CN106345388A - Multifunctional acid reaction kettle - Google Patents

Multifunctional acid reaction kettle Download PDF

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Publication number
CN106345388A
CN106345388A CN201610931017.8A CN201610931017A CN106345388A CN 106345388 A CN106345388 A CN 106345388A CN 201610931017 A CN201610931017 A CN 201610931017A CN 106345388 A CN106345388 A CN 106345388A
Authority
CN
China
Prior art keywords
shell cover
upper cover
reaction kettle
reaction vessel
multifunctional acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610931017.8A
Other languages
Chinese (zh)
Inventor
张志军
陈建斌
姜荣跃
赵忠廷
张会涛
黄济民
刘志国
陈琪
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanxi Xinhua Chemical Industry Co Ltd
Original Assignee
Shanxi Xinhua Chemical Industry Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shanxi Xinhua Chemical Industry Co Ltd filed Critical Shanxi Xinhua Chemical Industry Co Ltd
Priority to CN201610931017.8A priority Critical patent/CN106345388A/en
Publication of CN106345388A publication Critical patent/CN106345388A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/40Mixers using gas or liquid agitation, e.g. with air supply tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/40Mixers using gas or liquid agitation, e.g. with air supply tubes
    • B01F33/406Mixers using gas or liquid agitation, e.g. with air supply tubes in receptacles with gas supply only at the bottom
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/181Preventing generation of dust or dirt; Sieves; Filters
    • B01F35/187Preventing generation of dust or dirt; Sieves; Filters using filters in mixers, e.g. during venting
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/90Heating or cooling systems
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/90Heating or cooling systems
    • B01F2035/99Heating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24Stationary reactors without moving elements inside
    • B01J2219/2401Reactors comprising multiple separate flow channels
    • B01J2219/2402Monolithic-type reactors
    • B01J2219/2423Separation means, e.g. membrane inside the reactor
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/90Other properties not specified above

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)

Abstract

The invention discloses a multifunctional acid reaction kettle. The multifunctional acid reaction kettle comprises a reaction vessel (1) having an upper shell cover (2) and a lower shell cover (3), wherein the middle part of the upper shell cover (2) is provided with a feed port (21); the upper shell cover (2) is provided with an air/steam inlet pipe (22) extending to the bottom of the reaction vessel (1); the upper shell cover (2) is provided with an overflow pipe (23); the bottom of the lower shell cover (3) is provided with a discharge port (31) and a water outlet (32); and a screen plate (33) is mounted at the water outlet (32) side in the lower shell cover (3). The device disclosed by the invention is characterized in that a steam/air matched stirring and heating mode is adopted, the labor intensity of operators is low, the production continuity is favorable, and the prepared product has high performance.

Description

Multifunctional acid reactor
Technical field
The present invention relates to chemical field reaction vessel, specially a kind of multifunctional acid reaction being applied to activated carbon industry Kettle.
Background technology
China's activated carbon industry pickling, washing Activated Carbon Production adopt the trough-shaped container that fiberglass makes at present, and acid solution is soaked Realized with the technique that water rinses after bubble.But this Preparation equipment and method personnel labor intensity are big, carbon granule is obtained not with easy To being fully contacted, reaction is thorough, causes that the technical target of the product produced is relatively low, and scattered error is big.
Content of the invention
It is an object of the invention to provide a kind of multifunctional acid reactor, reduce operative employee's labor intensity, produce high-quality acid Wash activated carbon.
The present invention adopts the following technical scheme that realization:
A kind of multifunctional acid reactor, including the reaction vessel with upper cover and low head;In the middle part of described upper cover, setting adds Material mouth, described upper cover setting stretches to the air vapor inlet pipe of reaction container bottom, and described upper cover arranges overflow pipe;Described Low head bottom setting discharge port and outlet, are located at outlet side mounted sieve in described low head.
Material and solvent add acid reaction kettle by charge door, cover charge door, air and steam are entered by air vapor Mouth adds to reactor bottom, reaches heating and thermal insulation and the effect of stirring.After completion of the reaction, can directly by discharge port discharging to lower road Operation or reservation material, in reactor, are only drained solution, are added new solution reaction or the rinsing that adds water by outlet.Steam In the condensed water producing in vapour heating process and reactor, unnecessary gas is discharged by overflow pipe.
The innovative point of this device is to coordinate agitating heating using steam and air, and operative employee's labor intensity is low, the company of production Continuous property is good, and the properties of product produced are high.Apply this device, the ature of coal activity of low acid ash-dissolving value, low acid iron-dissolving value can be produced Charcoal, is smaller than 0.2%(w/w with its acid ash-dissolving value of activated carbon of the method preparation), acid iron-dissolving value is smaller than 0.008%(w/w).
Brief description
Fig. 1 represents the structural representation of the present invention.
In figure: 1- reaction vessel, 2- upper cover, 3- low head, 21- charge door, 22- air vapor inlet pipe, 23- overflow Pipe, 31- discharge port, 32- outlet, 33- sieve plate.
Specific embodiment
Below in conjunction with the accompanying drawings the specific embodiment of the present invention is described in detail
A kind of multifunctional acid reactor, as shown in figure 1, include the reaction vessel 1 with upper cover 2 and low head 3;Described upper envelope 2 middle part setting charge doors 21, described upper cover 2 setting stretches to the air vapor inlet pipe 22 of reaction vessel 1 bottom, described on End socket 2 arranges overflow pipe 23;Described low head 3 bottom setting discharge port 31 and outlet 32, are located at water outlet in described low head 3 Mouth 32 side mounted sieves 33.
Material and solvent add acid reaction kettle by charge door 21, cover charge door 21, air and steam are steamed by air Vapour inlet pipe 22 adds to reactor bottom, reaches heating and thermal insulation and the effect of stirring.After completion of the reaction, can directly be unloaded by discharge port 31 Expect to next procedure or retain material in reactor, only solution is drained by outlet 32, the new solution reaction of addition or Add water rinsing.The effect of sieve plate 33 is filter material, and only water energy is enough discharges from outlet 32.Produce in steam heating process In condensed water and reactor, unnecessary gas is discharged by overflow pipe.
Finally it should be noted that above example is only in order to illustrate technical scheme and unrestricted, although reference The embodiment of the present invention has been described in detail, it will be understood by those within the art that, technical scheme is entered Row modification or equivalent, without departure from the spirit and scope of technical scheme, it all should cover the power of the present invention In the claimed scope of profit.

Claims (1)

1. a kind of multifunctional acid reactor, including the reaction vessel (1) with upper cover (2) and low head (3);Its feature exists In: setting charge door (21) in the middle part of described upper cover (2), described upper cover (2) setting stretches to the sky of reaction vessel (1) bottom Gas steam inlet tube (22), described upper cover (2) setting overflow pipe (23);Described low head (3) bottom setting discharge port (31) and Outlet (32), is located at outlet (32) side mounted sieve (33) in described low head (3).
CN201610931017.8A 2016-10-31 2016-10-31 Multifunctional acid reaction kettle Pending CN106345388A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610931017.8A CN106345388A (en) 2016-10-31 2016-10-31 Multifunctional acid reaction kettle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610931017.8A CN106345388A (en) 2016-10-31 2016-10-31 Multifunctional acid reaction kettle

Publications (1)

Publication Number Publication Date
CN106345388A true CN106345388A (en) 2017-01-25

Family

ID=57863911

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610931017.8A Pending CN106345388A (en) 2016-10-31 2016-10-31 Multifunctional acid reaction kettle

Country Status (1)

Country Link
CN (1) CN106345388A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110586018A (en) * 2018-06-13 2019-12-20 中国石油化工股份有限公司 Acid reaction tank for preparing kerogen

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH02188406A (en) * 1989-01-18 1990-07-24 Fuji Electric Co Ltd Carbon monoxide converter
CN2832289Y (en) * 2004-08-06 2006-11-01 王兵 Magnetic drive synthesis autoclave
CN102328928A (en) * 2011-10-10 2012-01-25 浙江兴达活性炭有限公司 Equipment for producing active carbon
CN206139192U (en) * 2016-10-31 2017-05-03 山西新华化工有限责任公司 Multi -functional sour reation kettle

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH02188406A (en) * 1989-01-18 1990-07-24 Fuji Electric Co Ltd Carbon monoxide converter
CN2832289Y (en) * 2004-08-06 2006-11-01 王兵 Magnetic drive synthesis autoclave
CN102328928A (en) * 2011-10-10 2012-01-25 浙江兴达活性炭有限公司 Equipment for producing active carbon
CN206139192U (en) * 2016-10-31 2017-05-03 山西新华化工有限责任公司 Multi -functional sour reation kettle

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110586018A (en) * 2018-06-13 2019-12-20 中国石油化工股份有限公司 Acid reaction tank for preparing kerogen

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PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20170125