CN106353458A - Device and method for simulating sealing fluid for inhibiting gas desorption of coal samples - Google Patents

Device and method for simulating sealing fluid for inhibiting gas desorption of coal samples Download PDF

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Publication number
CN106353458A
CN106353458A CN201610808848.6A CN201610808848A CN106353458A CN 106353458 A CN106353458 A CN 106353458A CN 201610808848 A CN201610808848 A CN 201610808848A CN 106353458 A CN106353458 A CN 106353458A
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tank
gas
coal sample
pipeline
tank body
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CN106353458B (en
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陈学习
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North China Institute of Science and Technology
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North China Institute of Science and Technology
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
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  • General Health & Medical Sciences (AREA)
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Abstract

The invention provides a device and a method for simulating sealing fluid for inhibiting gas desorption of coal samples. The device comprises a support. A shaft which is horizontally arranged is rotationally connected onto the support and is fastened and connected with a tank, the inside of the tank is divided into an upper tank and a lower tank by a sieve plate, the upper tank is connected with an outlet of a gas distributing tank by a pipeline, and an inlet of the gas distributing tank is connected with a gas bottle by a pipeline; the lower tank is communicated with a desorption pipe via a pipeline, and the desorption pipe is arranged in a water tank in an inverted manner; a first valve is arranged on the pipeline positioned between the gas distributing tank and the upper tank, and a second valve is arranged on the pipeline positioned between the desorption pipe and the lower tank.

Description

A kind of simulation sealing fluid suppresses the device and method of coal sample desorbing gas
Technical field
The present invention relates to a kind of simulation sealing fluid suppresses the device and method of coal sample desorbing gas, belong to colliery technology neck Domain.
Background technology
Coal seam gas-bearing capacity is one of most basic parameter of coal-bed gas, and its assay method can be divided into direct method and indirect method Two big class.The maximum problem of Direct Determination coal seam gas-bearing capacity be drill through coal sample during gas loss cause evaluated error. For down-sampling process gas loss amount, improve gas bearing capacity and measure accuracy it is proposed that immediately in sampler after the completion of sampling Mouth sealing fluid sealing coal sample, coal sample desorption of mash gas in suppression sampler, thus reduce coal sample gas loss.For detecting sealing fluid Suppression coal sample desorbing gas effect and influence factor, need the device that a kind of simulation sealing fluid suppresses coal sample desorbing gas badly.
Content of the invention
For the problems referred to above, it is an object of the invention to provide a kind of simulation sealing fluid suppress coal sample desorbing gas device and Method.
For achieving the above object, the present invention takes a kind of technical scheme below: simulation sealing fluid suppression coal sample desorbing gas Device it is characterised in that: include a support, on the bracket rotate connect a horizontally disposed rotating shaft, described rotating shaft with One tank body is fastenedly connected, and described tank body is divided into upper tank body and lower tank by a sieve tray by described tank interior, described on Tank body is connected with the outlet of a distribution tank by pipeline, and the import of described distribution tank is connected with a gas bottle by pipeline;Described Lower tank is connected by the desorption tube that pipeline is upside down in tank with;Between described distribution tank and described upper tank body First valve is arranged on pipeline, the pipeline between described desorption tube and described lower tank arranges the second valve.
It is fastenedly connected a turning handle in one end of described rotating shaft.
A kind of method that simulation sealing fluid suppresses coal sample desorbing gas, comprises the following steps: 1) coal sample is placed on upper tank In body, sealing fluid is filled lower tank, water is filled tank;2) open gas bottle to inflate to distribution tank, when gas in distribution tank Gas pressure opens the first valve after reaching predetermined value, and methane gas are filled in upper tank body, and keeps a period of time to make coal Sample adsorption gas reach balance;3) close distribution tank, rotating shaft makes tank body rotate 180 °, makes lower tank be located at top, upper tank Body is located at bottom, and then makes the sealing fluid in lower tank be flowed in upper tank body by sieve tray to contact with coal sample, by coal sample table Face is fully wrapped around;4) open the valve on pipeline, it is laggard that the gas that the coal sample in upper tank body is released flows through pipeline by lower tank Enter in screw clamp, observe coal sample and solve under the parcel of sealing fluid by observing the drainage speed speed in desorption tube and volume change Inhale gas characteristic.
The present invention due to taking above technical scheme, its have the advantage that the present invention can simulate different sealing fluid properties, Coal sample desorbing Experiments on Gas under the conditions of the coal sample of different rank and granularity, different adsorption equilibrium gas pressure etc. are multiple, Have the advantages that multiple functional, simple to operate, observation is directly perceived.
Brief description
Fig. 1 is the overall structure diagram of the present invention.
Specific embodiment
With reference to the accompanying drawings and examples the present invention is described in detail.
As shown in figure 1, the present invention proposes the device that a kind of simulation sealing fluid suppresses coal sample desorbing gas, including a support 1, support 1 rotates and connects a horizontally disposed rotating shaft 2, rotating shaft 2 is fastenedly connected with a tank body 3.Tank body 3 is internal to be sieved by one Tank body 3 is divided into upper tank body 32 and lower tank 33 by orifice plate 31.Upper tank body 32 is connected with the outlet of a distribution tank 6 by pipeline 5, The import of distribution tank 6 is connected with a gas bottle 8 by pipeline 7.Lower tank 33 is upside down in the solution in tank 9 by pipeline 14 and Suction pipe 10 connects.Pipeline 5 and pipeline 14 are provided with valve 11.
In above-described embodiment, a turning handle 4 can be fastenedly connected in one end of rotating shaft 2.
Based on said apparatus, the invention allows for a kind of method that simulation sealing fluid suppresses coal sample desorbing gas, including Following steps:
1) coal sample 12 is placed in upper tank body 32, sealing fluid 13 is filled lower tank 33, water is filled tank 9;
2) open gas bottle 8 to inflate to distribution tank 6, after gas gas pressure reaches predetermined value in distribution tank 6, open pipe Valve 11 on road 5, methane gas are filled in upper tank body 32, and it is flat to keep a period of time so that coal sample 12 adsorption gas is reached Weighing apparatus;
3) close distribution tank 6, rotating shaft 2 makes tank body 3 rotate 180 °, make lower tank 33 be located at top, upper tank body 32 In bottom, and then make the sealing fluid 13 in lower tank 33 be flowed in upper tank body 32 by sieve tray 31 to contact with coal sample 12, will Coal sample 12 surface is fully wrapped around;
4) open the valve 11 on pipeline 14, the gas that the coal sample 12 in upper tank body 32 is released flows through pipe by lower tank 33 Enter behind road 8 in screw clamp 9, observe coal sample 12 airtight by observing the drainage speed speed in desorption tube 10 and volume change Desorbing gas characteristic under the parcel of liquid 13.
The various embodiments described above are merely to illustrate the present invention, and the structure of wherein each part, connected mode etc. are all can be Change, every equivalents carrying out on the basis of technical solution of the present invention and improvement, all should not exclude the present invention's Outside protection domain.

Claims (3)

1. a kind of simulation sealing fluid suppress coal sample desorbing gas device it is characterised in that: include a support, on the bracket Rotate and connect a horizontally disposed rotating shaft, described rotating shaft is fastenedly connected with a tank body, described tank interior passes through a sieve tray will Described tank body is divided into upper tank body and lower tank, and described upper tank body is connected with the outlet of a distribution tank by pipeline, described distribution The import of tank is connected with a gas bottle by pipeline;The desorption tube that described lower tank is upside down in tank by pipeline and connects Logical;Pipeline between described distribution tank and described upper tank body arranges the first valve, positioned at described desorption tube and institute State and the second valve is arranged on the pipeline between lower tank.
2. as claimed in claim 1 a kind of simulation sealing fluid suppress coal sample desorbing gas device it is characterised in that: described One end of rotating shaft is fastenedly connected a turning handle.
3. a kind of method that simulation sealing fluid implemented based on device as claimed in claim 1 or 2 suppresses coal sample desorbing gas, Comprise the following steps:
1) coal sample is placed in upper tank body, sealing fluid is filled lower tank, water is filled tank;
2) open gas bottle to inflate to distribution tank, open the first valve after gas gas pressure reaches predetermined value in distribution tank, Methane gas are filled in upper tank body, and keep a period of time to make coal sample adsorption gas reach balance;
3) close distribution tank, rotating shaft makes tank body rotate 180 °, makes lower tank be located at top, and upper tank body is located at bottom, and then Make the sealing fluid in lower tank be flowed in upper tank body by sieve tray to contact with coal sample, will be fully wrapped around for coal sample surface;
4) open the valve on pipeline, the gas that the coal sample in upper tank body is released enters screw clamp after lower tank flows through pipeline In, observe coal sample desorbing gas spy under the parcel of sealing fluid by observing the drainage speed speed in desorption tube and volume change Property.
CN201610808848.6A 2016-09-08 2016-09-08 A kind of simulation sealing fluid inhibits the device and method of coal sample desorption gas Active CN106353458B (en)

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CN201610808848.6A CN106353458B (en) 2016-09-08 2016-09-08 A kind of simulation sealing fluid inhibits the device and method of coal sample desorption gas

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CN201610808848.6A CN106353458B (en) 2016-09-08 2016-09-08 A kind of simulation sealing fluid inhibits the device and method of coal sample desorption gas

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108717033A (en) * 2018-05-14 2018-10-30 华北科技学院 A kind of experimental provision and experimental method improving coal gas desorption efficiency using magnetic-particle
CN111458260A (en) * 2020-05-26 2020-07-28 中煤科工集团重庆研究院有限公司 Coal gas desorption rule determination device, system and method
CN113695105A (en) * 2021-08-23 2021-11-26 中煤科工集团重庆研究院有限公司 System for reducing gas release in coal transportation process

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CN103196702A (en) * 2013-04-26 2013-07-10 中联煤层气国家工程研究中心有限责任公司 Method for measuring gas content of coal bed through airtight coring
CN104931383A (en) * 2015-05-05 2015-09-23 中煤科工集团西安研究院有限公司 Coal bed gas and methane gas coring and desorption measurement system and method
CN205252636U (en) * 2015-10-30 2016-05-25 天津法莫西医药科技有限公司 Pharmaceutical solid -liquid separation equipment
CN206002515U (en) * 2016-09-08 2017-03-08 华北科技学院 A kind of simulation sealing fluid suppresses the device of coal sample desorbing gas

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CN103196702A (en) * 2013-04-26 2013-07-10 中联煤层气国家工程研究中心有限责任公司 Method for measuring gas content of coal bed through airtight coring
CN104931383A (en) * 2015-05-05 2015-09-23 中煤科工集团西安研究院有限公司 Coal bed gas and methane gas coring and desorption measurement system and method
CN205252636U (en) * 2015-10-30 2016-05-25 天津法莫西医药科技有限公司 Pharmaceutical solid -liquid separation equipment
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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108717033A (en) * 2018-05-14 2018-10-30 华北科技学院 A kind of experimental provision and experimental method improving coal gas desorption efficiency using magnetic-particle
CN108717033B (en) * 2018-05-14 2021-03-16 华北科技学院 Experimental device and experimental method for improving coal gas desorption rate by using magnetic particles
CN111458260A (en) * 2020-05-26 2020-07-28 中煤科工集团重庆研究院有限公司 Coal gas desorption rule determination device, system and method
CN111458260B (en) * 2020-05-26 2022-08-30 中煤科工集团重庆研究院有限公司 Coal gas desorption rule determination device, system and method
CN113695105A (en) * 2021-08-23 2021-11-26 中煤科工集团重庆研究院有限公司 System for reducing gas release in coal transportation process

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