CN106356113A - Corrosion-resistant lubricating graphite slurry and preparation method thereof - Google Patents
Corrosion-resistant lubricating graphite slurry and preparation method thereof Download PDFInfo
- Publication number
- CN106356113A CN106356113A CN201610807862.4A CN201610807862A CN106356113A CN 106356113 A CN106356113 A CN 106356113A CN 201610807862 A CN201610807862 A CN 201610807862A CN 106356113 A CN106356113 A CN 106356113A
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- graphite
- corrosion
- resistant lubricating
- graphite slurry
- processing technology
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B1/00—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors
- H01B1/20—Conductive material dispersed in non-conductive organic material
- H01B1/24—Conductive material dispersed in non-conductive organic material the conductive material comprising carbon-silicon compounds, carbon or silicon
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B13/00—Apparatus or processes specially adapted for manufacturing conductors or cables
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- Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Lubricants (AREA)
- Carbon And Carbon Compounds (AREA)
Abstract
The invention provides corrosion-resistant lubricating graphite slurry. The corrosion-resistant lubricating graphite slurry is characterized by comprising, by weight percentage, 20-60% of graphite, 10-20% of glycine and 10-20% of bi-phenolic methane. The invention further provides a preparation method of the corrosion-resistant lubricating graphite slurry. The preparation method includes: grinding the graphite into powder for standby, grinding the ground graphite powder, the glycine and the bi-phenolic methane in a ball mill, and filtering to obtain the graphite slurry. The preparation method of the corrosion-resistant lubricating graphite slurry is simple and easy in material obtaining.
Description
Technical field
The invention provides a kind of processing technology of corrosion-resistant lubricating graphite slurry, the one kind especially for carbon crystalline substance plate is resistance to
The processing technology of corrosion lubricating graphite slurry.
Background technology
Graphite is the important mineral resources of China, has the continuous space researched and developed and lifted and development, in conductive field
Play its important effect, current graphite, to replace the conductive materials such as copper and iron, becomes the conductive new material of a new generation, uses graphite
The graphite slurry not only process is simple developed, environmental protection, more there is efficient conducting function, accelerate productivity ratio, improve industry
Quality, quality guarantee, is a very promising environmental-friendly natural material, has obtained consistent favorable comment and the trust of insider, uses
The heating board of this graphite slurry preparation is not oxidizable, long service life.
Content of the invention
The present invention is intended to provide a kind of corrosion-resistant lubricating graphite slurry, this black lead wash has excellent corrosion-resistant lubricity.
To achieve these goals, the invention provides a kind of corrosion-resistant lubricating graphite slurry is it is characterised in that press quality
Percentage ratio is: graphite 20-60%, glycine 10-20%, Bi-phenolic Methan e 10-20%.
Present invention also offers a kind of manufacture method of corrosion-resistant lubricating graphite slurry, comprise the steps of
(1) graphite is ground into powder and gets ready；It is placed in 80～160 DEG C in vacuum drying oven, drying time is 5～10
Hour；
(2) ground graphite powder, glycine, Bi-phenolic Methan e are sent into the grinding carrying out 10-20 hour in ball crusher；
(3) ground serosity is put in sieve aperture and filtered, put into after filtration and in filter press, make pie；
(4) pie object is sent into stirring in blender and make black lead wash.
By technique scheme, the present invention passes through to dry individual composition, grinds, and the black lead wash obtaining has corrosion-resistant profit
Slip, and preparation method is simple, raw material is easy to get.
The resistance to corrosion-resistant lubricating graphite slurry of one kind of the present invention, it is convenient to manufacture, and traditional plastic production technology need not change
Enter to can be used for it to produce and processing and fabricating, low production cost；Pollution-free, nontoxic, have no side effect, reliably trust.
Specific embodiment
Hereinafter the specific embodiment of the present invention is described in detail.It should be appreciated that it is described herein concrete
Embodiment is merely to illustrate and explains the present invention, is not limited to the present invention.
Hereinafter the specific embodiment of the present invention is described in detail.It should be appreciated that it is described herein concrete
Embodiment is merely to illustrate and explains the present invention, is not limited to the present invention.
A kind of corrosion-resistant lubricating graphite is starched it is characterised in that being by mass percentage: graphite 20-60%, glycine 10-
20%, Bi-phenolic Methan e 10-20%.
Present invention also offers a kind of manufacture method of corrosion-resistant lubricating graphite slurry, comprise the steps of
(1) graphite is ground into powder and gets ready；It is placed in 80～160 DEG C in vacuum drying oven, drying time is 5～10
Hour；
(2) ground graphite powder, glycine, Bi-phenolic Methan e are sent into the grinding carrying out 10-20 hour in ball crusher；
(3) ground serosity is put in sieve aperture and filtered, put into after filtration and in filter press, make pie；
(4) pie object is sent into stirring in blender and make black lead wash.
In the present invention, the temperature of drying, time can select in wide in range scope, but so that the stone being obtained
Ink slurry has corrosion-resistant lubricity it is preferable that 80～160 DEG C of temperature, and the time is 5～10 hours.
In the present invention, milling time with wide in range scope select, but so that be obtained black lead wash have
Corrosion-resistant lubricity is it is preferable that milling time is 10～20 hours.
Embodiment 1
1) a kind of making of corrosion-resistant lubricating graphite slurry, by mass percentage for graphite 20%, glycine 10%, two
Phenolic group methane 10%.
2) graphite is ground into powder and gets ready；It is placed in 80 DEG C in vacuum drying oven, drying time is 5 hours；To grind
The graphite powder of milled, glycine, Bi-phenolic Methan e send into the grinding carrying out in ball crusher 10 hours；
3) ground serosity is put in sieve aperture and filtered, put into after filtration and in filter press, make pie；By pie
Object is sent into stirring in blender and is made black lead wash a1.
Embodiment 2
1) a kind of making of corrosion-resistant lubricating graphite slurry, by mass percentage for graphite 60%, glycine 20%, two
Phenolic group methane 20%
2) graphite is ground into powder and gets ready；It is placed in 160 DEG C in vacuum drying oven, drying time is 10 hours；Will
Ground graphite powder, glycine, Bi-phenolic Methan e send into the grinding carrying out in ball crusher 20 hours；
3) ground serosity is put in sieve aperture and filtered, put into after filtration and in filter press, make pie；By pie
Object is sent into stirring in blender and is made black lead wash a2.
Embodiment 3
1) a kind of making of corrosion-resistant lubricating graphite slurry, by mass percentage for graphite 40%, glycine 15%, two
Phenolic group methane 15%.
2) graphite is ground into powder and gets ready；It is placed in 100 DEG C in vacuum drying oven, drying time is 8 hours；To grind
The graphite powder of milled, glycine, Bi-phenolic Methan e send into the grinding carrying out in ball crusher 15 hours；
(3) ground serosity is put in sieve aperture and filtered, put into after filtration and in filter press, make pie；By pie
Object is sent into stirring in blender and is made black lead wash a3.
Comparative example 1
Method according to embodiment 1 carries out sheet material b1 is obtained, and except for the difference that, does not add glycine.
Comparative example 2
Method according to embodiment 2 carries out sheet material b2 is obtained, and except for the difference that, does not add Bi-phenolic Methan e.
Comparative example 3
Method according to embodiment 3 carries out sheet material b3, except for the difference that, unselected graphite powder are obtained.
Detection example 1
, being detected, result is to the corrosion-resistant lubricity of above-mentioned black lead wash: the corrosion-resistant lubricity of black lead wash a1-a3 is equal
Corrosion-resistant lubricity better than black lead wash b1-b3.
The preferred embodiment of the present invention described in detail above, but, the present invention is not limited in above-mentioned embodiment
Detail, in the range of the technology design of the present invention, multiple simple variant can be carried out to technical scheme, this
A little simple variant belong to protection scope of the present invention.
It is further to note that each particular technique feature described in above-mentioned specific embodiment, in not lance
In the case of shield, can be combined by any suitable means, in order to avoid unnecessary repetition, the present invention to various can
The compound mode of energy no longer separately illustrates.
Additionally, combination in any can also be carried out between the various different embodiment of the present invention, as long as it is without prejudice to this
The thought of invention, it equally should be considered as content disclosed in this invention.
Claims (7)
1. a kind of making of corrosion-resistant lubricating graphite slurry is it is characterised in that be by mass percentage: graphite 20-60%, sweet ammonia
Sour 10-20%, Bi-phenolic Methan e 10-20%.
2. preparation method according to claim 1 is it is characterised in that described graphite is crystalline flake graphite.
3. a kind of processing technology of conductive graphite paste, comprises the following steps:
(1) graphite is ground into powder and gets ready；It is placed in 80～160 DEG C in vacuum drying oven, drying time is little for 5～10
When；
(2) ground graphite powder, glycine, Bi-phenolic Methan e are sent into the grinding carrying out 10-20 hour in ball crusher；
(3) ground serosity is put in sieve aperture and filtered, put into after filtration and in filter press, make pie；
(4) pie object is sent into stirring in blender and make graphite slurry.
4. corrosion-resistant lubricating graphite slurry according to claim 4 processing technology it is characterised in that: described composition passes through
The grinding of 10-20 hour, sieve aperture filter, compacting, stirring after make black lead wash.
5. corrosion-resistant lubricating graphite slurry according to claim 4 processing technology it is characterised in that: described ball milling turn
Speed is 800r/min.
6. corrosion-resistant lubricating graphite slurry according to claim 4 processing technology it is characterised in that: the temperature of drying baker
For 80～160 DEG C.
7. corrosion-resistant lubricating graphite slurry according to claim 4 processing technology it is characterised in that: drying time be 5
～10 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610807862.4A CN106356113B (en) | 2016-09-08 | 2016-09-08 | A kind of corrosion-resistant lubricating graphite slurry and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610807862.4A CN106356113B (en) | 2016-09-08 | 2016-09-08 | A kind of corrosion-resistant lubricating graphite slurry and preparation method thereof |
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| Publication Number | Publication Date |
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| CN106356113A true CN106356113A (en) | 2017-01-25 |
| CN106356113B CN106356113B (en) | 2018-04-10 |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6424345A (en) * | 1987-07-21 | 1989-01-26 | Nec Corp | Graphite paste |
| CN103130218A (en) * | 2013-03-25 | 2013-06-05 | 中国科学院上海硅酸盐研究所 | Preparation method of graphene |
| CN103137243A (en) * | 2011-11-22 | 2013-06-05 | 旭硝子株式会社 | Conductive paste, and preparing method of conductive paste |
| CN103409083A (en) * | 2013-08-22 | 2013-11-27 | 胡钧峰 | Graphite carbon black conductive adhesive and preparation method thereof |
| CN104658696A (en) * | 2013-11-20 | 2015-05-27 | 青岛古宇石墨有限公司 | Polymer conductive graphite slurry manufacturing technology |
| CN105060281A (en) * | 2015-07-22 | 2015-11-18 | 深圳市贝特瑞新能源材料股份有限公司 | Nano-graphite slurry preparation method |
-
2016
- 2016-09-08 CN CN201610807862.4A patent/CN106356113B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6424345A (en) * | 1987-07-21 | 1989-01-26 | Nec Corp | Graphite paste |
| CN103137243A (en) * | 2011-11-22 | 2013-06-05 | 旭硝子株式会社 | Conductive paste, and preparing method of conductive paste |
| CN103130218A (en) * | 2013-03-25 | 2013-06-05 | 中国科学院上海硅酸盐研究所 | Preparation method of graphene |
| CN103409083A (en) * | 2013-08-22 | 2013-11-27 | 胡钧峰 | Graphite carbon black conductive adhesive and preparation method thereof |
| CN104658696A (en) * | 2013-11-20 | 2015-05-27 | 青岛古宇石墨有限公司 | Polymer conductive graphite slurry manufacturing technology |
| CN105060281A (en) * | 2015-07-22 | 2015-11-18 | 深圳市贝特瑞新能源材料股份有限公司 | Nano-graphite slurry preparation method |
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| CN106356113B (en) | 2018-04-10 |
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Effective date of registration: 20210521 Address after: No. 200, Huaxing street, Sishui County, Jining City, Shandong Province 273200 Patentee after: Ren Yuan Address before: 233010 No.2, 3rd floor, No.319, zhanggongshan Road, Yuhui District, Bengbu City, Anhui Province Patentee before: Bengbu aochuang Intellectual Property Operation Co.,Ltd. |
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