, fluid infusion is carried out to storage barrel 2, so that the liquid level of storage barrel 2 remains balance.
It is molded in bucket 3 and is equipped with temperature sensor two, PH sensor, liquid level sensor two, temperature sensor two, PH sensings
Device, liquid level sensor two are connected by circuit with above-mentioned controller 26.Temperature sensor two can be to solution in molding bucket 3
Temperature monitor in real time, PH sensor can monitor the pH value of solution in molding bucket 3 in real time, liquid level sensor two can at
The liquid level of solution monitors in real time in type bucket 3.The distance between the high-order probe of liquid level sensor two and 3 the top of molding bucket
Also adjustment appropriate can be carried out to it according to the actual size of molding bucket 3, liquid level passes specifically, the distance is 6cm for 5-8cm
The distance between the low level probe of sensor two and 3 bottom of molding bucket are 1-3cm, specifically, the distance is 2cm, it also can basis
The actual size of molding bucket 3 carries out adjustment appropriate to it.As adsorption microspheres increase or decrease in molding bucket 3, work as liquid level
When sensor two monitors that liquid level rises or declines in molding bucket 3, controller 26 can be passed information to, controller 26 is ordered again
Enable the output shaft of motor 14 correspond to rotate forward or reversion, when the liquid level of molding bucket 3 being made to increase, mounting plate 5 also can with rising, at
When the liquid level of type bucket 3 declines, mounting plate 5 also can be such that the distance between mounting plate 5 and molding 3 liquid level of bucket protects always with decline
It holds certain.
This adsorption microspheres former with netted liquid pearl separator, operation principle is such:
1, first, stoste is loaded onto in storage barrel 2, loads onto solidification liquid in being molded bucket 3, and adjust magnetic stirring apparatus 4
Rotating speed and temperature, using magnetic stirring apparatus 4 to molding bucket 3 be stirred and control temperature;
2, secondly, using selecting mechanism, select suitable syringe needle 7 and and its matched magnet ring 6, syringe needle 7 is installed to
In the matched magnet ring 6, and magnet ring 6 is installed in the through-hole specified on mounting plate 5;
3, then, using elevation positioning structure, suitable height is adjusted to mounting plate 5, specifically, in the effect of motor 14
Under, make output shaft that lead screw 15 be driven to rotate forward, to make mounting plate 5 push downwards by nut 16 and bearing 17, until on mounting plate 5
Pointer 23 refer to specified graduation mark;
4, then, it extracts the stoste in storage barrel 2 using delivery pump 9 and flow to syringe needle through flow control valve 10 and inlet tube 8
7, and instilled into molding bucket 3 across silk screen 20, adsorption microspheres are formed it into, the making of adsorption microspheres is completed, if storage barrel 2 is former
Liquid is insufficient, and under the action of the second cylinder 25, fluid infusion is carried out using 24 pairs of storage barrels 2 of fluid infusion bucket;
5, last, the adsorption microspheres solidified in being molded bucket 3 are transferred in storage box 31 using discharging net bucket 28, the
Under the action of four cylinders 44 and controller 26, automatically controlling for the 4th cylinder 44 is realized, will finally be sealed using third cylinder 33
Plate 34 covers in the feed inlet of storage box 31, under the action of third cylinder 33 and controller 26, realizes oneself of third cylinder 33
Dynamic control.
The present invention is with " the adsorption microspheres former with liquid pearl separator " and " a kind of former of adsorption microspheres "
The similar patent of invention applied on the same day, with " the adsorption microspheres former with liquid pearl separator ", " a kind of adsorption microspheres
Former " is compared:Its main distinctive points is the liquid pearl separator of the present invention in reticular structure, thus can will be from
The liquid pearl of syringe needle drippage is separated into the smaller liquid pearl of diameter, and adsorption microspheres are just formed when liquid droplet drops down onto in molding bucket, this
The forming diameter of adsorption microspheres is generally between 0.1-1mm;And the liquid in " the adsorption microspheres former with liquid pearl separator "
The liquid pearl dripped from syringe needle can be separated into the smaller liquid of diameter in distributing shape and can rotate by pearl separator
Pearl just forms adsorption microspheres when liquid droplet drops down onto in molding bucket, and the forming diameter of this adsorption microspheres is generally in 0.01-
Between 0.1mm;And that liquid pearl separator is not added in " a kind of former of adsorption microspheres ", it is directly will be from using syringe needle
The stoste of syringe needle drippage is added dropwise in molding bucket, forms adsorption microspheres, the forming diameter of this adsorption microspheres is generally in 1-10mm
Between.
Because these similar patents are the common research of Jiaxing Vocational Technical College and Liang Ge schools of Institutes Of Technology Of Zhejiang.
Since different inventors has different improved methods, so specific scheme also has certain difference, therefore, the list of applicant
Position is different also according to actual conditions.
Specific embodiment described herein is only an example for the spirit of the invention.Technology belonging to the present invention is led
The technical staff in domain can make various modifications or additions to the described embodiments or replace by a similar method
In generation, however, it does not deviate from the spirit of the invention or beyond the scope of the appended claims.
Although 1, pedestal is used more herein;2, storage barrel;3, it is molded bucket;4, magnetic stirring apparatus;5, mounting plate;6,
Magnet ring;7, syringe needle;8, inlet tube;9, delivery pump;10, flow control valve;11, left column;12, right column;13, top plate;14, electric
Machine;15, lead screw;16, nut;17, bearing;18, guide cylinder;19, guide post;20, silk screen;21, clip one;22, clip two;
23, pointer;24, fluid infusion bucket;25, the second cylinder;26, controller;27, solenoid valve;28, discharge net bucket;29, left connection ring;30,
Right connection ring;31, storage box;32, placement plate;33, third cylinder;34, sealing plate;35, guide rail;36, holder;37, sliding block one;
38, sliding block two;39, spring;40, connecting rope one;41, one is linked up with;42, connecting rope two;43, two are linked up with;44, the arts such as the 4th cylinder
Language, but it does not preclude the possibility of using other terms.The use of these items is only for more easily describe and explain this
The essence of invention;Any one of the additional limitations is construed as all to disagree with spirit of that invention.
Claims (9)
1. the adsorption microspheres former with netted liquid pearl separator, including pedestal, are provided on pedestal for storing stoste
Storage barrel and molding bucket for balling-up, which is characterized in that solidification liquid is housed in molding bucket, equipped with original in storage barrel
Liquid;Magnetic stirring apparatus is provided on the pedestal, above-mentioned molding bucket is arranged on magnetic stirring apparatus, and molding bucket top has
Opening, the upper opening portion are provided with mounting plate, and mounting plate is set on the base by an elevation positioning structure, the liter
It includes left column and right column to drop location structure, and left column and right column are vertically fixed on pedestal, above-mentioned magnetic agitation
Device is between left column and right column, and the one side of the left column towards right column is plane, is provided in the plane
Graduation mark, graduation mark are from top to bottom arranged, and graduation mark from top to bottom is arranged using the alternate mode of the white three kinds of colors of red indigo plant,
It is fixed with top plate at left column top and right column top, portion is fixed with motor under the top plate, passes through connection on the output shaft of motor
Axis device is fixed with lead screw, and nut is threaded on the lead screw, and the outer wall of nut is equipped with bearing, the inner ring and spiral shell of bearing
Mother is fixed, and the outer ring of bearing is mutually fixed with mounting plate, and several guide cylinders and guiding are additionally provided between the mounting plate and top plate
Column, guide post are slidably arranged in guide cylinder, and one end of guide post is fixed on a mounting board, and one end of guide cylinder is fixed on top plate
On, it is fixed with pointer on mounting plate, the pointer is towards above-mentioned graduation mark;The mounting plate, which is equipped with, can select syringe needle
The selecting mechanism of pore size, selecting mechanism include several through-holes opened up on a mounting board, are fixed in the through-hole several
The internal diameter of magnet ring, the magnet ring is all different, and syringe needle is provided in a wherein magnet ring, and described syringe needle one end is liquid feeding end,
The other end is outlet end, and the liquid feeding end of syringe needle is connected by inlet tube with storage barrel, delivery pump is provided in inlet tube, institute
It states and is additionally provided with flow control valve in inlet tube;Netted liquid pearl separation is additionally provided in mounting plate and between being molded the opening of bucket
Device, the netted liquid pearl separator include a silk screen, and the silk screen is detachably arranged between left column and right column, silk
A diameter of 0.1-1mm of online mesh.
2. the adsorption microspheres former of the netted liquid pearl separator of band according to claim 1, which is characterized in that described
Controller is provided on pedestal, the motor is connected by circuit with the controller.
3. the adsorption microspheres former of the netted liquid pearl separator of band according to claim 2, which is characterized in that described
Fluid infusion bucket is additionally provided on pedestal, fluid infusion bucket upper end has outlet, and fluid infusion bucket one end is hinged on the upper end of storage barrel side
Place, the lower part of the fluid infusion bucket other end are provided with the second cylinder, and the cylinder body of the second cylinder is fixed on the base, the piston of the second cylinder
Straight up, the piston rod upper end of the second cylinder is connected with the fluid infusion bucket other end for bar upper end, the second cylinder by circuit with it is upper
The controller stated is connected;It is further opened with out fluid through-hole at the lower part of the side of storage barrel in fluid infusion bucket, is going out fluid through-hole
In be provided with solenoid valve, the solenoid valve is connected by circuit with above-mentioned controller.
4. the adsorption microspheres former of the netted liquid pearl separator of band according to claim 3, which is characterized in that described
Discharging net bucket is provided in molding bucket, discharging net bucket lower part and side offer several micropores, the left side on discharging net bucket top
It is fixed with left connection ring, discharging net bucket is fixed with right connection ring on the right side of top, is provided on pedestal micro- for storing absorption
The storage box of ball, storage upper box part have feed inlet, and placement plate is fixed with close to the side of molding bucket in storage box, placement plate with
It is molded bucket flush with each other, third cylinder is provided in placement plate, the piston rod of third cylinder is arranged far from storage box, third gas
It is fixed with sealing plate on the piston rod of cylinder, guide rail is additionally provided with above storage box, the top of guide rail towards molding bucket extends, leads
Rail is in below top plate, and guide rail both ends are fixed on the base by several holders, and sliding block one and sliding block two are provided on guide rail, sliding
It is fixed with spring between block one and sliding block two, is fixed with connecting rope one in one lower part of sliding block, the lower end of connecting rope one is fixed with extension
Hook one, one energy hanging support of hook are fixed with connecting rope two, the lower end of connecting rope two in the left connection ring in two lower part of sliding block
It is fixed with hook two, in the right connection ring, the sliding block two is driven two energy hanging support of hook by the 4th cylinder, and the 4th
The cylinder body of cylinder is fixed on holder, and the piston rod of the 4th cylinder is connected with sliding block two;The third cylinder and the 4th gas
Cylinder is connected by circuit with above-mentioned controller.
5. the adsorption microspheres former of the netted liquid pearl separator of band according to claim 1 or 2 or 3 or 4, feature exist
In the delivery pump is peristaltic pump.
6. the adsorption microspheres former of the netted liquid pearl separator of band according to claim 1 or 2 or 3 or 4, feature exist
In the solidification liquid is water, ethyl alcohol, acid solution or alkaline solution.
7. the adsorption microspheres former of the netted liquid pearl separator of band according to claim 1 or 2 or 3 or 4, feature exist
In the stoste is cellulose, chitin or Glucomannan lysate.
8. the adsorption microspheres former of the netted liquid pearl separator of band according to claim 4, which is characterized in that described
Temperature sensor one, liquid level sensor one are equipped in storage barrel, the high-order probe and storage barrel of the liquid level sensor one are most
The distance between upper end is 1-2cm, and the distance between the low level probe of liquid level sensor one and storage barrel bottom are 3-5cm,
Liquid level sensor one is connected by circuit with above-mentioned controller.
9. the adsorption microspheres former of the netted liquid pearl separator of band according to claim 4, which is characterized in that described
Be molded in bucket and be equipped with temperature sensor two, PH sensor, liquid level sensor two, the high-order probe of the liquid level sensor two with
It is 5-8cm, the distance between the low level probe of liquid level sensor two and molding bucket bottom to be molded the distance between bucket the top
For 1-3cm, liquid level sensor two is connected by circuit with above-mentioned controller.
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US3937668A (en) * | 1970-07-15 | 1976-02-10 | Ilse Zolle | Method for incorporating substances into protein microspheres |
CN1480123A (en) * | 2003-07-25 | 2004-03-10 | 瑞安市富昌制药机械有限公司 | Device for displaying height difference between dripper of solid drop pills machine and liquid level of dripping bucket |
CN201052459Y (en) * | 2006-08-17 | 2008-04-30 | 温州医学院 | High-efficiency multi-needle electrostatic microcapsule, microsphere production equipment |
CN206392081U (en) * | 2016-10-18 | 2017-08-11 | 嘉兴职业技术学院 | Adsorption microspheres former with netted liquid pearl separator |
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2016
- 2016-10-18 CN CN201610906788.1A patent/CN106362715B/en active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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US3937668A (en) * | 1970-07-15 | 1976-02-10 | Ilse Zolle | Method for incorporating substances into protein microspheres |
CN1480123A (en) * | 2003-07-25 | 2004-03-10 | 瑞安市富昌制药机械有限公司 | Device for displaying height difference between dripper of solid drop pills machine and liquid level of dripping bucket |
CN201052459Y (en) * | 2006-08-17 | 2008-04-30 | 温州医学院 | High-efficiency multi-needle electrostatic microcapsule, microsphere production equipment |
CN206392081U (en) * | 2016-10-18 | 2017-08-11 | 嘉兴职业技术学院 | Adsorption microspheres former with netted liquid pearl separator |
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